CN109097216A - A kind of Chinese prickly ash antibacterial toilet soap and preparation method thereof - Google Patents
A kind of Chinese prickly ash antibacterial toilet soap and preparation method thereof Download PDFInfo
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- CN109097216A CN109097216A CN201811167791.1A CN201811167791A CN109097216A CN 109097216 A CN109097216 A CN 109097216A CN 201811167791 A CN201811167791 A CN 201811167791A CN 109097216 A CN109097216 A CN 109097216A
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- prickly ash
- chinese prickly
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention provides a kind of Chinese prickly ash antibacterial toilet soap, is made of the raw material of following parts by weight: 50-75 parts of soap base, 1-5 parts of lauryl sodium sulfate, 140-180 parts of pure water, 1-5 parts of ethyl alcohol, 14-20 parts of Chinese prickly ash, 8-15 parts of Mongollian Thyme Herb, 1-4 parts of tremella.Meanwhile the present invention also provides the preparation methods of the antibacterial toilet soap.Effective antipathogenic composition in Chinese prickly ash and Mongollian Thyme Herb can be released, the perfumed soap good antimicrobial effect of preparation by pretreatment, can play cleaning, antibacterial, skin care effect by Chinese prickly ash antibacterial toilet soap provided by the invention, Chinese prickly ash and Mongollian Thyme Herb.
Description
Technical field
The invention belongs to daily use chemicals technical fields, and in particular to a kind of Chinese prickly ash antibacterial toilet soap and preparation method thereof.
Background technique
Chinese prickly ash (Zanthexylum bungeanum maxin) is Rutaceae xanthoxylum, is the important pungent perfume (or spice) in China
Material and medicinal plant.Modern natural product chemistry and pharmaceutical research show that the extract of Chinese prickly ash has antitumor, anti-inflammatory town
Bitterly, a variety of physiological activity such as human Demodex, desinsection and antibacterial anti-corrosion are killed in suppression.Chinese medicine thinks that the warm-natured acrid flavour of Chinese prickly ash has middle benefit gas
The effect of cold dispelling, stomach invigorating dehumidifying, analgesic desinsection, removing toxic substances qi-regulating, antipruritic deodorization.
In daily life, hand is the position being in the most contact with the external world, it is often necessary to fetch article with hand, this will lead to
Bacterium infection.If not paying attention to hygiene on hand, it is easy for causing that illness finds its way in by the mouth.Sterilization class hand cleanser, which is compared, generally washes one's hands
Liquid, in addition to can also can effectively kill germ for other than hand washing completely.The sterilization component of disinfection hand cleanser is mainly that spectrum kills at present
Microbial inoculum, this kind of fungicide stability is poor, sterilizing time is short, and is harmful to the human body, even can also wash away the rouge layer of skin surface, makes
Skin is dry.
Summary of the invention
In view of the drawbacks of the prior art, the present invention provides a kind of Chinese prickly ash antibacterial toilet soap and preparation method thereof, the perfumed soap of preparation
Good antimicrobial effect.
A kind of Chinese prickly ash antibacterial toilet soap, is made of the raw material of following parts by weight:
50-75 parts of soap base, 1-5 parts of lauryl sodium sulfate, 140-180 parts of pure water, 1-5 parts of ethyl alcohol, 14-20 parts of Chinese prickly ash,
8-15 parts of green pepper, 1-4 parts of tremella.
Preferably, a kind of Chinese prickly ash antibacterial toilet soap, is made of the raw material of following parts by weight: 69 parts of soap base, dodecyl
3 parts of sodium sulphate, 165 parts of pure water, 3 parts of ethyl alcohol, 18 parts of Chinese prickly ash, 10 parts of Mongollian Thyme Herb, 2 parts of tremella.
A kind of preparation method of Chinese prickly ash antibacterial toilet soap, comprising the following steps:
(1) tremella is added in pure water, impregnates 1-1.5h at room temperature, then impregnate 30min at 40-50 DEG C, at ultrasound
3-6min is managed, filtering obtains tremella extract；
(2) Chinese prickly ash and Mongollian Thyme Herb are crushed, is placed in extraction kettle, supercritical carbon dioxide is passed through with the flow velocity of 300-400L/h, in 30-
40 DEG C, extract 2-3h under conditions of 30-40MPa, the extract of Chinese prickly ash and Mongollian Thyme Herb is obtained from knockout drum；
(3) soap base is heated to molten condition, addition tremella extract, the extract of Chinese prickly ash and Mongollian Thyme Herb, 12 at 60-80 DEG C
Sodium alkyl sulfate, ethyl alcohol, the heating stirring 40-50min at 80-90 DEG C, obtain perfumed soap material；
(4) perfumed soap material is poured into mold and is cooled and shaped, after taking-up, dried at 45-55 DEG C and dry 3-4h, after natural cooling,
Packaging.
Preferably, the condition being ultrasonically treated in step (1) is equal are as follows: supersonic frequency 45KHz, ultrasonic input power are
300W。
Preferably, Chinese prickly ash and Mongollian Thyme Herb crushed 40 meshes in step (2).
Advantages of the present invention:
Chinese prickly ash antibacterial toilet soap provided by the invention can release effective antipathogenic composition in Chinese prickly ash and Mongollian Thyme Herb, the perfume (or spice) of preparation
Soap good antimicrobial effect can play cleaning, antibacterial, skin care effect.
Specific embodiment
Embodiment 1
1. a kind of Chinese prickly ash antibacterial toilet soap, is made of the raw material of following parts by weight: 50 parts of soap base, 1 part of lauryl sodium sulfate, pure
140 parts of water purification, 1 part of ethyl alcohol, 14 parts of Chinese prickly ash, 8 parts of Mongollian Thyme Herb, 1 part of tremella.
2. a kind of preparation method of Chinese prickly ash antibacterial toilet soap, comprising the following steps:
(1) tremella is added in pure water, impregnates 1h at room temperature, then impregnate 30min at 40 DEG C, is in supersonic frequency
45KHz, ultrasonic input power are ultrasonically treated 3min under conditions of being 300W, filter, obtain tremella extract；
(2) Chinese prickly ash and Mongollian Thyme Herb be crushed into 40 meshes, are placed in extraction kettle, supercritical carbon dioxide is passed through with the flow velocity of 300L/h,
2h is extracted under conditions of 30 DEG C, 40MPa, the extract of Chinese prickly ash and Mongollian Thyme Herb is obtained from knockout drum；
(3) soap base is heated at 60 DEG C molten condition, extract, the dodecane of tremella extract, Chinese prickly ash and Mongollian Thyme Herb is added
Base sodium sulphate, ethyl alcohol, the heating stirring 50min at 80 DEG C, obtain perfumed soap material；
(4) perfumed soap material is poured into mold and is cooled and shaped, after taking-up, dried at 45 DEG C and dry 4h, after natural cooling, packaging is
It can.
Embodiment 2
1. a kind of Chinese prickly ash antibacterial toilet soap, is made of the raw material of following parts by weight: 75 parts of soap base, 5 parts of lauryl sodium sulfate, pure
180 parts of water purification, 5 parts of ethyl alcohol, 20 parts of Chinese prickly ash, 15 parts of Mongollian Thyme Herb, 4 parts of tremella.
2. a kind of preparation method of Chinese prickly ash antibacterial toilet soap, comprising the following steps:
(1) tremella is added in pure water, impregnates 1.5h at room temperature, then impregnate 30min at 50 DEG C, is in supersonic frequency
45KHz, ultrasonic input power are ultrasonically treated 6min under conditions of being 300W, filter, obtain tremella extract；
(2) Chinese prickly ash and Mongollian Thyme Herb be crushed into 40 meshes, are placed in extraction kettle, supercritical carbon dioxide is passed through with the flow velocity of 400L/h,
3h is extracted under conditions of 40 DEG C, 30MPa, the extract of Chinese prickly ash and Mongollian Thyme Herb is obtained from knockout drum；
(3) soap base is heated at 80 DEG C molten condition, extract, the dodecane of tremella extract, Chinese prickly ash and Mongollian Thyme Herb is added
Base sodium sulphate, ethyl alcohol, the heating stirring 40min at 90 DEG C, obtain perfumed soap material；
(4) perfumed soap material is poured into mold and is cooled and shaped, after taking-up, dried at 55 DEG C and dry 3h, after natural cooling, packaging is
It can.
Embodiment 3
1. a kind of Chinese prickly ash antibacterial toilet soap, is made of the raw material of following parts by weight: 69 parts of soap base, 3 parts of lauryl sodium sulfate, pure
165 parts of water purification, 3 parts of ethyl alcohol, 18 parts of Chinese prickly ash, 10 parts of Mongollian Thyme Herb, 2 parts of tremella.
2. a kind of preparation method of Chinese prickly ash antibacterial toilet soap, comprising the following steps:
(1) tremella is added in pure water, impregnates 1.2h at room temperature, then impregnate 30min at 45 DEG C, is in supersonic frequency
45KHz, ultrasonic input power are ultrasonically treated 5min under conditions of being 300W, filter, obtain tremella extract；
(2) Chinese prickly ash and Mongollian Thyme Herb be crushed into 40 meshes, are placed in extraction kettle, supercritical carbon dioxide is passed through with the flow velocity of 300L/h,
2.5h is extracted under conditions of 35 DEG C, 35MPa, the extract of Chinese prickly ash and Mongollian Thyme Herb is obtained from knockout drum；
(3) soap base is heated at 70 DEG C molten condition, extract, the dodecane of tremella extract, Chinese prickly ash and Mongollian Thyme Herb is added
Base sodium sulphate, ethyl alcohol, the heating stirring 45min at 85 DEG C, obtain perfumed soap material；
(4) perfumed soap material is poured into mold and is cooled and shaped, after taking-up, dried at 50 DEG C and dry 3.5h, after natural cooling, packaging
?.
Tremella is not added in comparative example 1(, other are with embodiment 3)
1. a kind of Chinese prickly ash antibacterial toilet soap, is made of the raw material of following parts by weight: 69 parts of soap base, 3 parts of lauryl sodium sulfate, pure
165 parts of water purification, 3 parts of ethyl alcohol, 18 parts of Chinese prickly ash, 10 parts of Mongollian Thyme Herb.
2. a kind of preparation method of Chinese prickly ash antibacterial toilet soap, comprising the following steps:
(1) Chinese prickly ash and Mongollian Thyme Herb be crushed into 40 meshes, are placed in extraction kettle, supercritical carbon dioxide is passed through with the flow velocity of 300L/h,
2.5h is extracted under conditions of 35 DEG C, 35MPa, the extract of Chinese prickly ash and Mongollian Thyme Herb is obtained from knockout drum；
(2) soap base is heated at 70 DEG C molten condition, Chinese prickly ash and the extract of Mongollian Thyme Herb, lauryl sodium sulfate, second is added
Alcohol, the heating stirring 45min at 85 DEG C, obtains perfumed soap material；
(3) perfumed soap material is poured into mold and is cooled and shaped, after taking-up, dried at 50 DEG C and dry 3.5h, after natural cooling, packaging
?.
Bacteriostatic test
Test method foundation: QB/T 2738-2012 " evaluation method of daily chemical products antibacterial bacteriostatic effect "；
Test specimen: perfumed soap prepared by embodiment 1-3 and comparative example 1 takes 5g respectively, is put into conical flask, sterile steaming is added
Distilled water 25mL, water-bath is shaken to perfumed soap and is dissolved at 45 DEG C, obtains test specimen；
Strain: staphylococcus aureus, Escherichia coli, Candida albicans (Shaanxi Biao Pu Pharmaceutical Technology Co., Ltd)；
Culture medium: nutrient agar (bacterium) is improved Martin's culture medium (fungi)；
Method: the measurement of sample bacteriostasis property is carried out using filter paper enzyme, it is 5.5mm's that filter paper, which is fabricated to diameter, with punch
The roundlet scraps of paper are affixed on the culture medium of even spread bacteria suspension by the roundlet scraps of paper, and separately sampled 50 μ L of product drips to every roundlet
On the scraps of paper, use sterile distilled water as blank control, in incubator；30 DEG C of bacterium are cultivated for 24 hours, after 27 DEG C of culture 72h of fungi
Observe result.Antibacterial circle diameter is measured, is repeated 3 times, the results are shown in Table 1.
The antibacterial circle diameter (mm) of 1 strain of table
As shown in Table 1, perfumed soap provided by the invention, good antimicrobial effect.
Claims (5)
1. a kind of Chinese prickly ash antibacterial toilet soap, it is characterised in that: be made of the raw material of following parts by weight:
50-75 parts of soap base, 1-5 parts of lauryl sodium sulfate, 140-180 parts of pure water, 1-5 parts of ethyl alcohol, 14-20 parts of Chinese prickly ash,
8-15 parts of green pepper, 1-4 parts of tremella.
2. a kind of Chinese prickly ash antibacterial toilet soap according to claim 1, it is characterised in that: be made of the raw material of following parts by weight: soap
69 parts of base, 3 parts of lauryl sodium sulfate, 165 parts of pure water, 3 parts of ethyl alcohol, 18 parts of Chinese prickly ash, 10 parts of Mongollian Thyme Herb, 2 parts of tremella.
3. a kind of preparation method of Chinese prickly ash antibacterial toilet soap described in claim 1, it is characterised in that: the following steps are included:
(1) tremella is added in pure water, impregnates 1-1.5h at room temperature, then impregnate 30min at 40-50 DEG C, at ultrasound
3-6min is managed, filtering obtains tremella extract；
(2) Chinese prickly ash and Mongollian Thyme Herb are crushed, is placed in extraction kettle, supercritical carbon dioxide is passed through with the flow velocity of 300-400L/h, in 30-
40 DEG C, extract 2-3h under conditions of 30-40MPa, the extract of Chinese prickly ash and Mongollian Thyme Herb is obtained from knockout drum；
(3) soap base is heated to molten condition, addition tremella extract, the extract of Chinese prickly ash and Mongollian Thyme Herb, 12 at 60-80 DEG C
Sodium alkyl sulfate, ethyl alcohol, the heating stirring 40-50min at 80-90 DEG C, obtain perfumed soap material；
(4) perfumed soap material is poured into mold and is cooled and shaped, after taking-up, dried at 45-55 DEG C and dry 3-4h, after natural cooling,
Packaging.
4. a kind of preparation method of Chinese prickly ash antibacterial toilet soap according to claim 3, it is characterised in that: in step (1) at ultrasound
The condition of reason is equal are as follows: supersonic frequency 45KHz, ultrasonic input power are 300W.
5. a kind of preparation method of Chinese prickly ash antibacterial toilet soap according to claim 3, it is characterised in that: in step (2) Chinese prickly ash and
Mongollian Thyme Herb crushed 40 meshes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811167791.1A CN109097216B (en) | 2018-10-08 | 2018-10-08 | Prickly ash bacteriostatic soap and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811167791.1A CN109097216B (en) | 2018-10-08 | 2018-10-08 | Prickly ash bacteriostatic soap and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109097216A true CN109097216A (en) | 2018-12-28 |
| CN109097216B CN109097216B (en) | 2021-02-02 |
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ID=64868352
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811167791.1A Active CN109097216B (en) | 2018-10-08 | 2018-10-08 | Prickly ash bacteriostatic soap and preparation method thereof |
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| Country | Link |
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| CN (1) | CN109097216B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110699197A (en) * | 2019-09-18 | 2020-01-17 | 重庆第二师范学院 | Preparation method and preparation system of pepper degerming soap |
| CN112375631A (en) * | 2020-11-24 | 2021-02-19 | 云南超越日化有限公司 | Antibacterial laundry detergent and preparation method thereof |
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| CN1568930A (en) * | 2003-07-12 | 2005-01-26 | 郦安江 | Method for applying active constitutent of Bunge prickly ash to daily used chemical products |
| CN1670159A (en) * | 2005-04-16 | 2005-09-21 | 王浩贵 | Forsythia fruit cleaning products |
| CN103351962A (en) * | 2013-05-09 | 2013-10-16 | 吉首大学 | Novel artemisia annua health care toilet soap |
| CN103361201A (en) * | 2012-03-28 | 2013-10-23 | 孔希 | Pepper seed soap |
| CN106675867A (en) * | 2016-12-12 | 2017-05-17 | 雅安职业技术学院 | Pericarpium zanthoxyli volatile oil perfumed soap making method |
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2018
- 2018-10-08 CN CN201811167791.1A patent/CN109097216B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1568930A (en) * | 2003-07-12 | 2005-01-26 | 郦安江 | Method for applying active constitutent of Bunge prickly ash to daily used chemical products |
| CN1670159A (en) * | 2005-04-16 | 2005-09-21 | 王浩贵 | Forsythia fruit cleaning products |
| CN103361201A (en) * | 2012-03-28 | 2013-10-23 | 孔希 | Pepper seed soap |
| CN103351962A (en) * | 2013-05-09 | 2013-10-16 | 吉首大学 | Novel artemisia annua health care toilet soap |
| CN106675867A (en) * | 2016-12-12 | 2017-05-17 | 雅安职业技术学院 | Pericarpium zanthoxyli volatile oil perfumed soap making method |
Non-Patent Citations (1)
| Title |
|---|
| 钟英英，张莹，李翠莲: "银耳、枸杞多糖联合啤酒酵母的体外抑菌研究", 《湖北农业科学》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110699197A (en) * | 2019-09-18 | 2020-01-17 | 重庆第二师范学院 | Preparation method and preparation system of pepper degerming soap |
| CN110699197B (en) * | 2019-09-18 | 2021-09-03 | 重庆第二师范学院 | Preparation method and preparation system of pepper degerming soap |
| CN112375631A (en) * | 2020-11-24 | 2021-02-19 | 云南超越日化有限公司 | Antibacterial laundry detergent and preparation method thereof |
| CN112375631B (en) * | 2020-11-24 | 2021-11-09 | 云南超越日化有限公司 | Antibacterial laundry detergent and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN109097216B (en) | 2021-02-02 |
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Address after: 715412 national Prickly Ash Industrial Park, Zhiyang Town, Hancheng City, Weinan City, Shaanxi Province Patentee after: Shaanxi Weikang Biotechnology Co.,Ltd. Address before: 715400 National Prickly Pepper Industrial Park, Zhiyang Town, Hancheng City, Weinan City, Shaanxi Province Patentee before: SHAANXI WEIKANG FOOD TECHNOLOGY Co.,Ltd. |
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