CN109092926A - A kind of production technology of the copper of diameter less than 15mm and its alloy bar material - Google Patents

A kind of production technology of the copper of diameter less than 15mm and its alloy bar material Download PDF

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Publication number
CN109092926A
CN109092926A CN201810819336.9A CN201810819336A CN109092926A CN 109092926 A CN109092926 A CN 109092926A CN 201810819336 A CN201810819336 A CN 201810819336A CN 109092926 A CN109092926 A CN 109092926A
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CN
China
Prior art keywords
stretching
diameter
bar
bar stock
skin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810819336.9A
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Chinese (zh)
Inventor
郭慧稳
蒋小亮
杜家荣
杨海丽
冷建伟
白志勇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Aluminum Luoyang Copper Processing Co Ltd
Original Assignee
China Aluminum Luoyang Copper Processing Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Aluminum Luoyang Copper Processing Co Ltd filed Critical China Aluminum Luoyang Copper Processing Co Ltd
Priority to CN201810819336.9A priority Critical patent/CN109092926A/en
Publication of CN109092926A publication Critical patent/CN109092926A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C37/00Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
    • B21C37/04Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire

Abstract

The production technology of a kind of copper of diameter less than 15mm and its alloy bar material, horizontal casting bar stock → sawing → production tensioning chuck → whole diameter stretches → strip off the skin stretching → intermediate annealing → pickling → tube reducing stretching → aligning → finished products → inspection, detection and packaging;Tube reducing stretches: using at least two passages are stretched on chain type stretching-machine, each diameter reduces 1mm, the modular angle of stretching die: 6 °~12 °;Strip off the skin stretching: being stripped off the skin using stretching-machine to bar stock, to remove bar stock surface casting flaw, strips off the skin stretching at least once, each diameter reduces by 1~2mm, and the stretching that strips off the skin is gradually reduced the diameter of bar stock;The process circulation that intermediate annealing, pickling and tube reducing stretch carries out finally being stretched to the trimmed size bar that diameter is less than 15mm at least once;Present invention diameter produced is less than the copper and its alloy bar material of 15mm, is particularly suitable for hot extrusion and processes difficult alloy, compared with traditional handicraft, is not limited by single ingot casting weight, production efficiency can be improved.

Description

A kind of production technology of the copper of diameter less than 15mm and its alloy bar material
Technical field
The present invention relates to nonferrous materials processing technique field, a kind of copper more particularly, to diameter less than 15mm and its The production technology of alloy bar material.
Background technique
The production technology of copper of traditional diameter less than 15mm and its alloy bar material are as follows:
Process flow 1: founding garden ingot → sawing → extruding copper and its alloy bar material → sawing → pickling → are aligned → are tied up Packaging;
Process flow 2: founding garden ingot → sawing → extruding bar stock → sawing → pickling → vertical bar stretches (can be with multi-pass) → aligning → scale sawing → finished products → enlacement packaging;
Due to the processing characteristics difference of different-alloy, the production technology of traditional minor diameter copper and its alloy bar material is for producing When certain alloys, manifest that process is too long, the excessively high drawback of functions of the equipments demand.Below with QSn6.5-0.1 and QSn7-0.2 tin For the production of phosphor bronze Thin-diameter rod, it is illustrated:
QSn6.5-0.1 and QSn7-0.2 tin-phosphor bronze bar can carry out hot extrusion processing, but the hot extrusion performance of the alloy There is its particularity.Consult metallurgical industry publishing house " heavy non-ferrous metal material processes handbook " (the 4th fascicle, P38) alloy bar material The forward extrusion metal rate of outflow allowable only 0.03~0.06 meter per second, the requirement in various copper and copper alloy, to extrusion speed It is most slow one of alloy.In specific production practices, it is believed that QSn6.5-0.1 and QSn7-0.2 tin-phosphor bronze bar hot extrusion Pressing element is difficult.The garden ingot system of a certain extruder can be squeezed because being limited by the tin-phosphor bronze forward extrusion metal rate of outflow Tin-phosphor bronze stick diameter out has a lower limit.For example, the φ 245mm extrusion system of 40MN hydraulic press, it is squeezable Minimum QSn6.5-0.1 and QSn7-0.2 tin-phosphor bronze stick diameter is φ 55mm, and can not squeeze the bar stock less than φ 55mm.Such as The bar stock for being less than φ 55mm is squeezed, then easily occurs squeezing crackle, it can not output qualified products.
If demand diameter is less than QSn6.5-0.1 the and QSn7-0.2 tin-phosphor bronze bar of 15mm, by traditional mode of production work Skill need to then squeeze bar stock from φ 55mm and carry out multi-pass stretching, and stretching passage is excessive, and process is too long.Or use small extruding garden Ingot system, then production efficiency is extremely inefficient.
In view of the foregoing, the production technology of a kind of copper of diameter less than 15mm and its alloy bar material is now developed.
Summary of the invention
Purpose of the invention is to overcome the shortcomings in the prior art, provides a kind of copper of diameter less than 15mm and its conjunction The production technology of golden bar, present invention diameter produced are less than the copper and its alloy bar material of 15mm, are particularly suitable for hot extrusion Difficult alloy is processed, compared with traditional handicraft, is not limited by single ingot casting weight, production efficiency can be improved.
The present invention to achieve the goals above, adopts the following technical scheme that a kind of diameter is less than the copper and its alloy of 15mm The production technology of bar, horizontal casting bar stock → sawing → production tensioning chuck → whole diameter stretches → strip off the skin stretching → intermediate annealing → pickling → tube reducing stretching → aligning → finished products → inspection, detection and packaging.
The first step, horizontal casting bar stock: carrying out horizontal type level continuously casting using Ajax-Wyatt furnace, casts setting specification Casting rod base, smelting temperature: 1150~1250 DEG C, casting speed: 25~30m/h, chemical component meet GB5231-2012;
Second step, sawing: sawing casting rod base is at required length;
Third step, make tensioning chuck: every bar stock makes tensioning chuck, according to the tonnage of postorder stretching-machine, stretches folder Head production length is 100~150mm;
4th step, whole diameter stretch: stretching to bar stock, reduce the diameter of bar stock;
5th step, strip off the skin stretching: being stripped off the skin using stretching-machine to bar stock, to remove bar stock surface casting flaw, is stripped off the skin It stretches at least once, each diameter reduces by 1~2mm, and the stretching that strips off the skin is gradually reduced the diameter of bar stock.
6th step, intermediate annealing: bar stock is put into annealing furnace by the gross, at 250~300 DEG C of temperature, keeps the temperature 55~65 minutes, 630~650 DEG C are warming up to, keeps the temperature 90~120 minutes;
7th step, pickling: bar progress sulfuric acid is washed, is washed by the gross;
8th step, tube reducing stretch: using at least two passages are stretched on chain type stretching-machine, each diameter reduces 1mm, The modular angle of stretching die: 6 °~12 °;The process circulation that intermediate annealing, pickling and tube reducing stretch at least once, be finally stretched to Diameter is less than the trimmed size bar of 15mm;
Aligning: 9th step trimmed size bar obtained is aligned;
Tenth step, finished products: at 250~280 DEG C of in-furnace temperature of annealing, trimmed size bar by the gross is put into annealing furnace It is interior, keep the temperature 100~120 minutes;
11st step checks, detects and packs: checking surface quality, the size of bar, detects final performance are as follows: and Rm >= 470Mpa, A >=13% after meeting production requirement, carry out finished product packing.
The beneficial effects of the present invention are: present invention diameter produced is less than the copper and its alloy bar material of 15mm, it is especially suitable Difficult alloy is processed for hot extrusion, compared with traditional handicraft, is not limited by single ingot casting weight, and production effect can be improved Rate.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings:
Fig. 1 is process flow chart.
Specific embodiment
Below with reference to embodiment, invention is further described in detail with specific embodiment:
Embodiment 1
Produce QSn6.5-0.1 tin-phosphor bronze vertical bar stick, specification: φ 8mm, length 1000mm or more.State: Y state;Rm ≥ 470Mpa, A >=13%:
Horizontal casting bar stock: the first step carries out horizontal type level continuously casting using Ajax-Wyatt furnace, casts φ 22mm specification Casting rod base, smelting temperature: 1200 DEG C, casting speed: 25~30m/h, chemical component meet GB5231-2012;
Second step, sawing: the casting rod base of sawing φ 22mm is at required length;
Third step, make tensioning chuck: every bar stock makes tensioning chuck, according to the tonnage of postorder stretching-machine, stretches folder Head production length is 100~150mm;
4th step, whole diameter stretch: stretching to bar stock, be stretched to the bar stock of φ 20mm;
5th step, once strip off the skin stretching: it is stripped off the skin using stretching-machine to bar stock, to remove bar stock surface casting flaw, It strips off the skin and is stretched to the bar stock of φ 19.2mm;
The secondary stretching that strips off the skin: it strips off the skin and is stretched to the bar stock of φ 18.5mm;
6th step, an intermediate annealing: bar stock is put into annealing furnace by the gross, at 250~300 DEG C of temperature, keeps the temperature 60 minutes, 630~650 DEG C are warming up to, keeps the temperature 90~120 minutes;
7th step, a pickling: bar progress sulfuric acid is washed, is washed by the gross;
8th step, one time tube reducing stretches: using being stretched on chain type stretching-machine, it is stretched to the bar stock of φ 17.5mm, The modular angle of stretching die: 6 °~12 °;
Secondary tube reducing stretches: being stretched to the bar stock of φ 16.5mm;
Tube reducing stretches three times: being stretched to the bar stock of φ 15.5mm;
Secondary intermediate annealing: bar stock is put into annealing furnace by the gross, at 250~300 DEG C of temperature, is kept the temperature 60 minutes, is warming up to 630~650 DEG C, keep the temperature 100~120 minutes;
White picking: bar progress sulfuric acid is washed, is washed by the gross;
Four times tube reducing stretches: being stretched to the bar stock of φ 13.5mm;
Five times tube reducing stretches: being stretched to the bar stock of φ 12mm;
Intermediate annealing three times: bar stock is put into annealing furnace by the gross, at 250~300 DEG C of temperature, is kept the temperature 60 minutes, is warming up to 630~650 DEG C, keep the temperature 100~120 minutes;
Pickling three times: bar progress sulfuric acid is washed, is washed by the gross;
Six times tube reducing stretches: being stretched to the bar stock of φ 9.5mm;
Four intermediate annealing: bar stock is put into annealing furnace by the gross, at 250~300 DEG C of temperature, is kept the temperature 60 minutes, is warming up to 630~650 DEG C, keep the temperature 100~120 minutes;
Four pickling: bar progress sulfuric acid is washed, is washed by the gross;
Seven times tube reducing stretches: being stretched to the trimmed size bar of φ 8mm;
9th step, aligning: the bar of aligning φ 8mm;
Tenth step, finished products: at 250~280 DEG C of in-furnace temperature of annealing, the finished product bar of φ 8mm is put into annealing by the gross In furnace, 100~120 minutes are kept the temperature;
11st step checks, detects and packs: checking surface quality, the size of bar, detects final performance are as follows: and Rm >= 470Mpa, A >=13% after meeting production requirement, carry out finished product packing.
Part not in the detailed description of the invention is the prior art, therefore the present invention is not described in detail.

Claims (3)

1. the production technology of a kind of copper of diameter less than 15mm and its alloy bar material, it is characterised in that: horizontal casting bar stock → saw Tensioning chuck → the whole diameter stretches → stretching → intermediate annealing → pickling → tube reducing stretching → aligning → finished product that strips off the skin is cut → makes to move back Fire → inspection, detection and packaging.
2. the production technology of a kind of copper of the diameter according to claim 1 less than 15mm and its alloy bar material, feature exist In: horizontal casting bar stock: the first step carries out horizontal type level continuously casting using Ajax-Wyatt furnace, casts the casting rod of setting specification Base, smelting temperature: 1150~1250 DEG C, casting speed: 25~30m/h, chemical component meet GB5231-2012;
Second step, sawing: sawing casting rod base is at required length;
Third step, make tensioning chuck: every bar stock makes tensioning chuck, according to the tonnage of postorder stretching-machine, tensioning chuck system Making length is 100~150mm;
4th step, whole diameter stretch: stretching to bar stock, reduce the diameter of bar stock;
5th step, strip off the skin stretching: being stripped off the skin using stretching-machine to bar stock, to remove bar stock surface casting flaw, strip off the skin stretching At least once, each diameter reduces by 1~2mm, and the stretching that strips off the skin is gradually reduced the diameter of bar stock.
3. the production technology of a kind of copper of the diameter according to claim 1 less than 15mm and its alloy bar material, feature exist In: the 6th step, intermediate annealing: bar stock is put into annealing furnace by the gross, at 250~300 DEG C of temperature, keeps the temperature 55~65 minutes, heating To 630~650 DEG C, 90~120 minutes are kept the temperature;
7th step, pickling: bar progress sulfuric acid is washed, is washed by the gross;
8th step, tube reducing stretch: using at least two passages are stretched on chain type stretching-machine, each diameter reduces 1mm, stretches The modular angle of mould: 6 °~12 °;The process circulation that intermediate annealing, pickling and tube reducing stretch carries out at least once, being finally stretched to diameter Trimmed size bar less than 15mm;
Aligning: 9th step trimmed size bar obtained is aligned;
Tenth step, finished products: at 250~280 DEG C of in-furnace temperature of annealing, trimmed size bar by the gross is put into annealing furnace, Heat preservation 100~120 minutes;
11st step checks, detects and packs: checking surface quality, the size of bar, detects final performance are as follows: and Rm >= 470Mpa, A >=13% after meeting production requirement, carry out finished product packing.
CN201810819336.9A 2018-07-24 2018-07-24 A kind of production technology of the copper of diameter less than 15mm and its alloy bar material Pending CN109092926A (en)

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Application Number Priority Date Filing Date Title
CN201810819336.9A CN109092926A (en) 2018-07-24 2018-07-24 A kind of production technology of the copper of diameter less than 15mm and its alloy bar material

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114472580A (en) * 2021-12-20 2022-05-13 上海海亮铜业有限公司 Preparation method of high-strength super-long cupronickel alloy capillary tube

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3848319A (en) * 1973-03-08 1974-11-19 Ciardi A Procedure for fabricating ultra-small gold wire
CN1948531A (en) * 2006-11-03 2007-04-18 宁波博威集团有限公司 High manganese copper nickel zinc alloy and preparation method of its wire, rod and plate belt material
CN103320596A (en) * 2013-06-25 2013-09-25 中铝洛阳铜业有限公司 Manufacturing process of tin-phosphor bronze stretching rod
CN105886832A (en) * 2016-05-17 2016-08-24 安徽鑫科新材料股份有限公司 Bronze bar and production method thereof
CN106040774A (en) * 2016-06-07 2016-10-26 浙江三瑞铜业有限公司 Bronze wire production technology

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3848319A (en) * 1973-03-08 1974-11-19 Ciardi A Procedure for fabricating ultra-small gold wire
CN1948531A (en) * 2006-11-03 2007-04-18 宁波博威集团有限公司 High manganese copper nickel zinc alloy and preparation method of its wire, rod and plate belt material
CN103320596A (en) * 2013-06-25 2013-09-25 中铝洛阳铜业有限公司 Manufacturing process of tin-phosphor bronze stretching rod
CN105886832A (en) * 2016-05-17 2016-08-24 安徽鑫科新材料股份有限公司 Bronze bar and production method thereof
CN106040774A (en) * 2016-06-07 2016-10-26 浙江三瑞铜业有限公司 Bronze wire production technology

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114472580A (en) * 2021-12-20 2022-05-13 上海海亮铜业有限公司 Preparation method of high-strength super-long cupronickel alloy capillary tube
CN114472580B (en) * 2021-12-20 2024-04-02 上海海亮铜业有限公司 Preparation method of high-strength ultra-long white copper alloy capillary

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Application publication date: 20181228

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