CN109077977B - Plant repairing shampoo and preparation method thereof - Google Patents
Plant repairing shampoo and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention relates to the technical field of daily chemical articles, in particular to a plant repairing shampoo and a preparation method thereof. The plant repairing shampoo is prepared from at least the following raw materials: alkylolamide, sodium laureth sulfate, sodium cocoyl glycinate, sodium lauroyl amphoacetate, guar gum hydroxypropyl trimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride, tert-butyl-4-hydroxy anisole, sodium pyrrolidone carboxylate, sodium lactate, L-malic acid, fructus amomi bamboo extract, asparagus fern root extract, guava fruit extract, illicium verum fruit extract, citric acid, essence and deionized water. The invention is compounded by plant essences of bamboo amomum fruit extract, asparagus fern root extract, guava fruit extract, illicium verum fruit extract and the like and a plurality of cleaning components, and the components are mutually cooperated, so that the efficacy is fully enhanced, and the invention has good foaming performance, combing performance and moisture retention.
Description
Technical Field
The invention relates to the technical field of daily chemical articles, in particular to a plant repairing shampoo and a preparation method thereof.
Background
Hair is one of the important physiological features of mammals, and has the main functions of protecting skin, regulating body temperature, feeling, hiding, and the like. With the development of society, one of the most important social functions of human hair is "beauty". In daily communication and activities, healthy, beautiful hair and beautiful hair style can bring endless charm to people. Therefore, the health and maintenance of hair is very important to the personal image. In daily life, various external factors can cause damage along with hair, and the damage mainly comprises physical damage, chemical damage, thermal damage, sunlight aging damage and the like. The physical damage refers to damage to hair caused by external force, such as stretching force caused by a comb and friction force caused by comb teeth during combing of hair. Chemical damage refers to damage caused by changes in the structural composition of the hair, such as damage to hair scales from hair dyes, perming agents, bleaches, and straighteners. The heat damage refers to hair damage caused by over-high temperature during the hair drier or hair perming process. Photoaging damage refers to ultraviolet light that causes changes in hair structure and photodegradation of proteins.
Shampoo is a common bathing product, is very commonly used, and has a plurality of shampoo products with different functions on the market. Although the shampoo in the prior art has good effects on cleaning and decontaminating, the hair repairing and repairing needs to be further improved on the aspect of repairing damaged hair which is easy to break, split, dry and the like, so the hair repairing and repairing are always the key points of research. The silicone oil has high molecule flexibility, weak intermolecular attraction, low surface energy, excellent spreadability, good waterproof performance and film forming performance, and the characteristics enable the silicone oil to uniformly cover on a hair shaft to form a compact hydrophobic film, so that the hair surface is smooth and flat, consumers can easily realize excellent conditioning performance, and the silicone oil is a common raw material for personal care products with high cost performance. For example, the hair lotion of CN103349622 has a silky texture by adding a softener such as silicone emulsion. However, excessive silicone oil deposition can cause collapse of hair, clogging of hair follicles, and drying out of hair with prolonged use. In addition, the silicone oil is not easy to degrade and is easy to cause serious pollution to the environment.
Disclosure of Invention
In order to solve the above technical problems, a first aspect of the present invention provides a plant repairing shampoo, which is prepared from at least the following components:
alkylolamide, sodium laureth sulfate, sodium cocoyl glycinate, sodium lauroyl amphoacetate, guar gum hydroxypropyl trimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride, tert-butyl-4-hydroxy anisole, sodium pyrrolidone carboxylate, sodium lactate, L-malic acid, fructus amomi bamboo extract, asparagus fern root extract, guava fruit extract, illicium verum fruit extract, citric acid, essence and deionized water.
As a preferred technical scheme, the weight ratio of the asparagus fern root extract, the guava fruit extract and the illicium verum fruit extract is 2: 2: 1.
as a preferred technical scheme, the plant repairing shampoo at least comprises the following components in parts by weight:
30-36 parts of alkylolamide, 80-100 parts of sodium lauryl polyoxyethylene ether sulfate, 65-85 parts of sodium cocoyl glycinate, 20-25 parts of sodium lauroyl amphoacetate, 9-12 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6-8 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5-6 parts of tert-butyl-4-hydroxy anisole, 8-10 parts of sodium pyrrolidone carboxylate, 2.5-3 parts of sodium lactate, 2-3 parts of L-malic acid, 7-17 parts of bamboo fructus amomi extract, 10-20 parts of asparagus fern root extract, 10-20 parts of guava fruit extract, 5-10 parts of illicium verum fruit extract, 0.5-1.5 parts of citric acid, 2-6 parts of essence and 800-1000 parts of deionized water.
As a preferred technical scheme, the plant repairing shampoo at least comprises the following components in parts by weight:
32 parts of alkylolamide, 90 parts of lauryl alcohol polyoxyethylene ether sodium sulfate, 70 parts of sodium cocoyl glycinate, 22 parts of sodium lauroyl amphoacetate, 10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 7 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5.5 parts of tert-butyl-4-hydroxy anisole, 9 parts of pyrrolidone carboxylic acid sodium, 2.8 parts of sodium lactate, 2.5 parts of L-malic acid, 10 parts of fructus amomi bambusae extract, 14 parts of asparagus fern root extract, 14 parts of guava fruit extract, 7 parts of illicium verum fruit extract, 1 part of citric acid, 5 parts of essence and 900 parts of deionized water.
As a preferred technical solution, the alkylolamide is at least one selected from coconut oil diethanolamide, lauroyl-linoleoyl diethanolamide, lauroyl-myristoyl diethanolamide, isostearyl diethanolamide, linoleoyl diethanolamide, myristoyl diethanolamide, oleyl diethanolamide, sesame diethanolamide, soybean diethanolamide, stearyldiethanolamide and wheat germ diethanolamide.
As a preferred technical solution, the alkylolamide is coconut diethanolamide and/or stearyl diethanolamide.
The second aspect of the invention provides a preparation method of the plant repairing shampoo, which at least comprises the following steps:
s1, adding alkylolamide, sodium lauryl polyoxyethylene ether sulfate, sodium cocoyl glycinate, sodium lauroyl amphoacetate and tert-butyl-4-hydroxyanisole into deionized water, stirring at the speed of 200-300 rpm at the temperature of 75-85 ℃, and stirring for 20-30 min;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding guar gum hydroxypropyl trimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride and sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20-30 min;
s3, cooling the mixture obtained in the step S2, sequentially adding the bamboo fructus amomi extract, the asparagus fern root extract, the guava fruit extract and the illicium verum fruit extract, stirring at the speed of 600-700 rpm for 20-30 min;
s4, cooling the mixture in the step S3, sequentially adding sodium lactate, L-malic acid, citric acid and essence, and uniformly stirring to obtain the product.
As a preferable technical scheme, the preparation method of the plant repairing shampoo at least comprises the following steps in parts by weight:
s1, adding 30-36 parts of alkylolamide, 80-100 parts of sodium lauryl polyoxyethylene ether sulfate, 65-85 parts of sodium cocoyl glycinate, 20-25 parts of sodium lauroyl amphoacetate and 5-6 parts of tert-butyl-4-hydroxyanisole into 800-1000 parts of deionized water, and stirring at the temperature of 75-85 ℃ and the stirring speed of 200-300 rpm for 20-30 min;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding 9-12 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6-8 parts of dipalmitoyloxyethyl dimethyl ammonium chloride and 8-10 parts of sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20-30 min;
s3, cooling the mixture obtained in the step S2, sequentially adding 7-17 parts of fructus amomi extract, 10-20 parts of asparagus fern root extract, 10-20 parts of guava fruit extract and 5-10 parts of illicium verum fruit extract, stirring at the speed of 600-700 rpm for 20-30 min;
s4, cooling the mixture obtained in the step S3, sequentially adding 2.5-3 parts of sodium lactate, 2-3 parts of L-malic acid, 0.5-1.5 parts of citric acid and 2-6 parts of essence, and uniformly stirring to obtain the product.
As a preferable technical scheme, in the step S3, after the mixture in the step S2 is cooled to 50-60 ℃, the bamboo amomum fruit extract, the asparagus fern root extract, the guava fruit extract and the illicium verum fruit extract are sequentially added.
As a preferable technical scheme, in the step S4, after the temperature of the mixture in the step S3 is reduced to 40 ℃, sodium lactate, L-malic acid, citric acid and essence are sequentially added.
Has the advantages that: the invention is compounded by plant essences of bamboo amomum fruit extract, asparagus fern root extract, guava fruit extract, illicium verum fruit extract and the like and a plurality of cleaning components, and all the components are mutually cooperated, so that the efficacy is fully enhanced, and the invention has good foaming performance, combing performance and moisturizing performance.
The plant shampoo with the functions of repairing split hairs, drying, breaking easily and the like is prepared by optimally mixing various components of alkylolamide, sodium laureth sulfate, cocoyl sodium glycinate, sodium lauroyl amphoacetate, guar gum hydroxypropyl trimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride, tert-butyl-4-hydroxy anisole, sodium pyrrolidone carboxylate, sodium lactate, L-malic acid, a bamboo villous amonmum fruit extract, an asparagus fern root extract, a guava fruit extract, an illicium verum fruit extract, citric acid, essence and deionized water by adopting a comprehensive innovative technology and a fine optimized preparation process. After the shampoo is used for a long time, the hair is soft like silk, is bright and easy to comb, and has enhanced toughness.
Detailed Description
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In case of conflict, the present specification, including definitions, will control.
Notwithstanding that the numerical ranges and parameters setting forth the broad scope of the invention are approximations, the numerical values set forth in the specific examples are reported as precisely as possible. Any numerical value, however, inherently contains certain errors necessarily resulting from the standard deviation found in their respective testing measurements.
When a range of values is disclosed herein, the range is considered to be continuous and includes both the minimum and maximum values of the range, as well as each value between such minimum and maximum values. Further, when a range refers to an integer, each integer between the minimum and maximum values of the range is included. Further, when multiple range-describing features or characteristics are provided, the ranges may be combined. In other words, unless otherwise indicated, all ranges disclosed herein are to be understood to encompass any and all subranges subsumed therein. For example, a stated range from "1 to 10" should be considered to include any and all subranges between the minimum value of 1 and the maximum value of 10. Exemplary subranges of the range 1 to 10 include, but are not limited to, 1 to 6.1, 3.5 to 7.8, 5.5 to 10, and the like.
In order to solve the above problems, a first aspect of the present invention provides a plant repairing shampoo, which is prepared from at least the following ingredients:
alkylolamide, sodium laureth sulfate, sodium cocoyl glycinate, sodium lauroyl amphoacetate, guar gum hydroxypropyl trimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride, tert-butyl-4-hydroxy anisole, sodium pyrrolidone carboxylate, sodium lactate, L-malic acid, fructus amomi bamboo extract, asparagus fern root extract, guava fruit extract, illicium verum fruit extract, citric acid, essence and deionized water.
As a preferred embodiment, the weight ratio of the wenzhu root extract, the guava fruit extract and the illicium verum fruit extract is 2: 2: 1.
preferably, the plant repairing shampoo at least comprises the following components in parts by weight:
30-36 parts of alkylolamide, 80-100 parts of sodium lauryl polyoxyethylene ether sulfate, 65-85 parts of sodium cocoyl glycinate, 20-25 parts of sodium lauroyl amphoacetate, 9-12 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6-8 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5-6 parts of tert-butyl-4-hydroxy anisole, 8-10 parts of sodium pyrrolidone carboxylate, 2.5-3 parts of sodium lactate, 2-3 parts of L-malic acid, 7-17 parts of bamboo fructus amomi extract, 10-20 parts of asparagus fern root extract, 10-20 parts of guava fruit extract, 5-10 parts of illicium verum fruit extract, 0.5-1.5 parts of citric acid, 2-6 parts of essence and 800-1000 parts of deionized water.
More preferably, the plant repairing shampoo is prepared from the following raw materials in parts by weight:
32 parts of alkylolamide, 90 parts of lauryl alcohol polyoxyethylene ether sodium sulfate, 70 parts of sodium cocoyl glycinate, 22 parts of sodium lauroyl amphoacetate, 10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 7 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5.5 parts of tert-butyl-4-hydroxy anisole, 9 parts of pyrrolidone carboxylic acid sodium, 2.8 parts of sodium lactate, 2.5 parts of L-malic acid, 10 parts of fructus amomi bambusae extract, 14 parts of asparagus fern root extract, 14 parts of guava fruit extract, 7 parts of illicium verum fruit extract, 1 part of citric acid, 5 parts of essence and 900 parts of deionized water.
Bamboo amomum fruit extract
The fructus Amomi is a stroma of Hypocrella bambusae (Berk. et Br.) Sacc. Collected all the year round, and then dried in the sun for later use.
The original shape of the stroma is approximately hemispherical. When fresh, the color of pink or light flesh is looser, becomes grayish yellow or reddish brown after being dried, is harder, has irregular coracoid bulges on the surface, and has the internal pink to dark red color with the diameter of 0.7 to (1.5-2) cm.
The chemical components of fructus Amomi include 5% D-mannitol (D-mannitol), hypocrellin (hypocrellin) A, B, hypocrellin peroxide (peroxisporin), hexadecanoic acid (hexadecanoic acid) and octadecanoic acid (octadecanoic acid).
Pungent, astringent and mild in nature and taste. The functions are mainly used for dispelling wind and eliminating dampness, detoxifying and relieving itching, and mainly treating rheumatic arthritis and leukoplakia vulvae.
The extraction method of the bamboo amomum fruit extract comprises the following steps: taking 10g of dried bamboo fructus Amomi, adding 80mL of petroleum ether, soaking for 12h, and performing ultrasonic extraction for 3 times, each for 20 min. Filtering to obtain filtrate. Recovering petroleum ether from the filtrate by rotary evaporator to obtain fructus Amomi extract.
Wen bamboo root extract
The radix Phyllostachydis Henonis is Asparagus setaceae (Kunth) Jessop (Asparagus setaria Kunth; root of Asparagus plus Bak. Removing vine stem in autumn, digging out root tuber, removing soil, boiling with water or steaming to crack skin, peeling off skin, cutting into segments, and drying.
The radix Phyllostachys is slender and slightly fleshy, and has a length of 15-24cm and a diameter of 3-4 mm. The surface is yellowish white, with wrinkles of varying depth and fine rootlets. Flexible, not easy to break and yellow-white cross section. Slightly fragrant smell, bitter and slightly pungent taste.
The chemical components of the root of the Phyllostachys nigra comprise: aspartic acid (aspartic acid), threonine (threonine), serine (serine), glutamic acid (glutamic acid), glycine (glycine), alanine (alanine), valine (valine), methionine (methionine), isoleucine (isoluteine), lysine (lysine), histidine (histadine), arginine (arginine), proline (proline), cysteine (cysteine). Trace elements: calcium, manganese, iron, copper, zinc, chromium and lead.
Sweet in nature, slightly bitter and cold in nature. The function is mainly used for moistening lung and relieving cough; cooling blood and dredging forest; yin deficiency with dryness of the lung; cough; hemoptysis; and (4) dripping urine.
The extraction method of the asparagus fern root extract comprises the following steps:
a. washing Phyllostachys Pubescens root with distilled water, oven drying, and pulverizing. Weighing 1g of asparagus fern root powder, putting the asparagus fern root powder into a microwave digestion instrument, adding 20mL of water, putting the asparagus fern root powder into the microwave digestion instrument, heating to 60 ℃, and extracting for 20 min;
b. filtering, and fixing the volume of the filtrate to 50 mL; centrifuging the filtrate at 1000r/min for 10min, and collecting supernatant.
Guava fruit extract
The guava fruit is mature fruit of Psidium guajava Linn of Myrtaceae. Collected in autumn when the fruit is ripe, it is usually fresh, and the flesh is usually yellow and also white or carmine.
The chemical components of the mature fruit comprise quercetin (quercetin), guajatein (guaijaverin), gallic acid (gallic acid), gallic acid (ellagic acid), leucocyanidin (leucocyanidin), vitamin C (330 mg%), and rhamnose (rhamnose), xylose (xylose), ribose (ribose), arabinose (a rabi-nase), fructose (fructose), glucose (glucose), galactose (galactose), sucrose (sucrose), valine (valine), alanine (alanine), threonine (threonine), aspartic acid (aspartic acid), glutamic acid (glutamic acid), and cystine (cysteine). And contains herba Polygoni Avicularis glycoside (avicularin).
Sweet, astringent and mild in nature and taste. Has effects in lowering blood sugar and stopping bleeding.
The extraction method of the guava fruit extract comprises the following steps:
a. adding 1L deionized water into 10g of dried and pulverized guava fruit, placing in a flash extractor, and primarily extracting at room temperature for 1min at 12000r/min of the flash extractor; leaching in water bath oscillator at 50 deg.C for 40min, vacuum filtering the hot extractive solution, collecting filtrate, and cooling to room temperature to obtain extractive solution.
b. Adding 1.5 times volume of anhydrous ethanol into the extractive solution, standing at 4 deg.C overnight, centrifuging at 8000r/min for 15min, and collecting supernatant. The weight ratio of 10 ml: adding active carbon at a ratio of 1g, stirring for 15min, adsorbing for removing impurities and decolorizing, and filtering to obtain filtrate to obtain Psidium guajava fruit extract.
Radix et rhizoma Dysosmatis repens fruit extract
The Fatsia japonica fruit is the fruit of Fatsia japonica Fatscia japonica (Thunb.) Dexcne. Et Planch. [ Aralia japonica Thunb.) of Araliaceae, and the fruit is approximately spherical, 5mm in diameter and black when cooked.
The mature fruit contains echinocystic acid-3-alpha-L-arabinopyranose-28-O-alpha-L-rhamnopyranose (1 → 4) -beta-D-glucopyranose (1 → 4) -beta-D-glucopyranoside [ ethiocystic acid-3-alpha-L-arabi nopyranosyl-28-O-alpha-L-rhamnopyranose-nosyl (1 → 4) -beta-D-glucopyranosyl (1 → 4) -beta-D-glucopyranoside ], hederagenin-3-O-alpha-L-arabinopyranose-28-O-alpha-L-rhamnopyranose (1 → 4) -beta-D-glucopyranose (1 → 4) -beta-D-glucopyranoside [ heptaderinin-3- ] -3 -O-alpha-L-arabinopyranosyl system (1 → 4) -beta-D-glucopyranosyl (1 → 4) -beta-L-arabinopyranose-28-O-alpha-L-rhamnopyranose (1 → 4) -beta-D-glucopyranose (1 → 4) -D-glucopyranoside [ oleanolic acid-3-O-beta-D-glucopyranosyl (1 → 2) -alpha-L-arabinopyranosyl-28-O-alpha-L-rhamnopyranosyl (1 → 4) -beta-D-glucopyranosyl-3-O-beta-L-glucopyranosyl (1 → 4) -D-glucopyranoside ], hederagenin-3-O-beta-D-glucopyranosyl (1 → 2) -alpha-L-arabinopyranose-28-O-alpha-L-glucopyranosyl- Rhamnopyranose (1 → 4) - β -D-glucopyranose [ heliotropin-3-O- β -D-glucopyranosyl (1 → 2) - α -L-arabinopyranosyl-28-O- α -L-rhamnopyranoside-nosyl (1 → 4) - β -D-glucopyranosyl (1 → 4) - β -dgropyranoside), hederagenin-3-O- β -D-glucopyranose (1 → 4) - β -D-glucopyranoside [ heliotropin-3-O- β -D-glucopyranose (1 → 4) - β -D-glucopyranosyl (1 → 4) - β -D-glucopyranoside ], hederagenin-3-O-alpha-L-arabinopyranoside (i.e. gymnadenin B1), hederagenin-3-O-beta-D-glucopyranoside (hederagenin-3-O-beta-D-glucopyranoside), hederagenin-3-O-beta-D-glucopyranoside (1 → 4) -alpha-L-arabinopyranoside [ hederagenin-3-O-beta-D-glucopyranoside (1 → 4) -alpha-L-arabinopyranoside ]. It also contains squalene (squalene), beta-amyrin sterol (beta-amyrin sterol), triacylglycerol (triglyceride), lipid and acid (fat acid), fatty acid methyl ester (fat acid methyl ester), volatile oil, cyanidin-3-galactosyl xyloside (cyanidin-3-lathytoside).
Pungent, bitter, warm in nature and less toxic. The functions are mainly used for reducing phlegm and relieving cough; wind dispelling and dehumidification; removing blood stasis and relieving pain; cough with profuse sputum; rheumatic arthralgia; gout; traumatic injury.
The extraction method of the illicium verum fruit extract comprises the following steps:
a. washing the dried illicium verum fruits with distilled water, crushing to 20-60 meshes, wrapping with filter paper, binding with cotton ropes, and putting into a Soxhlet extraction column; adding petroleum ether with a boiling range of 60-70 ℃ into a Soxhlet flask to serve as an extracting solution, wherein the proportion of the extracting solution to raw materials is 100ml:2g, and heating, boiling and extracting for 10 hours;
b. cooling the leaching liquor obtained in the step, regulating the heating temperature of reduced pressure concentration to be 60 ℃, and reducing pressure concentration of the leaching liquor to 1/30 of the original volume to obtain concentrated solution;
c. closing the concentrated solution, placing the concentrated solution into a freezing chamber, refrigerating and standing the concentrated solution at a temperature of between 5 ℃ below zero and 30 ℃ below zero for 5 hours, taking the concentrated solution out, centrifuging the concentrated solution for 20 minutes at a speed of 10000r/min, and taking supernatant;
d. the supernatant was slowly transferred to a silica gel column, and the specific gravity of the filler and the amount of the sample was controlled at 40g:1 ml. And (3) taking petroleum ether-ethyl acetate as eluent, collecting the eluent in sections, and concentrating the middle section of the eluent under reduced pressure to obtain the illicium verum fruit extract.
The alkylolamide, the sodium lauryl polyoxyethylene ether sulfate, the sodium cocoyl glycinate and the sodium lauroamphoacetate are mild in property and low in irritation, and can play a role in cleaning hair and effectively cleaning scalp. Guar hydroxypropyltrimonium chloride can improve the softness of hair.
The asparagus fern root extract, the guava fruit extract and the illicium verum extract are mutually synergistic, and have good repairing effect and safety performance. Meanwhile, the radix et rhizoma Dysosmatis repens extract can promote the asparagus fern root extract and the guava fruit extract to rapidly penetrate into the hair core. The applicant finds that the weight ratio of the asparagus fern root extract, the guava fruit extract and the illicium verum fruit extract is 2: 2: 1, the shampoo has the best repairing effect. The possible reasons are that the main component of hair is keratin, that loss of keratin is one of the main causes of hair damage, and that the proportions of the three plant extracts are just as necessary to supplement the components required for keratin.
In a preferred embodiment, the alkylolamide is at least one selected from coconut diethanolamide, lauroyl-linoleoyl diethanolamide, lauroyl-myristoyl diethanolamide, isostearyl diethanolamide, linoleoyl diethanolamide, myristoyl diethanolamide, oleyldiethanolamide, sesamol diethanolamide, soyabean diethanolamide, stearyldiethanolamide and wheat germ diethanolamide.
Preferably, the alkylolamides are cocodiethanolamide and/or stearyldiethanolamide.
Adding fructus Amomi extract into radix Phyllostachydis Henonis extract, fructus Psidii Guajavae extract and radix et rhizoma Dysosmatis fruit extract. Dipalmitoyl oxyethyl dimethyl ammonium chloride, alkylolamide and bamboo fructus amomi extract interact to form a network structure on the surface layer of damaged hair scales, so that the moisture content in hair is kept stable, the moisture loss is reduced under the condition of low humidity, the excessive moisture absorption of the hair is prevented under the condition of high humidity, and the protective layer also has the wear resistance.
The essence is an essence commonly adopted in the industry. In the formula, corresponding essence can be freely selected according to the requirement.
The second aspect of the invention provides a preparation method of the plant repairing shampoo, which at least comprises the following steps in parts by weight:
s1, adding alkylolamide, sodium lauryl polyoxyethylene ether sulfate, sodium cocoyl glycinate, sodium lauroyl amphoacetate and tert-butyl-4-hydroxyanisole into deionized water, stirring at the speed of 200-300 rpm at the temperature of 75-85 ℃, and stirring for 20-30 min;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding guar gum hydroxypropyl trimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride and sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20-30 min;
s3, cooling the mixture obtained in the step S2, sequentially adding the bamboo fructus amomi extract, the asparagus fern root extract, the guava fruit extract and the illicium verum fruit extract, stirring at the speed of 600-700 rpm for 20-30 min;
s4, cooling the mixture in the step S3, sequentially adding sodium lactate, L-malic acid, citric acid and essence, and uniformly stirring to obtain the product.
Preferably, the preparation method of the plant repairing shampoo at least comprises the following steps in parts by weight:
s1, adding 30-36 parts of alkylolamide, 80-100 parts of sodium lauryl polyoxyethylene ether sulfate, 65-85 parts of sodium cocoyl glycinate, 20-25 parts of sodium lauroyl amphoacetate and 5-6 parts of tert-butyl-4-hydroxyanisole into 800-1000 parts of deionized water, and stirring at the stirring speed of 200-300 rpm for 20-30 min at the temperature of 75-85 ℃;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding 9-12 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6-8 parts of dipalmitoyloxyethyl dimethyl ammonium chloride and 8-10 parts of sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20-30 min;
s3, cooling the mixture obtained in the step S2, sequentially adding 7-17 parts of fructus amomi extract, 10-20 parts of asparagus fern root extract, 10-20 parts of guava fruit extract and 5-10 parts of illicium verum fruit extract, stirring at the speed of 600-700 rpm for 20-30 min;
s4, cooling the mixture obtained in the step S3, sequentially adding 2.5-3 parts of sodium lactate, 2-3 parts of L-malic acid, 0.5-1.5 parts of citric acid and 2-6 parts of essence, and uniformly stirring to obtain the product.
In a preferred embodiment, in step S3, after the mixture in S2 is cooled to 50 to 60 ℃, the bamboo amomum fruit extract, the asparagus fern root extract, the guava fruit extract and the illicium verum fruit extract are sequentially added.
As a preferable embodiment, in step S4, after the temperature of the mixture in S3 is reduced to 40 ℃, sodium lactate, L-malic acid, citric acid, and essence are sequentially added.
The pH value of the shampoo is adjusted to 5-6.5 through citric acid, and the hair scale closing can be promoted. After the hair flakes are closed, a network structure formed by dipalmitoyloxyethyl dimethyl ammonium chloride, alkylolamide and the bamboo fructus amomi extract can stably exist on the surface layer of the hair, so that the toughness of the hair is enhanced, and the hair can be silky, glossy and moist for a long time.
The present invention will be specifically described below by way of examples. It should be noted that the following examples are only for illustrating the present invention and should not be construed as limiting the scope of the present invention, and that the insubstantial modifications and adaptations of the present invention by those skilled in the art based on the above disclosure are still within the scope of the present invention.
In addition, the starting materials used are all commercially available, unless otherwise specified.
Examples
Example 1
The embodiment 1 provides a plant repairing shampoo which comprises the following components in parts by weight:
30 parts of coconut diethanolamide, 80 parts of sodium lauryl polyoxyethylene ether sulfate, 65 parts of sodium cocoyl glycinate, 20 parts of sodium lauroyl amphoacetate, 9 parts of guar hydroxypropyl trimethyl ammonium chloride, 6 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5 parts of tert-butyl-4-hydroxyanisole, 8 parts of pyrrolidone carboxylic acid, 2.5 parts of sodium lactate, 2 parts of L-malic acid, 7 parts of fructus amomi bambusae extract, 10 parts of asparagus officinalis extract, 10 parts of guava fruit extract, 5 parts of illicium verum fruit extract, 0.5 part of citric acid, 2 parts of essence and 800 parts of deionized water.
The preparation method of the plant repairing shampoo comprises the following steps of:
s1, adding 30 parts of coconut oil diethanolamide, 80 parts of sodium lauryl polyoxyethylene ether sulfate, 65 parts of sodium cocoyl glycinate, 20 parts of sodium lauroyl amphoacetate and 5 parts of tert-butyl-4-hydroxyanisole into 800 parts of deionized water, and stirring at the temperature of 80 ℃ and the stirring speed of 200-300 rpm for 20 min;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding 9 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6 parts of dipalmitoyloxyethyl dimethyl ammonium chloride and 8 parts of sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20 min;
s3, cooling the mixture in the step S2 to 55 ℃, sequentially adding 7 parts of bamboo fructus amomi extract, 10 parts of asparagus fern root extract, 10 parts of guava fruit extract and 5 parts of illicium verum fruit extract, stirring at the speed of 600-700 rpm, and stirring for 20 min;
s4, cooling the mixture in the step S3 to 40 ℃, sequentially adding 2.5 parts of sodium lactate, 2 parts of L-malic acid, 0.5 part of citric acid and 2 parts of essence, and uniformly stirring to obtain the product.
Example 2
The embodiment 2 provides a plant repairing shampoo which comprises the following components in parts by weight:
15 parts of coconut oil diethanolamide, 15 parts of stearyl diethanolamide, 80 parts of sodium lauryl polyoxyethylene ether sulfate, 65 parts of sodium cocoyl glycinate, 20 parts of sodium lauroyl amphoacetate, 9 parts of guar hydroxypropyl trimethyl ammonium chloride, 6 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5 parts of tert-butyl-4-hydroxyanisole, 8 parts of sodium pyrrolidone carboxylate, 2.5 parts of sodium lactate, 2 parts of L-malic acid, 7 parts of bamboo villous amomum fruit extract, 10 parts of asparagus fern root extract, 10 parts of guava fruit extract, 5 parts of illicium verum fruit extract, 0.5 part of citric acid, 2 parts of essence and 800 parts of deionized water.
The preparation method of the plant repairing shampoo comprises the following steps of:
s1, adding 15 parts of coconut oil diethanolamide, 15 parts of stearyl diethanolamide, 80 parts of sodium laureth sulfate, 65 parts of sodium cocoyl glycinate, 20 parts of sodium lauroyl amphoacetate and 5 parts of tert-butyl-4-hydroxyanisole into 800 parts of deionized water, stirring at the temperature of 80 ℃ at the stirring speed of 200-300 rpm for 20 min;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding 9 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6 parts of dipalmitoyloxyethyl dimethyl ammonium chloride and 8 parts of sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20 min;
s3, cooling the mixture in the step S2 to 55 ℃, sequentially adding 7 parts of bamboo fructus amomi extract, 10 parts of asparagus fern root extract, 10 parts of guava fruit extract and 5 parts of illicium verum fruit extract, stirring at the speed of 600-700 rpm, and stirring for 20 min;
s4, cooling the mixture in the step S3 to 40 ℃, sequentially adding 2.5 parts of sodium lactate, 2 parts of L-malic acid, 0.5 part of citric acid and 2 parts of essence, and uniformly stirring to obtain the product.
Example 3
Embodiment 3 provides a plant repairing shampoo, which comprises the following components in parts by weight:
30 parts of stearyl diethanolamide, 80 parts of sodium laureth sulfate, 65 parts of sodium cocoyl glycinate, 20 parts of sodium lauroyl amphoacetate, 9 parts of guar hydroxypropyl trimethyl ammonium chloride, 6 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5 parts of tert-butyl-4-hydroxyanisole, 8 parts of pyrrolidone carboxylic acid, 2.5 parts of sodium lactate, 2 parts of L-malic acid, 7 parts of fructus amomi bambusae extract, 10 parts of asparagus officinalis extract, 10 parts of guava fruit extract, 5 parts of illicium verum fruit extract, 0.5 part of citric acid, 2 parts of essence and 800 parts of deionized water.
The preparation method of the plant repairing shampoo comprises the following steps of:
s1, adding 30 parts of stearyl diethanolamide, 80 parts of sodium laureth sulfate, 65 parts of sodium cocoyl glycinate, 20 parts of sodium lauroyl amphoacetate and 5 parts of tert-butyl-4-hydroxyanisole into 800 parts of deionized water, and stirring at the stirring speed of 200-300 rpm for 20min at the temperature of 80 ℃;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding 9 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6 parts of dipalmitoyloxyethyl dimethyl ammonium chloride and 8 parts of sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20 min;
s3, cooling the mixture in the step S2 to 55 ℃, sequentially adding 7 parts of bamboo fructus amomi extract, 10 parts of asparagus fern root extract, 10 parts of guava fruit extract and 5 parts of illicium verum fruit extract, stirring at the speed of 600-700 rpm, and stirring for 20 min;
s4, cooling the mixture in the step S3 to 40 ℃, sequentially adding 2.5 parts of sodium lactate, 2 parts of L-malic acid, 0.5 part of citric acid and 2 parts of essence, and uniformly stirring to obtain the product.
Example 4
Embodiment 4 provides a plant repairing shampoo, which comprises the following components in parts by weight:
36 parts of stearyl diethanolamide, 100 parts of sodium lauryl polyoxyethylene ether sulfate, 85 parts of sodium cocoyl glycinate, 25 parts of sodium lauroyl amphoacetate, 12 parts of guar hydroxypropyl trimethyl ammonium chloride, 8 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 6 parts of tert-butyl-4-hydroxyanisole, 10 parts of sodium pyrrolidone carboxylate, 3 parts of sodium lactate, 3 parts of L-malic acid, 17 parts of fructus amomi bambusae extract, 20 parts of asparagus officinalis extract, 20 parts of guava fruit extract, 10 parts of illicium verum fruit extract, 1.5 parts of citric acid, 6 parts of essence and 1000 parts of deionized water.
The preparation method of the plant repairing shampoo comprises the following steps of:
s1, adding 36 parts of stearyl diethanolamide, 100 parts of sodium lauryl polyoxyethylene ether sulfate, 85 parts of sodium cocoyl glycinate, 25 parts of sodium lauroyl amphoacetate and 6 parts of tert-butyl-4-hydroxyanisole into 1000 parts of deionized water, and stirring at the stirring speed of 200-300 rpm for 30min at the temperature of 80 ℃;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding 12 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 8 parts of dipalmitoyloxyethyl dimethyl ammonium chloride and 10 parts of sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 30 min;
s3, cooling the mixture in the step S2 to 55 ℃, sequentially adding 17 parts of bamboo fructus amomi extract, 20 parts of asparagus fern root extract, 20 parts of guava fruit extract and 10 parts of illicium verum fruit extract, stirring at the speed of 600-700 rpm, and stirring for 30 min;
s4, cooling the mixture in the step S3 to 40 ℃, sequentially adding 3 parts of sodium lactate, 3 parts of L-malic acid, 1.5 parts of citric acid and 6 parts of essence, and uniformly stirring to obtain the product.
Example 5
Embodiment 5 provides a plant repairing shampoo, which comprises the following components in parts by weight:
32 parts of stearyl diethanolamide, 90 parts of sodium laureth sulfate, 70 parts of sodium cocoyl glycinate, 22 parts of sodium lauroyl amphoacetate, 10 parts of guar hydroxypropyl trimethyl ammonium chloride, 7 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5.5 parts of tert-butyl-4-hydroxyanisole, 9 parts of sodium pyrrolidone carboxylate, 2.8 parts of sodium lactate, 2.5 parts of L-malic acid, 10 parts of fructus amomi bambusae extract, 14 parts of asparagus officinalis extract, 14 parts of guava fruit extract, 7 parts of illicium verum fruit extract, 1 part of citric acid, 5 parts of essence and 900 parts of deionized water.
The preparation method of the plant repairing shampoo comprises the following steps of:
s1, adding 32 parts of stearyl diethanolamide, 90 parts of sodium laureth sulfate, 70 parts of sodium cocoyl glycinate, 22 parts of sodium lauroyl amphoacetate and 5.5 parts of tert-butyl-4-hydroxyanisole into 900 parts of deionized water, and stirring at the stirring speed of 300rpm for 30min at the temperature of 80 ℃;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding 10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 7 parts of dipalmitoyloxyethyl dimethyl ammonium chloride and 9 parts of sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 30 min;
s3, cooling the mixture in the step S2 to 55 ℃, sequentially adding 10 parts of bamboo fructus amomi extract, 14 parts of asparagus fern root extract, 14 parts of guava fruit extract and 7 parts of illicium verum fruit extract, stirring at the speed of 600-700 rpm, and stirring for 30 min;
s4, cooling the mixture in the step S3 to 40 ℃, sequentially adding 2.8 parts of sodium lactate, 2.5 parts of L-malic acid, 1 part of citric acid and 5 parts of essence, and uniformly stirring to obtain the product.
Comparative example 1
Comparative example 1 provides a plant repairing shampoo, which comprises the same raw materials and weight parts as example 5, and is different from the shampoo without the bamboo amomum fruit extract.
The preparation method of the plant repairing shampoo is the same as that of the example 5, and the difference is that the bamboo amomum fruit extract is not added.
Comparative example 2
Comparative example 2 provides a plant repairing shampoo, which was prepared from the same raw materials and in the same weight parts as example 5, except that the shampoo did not contain the asparagus fern root extract.
The preparation method of the plant repairing shampoo is the same as that of the example 5, and the difference is that the asparagus fern root extract is not added.
Comparative example 3
Comparative example 3 provides a plant repairing shampoo, which was prepared from the same raw materials and in the same weight parts as example 5, except that the shampoo did not contain guava fruit extract.
The preparation method of the plant repairing shampoo is the same as that of example 5, but the plant repairing shampoo is not added with the guava fruit extract.
Comparative example 4
Comparative example 4 provides a phytoremediation shampoo, which was prepared using the same raw materials and in the same parts by weight as in example 5, except that no extract from illicium verum fruit was contained.
The preparation method of the plant repairing shampoo is the same as that of the example 5, and the difference is that the illicium verum fruit extract is not added.
Comparative example 5
Comparative example 5 provides a plant repairing shampoo, which was prepared from the same raw materials and in the same weight parts as example 5, except that dipalmitoyloxyethyl dimethyl ammonium chloride was not included.
The preparation method of the plant repairing shampoo is the same as that of the example 5, and the difference is that dipalmitoyloxyethyl dimethyl ammonium chloride is not added.
Comparative example 6
Comparative example 6 provides a plant repairing shampoo, which was prepared from the same raw materials and in the same parts by weight as in example 5, except that stearyldiethanolamide was not contained.
The preparation method of the plant repairing shampoo is the same as that of the example 5, and the difference is that the stearyldiethanolamide is not added.
Comparative example 7
Comparative example 7 provides a plant repairing shampoo, which was prepared from the same raw materials and in the same parts by weight as in example 5, except that citric acid was not contained.
The preparation method of the plant repairing shampoo is the same as that of the example 5, and the difference is that no citric acid is added.
Comparative example 8
Comparative example 8 provides a plant repairing shampoo, which comprises the same raw materials and weight parts as example 5, except that 14 parts of illicium verum fruit extract.
The preparation method of the plant repairing shampoo is the same as that of the example 5, and the difference is that 14 parts of the illicium verum fruit extract are used.
Comparative example 9
Comparative example 9 provides a plant repairing shampoo, which was prepared from the same raw materials and in the same weight parts as in example 5, except that 3 parts of illicium verum fruit extract was used.
The preparation method of the plant repairing shampoo is the same as that in example 5, and the difference is that 3 parts of the illicium verum fruit extract are used.
Comparative example 10
Comparative example 10 provides a plant repairing shampoo, which was prepared from the same raw materials and in the same weight parts as in example 5, except that 30 parts of the asparagus fern root extract was used.
The preparation method of the plant repairing shampoo is the same as that of example 5, and the difference is that the asparagus fern root extract is 30 parts.
Comparative example 11
Comparative example 11 provides a plant repairing shampoo, which was prepared from the same raw materials and in the same weight parts as in example 5, except that 30 parts of guava fruit extract was used.
The preparation method of the plant repairing shampoo is the same as that of example 5, and the difference is that 30 parts of guava fruit extract is used.
Comparative example 12
Comparative example 12 provides a plant-repairing shampoo, which comprises the same raw materials and weight parts as in example 5, and is different from the shampoo without bamboo amomum fruit extract, asparagus fern root extract, guava fruit extract and illicium verum fruit extract.
The preparation method of the plant repairing shampoo is the same as that in example 5, but the plant repairing shampoo is not added with the bamboo amomum fruit extract, the asparagus fern root extract, the guava fruit extract and the illicium verum fruit extract.
Performance testing
Test materials: shampoos as described in examples 1-5 and comparative examples 1-12.
Test subjects: the test population comprises 510 people and has the age distribution of 18-55 years, wherein the number of the male people is 200, and the number of the female people is 310.
The test method comprises the following steps: the shampoo described in examples 1 to 5 and comparative examples 1 to 12 were subjected to sensory evaluation tests by dividing the test population into 17 groups of 30 persons each. Washing hair once every two days, continuously using for two months, filling out a test table for scoring after trial. Each using effect in the scoring table is divided into 5 points in total; score 5 is the highest score, indicating very satisfactory; 4 points are better and relatively satisfactory; score 3 is acceptable; the range of not more than 3 points is not acceptable, and the average score of each use effect is shown in table 1.
TABLE 1 shampoo test results of examples 1-5 and comparative examples 1-12
As is clear from the above table, the shampoos described in examples 1-5 all had excellent effects in hair restoration, smoothness, moisture retention, cleanliness, wet combing performance and dry combing performance, and were non-irritating.
By comparing example 5 with comparative examples 2 to 4, the repair function, the pliability, and the dry and wet combing properties of the shampoo were deteriorated by arbitrarily removing one of the plant extracts. By comparing example 5 with comparative examples 1 and 5 to 7, the shampoo in 4 comparative examples was inferior in repair function, pliability, moisturizing property, and dry and wet combing properties. The applicant believes that possible causes are: the network structure formed on the surface of the hair scales is the result of the interaction of the stearin glycol amide, the dipalmitoyloxyethyl dimethyl ammonium chloride and the bamboo amomum fruit extract under an acidic condition, any component is lacked, the network structure cannot be formed or is unstable, and the washing and protecting effect of the shampoo is poor.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in other forms, and any person skilled in the art may modify or change the technical content of the above disclosure into equivalent embodiments with equivalent changes, but all those simple modifications, equivalent changes and modifications made to the above embodiments according to the technical spirit of the present invention still belong to the protection scope of the present invention.
Claims (8)
1. The plant repairing shampoo is characterized in that the preparation raw materials at least comprise the following components:
alkylolamide, sodium laureth sulfate, sodium cocoyl glycinate, sodium lauroyl amphoacetate, guar hydroxypropyl trimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride, tert-butyl-4-hydroxy anisole, sodium pyrrolidone carboxylate, sodium lactate, L-malic acid, fructus Amomi extract, radix Phyllostachydis Henonis extract, fructus Psidii Guajavae Immaturus extract, radix Anisi Stellati fruit extract, citric acid, essence and deionized water;
the extraction method of the bamboo amomum fruit extract comprises the following steps:
taking 10g of dried bamboo fructus amomi, adding 80mL of petroleum ether, soaking for 12h, performing ultrasonic extraction for 3 times, 20min each time, filtering to obtain filtrate, and recovering the petroleum ether in the filtrate by using a rotary evaporator to obtain a bamboo fructus amomi extract;
the extraction method of the asparagus fern root extract comprises the following steps:
a. washing Phyllostachys nigra root with distilled water, oven drying, pulverizing, weighing 1g Phyllostachys nigra root powder, placing into microwave digestion instrument, adding 20mL water, placing into microwave digestion instrument, heating to 60 deg.C, extracting for 20 min;
b. filtering, and fixing the volume of the filtrate to 50 mL; centrifuging the filtrate at 1000r/min for 10min, and collecting supernatant; the extraction method of the guava fruit extract comprises the following steps:
a. adding 1L deionized water into 10g of dried and pulverized guava fruit, placing in a flash extractor, and primarily extracting at room temperature for 1min at 12000r/min of the flash extractor; leaching in a water bath oscillator at 50 deg.C for 40min, vacuum filtering the hot extractive solution, collecting filtrate, and cooling to room temperature to obtain extractive solution;
b. adding 1.5 times volume of anhydrous ethanol into the extract, standing at 4 deg.C overnight, centrifuging at 8000r/min for 15min, collecting supernatant, and mixing with 10 ml: adding active carbon at a ratio of 1g, stirring for 15min, adsorbing for removing impurities and decolorizing, and filtering to obtain filtrate to obtain Psidium guajava fruit extract;
the extraction method of the illicium verum fruit extract comprises the following steps:
a. washing the dried illicium verum fruits with distilled water, crushing to 20-60 meshes, wrapping with filter paper, binding with cotton ropes, and putting into a Soxhlet extraction column; adding petroleum ether with a boiling range of 60-70 ℃ into a Soxhlet flask to serve as an extracting solution, wherein the proportion of the extracting solution to raw materials is 100ml:2g, and heating, boiling and extracting for 10 hours;
b. cooling the leaching liquor obtained in the step, regulating the heating temperature of reduced pressure concentration to be 60 ℃, and reducing pressure concentration of the leaching liquor to 1/30 of the original volume to obtain concentrated solution;
c. closing the concentrated solution, placing the concentrated solution into a freezing chamber, refrigerating and standing the concentrated solution at a temperature of between 5 ℃ below zero and 30 ℃ below zero for 5 hours, taking the concentrated solution out, centrifuging the concentrated solution for 20 minutes at a speed of 10000r/min, and taking supernatant;
d. slowly transferring the supernatant into a silica gel column, controlling the specific gravity of the filler and the sample at 40g:1ml, taking petroleum ether-ethyl acetate as eluent, collecting the eluent in sections, and concentrating the middle section of the eluent under reduced pressure to obtain the illicium verum fruit extract;
the alkylolamides are coconut oil diethanolamide and/or stearic acid diethanolamide.
2. The phytoremediation shampoo of claim 1, wherein the weight ratio of the wenzhu root extract, the guava fruit extract and the illicium verum fruit extract is 2: 2: 1.
3. the plant repairing shampoo according to claim 2, wherein the preparation raw materials comprise, by weight:
30-36 parts of alkylolamide, 80-100 parts of sodium lauryl polyoxyethylene ether sulfate, 65-85 parts of sodium cocoyl glycinate, 20-25 parts of sodium lauroyl amphoacetate, 9-12 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6-8 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5-6 parts of tert-butyl-4-hydroxy anisole, 8-10 parts of sodium pyrrolidone carboxylate, 2.5-3 parts of sodium lactate, 2-3 parts of L-malic acid, 7-17 parts of bamboo fructus amomi extract, 10-20 parts of asparagus fern root extract, 10-20 parts of guava fruit extract, 5-10 parts of illicium verum fruit extract, 0.5-1.5 parts of citric acid, 2-6 parts of essence and 800-1000 parts of deionized water.
4. The plant repairing shampoo according to claim 3, wherein the preparation raw materials comprise, by weight:
32 parts of alkylolamide, 90 parts of lauryl alcohol polyoxyethylene ether sodium sulfate, 70 parts of sodium cocoyl glycinate, 22 parts of sodium lauroyl amphoacetate, 10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 7 parts of dipalmitoyloxyethyl dimethyl ammonium chloride, 5.5 parts of tert-butyl-4-hydroxy anisole, 9 parts of pyrrolidone carboxylic acid sodium, 2.8 parts of sodium lactate, 2.5 parts of L-malic acid, 10 parts of fructus amomi bambusae extract, 14 parts of asparagus fern root extract, 14 parts of guava fruit extract, 7 parts of illicium verum fruit extract, 1 part of citric acid, 5 parts of essence and 900 parts of deionized water.
5. A method for preparing a plant repairing shampoo according to any one of claims 1 to 4, characterized by comprising at least the following steps:
s1, adding alkylolamide, sodium lauryl polyoxyethylene ether sulfate, sodium cocoyl glycinate, sodium lauroyl amphoacetate and tert-butyl-4-hydroxyanisole into deionized water, stirring at the speed of 200-300 rpm at the temperature of 75-85 ℃, and stirring for 20-30 min;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding guar gum hydroxypropyl trimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride and sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20-30 min;
s3, cooling the mixture obtained in the step S2, sequentially adding the bamboo fructus amomi extract, the asparagus fern root extract, the guava fruit extract and the illicium verum fruit extract, stirring at the speed of 600-700 rpm for 20-30 min;
s4, cooling the mixture in the step S3, sequentially adding sodium lactate, L-malic acid, citric acid and essence, and uniformly stirring to obtain the product.
6. The preparation method of the plant repairing shampoo according to claim 5, characterized by comprising the following steps in parts by weight:
s1, adding 30-36 parts of alkylolamide, 80-100 parts of sodium lauryl polyoxyethylene ether sulfate, 65-85 parts of sodium cocoyl glycinate, 20-25 parts of sodium lauroyl amphoacetate and 5-6 parts of tert-butyl-4-hydroxyanisole into 800-1000 parts of deionized water, and stirring at the stirring speed of 200-300 rpm for 20-30 min at the temperature of 75-85 ℃;
s2, cooling the mixture in the S1 to 65-70 ℃, sequentially adding 9-12 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 6-8 parts of dipalmitoyloxyethyl dimethyl ammonium chloride and 8-10 parts of sodium pyrrolidone carboxylate, stirring at the speed of 400-500 rpm, and stirring for 20-30 min;
s3, cooling the mixture obtained in the step S2, sequentially adding 7-17 parts of fructus amomi extract, 10-20 parts of asparagus fern root extract, 10-20 parts of guava fruit extract and 5-10 parts of illicium verum fruit extract, stirring at the speed of 600-700 rpm for 20-30 min;
s4, cooling the mixture obtained in the step S3, sequentially adding 2.5-3 parts of sodium lactate, 2-3 parts of L-malic acid, 0.5-1.5 parts of citric acid and 2-6 parts of essence, and uniformly stirring to obtain the product.
7. The method for preparing the phytoremediation shampoo of claim 5, wherein in step S3, the mixture of step S2 is cooled to 50-60 ℃, and then bamboo amomum fruit extract, asparagus fern root extract, guava fruit extract and illicium verum fruit extract are sequentially added.
8. The method for preparing the phytoremediation shampoo of claim 5, wherein in step S4, after the temperature of the mixture in S3 is reduced to 40 ℃, sodium lactate, L-malic acid, citric acid, and essence are sequentially added.
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| CN105496897A (en) * | 2016-01-06 | 2016-04-20 | 张秀丽 | Plant essence shampoo and preparation method thereof |
| CN107951792A (en) * | 2017-12-29 | 2018-04-24 | 广州市科能化妆品科研有限公司 | Anti-dandruff and itching-relieving hair-washing composition and preparation method thereof |
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| CN105496897A (en) * | 2016-01-06 | 2016-04-20 | 张秀丽 | Plant essence shampoo and preparation method thereof |
| CN107951792A (en) * | 2017-12-29 | 2018-04-24 | 广州市科能化妆品科研有限公司 | Anti-dandruff and itching-relieving hair-washing composition and preparation method thereof |
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