CN109043556A - A kind of preparation method of mandarin orange fruit dreg dietary fiber - Google Patents
A kind of preparation method of mandarin orange fruit dreg dietary fiber Download PDFInfo
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- CN109043556A CN109043556A CN201811156259.XA CN201811156259A CN109043556A CN 109043556 A CN109043556 A CN 109043556A CN 201811156259 A CN201811156259 A CN 201811156259A CN 109043556 A CN109043556 A CN 109043556A
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- mandarin orange
- dietary fiber
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
- A23L33/21—Addition of substantially indigestible substances, e.g. dietary fibres
- A23L33/22—Comminuted fibrous parts of plants, e.g. bagasse or pulp
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Abstract
The present invention provides a kind of preparation method of mandarin orange fruit dreg dietary fiber, comprising the following steps: (1) by mandarin orange pomace after drying, crushing plus water boiling, potassium permanganate is added and carries out decolorization;(2) when the mandarin orange pomace solution of step (1) is cooled to 35-45 DEG C, addition and complex enzyme filter after being digested;(3) hydrochloric acid is added in the filtrate that step (2) obtains and is stirred evenly;(4) NaOH is added in the filter residue that step (3) obtains and is stirred evenly;(5) step (3) is added in the filtrate through the filtrate of acid processing using 95% ethyl alcohol, Precipitation to be had collects precipitating;(6) step (4) is mixed with the mandarin orange pomace water insoluble dietary fiber of step (5) and water-soluble dietary fiber, is then dried in vacuo up to mandarin orange fruit dreg dietary fiber.Method of the invention is turned waste into wealth using mandarin orange pomace as raw material, remarkable in economical benefits.
Description
Technical field
The invention belongs to food processing fields, and in particular to a kind of preparation method of mandarin orange fruit dreg dietary fiber.
Background technique
Dietary fiber is a kind of important non-nutritive element, it is a kind of non-starch polysaccharide and oligosaccharides etc. in carbohydrate
Indigestion part, it can neither be digested and assimilated by human gastrointestinal tract, can not generate energy.However in recent years, more and more
Research shows that the intake of dietary fiber is closely related with human health, constipation, obesity, glycosuria can be reduced by taking in enough dietary fibers
The danger that disease, cardiovascular disease and intestinal tract occur.For example, dietary fiber can largely absorb moisture in enteron aisle, make excrement
Soft condition is kept, effectively activates the beneficial bacteria in enteron aisle, promotes beneficial bacteria mass propagation, creates enteron aisle environmental health, especially
It is to be suitable for improving prolonged constipation;Meanwhile improving the dietary fiber content in diet can be such that the thermal energy of intake reduces, in enteron aisle
The digestion and absorption of interior nutrition also declines, the infiltration rate that can also extend food residence time in the intestine, reduce glucose, not only
Have effects that weight-reducing, and diabetic symptom can be improved.
Dietary fiber can be divided into soluble dietary fiber and non-soluble dietary fiber according to whether being dissolved in water.Many plants
Most dietary fibers are non-soluble dietary fiber in raw material and its byproduct.Such as mandarin orange pomace, it is that prepare mandarin orange general
The waste residue that tea time abandons, but its fibre composition for containing higher amount, therefore used also as preparing dietary fiber.In the food industry
Preparing most of soluble dietary fiber is that non-soluble dietary fiber modification is converted to soluble dietary fiber.However, passing
There is the problems such as low purity, low output, poor taste in the mandarin orange pomace soluble dietary fiber of the processing method production of system, have mostly
It even also will cause the reduction of product moisture holding capacity, influence dietary fiber effect.For this purpose, researching and developing a kind of above problem of being able to solve
The preparation method of mandarin orange fruit dreg dietary fiber is very important.
Summary of the invention
A kind of mandarin orange fruit dreg dietary fiber is provided it is an object of the invention to overcome in place of above-mentioned the deficiencies in the prior art
Preparation method, and the obtained mandarin orange fruit dreg dietary fiber prepared by this method.
To achieve the above object, the technical solution adopted by the present invention are as follows: a kind of preparation method of mandarin orange fruit dreg dietary fiber, packet
Include following steps:
(1) by mandarin orange pomace after drying, crushing plus water boiling, potassium permanganate is added and carries out decolorization, so that mandarin orange pomace
Solution becomes colorless solution;
(2) when the mandarin orange pomace solution of step (1) is cooled to 35-45 DEG C, addition and complex enzyme filter after being digested;
(3) hydrochloric acid is added in the filtrate that step (2) obtains, is stirred evenly under the conditions of temperature is 40-55 DEG C;
(4) NaOH is added in the filter residue that step (3) obtains, temperature be 50-60 DEG C under the conditions of stir evenly to get
Mandarin orange pomace water insoluble dietary fiber;
(5) step (3) is added in the filtrate through the filtrate of acid processing using 95% ethyl alcohol, wait there is precipitating to analyse
Out, precipitating is collected to get mandarin orange pomace water-soluble dietary fiber;
(6) step (4) is mixed with the mandarin orange pomace water insoluble dietary fiber of step (5) and water-soluble dietary fiber, so
After be dried in vacuo up to mandarin orange fruit dreg dietary fiber.
Preferably, the concentration of the potassium permanganate in the step (1) is 5-10%, and the weight ratio with mandarin orange pomace solution is 1-
5:10, pH value 7-9, time 50-90min.
Preferably, the weight ratio of complex enzyme described in the step (1) and mandarin orange pomace solution is 1-15:100, enzyme digestion reaction
Time is 3-4h, pH value 4-6.
Preferably, the weight ratio of the complex enzyme and mandarin orange pomace solution is 5-10:100.
Preferably, the complex enzyme is the mixture of neutral proteinase, lipase, cellulase, pectase, wherein various
The weight ratio of enzyme is neutral proteinase: lipase: cellulase: pectase=1-3:1-3:4-6:2-5.
Preferably, the concentration of hydrochloric acid described in the step (3) is 10-15%, and the weight ratio with the filtrate is 1:3-
6。
Preferably, the concentration of NaOH described in the step (4) is 2-6%, and the weight ratio with the filtrate is 1:2-8.
Preferably, the weight ratio of 95% ethyl alcohol described in the step (5) and the filtrate is 1:1-5, stands 6h.
Preferably, vacuum drying temperature described in the step (6) is 50-60 DEG C, time 5-8h.
The present invention also provides the mandarin orange pomaces that a kind of preparation method of mandarin orange fruit dreg dietary fiber as described above is prepared
Dietary fiber.
The beneficial effects of the present invention are: method of the invention to raw material carried out crushing, boiling and etc. can have
Effect destroys raw material mix tissue, exposes its content sufficiently, and further decreases non-diet fibre in raw material in conjunction with enzyme digestion reaction
Ingredient is tieed up, makes enzymatic hydrolysis more sufficiently to improve manufactured goods purity, and the palatability of manufactured goods can be effectively improved;After digesting
It is purified again, further increases purity, manufactured goods soluble dietary fiber has the advantages that purity is high, is particularly suitable for Gao Pin
The preparation of matter soluble dietary fiber;The present invention uses alkalinity extraction hydrophily hemicellulose to filtrate in pre-treatment, further
Improve soluble dietary fiber yield;Method manufactured goods soluble dietary fiber of the invention also has that fiber diameter is small, water holding
Ability and the strong advantage of swelliong power;Method of the invention is turned waste into wealth using mandarin orange pomace as raw material, and economic benefit is aobvious
It writes.
Specific embodiment
For more concise displaying technical solution of the present invention, objects and advantages, combined with specific embodiments below
The present invention is described in further detail.
Embodiment 1
(1) by mandarin orange pomace after drying, crushing plus water boiling, the potassium permanganate that concentration is 5% is added and carries out at decoloration
Reason is 1:10 with the weight ratio of mandarin orange pomace solution, pH value 7, time 50min so that mandarin orange pomace solution become colorless it is molten
Liquid;
(2) when the mandarin orange pomace solution of step (1) is cooled to 35-45 DEG C, addition and complex enzyme filter after being digested,
The weight ratio of the complex enzyme and mandarin orange pomace solution is 1:100, and the enzyme digestion reaction time is 3h, pH value 4, wherein the weight of various enzymes
Amount is than being neutral proteinase: lipase: cellulase: pectase=1:1:4:2;
(3) hydrochloric acid that concentration is 10% is added in the filtrate that step (2) obtains, the weight ratio with the filtrate is 1:
3, it is stirred evenly under the conditions of 40 DEG C;
(4) NaOH that concentration is 2% is added in the filter residue that step (3) obtains, the weight ratio with the filter residue is 1:
2, it is stirred evenly under the conditions of 50 DEG C to get mandarin orange pomace water insoluble dietary fiber;
(5) step (3) is added in the filtrate through the filtrate of acid processing using 95% ethyl alcohol, ethyl alcohol and the filter
The weight ratio of liquid is 1:1, stands 6h, and Precipitation to be had collects precipitating to get mandarin orange pomace water-soluble dietary fiber;
(6) step (4) is mixed with the mandarin orange pomace water insoluble dietary fiber of step (5) and water-soluble dietary fiber, so
After be dried in vacuo up to mandarin orange fruit dreg dietary fiber, temperature is 50 DEG C, time 5h.
Embodiment 2
The concentration that the present embodiment and embodiment 1 are uniquely distinguished as potassium permanganate is 7%.
Embodiment 3
The concentration that the present embodiment and embodiment 1 are uniquely distinguished as potassium permanganate is 9%.
Embodiment 4
The concentration that the present embodiment and embodiment 1 are uniquely distinguished as potassium permanganate is 10%.
Embodiment 5
The present embodiment and embodiment 1 are uniquely distinguished as with the weight ratio of mandarin orange pomace solution being 3:10.
Embodiment 6
The present embodiment and embodiment 1 are uniquely distinguished as with the weight ratio of mandarin orange pomace solution being 5:10.
Embodiment 7
It is 8 that the present embodiment and embodiment 1, which are uniquely distinguished as pH value,.
Embodiment 8
It is 9 that the present embodiment and embodiment 1, which are uniquely distinguished as decoloration pH value,.
Embodiment 9
It is 70min that the present embodiment and embodiment 1, which are uniquely distinguished as bleaching time,.
Embodiment 10
It is 90min that the present embodiment and embodiment 1, which are uniquely distinguished as bleaching time,.
Embodiment 11
It is 5:100 that the present embodiment and embodiment 1, which are uniquely distinguished as complex enzyme and the weight ratio of mandarin orange pomace solution,.
Embodiment 12
It is 1:10 that the present embodiment and embodiment 1, which are uniquely distinguished as complex enzyme and the weight ratio of mandarin orange pomace solution,.
Embodiment 13
It is 15:100 that the present embodiment and embodiment 1, which are uniquely distinguished as complex enzyme and the weight ratio of mandarin orange pomace solution,.
Embodiment 14
The present embodiment and embodiment 1 are uniquely distinguished as neutral proteinase: lipase: cellulase: the weight ratio of pectase
For 2:2:5:3.
Embodiment 15
The present embodiment and embodiment 1 are uniquely distinguished as neutral proteinase: lipase: cellulase: the weight ratio of pectase
For 3:3:6:5.
Embodiment 16
It is 12% that the present embodiment and embodiment 1, which are uniquely distinguished as concentration of hydrochloric acid,.
Embodiment 17
It is 15% that the present embodiment and embodiment 1, which are uniquely distinguished as concentration of hydrochloric acid,.
Embodiment 18
It is 1:4 that the present embodiment and embodiment 1, which are uniquely distinguished as hydrochloric acid and the weight ratio of the filtrate,.
Embodiment 19
It is 1:6 that the present embodiment and embodiment 1, which are uniquely distinguished as hydrochloric acid and the weight ratio of the filtrate,.
Embodiment 20
It is 4% that the present embodiment and embodiment 1, which are uniquely distinguished as NaOH concentration,.
Embodiment 21
It is 6% that the present embodiment and embodiment 1, which are uniquely distinguished as NaOH concentration,.
Embodiment 22
It is 1:4 that the present embodiment and embodiment 1, which are uniquely distinguished as NaOH and the weight ratio of the filter residue,.
Embodiment 23
It is 1:6 that the present embodiment and embodiment 1, which are uniquely distinguished as NaOH and the weight ratio of the filter residue,.
Embodiment 24
It is 1:8 that the present embodiment and embodiment 1, which are uniquely distinguished as NaOH and the weight ratio of the filter residue,.
Embodiment 25
It is 1:5 that the present embodiment and embodiment 1, which are uniquely distinguished as ethyl alcohol and the weight ratio of the filtrate,.
Mandarin orange fruit dreg dietary fiber prepared by above-described embodiment 1-26 measures its dietary fiber according to GB/T 5009.88
Content the results are shown in Table 1:
Table 1: the mandarin orange fruit dreg dietary fiber content of embodiment 1-26 preparation
Result above is analyzed, embodiment 1-10 is compared, it is seen that when the concentration of potassium permanganate is 7%, with
The weight ratio of mandarin orange pomace solution is 3:10, and pH value 8, when the time is 70min, fiber content highest illustrates potassium permanganate to system
The result of standby mandarin orange fruit dreg dietary fiber has certain influence;The weight of complex enzyme and mandarin orange pomace solution known to embodiment 1,11-15
Than for 1:10, weight ratio fiber content highest when being 3:3:6:5 of neutral proteinase, lipase, cellulase, pectase,
Illustrate that the different ratio of enzyme influences its enzyme digestion reaction effect;By embodiment 1,16-19 it is found that the concentration of hydrochloric acid and with mandarin orange pomace
The weight ratio of filtrate is prepared with certain influence to mandarin orange fruit dreg dietary fiber, when the weight ratio of hydrochloric acid and mandarin orange pomace filtrate is 1:4
When, effect is best;By embodiment 1,20-24 it is found that the concentration of NaOH and with the weight ratio of mandarin orange pomace filtrate to mandarin orange pomace meals
Food fiber is prepared with certain influence, when the weight ratio of NaOH and mandarin orange pomace filtrate is 1:6, fiber content highest;Embodiment
1,25 it is found that fiber content highest illustrates ethyl alcohol to mandarin orange fruit dreg dietary fiber when the weight ratio of ethyl alcohol and the filtrate is 1:5
Preparation be affected.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (10)
1. a kind of preparation method of mandarin orange fruit dreg dietary fiber, which comprises the following steps:
(1) by mandarin orange pomace after drying, crushing plus water boiling, potassium permanganate is added and carries out decolorization, so that mandarin orange pomace solution
Become colorless solution;
(2) when the mandarin orange pomace solution of step (1) is cooled to 35-45 DEG C, addition and complex enzyme filter after being digested;
(3) hydrochloric acid is added in the filtrate that step (2) obtains, is stirred evenly under the conditions of temperature is 40-55 DEG C;
(4) NaOH is added in the filter residue that step (3) obtains, is stirred evenly under the conditions of temperature is 50-60 DEG C to get mandarin orange fruit
Pulp water insoluble diedairy fiber;
(5) step (3) is added in the filtrate through the filtrate of acid processing using 95% ethyl alcohol, Precipitation to be had is received
Collection precipitating is to get mandarin orange pomace water-soluble dietary fiber;
(6) step (4) is mixed with the mandarin orange pomace water insoluble dietary fiber of step (5) and water-soluble dietary fiber, then very
Sky is drying to obtain mandarin orange fruit dreg dietary fiber.
2. the preparation method of mandarin orange fruit dreg dietary fiber as described in claim 1, which is characterized in that the height in the step (1)
The concentration of potassium manganate is 5-10%, and the weight ratio with mandarin orange pomace solution is 1-5:10, pH value 7-9, time 50-90min.
3. the preparation method of mandarin orange fruit dreg dietary fiber as described in claim 1, which is characterized in that described in the step (1)
The weight ratio of complex enzyme and mandarin orange pomace solution is 1-15:100, and the enzyme digestion reaction time is 3-4h, pH value 4-6.
4. the preparation method of mandarin orange fruit dreg dietary fiber as claimed in claim 3, which is characterized in that the complex enzyme and mandarin orange pomace
The weight ratio of solution is 5-10:100.
5. the preparation method of mandarin orange fruit dreg dietary fiber as claimed in claim 3, which is characterized in that the complex enzyme is neutral egg
White enzyme, lipase, cellulase, pectase mixture, wherein the weight ratio of various enzymes is neutral proteinase: lipase: fine
Tie up plain enzyme: pectase=1-3:1-3:4-6:2-5.
6. the preparation method of mandarin orange fruit dreg dietary fiber as described in claim 1, which is characterized in that described in the step (3)
The concentration of hydrochloric acid is 10-15%, and the weight ratio with the filtrate is 1:3-6.
7. the preparation method of mandarin orange fruit dreg dietary fiber as described in claim 1, which is characterized in that described in the step (4)
The concentration of NaOH is 2-6%, and the weight ratio with the filtrate is 1:2-8.
8. the preparation method of mandarin orange fruit dreg dietary fiber as described in claim 1, which is characterized in that described in the step (5)
The weight ratio of 95% ethyl alcohol and the filtrate is 1:1-5, stands 6h.
9. the preparation method of mandarin orange fruit dreg dietary fiber as described in claim 1, which is characterized in that described in the step (6)
Vacuum drying temperature is 50-60 DEG C, time 5-8h.
10. a kind of mandarin orange pomace that the preparation method such as the described in any item mandarin orange fruit dreg dietary fibers of claim 1-9 is prepared
Dietary fiber.
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Cited By (3)
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CN110025016A (en) * | 2019-04-29 | 2019-07-19 | 贵阳学院 | A kind of extracting method of blueberry dregs diet fibre |
CN110122886A (en) * | 2019-03-20 | 2019-08-16 | 广州市莱檬生物科技有限公司 | A kind of preparation method of citrus dietary fiber |
CN115287140A (en) * | 2022-06-30 | 2022-11-04 | 博白县三桦石柳生态农业开发有限责任公司 | Method for preparing wine beverage with special aromatic smell by using jack fruit peel |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110122886A (en) * | 2019-03-20 | 2019-08-16 | 广州市莱檬生物科技有限公司 | A kind of preparation method of citrus dietary fiber |
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CN115287140A (en) * | 2022-06-30 | 2022-11-04 | 博白县三桦石柳生态农业开发有限责任公司 | Method for preparing wine beverage with special aromatic smell by using jack fruit peel |
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