CN109042924A - A kind of grease microcapsule powder and preparation method thereof - Google Patents
A kind of grease microcapsule powder and preparation method thereof Download PDFInfo
- Publication number
- CN109042924A CN109042924A CN201810817108.8A CN201810817108A CN109042924A CN 109042924 A CN109042924 A CN 109042924A CN 201810817108 A CN201810817108 A CN 201810817108A CN 109042924 A CN109042924 A CN 109042924A
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- Prior art keywords
- grease
- microcapsule powder
- wall material
- oil
- grease microcapsule
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of grease microcapsule powder, the grease of wall material and 33%-67% weight ratio in the grease microcapsule powder including 33%-67% weight ratio；Wherein, the wall material includes soybean protein isolate and maltodextrin, the grease microcapsule powder further includes Arabic gum, glycerin monostearate and antioxidant, and in the wall material soybean protein isolate and maltodextrin weight ratio are as follows: 1: 1-2: 1, the mass ratio of Arabic gum is 1%-3%.The grease microcapsule powder prepared in the present invention has higher embedding efficiency, lower surface oil cut rate, grease is wrapped in wall material, the effective component being able to maintain in grease can add well in various food, greatly expand the scope of application of original grease.
Description
Technical field
The present invention relates to field of medicaments, and in particular to a kind of grease microcapsule powder and preparation method thereof.
Background technique
Such as not soluble in water due to the characteristic of grease itself, hardly possible uniformly mixes with other raw-food materials or contains unsaturated lipid
Fat acid influences vulnerable to air, daylight, water grading factors and oxidation reaction occurs, generate some aldehyde, ketone smell substance, drops
The quality of Low grease；Some greases such as garlic oil, fish oil etc. itself have peculiar smell, are not suitable for directly edible.
Wherein, perilla herb oil also known as Purple Perilla Seed Oil are the edible oils extracted using purple perilla seed as raw material.Purple perilla is national first batch of batch
The dual purpose plant of quasi- integration of drinking and medicinal herbs.Purple Perilla Seed Oil system from the dry fruit of Lamiaceae plant purple perilla maturation or purple perilla plant,
The multi-component mixtures such as obtained linolenic acid containing a- are extracted, wherein being a kind of high-quality health care food without harmful components such as erucic acid
With oil.Perilla herb oil is colourless to faint yellow or light green transparent oily liquid, has purple perilla and amber aroma.Purple Perilla Seed Oil is readily soluble
In ethyl alcohol, it is insoluble in glycerol and propylene glycol.Alpha-linolenic acid content is up to 60%~67% (it is than α-in linseed oil in Purple Perilla Seed Oil
Linolenic acid is taller), contain linoleic acid 12%~13%, also has obvious treatment containing 18 kinds of amino acid and a variety of pairs of a variety of diseases of human body
The substance of effect and health-care effect has very high nutritive and medicinal value.Long-term consumption, has the advantage that: increasing brain battalion
It supports, brain tonic and intelligence development, adjust cranial nerve and optic nerve function；Adjusting hypertension, reduces cholesterol at hyperlipidemia；Prevent artery athero-
Hardening, inhibition thrombosis；Reduce the breaking-out of cerebral thrombosis and cardiovascular disease；Enhance immune function of human body；It adjusts organism metabolism, prolong
Slow body aging；Slow down and prevent the generation of senile dementia；Prevent fatty liver and diabetes；Also have to health care skin and weight-reducing
Better effects.
Currently, product of the perilla herb oil in the market generally in the form of liquid oil occurs, the perilla herb oil of liquid needs to keep away oxygen and keeps away
Light low-temperature preservation is difficult to place the oxidational losses of wherein effective component alpha-linolenic acid if directly eating.Therefore, in addition have a small amount of
Edible perilla herb oil is fabricated to the form of soft capsule for directly oral.All there is products application range and compare in both edible forms
It is narrow, the problem of product is difficult to long-term preservation, it is prepared into soft capsule, although oil body and air exclusion can be made, is merely able to
It is taken orally, is unfavorable for being added in other food, lack being widely applied property, and more sensitive to temperature.Therefore, it needs
The shape that perilla herb oil is prepared into powder by new scheme is explored, and keeps its effective component.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of grease microcapsule powder and preparation method thereof, are able to maintain
Effective component in perilla herb oil, and can widely add in various food.
To achieve the goals above, the present invention adopts the following technical scheme: a kind of grease microcapsule powder, the grease are micro-
The perilla herb oil and additive of wall material and 33%-67% weight ratio in capsule powders including 33%-67% weight ratio；Wherein,
The wall material includes soybean protein isolate and maltodextrin, and the additive includes Arabic gum, glycerol monostearate and antioxygen
Agent.
Further, in the wall material soybean protein isolate and maltodextrin weight ratio are as follows: 1: 1-2: 1.
Further, the mass ratio of the Arabic gum is 1%-3%.
Further, the antioxidant is tert-butylhydroquinone.
Further, the grease is perilla herb oil or algae oil or linseed oil.
A kind of method for preparing grease microcapsule powder of the present invention, includes the following steps:
S01: weighing soybean protein isolate, maltodextrin, Arabic gum, glycerin monostearate and antioxidant respectively,
It is mixed, and forms wall material aqueous solution；
S02: above-mentioned resulting wall material aqueous solution is put into insulated sterilizing in thermostat water bath；
S03: being added perilla herb oil in the wall material aqueous solution after above-mentioned sterilizing, be uniformly mixed, and forming solid content is
The emulsion of 12%-28%；Wherein, the weight ratio of wall material is 1: 2-2: 1 in grease and step S01；
S04: by the emulsion with high pressure homogenizer homogeneous 2-3 times, the emulsion of stable homogeneous is obtained；
S05: it will be spray-dried to obtain grease microcapsule powder after emulsion filtering.
Further, the temperature of water bath with thermostatic control is 80-90 DEG C in the step S02, and the time is 30 minutes.
Further, it is added before grease in the step S03, the temperature of the wall material aqueous solution after the sterilizing is reduced
To 60-70 DEG C.
Further, when being spray-dried in the step S05, inlet air temperature control is 180-200 DEG C, leaving air temp control
It is 70-80 DEG C, feeding temperature control is 50-60 DEG C.
The invention has the benefit that the grease microcapsule powder prepared in the present invention, has higher embedding effect
Rate, lower surface oil cut rate, grease is wrapped in wall material, and the effective component being able to maintain in grease can add well
In various food, the scope of application of original grease is greatly expanded.The present invention passes through spray drying process for liquid fat
Microscapsule powder is made, the wall material of microcapsules has protective effect to the grease inside microcapsules, Oxidation of Fat and Oils can be effectively prevented.
And the storage-stable of grease microcapsule powder prepared by the present invention is better than former liquid fat.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, a specific embodiment of the invention is done below
It is further to be described in detail.
In the present invention grease can be perilla herb oil or the existing grease type of algae oil or linseed oil etc., following embodiment with
It is illustrated for perilla herb oil, when grease is other greases, preparation method and the microscapsule powder and perilla herb oil prepared
It is identical.
When grease is perilla herb oil, the grease microcapsule powder in the present invention is perilla herb oil microscapsule powder, including
The wall material of 33%-67% weight ratio and the perilla herb oil of 33%-67% weight ratio；Wherein, wall material includes soybean protein isolate and wheat
Bud dextrin；In addition to this, the perilla herb oil microscapsule powder in the present invention further includes Arabic gum, glycerin monostearate and antioxygen
Agent, and in wall material soybean protein isolate and maltodextrin weight ratio are as follows: 1: 1-2: 1, the mass ratio of Arabic gum is 1%-
3%, the present invention in antioxidant can choose tert-butylhydroquinone.
A kind of method preparing grease microcapsule powder provided by the invention, includes the following steps:
S01: it is 2: 1 soybean protein isolate and maltodextrin first, in accordance with mass ratio is weighed, then adds appropriate ratio
Arabic gum, glycerin monostearate and antioxidant are mixed, and wherein glycerin monostearate uses hot water dissolving, necessary
When can be used ultrasonic cleaner accelerate its dissolution, water is then added according to a certain percentage, wall material aqueous solution is made, wherein
The additive amount of Arabic gum accounts for the 2% of wall material gross mass.
S02: above-mentioned resulting aqueous solution is put into heat preservation 30min in the thermostat water bath that temperature is 80-90 DEG C and is gone out
Bacterium.
S03: being cooled to 60-70 DEG C for the sterilizing wall material aqueous solution that above-mentioned steps obtain, and then by perilla herb oil is added, stirs
15min mixes well it, and the emulsion that solid content is 20% is made, wherein wall material in perilla herb oil and step S01
Weight ratio be 1: 1.
S04: by emulsion with high pressure homogenizer homogeneous 2-3 times, the emulsion of stable homogeneous is obtained.
S05: it is spray-dried to obtain grease microcapsule powder-product after filtering.When spray drying, inlet air temperature control
It is 180-200 DEG C, leaving air temp control is 70-80 DEG C, and feeding temperature control is 50-60 DEG C, and controls charging rate.
The perilla herb oil microscapsule powder that above-described embodiment is prepared measures total oil content amount using soxhlet extraction methods, and product always contains
Oil mass refers to the total amount of perilla herb oil in microcapsules, including the oil embedded inside microcapsules and the surface oil not being embedded.Product
Total oil content content should reach certain level.Method particularly includes:
Each position of Soxhlet extractor is sufficiently washed and is completely dried afterwards wash with distilled water.Weigh flask weight
For m1, uniform sample powder is then accurately weighed, remembers that the gross mass of sample and flask is m2, while sample is packed into filtration paper cylinder
It is interior.Filtration paper cylinder is put into the extracting barrel of Soxhlet extractor, it is noted that the height of filtration paper cylinder is no more than soxhlet type pipe
Return pipe height, and it is attached with the flask dried to constant weight, is added by the condenser pipe upper end of Soxhlet extraction device
Enter at the petroleum ether to the 2/3 of bottle internal volume that boiling range is 60-90 DEG C, and connect condenser pipe, be passed through condensed water, guarantees condensed water
Bottom in and top out heats bottom bottle submergence in a water bath, and bath temperature is 60-90 DEG C, gently fills in condensation with one small absorbent cotton
It manages suitable for reading.Bath temperature, which should control, makes extracting solution once be advisable in every 6-8min reflux.Extraction times contain depending on grease in sample
Depending on amount, generally extraction 6-12h.At the end of extraction, a drop extracting solution is picked up with focussing glass, shows to have extracted if no oil mark
Finish.Flask is removed, is connected on rotary evaporator and is distilled to recover petroleum ether under conditions of 60 DEG C.Until again without petroleum ether liquid
When steaming, evaporation recycling terminates, and flask is then placed in vacuum desiccator drying, and to constant weight, (front and back weighs difference twice and is no more than
2mg), the total weight of flask and grease is referred to as m3,
Total oil content amount (%)=(m for the grease microcapsule powder that above-described embodiment is prepared3-m1)/(m2-m1) ×
100%=35.17%.
Surface oil content refers to the quality for not being embedded and being present in the grease of surface of microcapsule.Surface oil content is fewer, says
The effect that clean grease is embedded is better.The grease microcapsule powder that the present invention prepares carries out the specific side of surface oil content test
Method are as follows:
1.0g powder-product is accurately weighed, is put into the funnel of filter paper, with the petroleum ether sample of 30mL, filtering is simultaneously
Cleaning solution is collected with flask, recycling petroleum ether liquid is evaporated under conditions of 60 DEG C using rotary evaporator, until again
When no petroleum ether liquid steams, evaporation recycling terminates, and flask is then placed in vacuum desiccator drying, and to constant weight, (front and back is twice
Weigh difference and be no more than 2mg), surface oil quality of weighing to obtain.
The surface oil content (%) for the grease microcapsule powder that above-described embodiment is prepared=surface oil quality/sample quality
× 100%=3.21%
The efficiency of microcapsules refers to the mass ratio of the oil being embedded in wall material with oil total in microcapsules.The efficiency of microcapsules with
Embedding rate indicates.Microencapsulated oil powder is higher, i.e. total oil content amount is higher, and surface oil is fewer, illustrates that the embedding of grease is better, more not
It is easy to oxidize.The grease microcapsule powder that the present invention prepares carries out microencapsulated oil powder measurement method particularly includes:
Microencapsulated oil powder is one of the important indicator for evaluating powdered oil product quality quality, and microencapsulated oil powder is higher
Then show core material be exposed to surface of microcapsule quantity it is fewer, the quantity contacted with external environment is fewer, microcapsule product itself
Will more keep stable, loss of effective components it is fewer, storage phase also can be longer, therefore higher microencapsulated oil powder is raw
Produce the important indicator of powdered oil product.
The microencapsulated oil powder (%) for the grease microcapsule powder that above-described embodiment is prepared=[1- (surface oil content/total
Oil content)] × 100%=91.23%
Therefore, the perilla oil powder for preparing in the present invention, has a higher embedding efficiency, lower surface oil cut rate,
Perilla herb oil is wrapped in wall material, the effective component being able to maintain in perilla herb oil, can be added well in various food, pole
The earth expands the scope of application of original perilla herb oil.
The storage-stable of grease microcapsule powder prepared by the present invention is better than purple perilla crude oil.The perilla herb oil after embedding
Oxidation stability is significantly improved, and shelf life reaches 169.5 days, and the shelf life of purple perilla crude oil only has 52.8 days, explanation
Grease microcapsule powder prepared by the present invention plays a very good protection to grease, hence it is evident that improves the storage-stable of grease
Property.
In the present invention after protein-based wall material heat treatment, strand expansion, hydrophobic grouping exposure is adsorbed on grease surface,
The stability that can increase emulsion, in spray-drying process, the moisture in water phase is by rapid evaporation, and protein is then in core material
Surface forms network-like structure, and core material is embedded.But protein-based wall material content can excessively make microcapsules be cracked.And it fits
When the maltodextrin presence of ratio, then it can be used as filler, in the drying process, be filled in the gap of network structure or cover
It covers on protein cyst wall surface, increases the mechanical strength of microcapsules.Albumen containing part 1%~5% in Arabic gum molecule
Matter, thus it is with good emulsibility.Therefore, Arabic gum functions not only as wall material in system, but also plays as cream
The effect of agent and stabilizer.
The above description is only a preferred embodiment of the present invention, and the embodiment is not intended to limit patent protection of the invention
Range, thus it is all with the variation of equivalent structure made by description of the invention, it similarly should be included in institute of the present invention
In attached scope of protection of the claims.
Claims (9)
1. a kind of grease microcapsule powder, which is characterized in that including 33%-67% weight ratio in the grease microcapsule powder
The perilla herb oil and additive of wall material and 33%-67% weight ratio；Wherein, the wall material includes soybean protein isolate and malt paste
Essence, the additive include Arabic gum, glycerol monostearate and antioxidant.
2. a kind of grease microcapsule powder according to claim 1, which is characterized in that soybean protein isolate in the wall material
With the weight ratio of maltodextrin are as follows: 1: 1-2: 1.
3. a kind of grease microcapsule powder according to claim 1, which is characterized in that the mass ratio of the Arabic gum is
1%-3%.
4. a kind of grease microcapsule powder according to claim 1, which is characterized in that the antioxidant is tertiary butyl pair
Benzenediol.
5. a kind of grease microcapsule powder according to claim 1, which is characterized in that the grease is perilla herb oil or algae oil
Or linseed oil.
6. a kind of method for preparing grease microcapsule powder described in claim 1, which comprises the steps of:
S01: weighing soybean protein isolate, maltodextrin, Arabic gum, glycerin monostearate and antioxidant respectively, carries out
Mixing, and form wall material aqueous solution；
S02: above-mentioned resulting wall material aqueous solution is put into insulated sterilizing in thermostat water bath；
S03: being added perilla herb oil in the wall material aqueous solution after above-mentioned sterilizing, be uniformly mixed, and forming solid content is 12%-
28% emulsion；Wherein, the weight ratio of wall material is 1: 2-2: 1 in grease and step S01；
S04: by the emulsion with high pressure homogenizer homogeneous 2-3 times, the emulsion of stable homogeneous is obtained；
S05: it will be spray-dried to obtain grease microcapsule powder after emulsion filtering.
7. a kind of method for preparing grease microcapsule powder according to claim 6, which is characterized in that the step S02
The temperature of middle water bath with thermostatic control is 80-90 DEG C, and the time is 30 minutes.
8. a kind of method for preparing grease microcapsule powder according to claim 6, which is characterized in that the step S03
Before middle addition grease, the temperature of the wall material aqueous solution after the sterilizing is reduced to 60-70 DEG C.
9. a kind of method for preparing grease microcapsule powder according to claim 6, which is characterized in that the step S05
When middle spray drying, inlet air temperature control is 180-200 DEG C, and leaving air temp control is 70-80 DEG C, and feeding temperature control is 50-
60℃。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810817108.8A CN109042924A (en) | 2018-07-18 | 2018-07-18 | A kind of grease microcapsule powder and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810817108.8A CN109042924A (en) | 2018-07-18 | 2018-07-18 | A kind of grease microcapsule powder and preparation method thereof |
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| CN109042924A true CN109042924A (en) | 2018-12-21 |
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| CN201810817108.8A Pending CN109042924A (en) | 2018-07-18 | 2018-07-18 | A kind of grease microcapsule powder and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110269105A (en) * | 2019-07-23 | 2019-09-24 | 青海行源旅游文化有限公司 | It is a kind of anti-softening, anti-mildew butter flower to prepare material and preparation method thereof |
| CN112007584A (en) * | 2020-08-31 | 2020-12-01 | 胡勇刚 | Preparation process of supercritical particles of grease |
| CN112494454A (en) * | 2020-12-04 | 2021-03-16 | 宁波泰一健康产业有限公司 | DHA-containing oral instant microcapsule powder and preparation method and application thereof |
| CN113647628A (en) * | 2021-08-18 | 2021-11-16 | 重庆医科大学 | Preparation method of oil microcapsule and product thereof |
| CN114431471A (en) * | 2020-10-19 | 2022-05-06 | 中恩（天津）医药科技有限公司 | Oil microcapsule powder, preparation method and application |
| CN115428930A (en) * | 2022-09-19 | 2022-12-06 | 西北师范大学 | Spray drying preparation method of pepper essential oil microcapsules |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110269105A (en) * | 2019-07-23 | 2019-09-24 | 青海行源旅游文化有限公司 | It is a kind of anti-softening, anti-mildew butter flower to prepare material and preparation method thereof |
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| CN114431471A (en) * | 2020-10-19 | 2022-05-06 | 中恩（天津）医药科技有限公司 | Oil microcapsule powder, preparation method and application |
| CN112494454A (en) * | 2020-12-04 | 2021-03-16 | 宁波泰一健康产业有限公司 | DHA-containing oral instant microcapsule powder and preparation method and application thereof |
| CN113647628A (en) * | 2021-08-18 | 2021-11-16 | 重庆医科大学 | Preparation method of oil microcapsule and product thereof |
| CN115428930A (en) * | 2022-09-19 | 2022-12-06 | 西北师范大学 | Spray drying preparation method of pepper essential oil microcapsules |
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Application publication date: 20181221 |