CN109021853A - A kind of production technology of the adhesive label for upper machine Blood culture bottle - Google Patents
A kind of production technology of the adhesive label for upper machine Blood culture bottle Download PDFInfo
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- CN109021853A CN109021853A CN201810665491.XA CN201810665491A CN109021853A CN 109021853 A CN109021853 A CN 109021853A CN 201810665491 A CN201810665491 A CN 201810665491A CN 109021853 A CN109021853 A CN 109021853A
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- culture bottle
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/29—Laminated material
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
- C09J4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2203/00—Applications of adhesives in processes or use of adhesives in the form of films or foils
- C09J2203/334—Applications of adhesives in processes or use of adhesives in the form of films or foils as a label
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/10—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
- C09J2301/16—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the structure of the carrier layer
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2467/00—Presence of polyester
- C09J2467/006—Presence of polyester in the substrate
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The present invention relates to a kind of production technologies of adhesive label for upper machine Blood culture bottle, include the following steps: the preparation of S1 plane materiel；The preparation of S2 adhesive；The preparation of S3 base stock；The preparation of S4 film；The preparation of S5 adhesive label: the adhesive being prepared in S2 step is uniformly coated on to the one side of the plane materiel of S1 step preparation, glue-coated plane materiel is obtained by oven drying, the one side of glue-coated plane materiel gluing and obtained base stock prepared by S3 step are pressed again, the one side of film and the non-gluing of plane materiel in S4 step is carried out on compounding machine again compound, it is cured in curing chamber, adhesive label is prepared.The adhesive label that the present invention is prepared is suitable for upper machine Blood culture bottle, has the advantages that easily tearing, good antimicrobial effect and is less prone to human operational error.
Description
Technical field
The present invention relates to label technique fields, and in particular to a kind of production of the adhesive label for upper machine Blood culture bottle
Technique.
Background technique
Present label is for indicating your product objective and classification or content, seeming that you determine to your target
Crucial words searches and positions the tool of oneself target with other people convenient for you oneself.The so-called label of press is largely to use
Come identify oneself product related description printed matter, and largely is all that glue is carried with the back side.But there are also printings
When without glue, alternatively referred to as label.The label for having glue is exactly " adhesive label " of popular title.Label after instrument calibration is asked
Topic, this is (or the regulation inside the province of the oneself) label as defined in unification of the motherland, label can explicitly stated instrument be calibrated
Details afterwards.
Adhesive label with traditional label have without brush coating, without paste, without dip in water, it is pollution-free, save label
The advantages that time, has a wide range of application, convenient and efficient.Adhesive sticker is a kind of material, also cry self-adhesive label material with paper, film or
Other special materials are fabric, and the back side is coated with adhesive, to apply a kind of composite material of the silicon protection sheet as base stock.And printed,
Become finished product label after the processing such as cross cutting.
Adhesive sticker have many advantages, such as do not have to brush coating, without paste, without dip in water, it is pollution-free, save labeling the time, using model
It encloses extensively, it is convenient and efficient.All kinds of adhesive labels all can be applicable on the inefficient material of general paper sheet label institute, can be in this way
It says, adhesive label is a kind of omnipotent label, and pressure-sensitive table printing has very big compared with the printing of traditional printed matter
Difference, adhesive label print processing usually on label gear, and multi-process is once completed.In the prior art, it is used for
The label fungistatic effect that machine Blood culture bottle uses is bad, is not easy to tear.
Summary of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of adhesive sticker marks for upper machine Blood culture bottle
The production technology of label solves the problems, such as that the label fungistatic effect used for upper machine Blood culture bottle is bad and is not easily stripped.
The purpose of the present invention is achieved through the following technical solutions:
A kind of production technology of the adhesive label for upper machine Blood culture bottle, includes the following steps:
The preparation of S1 plane materiel: according to parts by weight prepare raw material: 40-50 parts of polyhydroxyalkanoate, 80-100 parts of polylactic acid,
20-30 parts of low density ethylene, 10-15 parts of glass fibre, 30-40 parts of polypropylene, 20-30 parts of polyisobutene, antistatic agent 5-10
Part, 3-8 parts of lubricant, 8-12 parts of bacteriostatic agent, by polyhydroxyalkanoate, polylactic acid, low density ethylene, glass fibre, poly- third
Alkene and polyisobutene, which are added in high speed disintegrator, premixes 30-60s, adds antistatic agent, lubricant and bacteriostatic agent and continuess to mix
20-30s, by mixed raw material, extrusion molding obtains sheet material in an extruder, then sheet material print stand-by up to plane materiel；
The preparation of S2 adhesive: according to parts by weight prepare raw material: 20-30 parts of starch, 10-20 parts of polyhydroxyalkanoate,
15-20 parts of acrylic acid, 5-8 parts of water-proofing agent, 5-8 parts of crosslinking agent, 10-15 parts of bacteriostatic agent, 100 parts of water, starch is soluble in water, it stirs
It mixes after mixing, acrylic acid is added and polyhydroxyalkanoate continues to be stirred 40-60min, be eventually adding water-proofing agent, hand over
It is stand-by to get adhesive that connection agent and bacteriostatic agent are stirred 1-2h；
The preparation of S3 base stock: it with silicon equipment is applied in base stock surface even spread silicone oil, places into baking oven and dries the bottom of to get
Paper is stand-by；
The preparation of S4 film: polyethylene film is placed in coating machine even spread polyvinylidene chloride to get film
For use；
The preparation of S5 adhesive label: the adhesive being prepared in S2 step is uniformly coated on to the face of S1 step preparation
The one side of material obtains glue-coated plane materiel by oven drying, then is prepared by the one side of glue-coated plane materiel gluing and S3 step
Obtained base stock pressing, then the one side of film and the non-gluing of plane materiel in S4 step carried out on compounding machine it is compound, ripe
Change and cured in room, adhesive label is prepared.
Antistatic agent, lubricant and bacteriostatic agent are added in the plane materiel of adhesive label for upper machine Blood culture bottle, can be increased
Antistatic property, processing performance and the fungistatic effect of strong plane materiel；After addition bacteriostatic agent adhesive label is had good
Fungistatic effect is not easy raw bacterium, use is safer, as a result more acurrate more suitable for using on upper machine Blood culture bottle.
Antistatic agent, lubricant and bacteriostatic agent are added in the plane materiel of adhesive label for upper machine Blood culture bottle, can be increased
Antistatic property, processing performance and the fungistatic effect of strong plane materiel；After addition bacteriostatic agent adhesive label is had good
Fungistatic effect is not easy raw bacterium, use is safer, as a result more acurrate more suitable for using on upper machine Blood culture bottle.
Adhesive label compound thin film on plane materiel, can protect the pattern printed on plane materiel, avoid using culture bottle
During label corroded by infiltration and cause label smudgy, to influence to judge, be unfavorable for being normally carried out for experiment；It does not do
The preparation process of glue label is simple, and inferior rate is low.
Further, in the S1 step antistatic agent be N, bis- (2- ethoxy) alkylamines of N-, polyglycerol ester and/or divide
At least one of son distillation monoglyceride；In the S1 step lubricant be magnesium stearate, calcium stearate, barium stearate and/or
At least one of odium stearate；Bacteriostatic agent is at least one in sulphur powder, copper sulphate and/or Kocide SD in the S1 step
Kind.
Further, extrusion temperature is 120-150 DEG C in the S1 step.
Further, water-proofing agent is in copper sulphate, zinc sulfate and/or trifluoroethyl methacrylate in the S2 step
It is at least one；The crosslinking agent is boric acid；The bacteriostatic agent is sulphur powder.
The source of electrostatic agent, lubricant and bacteriostatic agent is wide, at low cost, and small to the toxic of human body, not volatile, to training
The use influence for supporting bottle is small；While wherein sulphur powder has good fungistatic effect as bacteriostatic agent, also there is certain fill out
Use use as；And the surface of adhesive label is compound using polyethylene film, although so that be added to sulphur powder in plane materiel, sulphur
Powder does not contact directly with the external world, avoids security risk.
Further, the coating weight of silicone oil is 1.2-1.3g/m in the S3 step2, drying temperature is 140-150 DEG C.
Further, the coating weight of polyvinylidene chloride is 1.5-1.8g/m in the S4 step2。
Further, the coating weight of adhesive is 20-25g/m2 in the S5 step, and drying temperature is 100-120 DEG C.
Further, the pressure pressed in the S5 step is 300-500N, and pressing rate is 15-20m/min.
Further, the winding tension of compounding machine is 10.0-10.5kg, recombination velocity 120- in the S5 step
125m/min, the curing temperature of curing chamber are 50-55 DEG C, curing time 30-40h.
The beneficial effects of the present invention are:
1., can for adding antistatic agent, lubricant and bacteriostatic agent in the plane materiel of the adhesive label of upper machine Blood culture bottle
Enhance antistatic property, processing performance and the fungistatic effect of plane materiel；After addition bacteriostatic agent adhesive label is had good
Fungistatic effect be not easy raw bacterium, use is safer, as a result more acurrate more suitable for using on upper machine Blood culture bottle；
2. the adhesive of adhesive label is using starch, polyhydroxyalkanoate, acrylic acid, water-proofing agent, crosslinking agent, antibacterial
Agent, water, gluing effect is good and can tear, avoid abandon waste after misapplied again, tear label after can obviously with it is not used
Culture bottle is distinguished, and human operational error is avoided；
3. adhesive label compound thin film on plane materiel, can protect the pattern printed on plane materiel, avoid using culture
Label is corroded by infiltration during bottle causes label smudgy, to influence to judge, is unfavorable for being normally carried out for experiment；No
The preparation process of dry glue label is simple, and inferior rate is low；
4. the source of electrostatic agent, lubricant and bacteriostatic agent is wide, at low cost, and small to the toxic of human body, not volatile, right
The use of culture bottle influences small；While wherein sulphur powder has good fungistatic effect as bacteriostatic agent, also have centainly
Filling effect；And the surface of adhesive label is compound using polyethylene film, although so that be added to sulphur powder in plane materiel, sulphur
Sulphur powder does not contact directly with the external world, avoids security risk.
Specific embodiment
Technical solution of the present invention is described in further detail combined with specific embodiments below, but protection scope of the present invention is not
It is confined to as described below.
A kind of production technology of the adhesive label for upper machine Blood culture bottle, includes the following steps:
The preparation of S1 plane materiel: according to parts by weight prepare raw material: 40-50 parts of polyhydroxyalkanoate, 80-100 parts of polylactic acid,
20-30 parts of low density ethylene, 10-15 parts of glass fibre, 30-40 parts of polypropylene, 20-30 parts of polyisobutene, antistatic agent 5-10
Part, 3-8 parts of lubricant, 8-12 parts of bacteriostatic agent, by polyhydroxyalkanoate, polylactic acid, low density ethylene, glass fibre, poly- third
Alkene and polyisobutene, which are added in high speed disintegrator, premixes 30-60s, adds antistatic agent, lubricant and bacteriostatic agent and continuess to mix
20-30s, by mixed raw material, extrusion molding obtains sheet material in an extruder, then sheet material print stand-by up to plane materiel；
The preparation of S2 adhesive: according to parts by weight prepare raw material: 20-30 parts of starch, 10-20 parts of polyhydroxyalkanoate,
15-20 parts of acrylic acid, 5-8 parts of water-proofing agent, 5-8 parts of crosslinking agent, 10-15 parts of bacteriostatic agent, 100 parts of water, starch is soluble in water, it stirs
It mixes after mixing, acrylic acid is added and polyhydroxyalkanoate continues to be stirred 40-60min, be eventually adding water-proofing agent, hand over
It is stand-by to get adhesive that connection agent and bacteriostatic agent are stirred 1-2h；
The preparation of S3 base stock: it with silicon equipment is applied in base stock surface even spread silicone oil, places into baking oven and dries the bottom of to get
Paper is stand-by；
The preparation of S4 film: polyethylene film is placed in coating machine even spread polyvinylidene chloride to get film
For use；
The preparation of S5 adhesive label: the adhesive being prepared in S2 step is uniformly coated on to the face of S1 step preparation
The one side of material obtains glue-coated plane materiel by oven drying, then is prepared by the one side of glue-coated plane materiel gluing and S3 step
Obtained base stock pressing, then the one side of film and the non-gluing of plane materiel in S4 step carried out on compounding machine it is compound, ripe
Change and cured in room, adhesive label is prepared.
Specifically, antistatic agent is N, N- bis- (2- ethoxy) alkylamine, polyglycerol ester and/or molecules in the S1 step
Distill at least one of monoglyceride；Lubricant is magnesium stearate, calcium stearate, barium stearate and/or hard in the S1 step
At least one of resin acid sodium；Bacteriostatic agent is at least one in sulphur powder, copper sulphate and/or Kocide SD in the S1 step
Kind.
Specifically, extrusion temperature is 120-150 DEG C in the S1 step.
Specifically, in the S2 step water-proofing agent be copper sulphate, zinc sulfate and/or trifluoroethyl methacrylate in extremely
Few one kind；The crosslinking agent is boric acid；The bacteriostatic agent is sulphur powder.
Specifically, the coating weight of silicone oil is 1.2-1.3g/m in the S3 step2, drying temperature is 140-150 DEG C.
Specifically, the coating weight of polyvinylidene chloride is 1.5-1.8g/m in the S4 step2。
Specifically, the coating weight of adhesive is 20-25g/m in the S5 step2, drying temperature is 100-120 DEG C.
Specifically, the pressure pressed in the S5 step is 300-500N, and pressing rate is 15-20m/min.
Specifically, the winding tension of compounding machine is 10.0-10.5kg, recombination velocity 120-125m/ in the S5 step
Min, the curing temperature of curing chamber are 50-55 DEG C, curing time 30-40h.
The specific preparation parameter of embodiment 1- embodiment 6 is as shown in table 1, and wherein embodiment 1- embodiment 4 is present invention limit
Fixed technical parameter does not add bacteriostatic agent in embodiment 5, starch and polyhydroxyalkanoate, embodiment is not added in embodiment 6
5- embodiment 6 is comparative examples of the invention.
Table 1
The specific experiment data of embodiment 1- embodiment 6 are as shown in table 2, and wherein embodiment 1- embodiment 4 is present invention limit
Fixed technical parameter does not add bacteriostatic agent in embodiment 5, starch and polyhydroxyalkanoate, embodiment is not added in embodiment 6
5- embodiment 6 is comparative examples of the invention.Aerobic bacteria sum refers to the total bacterium grown on pancreas junket soya peptone agar medium
Fall number；Escherichia coli number refers to the total clump count grown on Mai Kangkai fluid nutrient medium.
Table 2
It can be seen that in embodiment 1- embodiment 5 from the data of table 2 and be added to starch and polyhydroxyalkanoate, enhance
The performance that label can be torn, during so that it is removed label will not residual fraction label facial tissue on culture bottle；Embodiment
Label is added to bacteriostatic agent in 1- embodiment 4 and embodiment 6, is considerably less than its clump count in microculture experiment and implements
Example 5.
The above is only a preferred embodiment of the present invention, it should be understood that the present invention is not limited to shape described herein
Formula should not be regarded as an exclusion of other examples, and can be used for other combinations, modifications, and environments, and can be herein
In the contemplated scope, modifications can be made through the above teachings or related fields of technology or knowledge.And those skilled in the art are carried out
Modifications and changes do not depart from the spirit and scope of the present invention, then all should be within the scope of protection of the appended claims of the present invention.
Claims (9)
1. a kind of production technology of the adhesive label for upper machine Blood culture bottle, which comprises the steps of:
The preparation of S1 plane materiel: prepare raw material according to parts by weight: 40-50 parts of polyhydroxyalkanoate, 80-100 parts of polylactic acid, low close
Ethylene 20-30 parts of degree, 10-15 parts of glass fibre, 30-40 parts of polypropylene, 20-30 parts of polyisobutene, 5-10 parts of antistatic agent, profit
3-8 parts of lubrication prescription, 8-12 parts of bacteriostatic agent by polyhydroxyalkanoate, polylactic acid, low density ethylene, glass fibre, polypropylene and gather
Isobutene is added in high speed disintegrator and premixes 30-60s, adds antistatic agent, lubricant and bacteriostatic agent and continuess to mix 20-30s,
By mixed raw material, extrusion molding obtains sheet material in an extruder, then sheet material print stand-by up to plane materiel；
The preparation of S2 adhesive: prepare raw material: 20-30 parts of starch, 10-20 parts of polyhydroxyalkanoate, propylene according to parts by weight
15-20 parts sour, 5-8 parts of water-proofing agent, 5-8 parts of crosslinking agent, 10-15 parts of bacteriostatic agent, 100 parts of water, starch is soluble in water, and stirring is mixed
After closing uniformly, acrylic acid is added and polyhydroxyalkanoate continues to be stirred 40-60min, is eventually adding water-proofing agent, crosslinking agent
It is stand-by to get adhesive that 1-2h is stirred with bacteriostatic agent；
The preparation of S3 base stock: it with silicon equipment is applied in base stock surface even spread silicone oil, places into drying in baking oven and is waited for get base stock
With；
The preparation of S4 film: by polyethylene film to be placed in even spread polyvinylidene chloride in coating machine stand-by to get film；
The preparation of S5 adhesive label: the adhesive being prepared in S2 step is uniformly coated on the plane materiel of S1 step preparation
On one side, glue-coated plane materiel is obtained by oven drying, then the one side of glue-coated plane materiel gluing is obtained with prepared by S3 step
The base stock pressing arrived, then the one side of film and the non-gluing of plane materiel in S4 step carried out on compounding machine it is compound, in curing chamber
Middle curing, is prepared adhesive label.
2. a kind of production technology of adhesive label for upper machine Blood culture bottle according to claim 1, feature exist
In antistatic agent is N in the S1 step, in bis- (2- ethoxy) alkylamines of N-, polyglycerol ester and/or molecular distillation monoglyceride
At least one；In the S1 step lubricant be magnesium stearate, calcium stearate, barium stearate and/or odium stearate in extremely
Few one kind；Bacteriostatic agent is at least one of sulphur powder, copper sulphate and/or Kocide SD in the S1 step.
3. a kind of production technology of adhesive label for upper machine Blood culture bottle according to claim 1, feature exist
In extrusion temperature is 120-150 DEG C in the S1 step.
4. a kind of production technology of adhesive label for upper machine Blood culture bottle according to claim 1, feature exist
In water-proofing agent is at least one of copper sulphate, zinc sulfate and/or trifluoroethyl methacrylate in the S2 step；It is described
Crosslinking agent is boric acid；The bacteriostatic agent is sulphur powder.
5. a kind of production technology of adhesive label for upper machine Blood culture bottle according to claim 1, feature exist
In the coating weight of silicone oil is 1.2-1.3g/m in the S3 step2, drying temperature is 140-150 DEG C.
6. a kind of production technology of adhesive label for upper machine Blood culture bottle according to claim 1, feature exist
In the coating weight of polyvinylidene chloride is 1.5-1.8g/m in the S4 step2。
7. a kind of production technology of adhesive label for upper machine Blood culture bottle according to claim 1, feature exist
In the coating weight of adhesive is 20-25g/m in the S5 step2, drying temperature is 100-120 DEG C.
8. a kind of production technology of adhesive label for upper machine Blood culture bottle according to claim 1, feature exist
In the pressure pressed in the S5 step is 300-500N, and pressing rate is 15-20m/min.
9. a kind of production technology of adhesive label for upper machine Blood culture bottle according to claim 1, feature exist
In, in the S5 step winding tension of compounding machine be 10.0-10.5kg, recombination velocity 120-125m/min, curing chamber
Curing temperature is 50-55 DEG C, curing time 30-40h.
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| CN113351429A (en) * | 2021-07-05 | 2021-09-07 | 温州高德复合材料有限公司 | Production process of adhesive sticker |
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| CN110176179A (en) * | 2019-05-17 | 2019-08-27 | 宁波卓越印务有限公司 | A kind of multi-functional adhesive label and preparation method thereof |
| CN110862680A (en) * | 2019-11-21 | 2020-03-06 | 济南大学 | Preparation method of fluorine-containing polyacrylic acid copolymer antibacterial composite material, obtained product and application |
| CN110862680B (en) * | 2019-11-21 | 2022-03-18 | 济南大学 | Preparation method of fluorine-containing polyacrylic acid copolymer antibacterial composite material, obtained product and application |
| CN112652228A (en) * | 2020-12-28 | 2021-04-13 | 江苏金大包装材料科技有限公司 | Production process of adhesive sticker composite material for white grids of writing stickers |
| CN113351429A (en) * | 2021-07-05 | 2021-09-07 | 温州高德复合材料有限公司 | Production process of adhesive sticker |
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Application publication date: 20181218 |