CN109019812A - A kind of environmentally friendly medicament and its preparation method and application for Industrial Waste Water Treatments - Google Patents
A kind of environmentally friendly medicament and its preparation method and application for Industrial Waste Water Treatments Download PDFInfo
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- CN109019812A CN109019812A CN201811005870.2A CN201811005870A CN109019812A CN 109019812 A CN109019812 A CN 109019812A CN 201811005870 A CN201811005870 A CN 201811005870A CN 109019812 A CN109019812 A CN 109019812A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
- C02F1/56—Macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
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- Hydrology & Water Resources (AREA)
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- Environmental & Geological Engineering (AREA)
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Abstract
The environmentally friendly medicament and its preparation method and application that the invention discloses a kind of for Industrial Waste Water Treatments, the raw material including following parts by weight: 8.6-10.7 parts of alum, 10.5-14.4 parts of Iron(III) chloride hexahydrate, 4.5-7.2 parts of bur beggar-ticks, 6-9.2 parts of neopelex, 7-9.5 parts of citric acid, 8-12.7 parts of bodied ferric sulfate, 4-6.4 parts of pine needle, 2.4-3.5 parts of heteroauxin, 3.8-6.6 parts of sodium peroxydisulfate, 4-6 parts of ethyl acetate, 4-5.8 parts of polyacrylamide, 5-7.5 parts of diatomite and 4-6 parts of Siberian cocklebur.The present invention plays synergistic effect by each component, and the finished product of preparation has good removal effect not only for heavy metal ion, moreover it is possible to and it is effective to remove COD and BOD, the cost of water process is reduced, sinking speed is fast, with good economic efficiency and social benefit.
Description
Technical field
The present invention relates to environment protection field, specifically a kind of environmentally friendly medicament for Industrial Waste Water Treatments.
Background technique
Industry is primarily referred to as the industry or engineering of feedstock capture and product processing and manufacturing.Industry is the production of division of labor in society development
Object, by handicraft, mordern industry, the several developing stage of modern industry.Industry is the important component of secondary industry,
It is broadly divided into light industry and heavy industry two major classes.
A large amount of sewage can be generated in industrial production, sewage disposal technology has the problems such as water-saving, energy saving particularly significant
Effect, sewage treatment drug is most common sewage treatment product.
As country is increasingly stringenter industrial wastewater discharge requirement, people are also finding a kind of effective sewage treatment
Agent can reach sewage discharge requirement after capable of making sewage treatment.Existing industrial sewage treating agent is to the huge sum of money in industrial wastewater
Belong to etc. harmful substances handled, and for the harmful substance in waste water other than heavy metal can not reach one it is good
Good removing effect, and also affect to environment in the use process of sewage treatment medicament, do not meet environmental protection
It is required that.
Summary of the invention
The purpose of the present invention is to provide a kind of environmentally friendly medicaments for Industrial Waste Water Treatments, to solve above-mentioned background technique
The problem of middle proposition.
To achieve the above object, the invention provides the following technical scheme:
A kind of environmentally friendly medicament for Industrial Waste Water Treatments, the raw material including following parts by weight: 8.6-10.7 parts of alum, six
10.5-14.4 parts of iron chloride hexahydrate, 4.5-7.2 parts of bur beggar-ticks, 6-9.2 parts of neopelex, citric acid 7-9.5
Part, 8-12.7 parts of bodied ferric sulfate, 4-6.4 parts of pine needle, 2.4-3.5 parts of heteroauxin, 3.8-6.6 parts of sodium peroxydisulfate, acetic acid second
4-6 parts of ester, 4-5.8 parts of polyacrylamide, 5-7.5 parts of diatomite and 4-6 parts of Siberian cocklebur.
As a further solution of the present invention: the environmentally friendly medicament for Industrial Waste Water Treatments, including following parts by weight
Raw material: 9.1-10.7 parts of alum, 11.5-14.4 parts of Iron(III) chloride hexahydrate, 5.4-7.2 parts of bur beggar-ticks, detergent alkylate
6.9-9.2 parts of sodium sulfonate, 7.7-9.5 parts of citric acid, 9.2-12.7 parts of bodied ferric sulfate, 4.7-6.4 parts of pine needle, heteroauxin
2.6-3.5 parts, 4.4-6.6 parts of sodium peroxydisulfate, 4.8-6 parts of ethyl acetate, 4.5-5.8 parts of polyacrylamide, diatomite 5.9-
7.5 parts and Siberian cocklebur 4.7-6 parts.
As a further solution of the present invention: the environmentally friendly medicament for Industrial Waste Water Treatments, including following parts by weight
Raw material: 9.7-10.7 parts of alum, 12.8-14.4 parts of Iron(III) chloride hexahydrate, 6.2-7.2 parts of bur beggar-ticks, detergent alkylate
7.7-9.2 parts of sodium sulfonate, 8.4-9.5 parts of citric acid, 10.6-12.7 parts of bodied ferric sulfate, 5.2-6.4 parts of pine needle, heteroauxin
2.9-3.5 parts, 5.1-6.6 parts of sodium peroxydisulfate, 5.4-6 parts of ethyl acetate, 5.3-5.8 parts of polyacrylamide, diatomite 6.6-
7.5 parts and Siberian cocklebur 5-6 parts.
As a further solution of the present invention: the environmentally friendly medicament for Industrial Waste Water Treatments, including following parts by weight
Raw material: 10.3 parts of alum, 13.9 parts of Iron(III) chloride hexahydrate, 6.8 parts of bur beggar-ticks, 8.7 parts of neopelex, lemon
Lemon acid 9.2 parts, 11.4 parts of bodied ferric sulfate, 5.9 parts of pine needle, 3.3 parts of heteroauxin, 6.2 parts of sodium peroxydisulfate, ethyl acetate 5.8
Part, 5.6 parts of polyacrylamide, 7.1 parts of diatomite and 5.7 parts of Siberian cocklebur.
The preparation method of the environmentally friendly medicament for Industrial Waste Water Treatments, the specific steps are as follows:
Siberian cocklebur and pine needle are crushed to 120-150 mesh respectively, the mass fraction of 6-9 times of its weight are then added by step 1
It is assisted for heating and refluxing extraction 3-4 times in the ethanol solution of 55-70% and using ultrasonic wave, filters and depressurize removal second
Alcohol obtains Siberian cocklebur extracting solution and pine needle extract；
Bur beggar-ticks is put into vegetable oil high fire and decocted 5-9 minute by step 2, removes bur beggar-ticks slag and bur beggar-ticks is oily
It is concentrated into the thick paste that relative density is 1.12-1.24, then mist projection granulating extracts particle to get to bur beggar-ticks；
Step 3, by pine needle extract, alum, Iron(III) chloride hexahydrate, neopelex and citric acid in ball
Ball milling and mistake 80-120 mesh, then handle 4-8 minutes in the electric field, obtain the first mixture in grinding machine；
Step 4, by bodied ferric sulfate, heteroauxin, sodium peroxydisulfate, ethyl acetate, polyacrylamide, diatomite and wolf
Grass is extracted particle heating at 60-80 degrees Celsius and is stirred evenly, the second mixture is obtained；
Step 5 stirs the deionized water of 4-7 times of the first mixture, the second mixture and the first mixture weight equal
It is even, divide 2-4 equivalent that Siberian cocklebur extracting solution is added while stirring, keeps the temperature 1-2.5 under 40-58 degrees Celsius after being added completely into
Hour, it stirs evenly and obtains finished product.
As a further solution of the present invention: the power of ultrasonic wave is 120-160W in step 1, and the frequency of ultrasonic wave is
18-34KHz。
As a further solution of the present invention: the temperature of mist projection granulating is 42-58 degrees Celsius in step 2, and pressure is
3.4-6.2MPa。
As a further solution of the present invention: electric field strength is 680-960V in step 3.
As a further solution of the present invention: the ratio of grinding media to material of ball mill is 75-96:1 in step 3, and the revolving speed of ball mill is
180-270rpm。
A kind of application of the environmentally friendly medicament for Industrial Waste Water Treatments in sewage treatment field.
Compared with prior art, the beneficial effects of the present invention are: raw material sources of the present invention are extensive, collaboration is played by each component
The finished product of effect, preparation has good removal effect not only for heavy metal ion, moreover it is possible to and it is effective to remove COD and BOD,
The cost of water process is reduced, it is a kind of environmentally protective medicament that sinking speed is fast, with good economic efficiency and social
Benefit.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of environmentally friendly medicament for Industrial Waste Water Treatments, the raw material including following parts by weight: 8.6 parts of alum, six hydrations
10.5 parts of ferric trichloride, 4.5 parts of bur beggar-ticks, 6 parts of neopelex, 7 parts of citric acid, 8 parts of bodied ferric sulfate, pine needle
4 parts, 2.4 parts of heteroauxin, 3.8 parts of sodium peroxydisulfate, 4 parts of ethyl acetate, 4 parts of polyacrylamide, 5 parts of diatomite and Siberian cocklebur 4
Part.
The preparation method of the environmentally friendly medicament for Industrial Waste Water Treatments, the specific steps are as follows:
Siberian cocklebur and pine needle are crushed to 130 mesh by step 1 respectively, and the mass fraction that 7 times of its weight is then added is 58%
Ethanol solution in heating and refluxing extraction 3 times and assisted using ultrasonic wave, the power of ultrasonic wave is 140W, the frequency of ultrasonic wave
Rate is 26KHz, filters and depressurizes removal ethyl alcohol, obtain Siberian cocklebur extracting solution and pine needle extract；
Bur beggar-ticks is put into vegetable oil high fire and decocted 6 minutes by step 2, removes bur beggar-ticks slag and bur beggar-ticks oil is dense
It is reduced to the thick paste that relative density is 1.17, then mist projection granulating extracts particle to get to bur beggar-ticks；
Step 3, by pine needle extract, alum, Iron(III) chloride hexahydrate, neopelex and citric acid in ball
It ball milling and is sieved with 100 mesh sieve in grinding machine, then handles 6 minutes in the electric field, obtain the first mixture；
Step 4, by bodied ferric sulfate, heteroauxin, sodium peroxydisulfate, ethyl acetate, polyacrylamide, diatomite and wolf
Grass is extracted particle heating at 67 degrees Celsius and is stirred evenly, the second mixture is obtained；
Step 5 stirs evenly the deionized water of 5 times of the first mixture, the second mixture and the first mixture weight,
Divide 3 equivalent that Siberian cocklebur extracting solution is added while stirring, keep the temperature 1.5 hours under 46 degrees Celsius after being added completely into, stirs
Uniformly obtain finished product.
A kind of application of the environmentally friendly medicament for Industrial Waste Water Treatments in sewage treatment field.
Embodiment 2
A kind of environmentally friendly medicament for Industrial Waste Water Treatments, the raw material including following parts by weight: 9.1 parts of alum, six hydrations
11.5 parts of ferric trichloride, 5.4 parts of bur beggar-ticks, 6.9 parts of neopelex, 7.7 parts of citric acid, bodied ferric sulfate 9.2
Part, 4.7 parts of pine needle, 2.6 parts of heteroauxin, 4.4 parts of sodium peroxydisulfate, 4.8 parts of ethyl acetate, 4.5 parts of polyacrylamide, diatom
5.9 parts and 4.7 parts of Siberian cocklebur of soil.
The preparation method of the environmentally friendly medicament for Industrial Waste Water Treatments, the specific steps are as follows:
Siberian cocklebur and pine needle are crushed to 140 mesh by step 1 respectively, and the mass fraction that 8 times of its weight is then added is 64%
Ethanol solution in heating and refluxing extraction 3 times and assisted using ultrasonic wave, filter and depressurize removal ethyl alcohol, obtain Siberian cocklebur
Extracting solution and pine needle extract；
Bur beggar-ticks is put into vegetable oil high fire and decocted 8 minutes by step 2, removes bur beggar-ticks slag and bur beggar-ticks oil is dense
It being reduced to the thick paste that relative density is 1.22, then mist projection granulating, the temperature of mist projection granulating is 52 degrees Celsius, pressure 5.5MPa,
It obtains bur beggar-ticks and extracts particle；
Step 3, by pine needle extract, alum, Iron(III) chloride hexahydrate, neopelex and citric acid in ball
Ball milling and 110 meshes excessively, then handle 6 minutes in the electric field, obtain the first mixture in grinding machine；
Step 4, by bodied ferric sulfate, heteroauxin, sodium peroxydisulfate, ethyl acetate, polyacrylamide, diatomite and wolf
Grass is extracted particle heating at 75 degrees Celsius and is stirred evenly, the second mixture is obtained；
Step 5 stirs evenly the deionized water of 5 times of the first mixture, the second mixture and the first mixture weight,
Divide 3 equivalent that Siberian cocklebur extracting solution is added while stirring, keep the temperature 1.8 hours under 46 degrees Celsius after being added completely into, stirs
Uniformly obtain finished product.
A kind of application of the environmentally friendly medicament for Industrial Waste Water Treatments in sewage treatment field.
Embodiment 3
A kind of environmentally friendly medicament for Industrial Waste Water Treatments, the raw material including following parts by weight: 9.7 parts of alum, six hydrations
12.8 parts of ferric trichloride, 6.2 parts of bur beggar-ticks, 7.7 parts of neopelex, 8.4 parts of citric acid, bodied ferric sulfate 10.6
Part, 5.2 parts of pine needle, 2.9 parts of heteroauxin, 5.1 parts of sodium peroxydisulfate, 5.4 parts of ethyl acetate, 5.3 parts of polyacrylamide, diatom
6.6 parts and 5 parts of Siberian cocklebur of soil.
The preparation method of the environmentally friendly medicament for Industrial Waste Water Treatments, the specific steps are as follows:
Siberian cocklebur and pine needle are crushed to 150 mesh by step 1 respectively, and the mass fraction that 6 times of its weight is then added is 58%
Ethanol solution in heating and refluxing extraction 3 times and assisted using ultrasonic wave, filter and depressurize removal ethyl alcohol, obtain Siberian cocklebur
Extracting solution and pine needle extract；
Bur beggar-ticks is put into vegetable oil high fire and decocted 8 minutes by step 2, removes bur beggar-ticks slag and bur beggar-ticks oil is dense
It is reduced to the thick paste that relative density is 1.17, then mist projection granulating extracts particle to get to bur beggar-ticks；
Step 3, by pine needle extract, alum, Iron(III) chloride hexahydrate, neopelex and citric acid in ball
Ball milling and 90 meshes excessively, then handle 6 minutes in the electric field of 840V, obtain the first mixture in grinding machine；
Step 4, by bodied ferric sulfate, heteroauxin, sodium peroxydisulfate, ethyl acetate, polyacrylamide, diatomite and wolf
Grass is extracted particle heating at 66 degrees Celsius and is stirred evenly, the second mixture is obtained；
Step 5 stirs evenly the deionized water of 5 times of the first mixture, the second mixture and the first mixture weight,
Divide 2 equivalent that Siberian cocklebur extracting solution is added while stirring, keep the temperature 2.2 hours under 49 degrees Celsius after being added completely into, stirs
Uniformly obtain finished product.
A kind of application of the environmentally friendly medicament for Industrial Waste Water Treatments in sewage treatment field.
Embodiment 4
A kind of environmentally friendly medicament for Industrial Waste Water Treatments, the raw material including following parts by weight: 10.3 parts of alum, six hydrations
13.9 parts of ferric trichloride, 6.8 parts of bur beggar-ticks, 8.7 parts of neopelex, 9.2 parts of citric acid, bodied ferric sulfate 11.4
Part, 5.9 parts of pine needle, 3.3 parts of heteroauxin, 6.2 parts of sodium peroxydisulfate, 5.8 parts of ethyl acetate, 5.6 parts of polyacrylamide, diatom
7.1 parts and 5.7 parts of Siberian cocklebur of soil.
The preparation method of the environmentally friendly medicament for Industrial Waste Water Treatments, the specific steps are as follows:
Siberian cocklebur and pine needle are crushed to 130 mesh by step 1 respectively, and the mass fraction that 8 times of its weight is then added is 64%
Ethanol solution in heating and refluxing extraction 4 times and assisted using ultrasonic wave, filter and depressurize removal ethyl alcohol, obtain Siberian cocklebur
Extracting solution and pine needle extract；
Bur beggar-ticks is put into vegetable oil high fire and decocted 7 minutes by step 2, removes bur beggar-ticks slag and bur beggar-ticks oil is dense
It is reduced to the thick paste that relative density is 1.21, then mist projection granulating extracts particle to get to bur beggar-ticks；
Step 3, by pine needle extract, alum, Iron(III) chloride hexahydrate, neopelex and citric acid in ball
Ball milling and 120 meshes excessively in grinding machine, the ratio of grinding media to material of ball mill are 84:1, and the revolving speed of ball mill is 210rpm, then
It handles 6 minutes in the electric field, obtains the first mixture；
Step 4, by bodied ferric sulfate, heteroauxin, sodium peroxydisulfate, ethyl acetate, polyacrylamide, diatomite and wolf
Grass is extracted particle heating at 69 degrees Celsius and is stirred evenly, the second mixture is obtained；
Step 5 stirs evenly the deionized water of 6 times of the first mixture, the second mixture and the first mixture weight,
Divide 3 equivalent that Siberian cocklebur extracting solution is added while stirring, keep the temperature 1.8 hours under 55 degrees Celsius after being added completely into, stirs
Uniformly obtain finished product.
A kind of application of the environmentally friendly medicament for Industrial Waste Water Treatments in sewage treatment field
Embodiment 5
A kind of environmentally friendly medicament for Industrial Waste Water Treatments, the raw material including following parts by weight: 10.7 parts of alum, six hydrations
14.4 parts of ferric trichloride, 7.2 parts of bur beggar-ticks, 9.2 parts of neopelex, 9.5 parts of citric acid, bodied ferric sulfate 12.7
Part, 6.4 parts of pine needle, 3.5 parts of heteroauxin, 6.6 parts of sodium peroxydisulfate, 6 parts of ethyl acetate, 5.8 parts of polyacrylamide, diatomite
7.5 parts and 6 parts of Siberian cocklebur.
The preparation method of the environmentally friendly medicament for Industrial Waste Water Treatments, the specific steps are as follows:
Siberian cocklebur and pine needle are crushed to 120 mesh by step 1 respectively, and the mass fraction that 6 times of its weight is then added is 64%
Ethanol solution in heating and refluxing extraction 4 times and assisted using ultrasonic wave, the power of ultrasonic wave is 145W, the frequency of ultrasonic wave
Rate is 27KHz, filters and depressurizes removal ethyl alcohol, obtain Siberian cocklebur extracting solution and pine needle extract；
Bur beggar-ticks is put into vegetable oil high fire and decocted 6 minutes by step 2, removes bur beggar-ticks slag and bur beggar-ticks oil is dense
It being reduced to the thick paste that relative density is 1.22, then mist projection granulating, the temperature of mist projection granulating is 54 degrees Celsius, pressure 5.8MPa,
It obtains bur beggar-ticks and extracts particle；
Step 3, by pine needle extract, alum, Iron(III) chloride hexahydrate, neopelex and citric acid in ball
Ball milling and 120 meshes excessively in grinding machine, the ratio of grinding media to material of ball mill are 92:1, and the revolving speed of ball mill is 270rpm, then
It is handled 6 minutes in the electric field of 850V, obtains the first mixture；
Step 4, by bodied ferric sulfate, heteroauxin, sodium peroxydisulfate, ethyl acetate, polyacrylamide, diatomite and wolf
Grass is extracted particle heating at 77 degrees Celsius and is stirred evenly, the second mixture is obtained；
Step 5 stirs evenly the deionized water of 7 times of the first mixture, the second mixture and the first mixture weight,
Divide 3 equivalent that Siberian cocklebur extracting solution is added while stirring, keep the temperature 2.5 hours under 43 degrees Celsius after being added completely into, stirs
Uniformly obtain finished product.
A kind of application of the environmentally friendly medicament for Industrial Waste Water Treatments in sewage treatment field.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, nothing
By from the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by institute
Attached claim rather than above description limit, it is intended that will fall within the meaning and scope of the equivalent elements of the claims
All changes be included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (10)
1. a kind of environmentally friendly medicament for Industrial Waste Water Treatments, which is characterized in that the raw material including following parts by weight: alum 8.6-
10.7 parts, 10.5-14.4 parts of Iron(III) chloride hexahydrate, 4.5-7.2 parts of bur beggar-ticks, 6-9.2 parts of neopelex, lemon
7-9.5 parts sour, 8-12.7 parts of bodied ferric sulfate, 4-6.4 parts of pine needle, 2.4-3.5 parts of heteroauxin, 3.8-6.6 parts of sodium peroxydisulfate,
4-6 parts of ethyl acetate, 4-5.8 parts of polyacrylamide, 5-7.5 parts of diatomite and 4-6 parts of Siberian cocklebur.
2. the environmentally friendly medicament according to claim 1 for Industrial Waste Water Treatments, which is characterized in that including following parts by weight
Raw material: 9.1-10.7 parts of alum, 11.5-14.4 parts of Iron(III) chloride hexahydrate, 5.4-7.2 parts of bur beggar-ticks, detergent alkylate sulphur
Sour sodium 6.9-9.2 parts, 7.7-9.5 parts of citric acid, 9.2-12.7 parts of bodied ferric sulfate, 4.7-6.4 parts of pine needle, heteroauxin 2.6-
3.5 parts, 4.4-6.6 parts of sodium peroxydisulfate, 4.8-6 parts of ethyl acetate, 4.5-5.8 parts of polyacrylamide, 5.9-7.5 parts of diatomite and
4.7-6 parts of Siberian cocklebur.
3. the environmentally friendly medicament according to claim 1 for Industrial Waste Water Treatments, which is characterized in that including following parts by weight
Raw material: 9.7-10.7 parts of alum, 12.8-14.4 parts of Iron(III) chloride hexahydrate, 6.2-7.2 parts of bur beggar-ticks, detergent alkylate sulphur
Sour sodium 7.7-9.2 parts, 8.4-9.5 parts of citric acid, 10.6-12.7 parts of bodied ferric sulfate, 5.2-6.4 parts of pine needle, heteroauxin
2.9-3.5 parts, 5.1-6.6 parts of sodium peroxydisulfate, 5.4-6 parts of ethyl acetate, 5.3-5.8 parts of polyacrylamide, diatomite 6.6-7.5
Part and Siberian cocklebur 5-6 parts.
4. the environmentally friendly medicament according to claim 1 for Industrial Waste Water Treatments, which is characterized in that including following parts by weight
Raw material: 10.3 parts of alum, 13.9 parts of Iron(III) chloride hexahydrate, 6.8 parts of bur beggar-ticks, 8.7 parts of neopelex, lemon
Acid 9.2 parts, 11.4 parts of bodied ferric sulfate, 5.9 parts of pine needle, 3.3 parts of heteroauxin, 6.2 parts of sodium peroxydisulfate, 5.8 parts of ethyl acetate,
5.6 parts of polyacrylamide, 7.1 parts of diatomite and 5.7 parts of Siberian cocklebur.
5. a kind of preparation method of the environmentally friendly medicament for Industrial Waste Water Treatments as described in claim 1-4 is any, feature
It is, the specific steps are as follows:
Siberian cocklebur and pine needle are crushed to 120-150 mesh by step 1 respectively, and the mass fraction that 6-9 times of its weight is then added is 55-
It heating and refluxing extraction 3-4 times and is assisted using ultrasonic wave in 70% ethanol solution, filters and depressurize removal ethyl alcohol, obtain
Siberian cocklebur extracting solution and pine needle extract；
Bur beggar-ticks is put into high fire in vegetable oil and decocted 5-9 minutes, removed bur beggar-ticks slag and bur beggar-ticks oil is concentrated by step 2
The thick paste for being 1.12-1.24 to relative density, then mist projection granulating extracts particle to get to bur beggar-ticks；
Step 3, by pine needle extract, alum, Iron(III) chloride hexahydrate, neopelex and citric acid in ball mill
Middle ball milling and excessively 80-120 mesh, then handle 4-8 minutes in the electric field, obtain the first mixture；
Step 4, by bodied ferric sulfate, heteroauxin, sodium peroxydisulfate, ethyl acetate, polyacrylamide, diatomite and bur beggar-ticks
Particle heating is extracted at 60-80 degrees Celsius and is stirred evenly, the second mixture is obtained；
Step 5 stirs evenly the deionized water of 4-7 times of the first mixture, the second mixture and the first mixture weight, side
Stirring side divides 2-4 equivalent that Siberian cocklebur extracting solution is added, and keeps the temperature 1-2.5 hours under 40-58 degrees Celsius after being added completely into, stirs
It mixes and uniformly obtains finished product.
6. the preparation method of the environmentally friendly medicament according to claim 5 for Industrial Waste Water Treatments, which is characterized in that described
The power of ultrasonic wave is 120-160W in step 1, and the frequency of ultrasonic wave is 18-34KHz.
7. the preparation method of the environmentally friendly medicament according to claim 5 for Industrial Waste Water Treatments, which is characterized in that described
The temperature of mist projection granulating is 42-58 degrees Celsius in step 2, pressure 3.4-6.2MPa.
8. the preparation method of the environmentally friendly medicament according to claim 5 for Industrial Waste Water Treatments, which is characterized in that described
Electric field strength is 680-960V in step 3.
9. the preparation method of the environmentally friendly medicament according to claim 5 for Industrial Waste Water Treatments, which is characterized in that described
The ratio of grinding media to material of ball mill is 75-96:1 in step 3, and the revolving speed of ball mill is 180-270rpm.
10. a kind of environmentally friendly medicament for Industrial Waste Water Treatments as described in claim 1-4 is any is in sewage treatment field
Using.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110526417A (en) * | 2019-07-25 | 2019-12-03 | 江苏力鼎环保装备有限公司 | A kind of efficient removal total nitrogen bacteria agent applied to domestic sewage processing system |
-
2018
- 2018-08-30 CN CN201811005870.2A patent/CN109019812A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110526417A (en) * | 2019-07-25 | 2019-12-03 | 江苏力鼎环保装备有限公司 | A kind of efficient removal total nitrogen bacteria agent applied to domestic sewage processing system |
| CN110526417B (en) * | 2019-07-25 | 2020-07-07 | 江苏力鼎环保装备有限公司 | Biological agent for efficiently removing total nitrogen applied to domestic sewage treatment system |
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Application publication date: 20181218 |