CN106336950A - Method for extracting essential oil from lemongrass - Google Patents

Method for extracting essential oil from lemongrass Download PDF

Info

Publication number
CN106336950A
CN106336950A CN201610793295.1A CN201610793295A CN106336950A CN 106336950 A CN106336950 A CN 106336950A CN 201610793295 A CN201610793295 A CN 201610793295A CN 106336950 A CN106336950 A CN 106336950A
Authority
CN
China
Prior art keywords
lemon
grass
essential oil
lemongrass
mixing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610793295.1A
Other languages
Chinese (zh)
Inventor
周丽珠
陈明江
廖慧玲
吴美玉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fangchenggang Lvhuayuan Agriculture and Forestry Technology Co Ltd
Original Assignee
Fangchenggang Lvhuayuan Agriculture and Forestry Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fangchenggang Lvhuayuan Agriculture and Forestry Technology Co Ltd filed Critical Fangchenggang Lvhuayuan Agriculture and Forestry Technology Co Ltd
Priority to CN201610793295.1A priority Critical patent/CN106336950A/en
Publication of CN106336950A publication Critical patent/CN106336950A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to the field of essential oil preparation, in particular to a method for extracting essential oil from lemongrass. The method comprises the steps of uniformly mixing lemongrass and sodium chloride, laying aside, adding water for mixing, smashing into lemongrass slurry, performing ultrasonic extraction, separating mixed liquid of filtrate with a centrifugal machine, taking supernate, and performing pressure reduction under a thermostatic water bath condition to remove an organic solvent so as to obtain the essential oil. The method of extracting the essential oil from the lemongrass is short in extraction time and high in extraction rate; after the lemongrass is cured, cell walls and mesenchymal structures of the cell walls produce changes such as local looseness and expansion; the essential oil enters a solvent quickly during subsequent extraction working; the extraction time is greatly shortened; and the extraction rate of the essential oil is increased.

Description

A kind of method that lemon-grass extracts essential oil
Technical field
The present invention relates to essential oil preparation field and in particular to a kind of lemon-grass extract essential oil method.
Background technology
Lemon-grass is to be grown in a kind of semi-tropical cogongrass spices, and lemon-grass gives out a kind of lemon of natural strong in itself Fragrance, has the special efficacy promoted the sexual maturity with stomach ventilation, restoring consciouness.Tool antibacterial ability, can treat cholera, acute gastroenteritis and chronic abdomen Rush down, Glycerin contributes to women skin maintenance and is used, containing substantial amounts of vitamin c, be also the good merchantable brand of cosmetology.Adjust oil Fat is secreted, and is beneficial to oily skin and hair quality, can be added to the water cleaning skin, stimulate circulation.Tradition extracts lemon-grass essence The method of oil, recovery rate is low.
Content of the invention
The present invention provides a kind of recovery rate method that high lemon-grass extracts essential oil.
The technical solution adopted in the present invention is:
A kind of method that lemon-grass extracts essential oil, comprises the following steps:
(1) pluck fresh lemon-grass, in lemon-grass: the part by weight of sodium chloride is 1: 0.23-0.34 ratio mixing, mixes Close and uniformly place 60-100 hour afterwards, and repeatedly stirred mixing, then press lemon-grass: the part by weight of distilled water is 1: 2- 3.5 ratio adds water after mixing, is broken into lemon-grass slurries;
(2) extract: add the rosemary of lemon-grass weight 1-3%, the extractant of 3-5% in lemon-grass slurries, adopt Ultrasonic extraction 30-50 minute, extracts and is filtered after terminating, and collects filtrate, adds the second that mass concentration is 80-90% in filter residue Alcoholic solution, repeats above-mentioned ultrasonic extraction and filter operation twice, merges all filtrates;
(3) mixed liquor of filtrate is carried out with centrifuge separating, take supernatant, decompression removal under the conditions of water bath with thermostatic control has Machine solvent, obtains essential oil.
Extractant described in step (2) is 30-60 degree benzin.
Compared with the prior art, beneficial effects of the present invention are as follows:
The method extracting essential oil from lemon-grass of the present invention, extraction time is short, and recovery rate is high, after lemon-grass is pickled, carefully Cell wall and its interstitial structure produce the changes such as the loose, expansion of local, so that essential oil during follow-up extraction work is quickly entered into In solvent, substantially reduce extraction time, improve the recovery rate of essential oil.
Specific embodiment
The present invention is further illustrated with reference to embodiments, but the present invention is not limited only to these embodiments, not On the premise of departing from present inventive concept, any improvement made is within the scope of the present invention.Embodiment 1
A kind of method that lemon-grass extracts essential oil, comprises the following steps:
(1) pluck fresh lemon-grass, in lemon-grass: the part by weight of sodium chloride is 1: 0.23 ratio mixing, and mixing is all Place 100 hours after even, and repeatedly stirred mixing, then by lemon-grass: the ratio for 1: 2 for the part by weight of distilled water adds water After mixing, it is broken into lemon-grass slurries;
(2) extract: add the rosemary of lemon-grass weight 1-3%, 3% 30 degree of benzins in lemon-grass slurries, adopt With ultrasonic extraction 50 minutes, extract and filtered after terminating, collect filtrate, in filter residue, add the second that mass concentration is 80-90% Alcoholic solution, repeats above-mentioned ultrasonic extraction and filter operation twice, merges all filtrates;
(3) mixed liquor of filtrate is carried out with centrifuge separating, take supernatant, decompression removal under the conditions of water bath with thermostatic control has Machine solvent, obtains essential oil.
Embodiment 2
A kind of method that lemon-grass extracts essential oil, comprises the following steps:
(1) pluck fresh lemon-grass, in lemon-grass: the part by weight of sodium chloride is 1: 0.34 ratio mixing, and mixing is all Place 60 hours after even, and repeatedly stirred mixing, then by lemon-grass: the ratio for 1: 3.5 for the part by weight of distilled water adds After water mixing, it is broken into lemon-grass slurries;
(2) extract: add the rosemary of lemon-grass weight 1-3%, 3% 60 degree of benzins in lemon-grass slurries, adopt With ultrasonic extraction 30 minutes, extract and filtered after terminating, collect filtrate, in filter residue, add the second that mass concentration is 80-90% Alcoholic solution, repeats above-mentioned ultrasonic extraction and filter operation twice, merges all filtrates;
(3) mixed liquor of filtrate is carried out with centrifuge separating, take supernatant, decompression removal under the conditions of water bath with thermostatic control has Machine solvent, obtains essential oil.

Claims (2)

1. a kind of lemon-grass extract essential oil method it is characterised in that: comprise the following steps:
(1) pluck fresh lemon-grass, in lemon-grass: the part by weight of sodium chloride is the ratio mixing of 1:0.23-0.34, and mixing is all Place 60-100 hour after even, and repeatedly stirred mixing, then press lemon-grass: the part by weight of distilled water is 1:2-3.5 Ratio add water mixing after, be broken into lemon-grass slurries;
(2) extract: add the rosemary of lemon-grass weight 1-3% in lemon-grass slurries, the extractant of 3-5%, using ultrasonic Extract 30-50 minute, extract and filtered after terminating, collect filtrate, the ethanol adding mass concentration to be 80-90% in filter residue is molten Liquid, repeats above-mentioned ultrasonic extraction and filter operation twice, merges all filtrates;
(3) mixed liquor of filtrate is carried out with centrifuge separating, take supernatant, decompression removal is organic molten under the conditions of water bath with thermostatic control Agent, obtains essential oil.
2. a kind of lemon-grass according to claim 1 extract essential oil method it is characterised in that: described in step (2) Extractant is 30-60 degree benzin.
CN201610793295.1A 2016-08-31 2016-08-31 Method for extracting essential oil from lemongrass Pending CN106336950A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610793295.1A CN106336950A (en) 2016-08-31 2016-08-31 Method for extracting essential oil from lemongrass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610793295.1A CN106336950A (en) 2016-08-31 2016-08-31 Method for extracting essential oil from lemongrass

Publications (1)

Publication Number Publication Date
CN106336950A true CN106336950A (en) 2017-01-18

Family

ID=57822951

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610793295.1A Pending CN106336950A (en) 2016-08-31 2016-08-31 Method for extracting essential oil from lemongrass

Country Status (1)

Country Link
CN (1) CN106336950A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113951676A (en) * 2021-09-27 2022-01-21 杭州顾家寝具有限公司 Mattress capable of improving sleep
CN114381335A (en) * 2022-01-19 2022-04-22 海南热带海洋学院 Preparation method of lemongrass essential oil

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104789359A (en) * 2015-04-15 2015-07-22 芜湖市丹洋现代农业科技发展有限公司 Method for extracting essential oil from peony flowers
CN104928039A (en) * 2015-05-30 2015-09-23 防城港市防城区那梭香料厂 Preparation method for lemongrass essential oil

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104789359A (en) * 2015-04-15 2015-07-22 芜湖市丹洋现代农业科技发展有限公司 Method for extracting essential oil from peony flowers
CN104928039A (en) * 2015-05-30 2015-09-23 防城港市防城区那梭香料厂 Preparation method for lemongrass essential oil

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113951676A (en) * 2021-09-27 2022-01-21 杭州顾家寝具有限公司 Mattress capable of improving sleep
CN114381335A (en) * 2022-01-19 2022-04-22 海南热带海洋学院 Preparation method of lemongrass essential oil

Similar Documents

Publication Publication Date Title
CN103463123B (en) Method for extracting effective constituents from maca
CN101362983B (en) Extraction method of orange peel essential oil
CN103436350A (en) Aqueous enzymatic method for extracting rapeseed oil and recovering protein
CN104490968A (en) Extracting method of chamomile extract
CN103614230A (en) Preparation method of garlic oil
CN104928012A (en) Method for extracting tea oil by demulsification based on aqueous enzymatic method
CN104997817A (en) Extraction method of moringa oleifera leaf extractive
CN106265456A (en) A kind of Moringa facial film and preparation method thereof
CN106336950A (en) Method for extracting essential oil from lemongrass
CN105754716B (en) Method for extracting snake oil at low temperature and removing fishy smell and decoloring of snake oil
CN104789359A (en) Method for extracting essential oil from peony flowers
CN102796618B (en) Method for extracting essential oil from orange peel
CN104688788A (en) Extraction method of okra mucilage
CN107397699A (en) A kind of extracting method of Lignum Aquilariae Resinatum extract
CN104845730A (en) Avocado oil extraction method
CN102228473A (en) Extraction method for active substances in cornua cervi pantotrichum
CN105646501A (en) Method used for extracting chlorophyll, pectin, and leaf protein from silkworm excrement
CN108567668A (en) A kind of natural skin care hand cleanser
CN106281703A (en) A kind of extracting method of Bergamot
CN101831349A (en) Method for extracting wheat-germ oil continuously by using microwave secondary solvent
CN103409226B (en) Method for producing pomegranate seed oil
CN104928039A (en) Preparation method for lemongrass essential oil
CN110724603A (en) Supercritical CO of water lily essential oil2Extraction and pigment extraction process from flower residue
CN106810625A (en) The method for extracting sodium chondroitin sulfate with solid phase alkaline hydrolysiss from animal cartilage
CN106038428A (en) Cucumber toning lotion and preparation process thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
CB02 Change of applicant information

Address after: Fangcheng District Nasuo town Fangchenggang city the Guangxi Zhuang Autonomous Region 538000 to the summer village of Bayi group

Applicant after: FANGCHENGGANG LVHUAYUAN AGRICULTURE AND FORESTRY SCIENCE AND TECHNOLOGY CO., LTD.

Address before: 538000 the Guangxi Zhuang Autonomous Region, Fangchenggang port area Peach Peach Blossom Road, Hubei side of the new business incubator building, floor 3

Applicant before: FANGCHENGGANG LVHUAYUAN AGRICULTURE AND FORESTRY SCIENCE AND TECHNOLOGY CO., LTD.

COR Change of bibliographic data
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170118