CN106336950A - Method for extracting essential oil from lemongrass - Google Patents
Method for extracting essential oil from lemongrass Download PDFInfo
- Publication number
- CN106336950A CN106336950A CN201610793295.1A CN201610793295A CN106336950A CN 106336950 A CN106336950 A CN 106336950A CN 201610793295 A CN201610793295 A CN 201610793295A CN 106336950 A CN106336950 A CN 106336950A
- Authority
- CN
- China
- Prior art keywords
- lemon
- grass
- essential oil
- lemongrass
- mixing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the field of essential oil preparation, in particular to a method for extracting essential oil from lemongrass. The method comprises the steps of uniformly mixing lemongrass and sodium chloride, laying aside, adding water for mixing, smashing into lemongrass slurry, performing ultrasonic extraction, separating mixed liquid of filtrate with a centrifugal machine, taking supernate, and performing pressure reduction under a thermostatic water bath condition to remove an organic solvent so as to obtain the essential oil. The method of extracting the essential oil from the lemongrass is short in extraction time and high in extraction rate; after the lemongrass is cured, cell walls and mesenchymal structures of the cell walls produce changes such as local looseness and expansion; the essential oil enters a solvent quickly during subsequent extraction working; the extraction time is greatly shortened; and the extraction rate of the essential oil is increased.
Description
Technical field
The present invention relates to essential oil preparation field and in particular to a kind of lemon-grass extract essential oil method.
Background technology
Lemon-grass is to be grown in a kind of semi-tropical cogongrass spices, and lemon-grass gives out a kind of lemon of natural strong in itself
Fragrance, has the special efficacy promoted the sexual maturity with stomach ventilation, restoring consciouness.Tool antibacterial ability, can treat cholera, acute gastroenteritis and chronic abdomen
Rush down, Glycerin contributes to women skin maintenance and is used, containing substantial amounts of vitamin c, be also the good merchantable brand of cosmetology.Adjust oil
Fat is secreted, and is beneficial to oily skin and hair quality, can be added to the water cleaning skin, stimulate circulation.Tradition extracts lemon-grass essence
The method of oil, recovery rate is low.
Content of the invention
The present invention provides a kind of recovery rate method that high lemon-grass extracts essential oil.
The technical solution adopted in the present invention is:
A kind of method that lemon-grass extracts essential oil, comprises the following steps:
(1) pluck fresh lemon-grass, in lemon-grass: the part by weight of sodium chloride is 1: 0.23-0.34 ratio mixing, mixes
Close and uniformly place 60-100 hour afterwards, and repeatedly stirred mixing, then press lemon-grass: the part by weight of distilled water is 1: 2-
3.5 ratio adds water after mixing, is broken into lemon-grass slurries；
(2) extract: add the rosemary of lemon-grass weight 1-3%, the extractant of 3-5% in lemon-grass slurries, adopt
Ultrasonic extraction 30-50 minute, extracts and is filtered after terminating, and collects filtrate, adds the second that mass concentration is 80-90% in filter residue
Alcoholic solution, repeats above-mentioned ultrasonic extraction and filter operation twice, merges all filtrates；
(3) mixed liquor of filtrate is carried out with centrifuge separating, take supernatant, decompression removal under the conditions of water bath with thermostatic control has
Machine solvent, obtains essential oil.
Extractant described in step (2) is 30-60 degree benzin.
Compared with the prior art, beneficial effects of the present invention are as follows:
The method extracting essential oil from lemon-grass of the present invention, extraction time is short, and recovery rate is high, after lemon-grass is pickled, carefully
Cell wall and its interstitial structure produce the changes such as the loose, expansion of local, so that essential oil during follow-up extraction work is quickly entered into
In solvent, substantially reduce extraction time, improve the recovery rate of essential oil.
Specific embodiment
The present invention is further illustrated with reference to embodiments, but the present invention is not limited only to these embodiments, not
On the premise of departing from present inventive concept, any improvement made is within the scope of the present invention.Embodiment 1
A kind of method that lemon-grass extracts essential oil, comprises the following steps:
(1) pluck fresh lemon-grass, in lemon-grass: the part by weight of sodium chloride is 1: 0.23 ratio mixing, and mixing is all
Place 100 hours after even, and repeatedly stirred mixing, then by lemon-grass: the ratio for 1: 2 for the part by weight of distilled water adds water
After mixing, it is broken into lemon-grass slurries；
(2) extract: add the rosemary of lemon-grass weight 1-3%, 3% 30 degree of benzins in lemon-grass slurries, adopt
With ultrasonic extraction 50 minutes, extract and filtered after terminating, collect filtrate, in filter residue, add the second that mass concentration is 80-90%
Alcoholic solution, repeats above-mentioned ultrasonic extraction and filter operation twice, merges all filtrates；
(3) mixed liquor of filtrate is carried out with centrifuge separating, take supernatant, decompression removal under the conditions of water bath with thermostatic control has
Machine solvent, obtains essential oil.
Embodiment 2
A kind of method that lemon-grass extracts essential oil, comprises the following steps:
(1) pluck fresh lemon-grass, in lemon-grass: the part by weight of sodium chloride is 1: 0.34 ratio mixing, and mixing is all
Place 60 hours after even, and repeatedly stirred mixing, then by lemon-grass: the ratio for 1: 3.5 for the part by weight of distilled water adds
After water mixing, it is broken into lemon-grass slurries；
(2) extract: add the rosemary of lemon-grass weight 1-3%, 3% 60 degree of benzins in lemon-grass slurries, adopt
With ultrasonic extraction 30 minutes, extract and filtered after terminating, collect filtrate, in filter residue, add the second that mass concentration is 80-90%
Alcoholic solution, repeats above-mentioned ultrasonic extraction and filter operation twice, merges all filtrates；
(3) mixed liquor of filtrate is carried out with centrifuge separating, take supernatant, decompression removal under the conditions of water bath with thermostatic control has
Machine solvent, obtains essential oil.
Claims (2)
1. a kind of lemon-grass extract essential oil method it is characterised in that: comprise the following steps:
(1) pluck fresh lemon-grass, in lemon-grass: the part by weight of sodium chloride is the ratio mixing of 1:0.23-0.34, and mixing is all
Place 60-100 hour after even, and repeatedly stirred mixing, then press lemon-grass: the part by weight of distilled water is 1:2-3.5
Ratio add water mixing after, be broken into lemon-grass slurries；
(2) extract: add the rosemary of lemon-grass weight 1-3% in lemon-grass slurries, the extractant of 3-5%, using ultrasonic
Extract 30-50 minute, extract and filtered after terminating, collect filtrate, the ethanol adding mass concentration to be 80-90% in filter residue is molten
Liquid, repeats above-mentioned ultrasonic extraction and filter operation twice, merges all filtrates；
(3) mixed liquor of filtrate is carried out with centrifuge separating, take supernatant, decompression removal is organic molten under the conditions of water bath with thermostatic control
Agent, obtains essential oil.
2. a kind of lemon-grass according to claim 1 extract essential oil method it is characterised in that: described in step (2)
Extractant is 30-60 degree benzin.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610793295.1A CN106336950A (en) | 2016-08-31 | 2016-08-31 | Method for extracting essential oil from lemongrass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610793295.1A CN106336950A (en) | 2016-08-31 | 2016-08-31 | Method for extracting essential oil from lemongrass |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106336950A true CN106336950A (en) | 2017-01-18 |
Family
ID=57822951
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610793295.1A Pending CN106336950A (en) | 2016-08-31 | 2016-08-31 | Method for extracting essential oil from lemongrass |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106336950A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113951676A (en) * | 2021-09-27 | 2022-01-21 | 杭州顾家寝具有限公司 | Mattress capable of improving sleep |
| CN114381335A (en) * | 2022-01-19 | 2022-04-22 | 海南热带海洋学院 | Preparation method of lemongrass essential oil |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104789359A (en) * | 2015-04-15 | 2015-07-22 | 芜湖市丹洋现代农业科技发展有限公司 | Method for extracting essential oil from peony flowers |
| CN104928039A (en) * | 2015-05-30 | 2015-09-23 | 防城港市防城区那梭香料厂 | Preparation method for lemongrass essential oil |
-
2016
- 2016-08-31 CN CN201610793295.1A patent/CN106336950A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104789359A (en) * | 2015-04-15 | 2015-07-22 | 芜湖市丹洋现代农业科技发展有限公司 | Method for extracting essential oil from peony flowers |
| CN104928039A (en) * | 2015-05-30 | 2015-09-23 | 防城港市防城区那梭香料厂 | Preparation method for lemongrass essential oil |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113951676A (en) * | 2021-09-27 | 2022-01-21 | 杭州顾家寝具有限公司 | Mattress capable of improving sleep |
| CN114381335A (en) * | 2022-01-19 | 2022-04-22 | 海南热带海洋学院 | Preparation method of lemongrass essential oil |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| CB02 | Change of applicant information |
Address after: Fangcheng District Nasuo town Fangchenggang city the Guangxi Zhuang Autonomous Region 538000 to the summer village of Bayi group Applicant after: FANGCHENGGANG LVHUAYUAN AGRICULTURE AND FORESTRY SCIENCE AND TECHNOLOGY CO., LTD. Address before: 538000 the Guangxi Zhuang Autonomous Region, Fangchenggang port area Peach Peach Blossom Road, Hubei side of the new business incubator building, floor 3 Applicant before: FANGCHENGGANG LVHUAYUAN AGRICULTURE AND FORESTRY SCIENCE AND TECHNOLOGY CO., LTD. |
|
| COR | Change of bibliographic data | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170118 |