CN109006877A - The tickicide preparation and preparation method of one Plant Extracts - Google Patents
The tickicide preparation and preparation method of one Plant Extracts Download PDFInfo
- Publication number
- CN109006877A CN109006877A CN201811238913.1A CN201811238913A CN109006877A CN 109006877 A CN109006877 A CN 109006877A CN 201811238913 A CN201811238913 A CN 201811238913A CN 109006877 A CN109006877 A CN 109006877A
- Authority
- CN
- China
- Prior art keywords
- preparation
- parts
- weight
- tickicide
- hours
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/10—Apiaceae or Umbelliferae [Carrot family], e.g. parsley, caraway, dill, lovage, fennel or snakebed
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/38—Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention discloses a kind of preparation and preparation method for being used to kill tick for extracting active component from different plants and being mixed to form.The tickicide preparation of plant extracts of the invention is made of 10~40 parts of parts by weight of tobacco leaf and the ethanol extract of 10~40 parts of frutus cnidiis.Plant source tick-killing agent complicated component of the invention, can act on the multiple targets of insect pest, is not likely to produce drug resistance；And its active constituent is derived from naturally, nature can be environmental-friendly to its degradation rapidly.Preparation tickicide effect of the invention is obvious, is not likely to produce drug resistance, low in cost, drug residue free, free from environmental pollution to safety of human and livestock, insect pest.
Description
Technical field
The present invention relates to a kind of insecticide, what especially a kind of extraction active component from different plants was mixed to form is used for
Kill the preparation and preparation method of tick.
Background technique
Tick (Tick) is a kind of common epizoa, can be by biting the invasion mankind, mammal, birds, reptiles
And amphibian animal.The harm of tick, which directly translates into, is bitten animal anaemia, weight loss, appetite stimulator etc., while tick or a variety of
The communication media of disease is only second to mosquito class in the effect that certain disease of natural focus play in the groove.Tick and tick pass disease
(TTBD) serious financial consequences not only are caused to animal husbandry, returns human health and animal productiong brings threat, it has also become the whole world
The public health problem that medical field and animal doctor educational circles extraordinarily pay close attention to.It is always the main method of prevention and control tick using chemicals,
But chemicals are big to people and animals' toxicity, the drug residual period is long, cause great environmental pollution, and insect pest is also easy to produce drug resistance.Just
Therefore, there is now some chemicals to be forbidden to use by bright life, and other are then used by limitation.Simultaneously prepared by chemicals
In be also also easy to produce pollution.Have not yet to see the insecticide report for the dedicated non-heavy chemicals of tick evil.
Summary of the invention
The present invention provides a kind of plant source tick-killing agent being never re-dubbed with the active ingredient extracted in natural plants and system
Preparation Method.
The tickicide preparation of plant extracts of the invention is by 10~40 parts of parts by weight of tobacco leaf and 10~40 parts of frutus cnidiis
Ethanol extract constitute.
Preferably, the tickicide preparation of plant extracts of the invention is by the tobacco leaf of parts by weight 10 and 10~40 parts of frutus cnidiis
Ethanol extract is constituted.
The preparation method of the tickicide preparation of plant extracts of the invention is: weighed tobacco leaf and frutus cnidii are distinguished powder
Broken, 50 meshes excessively, use alcohol dipping 48 hours after then mixing, are then refluxed for extracting twice, 2 hours every time, merge after filtration
Extracting solution, then extracting solution is concentrated into 1g/mL.
It is the preparation method of the tickicide preparation of several preferable plant extracts of tickicide effect of the invention below:
First method is to weigh 10 parts by weight of tobacco leaf, 10 parts by weight of frutus cnidii, then crushes respectively, crosses 50 meshes, so
Alcohol dipping 48 hours that 100 parts by weight of parts by weight are used after mixing afterwards, are then refluxed for extracting twice, 2 hours every time, close after filtration
And extracting solution, then extracting solution is concentrated into 1g/mL.
Second method is to weigh 10 parts by weight of tobacco leaf, 20 parts by weight of frutus cnidii, then crushes respectively, crosses 50 meshes, so
Alcohol dipping 48 hours that 150 parts by weight of parts by weight are used after mixing afterwards, are then refluxed for extracting twice, 2 hours every time, close after filtration
And extracting solution, then extracting solution is concentrated into 1g/mL, obtain tickicide preparation.
The third method is to weigh 10 parts by weight of tobacco leaf, 40 parts by weight of frutus cnidii, then crushes respectively, crosses 50 meshes, so
Alcohol dipping 48 hours that 250 parts by weight of parts by weight are used after mixing afterwards, are then refluxed for extracting twice, 2 hours every time, close after filtration
And extracting solution, then extracting solution is concentrated into 1g/mL, obtain tickicide preparation.
Above-mentioned three kinds of preparation methods can prepare the preferable tickicide preparation of effect respectively.
Plant source tick-killing agent complicated component of the invention, can act on the multiple targets of insect pest, is not likely to produce drug resistance；And
Its active constituent is derived from naturally, nature can be environmental-friendly to its degradation rapidly.Preparation tickicide effect of the invention is obvious, right
Safety of human and livestock, insect pest are not likely to produce drug resistance, low in cost, drug residue free, free from environmental pollution.
Specific embodiment
Below with reference to preparation and the embodiment detected, the present invention is further illustrated, and part as described below refers to weight
Part.
One, embodiment is prepared
Embodiment 1:
It weighs respectively: 10 parts of tobacco leaf, 10 parts of frutus cnidii, 100 parts of ethyl alcohol
The preparation method comprises the following steps:
Step 1: 10 parts of tobacco leaf, 10 parts of frutus cnidii crushing (crossing 50 meshes) are weighed, is mixed；
Step 2: 100 parts of ethyl alcohol, which are added, makes drug complete wetting, and room temperature immersion 48 hours；
Step 3: refluxing extraction twice, 2 hours every time, filters；
Step 4: combined extract is concentrated into 1g/mL up to plant insecticide.
Embodiment 2:
It weighs respectively: 10 parts of tobacco leaf, 20 parts of frutus cnidii, 150 parts of ethyl alcohol；
The preparation method comprises the following steps:
Step 1: 10 parts of tobacco leaf, 20 parts of frutus cnidii crushing (crossing 50 meshes) are weighed, is mixed；
Step 2: ethyl alcohol, which is added, makes drug complete wetting, and room temperature immersion 48 hours；
Step 3: refluxing extraction twice, 2 hours every time, filters；
Step 4: combined extract is concentrated into 1g/mL up to plant insecticide.
Embodiment 3:
It weighs respectively: 20 parts of tobacco leaf, 10 parts of frutus cnidii, 150 parts of ethyl alcohol；
The preparation method comprises the following steps:
Step 1: 20 parts of tobacco leaf, 10 parts of frutus cnidii crushing (crossing 50 meshes) are weighed, is mixed；
Step 2: ethyl alcohol, which is added, makes drug complete wetting, and room temperature immersion 48 hours；
Step 3: refluxing extraction twice, 2 hours every time, filters；
Step 4: combined extract is concentrated into 1g/mL up to plant insecticide.
Embodiment 4:
It weighs respectively: 10 parts of tobacco leaf, 30 parts of frutus cnidii, 200 parts of ethyl alcohol；
The preparation method comprises the following steps:
Step 1: 10 parts of tobacco leaf, 30 parts of frutus cnidii crushing (crossing 50 meshes) are weighed, is mixed；
Step 2: ethyl alcohol, which is added, makes drug complete wetting, and room temperature immersion 48 hours；
Step 3: refluxing extraction twice, 2 hours every time, filters；
Step 4: combined extract is concentrated into 1g/mL up to plant insecticide.
Embodiment 5:
It weighs respectively: 30 parts of tobacco leaf, 10 parts of frutus cnidii, 200 parts of ethyl alcohol；
The preparation method comprises the following steps:
Step 1: 30 parts of tobacco leaf, 10 parts of frutus cnidii crushing (crossing 50 meshes) are weighed, is mixed；
Step 2: ethyl alcohol, which is added, makes drug complete wetting, and room temperature immersion 48 hours；
Step 3: refluxing extraction twice, 2 hours every time, filters；
Step 4: combined extract is concentrated into 1g/mL up to plant insecticide.
Embodiment 6:
It weighs respectively: 10 parts of tobacco leaf, 40 parts of frutus cnidii, 250 parts of ethyl alcohol；
Preparation method:
Step 1: 10 parts of tobacco leaf, 10 parts of frutus cnidii crushing (crossing 50 meshes) are weighed, is mixed；
Step 2: ethyl alcohol, which is added, makes drug complete wetting, and room temperature immersion 48 hours；
Step 3: refluxing extraction twice, 2 hours every time, filters；
Step 4: combined extract is concentrated into 1g/mL up to plant insecticide.
Embodiment 7:
It weighs respectively: 40 parts of tobacco leaf, 10 parts of frutus cnidii, 250 parts of ethyl alcohol；
The preparation method comprises the following steps:
Step 1: 40 parts of tobacco leaf, 10 parts of frutus cnidii crushing (crossing 50 meshes) are weighed, is mixed；
Step 2: ethyl alcohol, which is added, makes drug complete wetting, and room temperature immersion 48 hours；
Step 3: refluxing extraction twice, 2 hours every time, filters；
Step 4: combined extract is concentrated into 1g/mL up to plant insecticide.
Two, tickicide is tested:
The embodiment of the present invention uses indoor toxicity test, and when test presses the 1:1 of drug in prescription respectively；1:2；1:3；1:4；
2:1；2:1；3:1；4:1 is divided into 7 groups.If brown dog tick blood tick of satisfying is randomly divided into 3 groups (every group 10), using external leaching
Every group of tick is immersed respectively and impregnates 5min in different pharmaceutical by stain method, and the medical fluid on tick surface is then blotted with filter paper, is transferred to glass
It in glass pipe, is tightened, is placed under conditions of 28 DEG C, relative humidity 85%, each processing with rubber glue after encasing both ends with woven fabric
If three repetitions, the tick to distill water process and not do any processing observes and records result as control daily.
The experimental result of 1 embodiment 1-7 of table
Three, comparative test:
1. the preparation method comprises the following steps:
Step 1: 10 parts of tobacco leaf, 10 parts of frutus cnidii crushing (crossing 50 meshes) are weighed respectively, is mixed；
Step 2: being separately added into ethyl alcohol makes drug complete wetting, and room temperature immersion 48 hours；
Step 3: refluxing extraction twice, 2 hours every time, filters respectively；
Step 4: it is concentrated into 1g/mL respectively to obtain the final product.
2. tickicide is tested:
Ibid
2 contrast and experiment of table
From Table 1 and Table 2, compound preparation effect of the invention is far superior to single extract.
Claims (7)
1. the tickicide preparation of a Plant Extracts, it is characterized in that tobacco leaf and 10~40 of the tickicide preparation by 10~40 parts of parts by weight
Part frutus cnidii ethanol extract is constituted.
2. the tickicide preparation of plant extracts according to claim 1, it is characterized in that tickicide preparation is by parts by weight parts by weight
10~30 tobacco leaf and 10~40 parts of frutus cnidii ethanol extracts are constituted.
3. the preparation method of the tickicide preparation of plant extracts of any of claims 1 or 2, it is characterized in that by weighed tobacco leaf and
Frutus cnidii crushes respectively, crosses 50 meshes, uses alcohol dipping 48 hours after then mixing, is then refluxed for extracting twice, 2 is small every time
When, combined extract after filtration, then extracting solution is concentrated into 1g/mL.
4. the preparation method of the tickicide preparation of plant extracts according to claim 3, it is characterized in that weighing 10 weight of tobacco leaf
Part, 30 parts by weight of frutus cnidii are measured, then crushes respectively, cross 50 meshes, soaked after then mixing with the ethyl alcohol of 100 parts by weight of parts by weight
It stain 48 hours, is then refluxed for extracting twice, 2 hours every time, combined extract after filtration, then extracting solution is concentrated into 1g/mL.
5. the preparation method of the tickicide preparation of plant extracts according to claim 3, it is characterized in that weighing 30 weight of tobacco leaf
Part, 10 parts by weight of frutus cnidii are measured, then crushes respectively, cross 50 meshes, soaked after then mixing with the ethyl alcohol of 150 parts by weight of parts by weight
It stain 48 hours, is then refluxed for extracting twice, 2 hours every time, combined extract after filtration, then extracting solution is concentrated into 1g/mL.
6. the preparation method of the tickicide preparation of plant extracts according to claim 3, it is characterized in that weighing 10 weight of tobacco leaf
Part, 40 parts by weight of frutus cnidii are measured, then crushes respectively, cross 50 meshes, soaked after then mixing with the ethyl alcohol of 250 parts by weight of parts by weight
It stain 48 hours, is then refluxed for extracting twice, 2 hours every time, combined extract after filtration, then extracting solution is concentrated into 1g/mL.
7. tickicide preparation prepared by the preparation method of the tickicide preparation of plant extracts described in claim 3 or 4 or 5 or 6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811238913.1A CN109006877A (en) | 2018-10-23 | 2018-10-23 | The tickicide preparation and preparation method of one Plant Extracts |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811238913.1A CN109006877A (en) | 2018-10-23 | 2018-10-23 | The tickicide preparation and preparation method of one Plant Extracts |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109006877A true CN109006877A (en) | 2018-12-18 |
Family
ID=64613915
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811238913.1A Withdrawn CN109006877A (en) | 2018-10-23 | 2018-10-23 | The tickicide preparation and preparation method of one Plant Extracts |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109006877A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110314191A (en) * | 2019-07-31 | 2019-10-11 | 青海省动物疫病预防控制中心 | A kind of method that Chinese medicine composition combination ultrasonic wave kills tick worm |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1179887A (en) * | 1997-02-18 | 1998-04-29 | 山东农业大学 | Extraction of tobacco extract and its composition |
| CN101564519A (en) * | 2009-06-05 | 2009-10-28 | 中国人民解放军军事医学科学院军事兽医研究所 | External medicine for treating parasitic infection, fungal infection and bacterial infection of pets and preparation method thereof |
| CN106490053A (en) * | 2016-09-26 | 2017-03-15 | 塔里木大学 | A kind of Tickss worm repellant medicament and preparation method thereof |
-
2018
- 2018-10-23 CN CN201811238913.1A patent/CN109006877A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1179887A (en) * | 1997-02-18 | 1998-04-29 | 山东农业大学 | Extraction of tobacco extract and its composition |
| CN101564519A (en) * | 2009-06-05 | 2009-10-28 | 中国人民解放军军事医学科学院军事兽医研究所 | External medicine for treating parasitic infection, fungal infection and bacterial infection of pets and preparation method thereof |
| CN106490053A (en) * | 2016-09-26 | 2017-03-15 | 塔里木大学 | A kind of Tickss worm repellant medicament and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110314191A (en) * | 2019-07-31 | 2019-10-11 | 青海省动物疫病预防控制中心 | A kind of method that Chinese medicine composition combination ultrasonic wave kills tick worm |
| CN110314191B (en) * | 2019-07-31 | 2021-09-03 | 青海省动物疫病预防控制中心 | Method for repelling and killing ticks by combining traditional Chinese medicine composition with ultrasonic waves |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109006877A (en) | The tickicide preparation and preparation method of one Plant Extracts | |
| CN104705349B (en) | The preparation at white lotus parthenium extract different activities position and its application as acaricidal activity material | |
| CN106386885A (en) | Preparation process of mandarin orange peel composite plant agricultural insecticide | |
| CN100553459C (en) | A kind of pokeberry extract and new purposes thereof | |
| CN100569077C (en) | A kind of mixed pesticide of radix euphorbiae lantu chromocor and preparation method thereof | |
| CN109122739A (en) | A kind of plant source tickicide preparation and preparation method | |
| CN107889857A (en) | A kind of preparation method for killing thrips pharmaceutical composition | |
| CN110338196A (en) | A kind of compound botanical preparation for killing tick | |
| CN103315008B (en) | Preparation method of Suaeda salsa used as agricultural pesticide and application | |
| CN107668092A (en) | A kind of pharmaceutical composition used for beetle | |
| CN107320671B (en) | Insecticidal traditional Chinese medicine composition and preparation method thereof | |
| CN107873752A (en) | A kind of preparation method for killing diamondback moth pharmaceutical composition | |
| CN107889847A (en) | A kind of preparation method for killing wheat aphid pharmaceutical composition | |
| CN107751259A (en) | A kind of preparation method of the quick-acting pharmaceutical compositions for killing heart-eating worm | |
| CN107624828A (en) | A kind of preparation method for killing bollworm pharmaceutical composition | |
| CN107889856A (en) | A kind of preparation method for killing trialeurodes vaporariorum pharmaceutical composition | |
| CN107691495A (en) | A kind of preparation method for killing suction pulp worm pharmaceutical composition | |
| CN107668087A (en) | A kind of potent preparation method for killing chafer pharmaceutical composition | |
| CN107889858A (en) | A kind of mole cricket killing agent preparation method for being not likely to produce drug resistance | |
| CN107810988A (en) | A kind of preparation method for killing aphid pharmaceutical composition | |
| CN107711908A (en) | A kind of fore-telling mud killing agent preparation method suitable for mass production | |
| CN107668084A (en) | A kind of pharmaceutical composition for killing prodenia litura | |
| CN107889849A (en) | A kind of preparation method of the pear sucker killing agent of good penetrability | |
| CN103749565A (en) | Nuisance-free botanical pesticide and preparation method thereof | |
| CN101584348A (en) | A kind of inula flower extractive and its production and use |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20181218 |
|
| WW01 | Invention patent application withdrawn after publication |