CN108978280A - A kind of dyeing for the terylene ribbon that color fastness is high - Google Patents
A kind of dyeing for the terylene ribbon that color fastness is high Download PDFInfo
- Publication number
- CN108978280A CN108978280A CN201810773029.1A CN201810773029A CN108978280A CN 108978280 A CN108978280 A CN 108978280A CN 201810773029 A CN201810773029 A CN 201810773029A CN 108978280 A CN108978280 A CN 108978280A
- Authority
- CN
- China
- Prior art keywords
- dyeing
- ribbon
- color fastness
- terylene ribbon
- terylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000005020 polyethylene terephthalate Substances 0.000 title claims abstract description 78
- 238000004043 dyeing Methods 0.000 title claims abstract description 62
- 229920004933 Terylene® Polymers 0.000 title claims abstract description 55
- 239000000975 dye Substances 0.000 claims abstract description 34
- 241000207929 Scutellaria Species 0.000 claims abstract description 31
- 229920004934 Dacron® Polymers 0.000 claims abstract description 23
- 238000012545 processing Methods 0.000 claims abstract description 7
- 238000009423 ventilation Methods 0.000 claims abstract description 6
- 230000004048 modification Effects 0.000 claims abstract description 4
- 238000012986 modification Methods 0.000 claims abstract description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical group O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 15
- 238000002156 mixing Methods 0.000 claims description 13
- 238000002360 preparation method Methods 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 229920005610 lignin Polymers 0.000 claims description 12
- 239000008367 deionised water Substances 0.000 claims description 10
- 229910021641 deionized water Inorganic materials 0.000 claims description 10
- 150000007524 organic acids Chemical class 0.000 claims description 10
- 239000003431 cross linking reagent Substances 0.000 claims description 9
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 5
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 5
- 239000011976 maleic acid Substances 0.000 claims description 5
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 5
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical group [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 238000004132 cross linking Methods 0.000 claims 1
- 239000000706 filtrate Substances 0.000 claims 1
- 230000010148 water-pollination Effects 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 9
- 230000000694 effects Effects 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 229930182559 Natural dye Natural products 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 239000012530 fluid Substances 0.000 description 4
- 239000000978 natural dye Substances 0.000 description 4
- 230000008569 process Effects 0.000 description 3
- 229920000728 polyester Polymers 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- IPQKDIRUZHOIOM-UHFFFAOYSA-N Oroxin A Natural products OC1C(O)C(O)C(CO)OC1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 IPQKDIRUZHOIOM-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- IKIIZLYTISPENI-ZFORQUDYSA-N baicalin Chemical compound O1[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 IKIIZLYTISPENI-ZFORQUDYSA-N 0.000 description 1
- 229960003321 baicalin Drugs 0.000 description 1
- AQHDANHUMGXSJZ-UHFFFAOYSA-N baicalin Natural products OC1C(O)C(C(O)CO)OC1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 AQHDANHUMGXSJZ-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 239000002352 surface water Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/12—Aldehydes; Ketones
- D06M13/127—Mono-aldehydes, e.g. formaldehyde; Monoketones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/203—Unsaturated carboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The invention discloses a kind of dyeings of terylene ribbon that color fastness is high, are related to technical field of biological environmental protection, are modified processing to terylene ribbon, modified dacron ribbon is obtained, modified dacron ribbon is dyed using scutellaria dyestuff, is then taken out, it dries ventilation；Modification by the present invention to terylene, hydrophily are greatly improved, and the compatibility on surface is significantly improved, and terylene ribbon can be promoted to combine with scutellaria dyestuff, to improve dyefastness.
Description
Technical field
The invention belongs to technical field of biological environmental protection, and in particular to a kind of dyeing for the terylene ribbon that color fastness is high.
Background technique
Ribbon is to be widely used in dress ornament, shoes using various yarns as narrow web fabric or tubing made of raw material
Material, luggage, industry, agricultural, military supplies, communications and transportation Deng Ge branch of industry, the protection safety band, mountain-climbing knapsack of camping of being climbed the mountain with production
Band, tent, sports bag, fitness equipment, traction rope, security against fire band, parachute safety belt.Natural dye is since it is naturally without dirt
Metachromia and the strong effect of special functionality, are suitably applied the green product of exploitation high added value, radix scutellariae belongs to yellow class, flavones
Class natural dye, but existing method preparation radix scutellariae natural dye it is general to the dyeing effect of terylene ribbon, dyefastness compared with
It is low.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of dyeing of terylene ribbon that color fastness is high is provided.
The present invention is achieved by the following technical solutions:
A kind of dyeing for the terylene ribbon that color fastness is high, is modified processing to terylene ribbon, obtains modified dacron ribbon,
Modified dacron ribbon is dyed using scutellaria dyestuff, is then taken out, ventilation is dried.
Further, the modified dacron ribbon is the preparation method comprises the following steps: press 100-120g for terylene ribbon and deionized water:
The ratio of 400mL mixes, and is heated to 65 DEG C, then the lignin for then adding terylene ribbon quality 10% adds after mixing evenly
Add the organic acid of the quality such as lignin, after mixing evenly, adjust the temperature to 80 DEG C, with 120r/min revolving speed stirring 1 hour, then
Add the crosslinking agent of lignin quality 0.15% again, continue insulated and stirred 2 hours, then filter, using deionized water to filtering after
Terylene ribbon clean to neutrality, drying to constant weight to get modified dacron ribbon.
Further, the crosslinking agent is formaldehyde.
Further, the organic acid is maleic acid.
Further, the scutellaria dyestuff obtains scutellaria powder the preparation method comprises the following steps: radix scutellariae is crushed to 120 meshes, will be yellow
The mass concentration that Cen Fenmo is added to 10 times of its quality is to be forced into 1.2- in the aqueous solution of boride of 0.2-0.5%
1.5MPa is kept for 2-3 hours, then carries out pressure release, vacuumize, and is heated to 100 DEG C, is kept for 1.5 hours, is then filtered,
Extraction 2 times is repeated to filter residue, merges 3 filtered fluids to get scutellaria dyestuff.
Further, the boride is zinc borate.
Further, described vacuumize to be evacuated to vacuum degree is 0.01-0.03MPa.
Further, the bath raio of the dyeing is 1:20.
Further, the time of the dyeing is 50min.
Further, the temperature of the dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, dyes back segment 20min
In dyeing temperature be 75 DEG C.
The present invention has the advantage that the modification by the present invention to terylene compared with prior art, and hydrophily obtains
Greatly improve, the compatibility on surface is significantly improved, and terylene ribbon can be promoted to combine with scutellaria dyestuff, to mention
High dyefastness, by the modification to terylene ribbon, most importantly so that terylene ribbon surface water contact angle obtain it is bright
It is aobvious to reduce, so that the hydrophily of dacron significantly improves；The present invention is when preparing terylene ribbon dyestuff, with radix scutellariae
In the pigment that contains as natural dye, radix scutellariae itself is nontoxic, harmless, has certain health-care effect to human body, as washing
There is the dye component of synthetic fibre ribbon preferable profit to contaminate effect, obtained terylene ribbon soft comfortable, the Huang of terylene ribbon of the present invention
Cen dyeing, the scutellaria dyestuff of use may be reused repeatedly, can meet water-saving, energy saving, emission reduction national industry political affairs
Plan；The scutellaria dyestuff prepared in through the invention, the baicalin contained can not only be faster under the action of boride
It is extracted from scutellaria, while can be easier to combine with terylene woven fabric, dye aberration is small, and color fastness is high, upper dye percentage
Rate is high, greatly reduces the loss of the energy, reduces the use condition and dyeing cost of dyeing installation.
Specific embodiment
Embodiment 1
A kind of dyeing for the terylene ribbon that color fastness is high, is modified processing to terylene ribbon, obtains modified dacron ribbon,
Modified dacron ribbon is dyed using scutellaria dyestuff, is then taken out, ventilation is dried.
Further, the modified dacron ribbon is the preparation method comprises the following steps: press 100g:400mL for terylene ribbon and deionized water
Ratio mixing, be heated to 65 DEG C, then add terylene ribbon quality 10% lignin then add wooden after mixing evenly
The organic acid of the quality such as element adjusts the temperature to 80 DEG C after mixing evenly, with 120r/min revolving speed stirring 1 hour, then adds again
The crosslinking agent of lignin quality 0.15% continues insulated and stirred 2 hours, then filters, using deionized water to filtered terylene
Ribbon is cleaned to neutrality, and drying to constant weight to get modified dacron ribbon.
Further, the crosslinking agent is formaldehyde.
Further, the organic acid is maleic acid.
Further, the scutellaria dyestuff obtains scutellaria powder the preparation method comprises the following steps: radix scutellariae is crushed to 120 meshes, will be yellow
Cen Fenmo is added in the aqueous solution for the boride that the mass concentration of 10 times of its quality is 0.2%, is forced into 1.2MPa, keeps 2
Hour, pressure release is then carried out, is vacuumized, is heated to 100 DEG C, is kept for 1.5 hours, is then filtered, filter residue is repeated and is mentioned
It takes 2 times, merges 3 filtered fluids to get scutellaria dyestuff.
Further, the boride is zinc borate.
Further, described vacuumize to be evacuated to vacuum degree is 0.01MPa.
Further, the bath raio of the dyeing is 1:20.
Further, the time of the dyeing is 50min.
Further, the temperature of the dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, dyes back segment 20min
In dyeing temperature be 75 DEG C.
Embodiment 2
A kind of dyeing for the terylene ribbon that color fastness is high, is modified processing to terylene ribbon, obtains modified dacron ribbon,
Modified dacron ribbon is dyed using scutellaria dyestuff, is then taken out, ventilation is dried.
Further, the modified dacron ribbon is the preparation method comprises the following steps: press 120g:400mL for terylene ribbon and deionized water
Ratio mixing, be heated to 65 DEG C, then add terylene ribbon quality 10% lignin then add wooden after mixing evenly
The organic acid of the quality such as element adjusts the temperature to 80 DEG C after mixing evenly, with 120r/min revolving speed stirring 1 hour, then adds again
The crosslinking agent of lignin quality 0.15% continues insulated and stirred 2 hours, then filters, using deionized water to filtered terylene
Ribbon is cleaned to neutrality, and drying to constant weight to get modified dacron ribbon.
Further, the crosslinking agent is formaldehyde.
Further, the organic acid is maleic acid.
Further, the scutellaria dyestuff obtains scutellaria powder the preparation method comprises the following steps: radix scutellariae is crushed to 120 meshes, will be yellow
Cen Fenmo is added in the aqueous solution for the boride that the mass concentration of 10 times of its quality is 0.5%, is forced into 1.5MPa, keeps 3
Hour, pressure release is then carried out, is vacuumized, is heated to 100 DEG C, is kept for 1.5 hours, is then filtered, filter residue is repeated and is mentioned
It takes 2 times, merges 3 filtered fluids to get scutellaria dyestuff.
Further, the boride is zinc borate.
Further, described vacuumize to be evacuated to vacuum degree is 0.03MPa.
Further, the bath raio of the dyeing is 1:20.
Further, the time of the dyeing is 50min.
Further, the temperature of the dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, dyes back segment 20min
In dyeing temperature be 75 DEG C.
Embodiment 3
A kind of dyeing for the terylene ribbon that color fastness is high, is modified processing to terylene ribbon, obtains modified dacron ribbon,
Modified dacron ribbon is dyed using scutellaria dyestuff, is then taken out, ventilation is dried.
Further, the modified dacron ribbon is the preparation method comprises the following steps: press 110g:400mL for terylene ribbon and deionized water
Ratio mixing, be heated to 65 DEG C, then add terylene ribbon quality 10% lignin then add wooden after mixing evenly
The organic acid of the quality such as element adjusts the temperature to 80 DEG C after mixing evenly, with 120r/min revolving speed stirring 1 hour, then adds again
The crosslinking agent of lignin quality 0.15% continues insulated and stirred 2 hours, then filters, using deionized water to filtered terylene
Ribbon is cleaned to neutrality, and drying to constant weight to get modified dacron ribbon.
Further, the crosslinking agent is formaldehyde.
Further, the organic acid is maleic acid.
Further, the scutellaria dyestuff obtains scutellaria powder the preparation method comprises the following steps: radix scutellariae is crushed to 120 meshes, will be yellow
Cen Fenmo is added in the aqueous solution for the boride that the mass concentration of 10 times of its quality is 0.3%, is forced into 1.3MPa, keeps
2.3 hours, pressure release is then carried out, is vacuumized, be heated to 100 DEG C, kept for 1.5 hours, be then filtered, filter residue is repeated
It extracts 2 times, merges 3 filtered fluids to get scutellaria dyestuff.
Further, the boride is zinc borate.
Further, described vacuumize to be evacuated to vacuum degree is 0.02MPa.
Further, the bath raio of the dyeing is 1:20.
Further, the time of the dyeing is 50min.
Further, the temperature of the dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, dyes back segment 20min
In dyeing temperature be 75 DEG C.
Comparative example 1: it is distinguished with embodiment 1 and is only that the aqueous solution by boride in the preparation of scutellaria dyestuff replaces with clear water.
Comparative example 2: it is only that in the preparation of scutellaria dyestuff with the difference of embodiment 1 without vacuumize process.
Comparative example 3: it is only that scutellaria dyestuff merges to obtain using 100 DEG C of hot water 3 times extractions with the difference of embodiment 1, scutellaria
It is 1:10 with hot water quality's ratio.
Comparative example 7: it is only that not with the difference of embodiment 1 to polyester modified processing.
Comparative example 7: it is only that polyester modified processing method replaces with application number with the difference of embodiment 1:
201711136852.3
Test
Embodiment and same batch of terylene ribbon of comparative example dyeing are detected:
Colour fastness to rubbing is measured according to GB/T 3920-2008 " textile color stability test colour fastness to rubbing ";Washable color
Fastness is measured according to GB/T 3921-2008 " textile color stability test fastness to soaping ".3 kinds of assessments of fastness make
It is evaluated with " evaluation discoloration gray scale " (GB/T 250-2008)；
Table 1
As can be seen from Table 1, there is good fade resistant effect and dry fastness after present invention process dyes terylene ribbon；
Table 2
As can be seen from Table 2, there is good resistance to staining effect and fastness to wet rubbing after present invention process dyes terylene ribbon.
By taking embodiment 1 as an example, dacron dyeing percentage is compared for different dyeing temperatures:
Comparative example 4: it is only that dyeing temperature is fixed as 82 DEG C with the difference of embodiment 1.
Comparative example 5: it is only that dyeing temperature is fixed as 75 DEG C with the difference of embodiment 1.
Comparative example 6: it is only that dyeing temperature is fixed as 90 DEG C with the difference of embodiment 1.
Table 3
As can be seen from Table 3, upper dye can effectively be improved by the dyeing temperature that adjusts corresponding in dyeing course in the present invention
Percentage.
Claims (10)
1. a kind of dyeing for the terylene ribbon that color fastness is high, which is characterized in that be modified processing to terylene ribbon, obtain
Modified dacron ribbon is dyed using scutellaria dyestuff, is then taken out, ventilation is dried by modified dacron ribbon.
2. a kind of dyeing of the high terylene ribbon of color fastness according to claim 1, which is characterized in that the modification
Terylene ribbon is heated to 65 DEG C the preparation method comprises the following steps: by terylene ribbon and deionized water in the ratio mixing of 100-120g:400mL,
Then the lignin of terylene ribbon quality 10% is added, after mixing evenly, then adds the organic acid of the quality such as lignin, stirring
After uniformly, 80 DEG C are adjusted the temperature to, with 120r/min revolving speed stirring 1 hour, then adds the crosslinking of lignin quality 0.15% again
Agent is continued insulated and stirred 2 hours, then filters, cleaned filtered terylene ribbon to neutrality using deionized water, be dried to
Constant weight is to get modified dacron ribbon.
3. a kind of dyeing of the high terylene ribbon of color fastness according to claim 1, which is characterized in that the crosslinking
Agent is formaldehyde.
4. a kind of dyeing of the high terylene ribbon of color fastness according to claim 1, which is characterized in that described organic
Acid is maleic acid.
5. a kind of dyeing of the high terylene ribbon of color fastness according to claim 1, which is characterized in that the scutellaria
Dyestuff obtains scutellaria powder, scutellaria powder is added to 10 times of its quality the preparation method comprises the following steps: radix scutellariae is crushed to 120 meshes
Mass concentration is to be forced into 1.2-1.5MPa in the aqueous solution of the boride of 0.2-0.5%, is kept for 2-3 hours, is then let out
Pressure, vacuumizes, and is heated to 100 DEG C, is kept for 1.5 hours, is then filtered, and repeats extraction 2 times to filter residue, merges 3 mistakes
Filtrate is to get scutellaria dyestuff.
6. a kind of dyeing of the high terylene ribbon of color fastness according to claim 5, which is characterized in that the boronation
Object is zinc borate.
7. a kind of dyeing of the high terylene ribbon of color fastness according to claim 5, which is characterized in that described to take out very
Sky is 0.01-0.03MPa to be evacuated to vacuum degree.
8. a kind of dyeing of the high terylene ribbon of color fastness according to claim 1, which is characterized in that the dyeing
Bath raio be 1:20.
9. a kind of dyeing of the high terylene ribbon of color fastness according to claim 1, which is characterized in that the dyeing
Time be 50min.
10. a kind of dyeing of the high terylene ribbon of color fastness according to claim 1 or claim 7, which is characterized in that described
The temperature of dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, and dyeing dyeing temperature in back segment 20min is 75 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810773029.1A CN108978280A (en) | 2018-07-14 | 2018-07-14 | A kind of dyeing for the terylene ribbon that color fastness is high |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810773029.1A CN108978280A (en) | 2018-07-14 | 2018-07-14 | A kind of dyeing for the terylene ribbon that color fastness is high |
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| Publication Number | Publication Date |
|---|---|
| CN108978280A true CN108978280A (en) | 2018-12-11 |
Family
ID=64548951
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810773029.1A Pending CN108978280A (en) | 2018-07-14 | 2018-07-14 | A kind of dyeing for the terylene ribbon that color fastness is high |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20050048299A (en) * | 2003-11-19 | 2005-05-24 | 대한민국(광주.전남지방중소기업청) | Dye having antivirus efficacy and dyeing tissue thereof |
| CN101955692A (en) * | 2010-08-10 | 2011-01-26 | 浙江理工大学 | Method for preparing pulpy disperse dye for low-temperature dyeing of terylene |
| CN103668829A (en) * | 2013-06-13 | 2014-03-26 | 盐城工业职业技术学院 | Continuous hot melting dyeing technology for polyester fiber fabric |
| CN104784254A (en) * | 2015-04-03 | 2015-07-22 | 宝鸡市虹源生物科技有限公司 | Extraction method for producing baicalin with biological enzyme method |
| CN106758380A (en) * | 2016-12-21 | 2017-05-31 | 嘉兴富胜达染整有限公司 | A kind of dyeing and printing process of dacron cotton yarn weaved fabric |
| CN108086025A (en) * | 2017-12-21 | 2018-05-29 | 嘉兴学院 | New terylene Glove suede fabric dyeing process and application |
-
2018
- 2018-07-14 CN CN201810773029.1A patent/CN108978280A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20050048299A (en) * | 2003-11-19 | 2005-05-24 | 대한민국(광주.전남지방중소기업청) | Dye having antivirus efficacy and dyeing tissue thereof |
| CN101955692A (en) * | 2010-08-10 | 2011-01-26 | 浙江理工大学 | Method for preparing pulpy disperse dye for low-temperature dyeing of terylene |
| CN103668829A (en) * | 2013-06-13 | 2014-03-26 | 盐城工业职业技术学院 | Continuous hot melting dyeing technology for polyester fiber fabric |
| CN104784254A (en) * | 2015-04-03 | 2015-07-22 | 宝鸡市虹源生物科技有限公司 | Extraction method for producing baicalin with biological enzyme method |
| CN106758380A (en) * | 2016-12-21 | 2017-05-31 | 嘉兴富胜达染整有限公司 | A kind of dyeing and printing process of dacron cotton yarn weaved fabric |
| CN108086025A (en) * | 2017-12-21 | 2018-05-29 | 嘉兴学院 | New terylene Glove suede fabric dyeing process and application |
Non-Patent Citations (6)
| Title |
|---|
| 上海市纺织工业局: "《染料应用手册 第五分册 分散染料》", 30 June 1985, 纺织工业出版社 * |
| 周蓉，聂建斌: "《纺织品设计》", 31 May 2011, 东华大学出版社 * |
| 平郑骅，汪长春: "《高分子世界》", 31 May 2001, 复旦大学出版社 * |
| 盛连波: "涤纶染色与分散均染剂研究", 《中国优秀硕士学位论文全文数据库》 * |
| 詹益兴: "《绿色精细化工 天然产品制造法 第1集》", 31 May 2005, 科学技术文献出版社 * |
| 郜世博: "涤纶织物的黄芩染色", 《纺织学报》 * |
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