CN109235075A - A kind of scutellaria dyeing of terylene ribbon - Google Patents
A kind of scutellaria dyeing of terylene ribbon Download PDFInfo
- Publication number
- CN109235075A CN109235075A CN201810773030.4A CN201810773030A CN109235075A CN 109235075 A CN109235075 A CN 109235075A CN 201810773030 A CN201810773030 A CN 201810773030A CN 109235075 A CN109235075 A CN 109235075A
- Authority
- CN
- China
- Prior art keywords
- dyeing
- scutellaria
- terylene ribbon
- temperature
- terylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004043 dyeing Methods 0.000 title claims abstract description 61
- 241000207929 Scutellaria Species 0.000 title claims abstract description 43
- 239000005020 polyethylene terephthalate Substances 0.000 title claims abstract description 39
- 229920004933 Terylene® Polymers 0.000 title claims abstract description 38
- 239000000975 dye Substances 0.000 claims abstract description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 239000000843 powder Substances 0.000 claims description 10
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 5
- 238000011067 equilibration Methods 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 5
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical group [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 229910052796 boron Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 6
- 229930182559 Natural dye Natural products 0.000 abstract description 5
- 239000000978 natural dye Substances 0.000 abstract description 5
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 239000000049 pigment Substances 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 7
- 238000000034 method Methods 0.000 description 5
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical group [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 description 4
- 230000008569 process Effects 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 229920004934 Dacron® Polymers 0.000 description 1
- IPQKDIRUZHOIOM-UHFFFAOYSA-N Oroxin A Natural products OC1C(O)C(O)C(CO)OC1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 IPQKDIRUZHOIOM-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- IKIIZLYTISPENI-ZFORQUDYSA-N baicalin Chemical compound O1[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 IKIIZLYTISPENI-ZFORQUDYSA-N 0.000 description 1
- 229960003321 baicalin Drugs 0.000 description 1
- AQHDANHUMGXSJZ-UHFFFAOYSA-N baicalin Natural products OC1C(O)C(C(O)CO)OC1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 AQHDANHUMGXSJZ-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/20—Physical treatments affecting dyeing, e.g. ultrasonic or electric
- D06P5/2066—Thermic treatments of textile materials
- D06P5/2072—Thermic treatments of textile materials before dyeing
Abstract
The invention discloses a kind of scutellaria dyeings of terylene ribbon, are related to technical field of biological environmental protection, comprising the following steps: (1) radix scutellariae dyestuff；(2) steam treatment；(3) it dyes；For the present invention when preparing terylene ribbon dyestuff, for the pigment contained using in radix scutellariae as natural dye, radix scutellariae itself is nontoxic, harmless, there is certain health-care effect to human body, as the dye component of terylene ribbon, there is preferable profit to contaminate effect, obtained terylene ribbon soft comfortable.
Description
Technical field
The invention belongs to technical field of biological environmental protection, and in particular to a kind of scutellaria dyeing of terylene ribbon.
Background technique
Ribbon is to be widely used in dress ornament, shoes using various yarns as narrow web fabric or tubing made of raw material
Material, luggage, industry, agricultural, military supplies, communications and transportation Deng Ge branch of industry, the protection safety band, mountain-climbing knapsack of camping of being climbed the mountain with production
Band, tent, sports bag, fitness equipment, traction rope, security against fire band, parachute safety belt.Natural dye is since it is naturally without dirt
Metachromia and the strong effect of special functionality, are suitably applied the green product of exploitation high added value, radix scutellariae belongs to yellow class, flavones
Class natural dye, but existing method preparation radix scutellariae natural dye it is general to the dyeing effect of terylene ribbon, dyefastness compared with
It is low.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of scutellaria dyeing of terylene ribbon is provided.
The present invention is achieved by the following technical solutions:
A kind of scutellaria dyeing of terylene ribbon, comprising the following steps:
(1) radix scutellariae dyestuff: being crushed to 120 meshes for radix scutellariae, obtain scutellaria powder, and scutellaria powder is added to 10 times of its quality
Mass concentration be to be forced into 1.2-1.5MPa in the aqueous solution of boride of 0.2-0.5%, kept for 2-3 hours, then carried out
Pressure release vacuumizes, and is heated to 100 DEG C, is kept for 1.5 hours, is then filtered, and repeats extraction 2 times to filter residue, merges 3 times
Filtered fluid is to get scutellaria dyestuff；
(2) steam treatment: terylene ribbon is used into high-temperature steam suffocating treatment 40-45min, is then placed in water balance room
Carry out moisture equilibration 1 hour, then cooled to room temperature again；
(3) it dyes: treated terylene ribbon being put into scutellaria dyestuff obtained above and is dyed, after the completion
It takes out, is placed on ventilating and cooling place and dries.
Further, the boride is zinc borate.
Further, described vacuumize to be evacuated to vacuum degree is 0.01-0.03MPa.
Further, the high temperature steam temperature is 115 DEG C.
Further, the water balance room temperature is 60 DEG C, relative air humidity 70%.
Further, the bath raio of the dyeing is 1:20.
Further, the time of the dyeing is 50min.
Further, the temperature of the dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, dyes back segment 20min
In dyeing temperature be 75 DEG C.
The present invention has the advantage that the present invention when preparing terylene ribbon dyestuff compared with prior art, to contain in radix scutellariae
For some pigments as natural dye, radix scutellariae itself is nontoxic, harmless, has certain health-care effect to human body, knits as terylene
There is the dye component of band preferable profit to contaminate effect, obtained terylene ribbon soft comfortable, the scutellaria dye of terylene ribbon of the present invention
Color technique, the scutellaria dyestuff of use may be reused repeatedly, can meet water-saving, energy saving, emission reduction national industrial policies；It is logical
The scutellaria dyestuff prepared in the present invention is crossed, the baicalin contained can not only be faster from scutellaria under the action of boride
In extract, while can be easier to combine with terylene woven fabric, dye aberration is small, and color fastness is high, and dyeing percentage is high, pole
The big loss for reducing the energy reduces the use condition and dyeing cost of dyeing installation.
Specific embodiment
Embodiment 1
A kind of scutellaria dyeing of terylene ribbon, comprising the following steps:
(1) radix scutellariae dyestuff: being crushed to 120 meshes for radix scutellariae, obtain scutellaria powder, and scutellaria powder is added to 10 times of its quality
Mass concentration be 0.2% boride aqueous solution in, be forced into 1.2MPa, kept for 2 hours, then carry out pressure release, take out true
Sky is heated to 100 DEG C, is kept for 1.5 hours, is then filtered, and repeats extraction 2 times to filter residue, merges 3 filtered fluids, i.e.,
Obtain scutellaria dyestuff；
(2) steam treatment: terylene ribbon is used into high-temperature steam suffocating treatment 40min, is then placed in water balance room and carries out
Moisture equilibration 1 hour, then cooled to room temperature again；
(3) it dyes: treated terylene ribbon being put into scutellaria dyestuff obtained above and is dyed, after the completion
It takes out, is placed on ventilating and cooling place and dries.
Further, the boride is zinc borate.
Further, described vacuumize to be evacuated to vacuum degree is 0.01MPa.
Further, the high temperature steam temperature is 115 DEG C.
Further, the water balance room temperature is 60 DEG C, relative air humidity 70%.
Further, the bath raio of the dyeing is 1:20.
Further, the time of the dyeing is 50min.
Further, the temperature of the dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, dyes back segment 20min
In dyeing temperature be 75 DEG C.
Embodiment 2
A kind of scutellaria dyeing of terylene ribbon, comprising the following steps:
(1) radix scutellariae dyestuff: being crushed to 120 meshes for radix scutellariae, obtain scutellaria powder, and scutellaria powder is added to 10 times of its quality
Mass concentration be 0.5% boride aqueous solution in, be forced into 1.5MPa, kept for 2-3 hour, then carry out pressure release, pumping
Vacuum is heated to 100 DEG C, is kept for 1.5 hours, is then filtered, and repeats extraction 2 times to filter residue, merges 3 filtered fluids,
Up to scutellaria dyestuff；
(2) steam treatment: terylene ribbon is used into high-temperature steam suffocating treatment 45min, is then placed in water balance room and carries out
Moisture equilibration 1 hour, then cooled to room temperature again；
(3) it dyes: treated terylene ribbon being put into scutellaria dyestuff obtained above and is dyed, after the completion
It takes out, is placed on ventilating and cooling place and dries.
Further, the boride is zinc borate.
Further, described vacuumize to be evacuated to vacuum degree is 0.03MPa.
Further, the high temperature steam temperature is 115 DEG C.
Further, the water balance room temperature is 60 DEG C, relative air humidity 70%.
Further, the bath raio of the dyeing is 1:20.
Further, the time of the dyeing is 50min.
Further, the temperature of the dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, dyes back segment 20min
In dyeing temperature be 75 DEG C.
Embodiment 3
A kind of scutellaria dyeing of terylene ribbon, comprising the following steps:
(1) radix scutellariae dyestuff: being crushed to 120 meshes for radix scutellariae, obtain scutellaria powder, and scutellaria powder is added to 10 times of its quality
Mass concentration be 0.3% boride aqueous solution in, be forced into 1.4MPa, kept for 2.3 hours, then carry out pressure release, take out
Vacuum is heated to 100 DEG C, is kept for 1.5 hours, is then filtered, and repeats extraction 2 times to filter residue, merges 3 filtered fluids,
Up to scutellaria dyestuff；
(2) steam treatment: terylene ribbon is used into high-temperature steam suffocating treatment 42min, is then placed in water balance room and carries out
Moisture equilibration 1 hour, then cooled to room temperature again；
(3) it dyes: treated terylene ribbon being put into scutellaria dyestuff obtained above and is dyed, after the completion
It takes out, is placed on ventilating and cooling place and dries.
Further, the boride is zinc borate.
Further, described vacuumize to be evacuated to vacuum degree is 0.02MPa.
Further, the high temperature steam temperature is 115 DEG C.
Further, the water balance room temperature is 60 DEG C, relative air humidity 70%.
Further, the bath raio of the dyeing is 1:20.
Further, the time of the dyeing is 50min.
Further, the temperature of the dyeing is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, dyes back segment 20min
In dyeing temperature be 75 DEG C.
Comparative example 1: it is only that the aqueous solution of boride in step (1) replaces with clear water with the difference of embodiment 1.
Comparative example 2: it is only that in step (1) with the difference of embodiment 1 without vacuumize process.
Comparative example 3: it is only that scutellaria dyestuff merges to obtain using 100 DEG C of hot water 3 times extractions with the difference of embodiment 1, scutellaria
It is 1:10 with hot water quality's ratio.
Test
Embodiment and same batch of terylene ribbon of comparative example dyeing are detected:
Colour fastness to rubbing is measured according to GB/T 3920-2008 " textile color stability test colour fastness to rubbing ";Washable color
Fastness is measured according to GB/T 3921-2008 " textile color stability test fastness to soaping ".3 kinds of assessments of fastness make
It is evaluated with " evaluation discoloration gray scale " (GB/T 250-2008)；
Table 1
As can be seen from Table 1, for present invention process to having good dyefastness after the dyeing of terylene ribbon, especially washable color is firm
Degree and fastness to rubbing are excellent.
By taking embodiment 1 as an example, dacron dyeing percentage is compared for different dyeing temperatures:
Comparative example 4: it is only that dyeing temperature is fixed as 82 DEG C with the difference of embodiment 1.
Comparative example 5: it is only that dyeing temperature is fixed as 75 DEG C with the difference of embodiment 1.
Comparative example 6: it is only that dyeing temperature is fixed as 90 DEG C with the difference of embodiment 1.
Table 2
As can be seen from Table 2, upper dye can effectively be improved by the dyeing temperature that adjusts corresponding in dyeing course in the present invention
Percentage.
Claims (8)
1. a kind of scutellaria dyeing of terylene ribbon, which comprises the following steps:
(1) radix scutellariae dyestuff: being crushed to 120 meshes for radix scutellariae, obtain scutellaria powder, and scutellaria powder is added to 10 times of its quality
Mass concentration be to be forced into 1.2-1.5MPa in the aqueous solution of boride of 0.2-0.5%, kept for 2-3 hours, then carried out
Pressure release vacuumizes, and is heated to 100 DEG C, is kept for 1.5 hours, is then filtered, and repeats extraction 2 times to filter residue, merges 3 times
Filtered fluid is to get scutellaria dyestuff；
(2) steam treatment: terylene ribbon is used into high-temperature steam suffocating treatment 40-45min, is then placed in water balance room
Carry out moisture equilibration 1 hour, then cooled to room temperature again；
(3) it dyes: treated terylene ribbon being put into scutellaria dyestuff obtained above and is dyed, after the completion
It takes out, is placed on ventilating and cooling place and dries.
2. a kind of scutellaria dyeing of terylene ribbon according to claim 1, which is characterized in that the boride is boron
Sour zinc.
3. a kind of scutellaria dyeing of terylene ribbon according to claim 1, which is characterized in that described to vacuumize to take out
Vacuum to vacuum degree is 0.01-0.03MPa.
4. a kind of scutellaria dyeing of terylene ribbon according to claim 1, which is characterized in that the high-temperature steam temperature
Degree is 115 DEG C.
5. a kind of scutellaria dyeing of terylene ribbon according to claim 1, which is characterized in that the water balance room
Interior temperature is 60 DEG C, relative air humidity 70%.
6. a kind of scutellaria dyeing of terylene ribbon according to claim 1, which is characterized in that the bath raio of the dyeing
For 1:20.
7. a kind of scutellaria dyeing of terylene ribbon according to claim 1, which is characterized in that the time of the dyeing
For 50min.
8. a kind of scutellaria dyeing of terylene ribbon according to claim 1 or claim 7, which is characterized in that the dyeing
Temperature is that dyeing temperature is 82 DEG C in dyeing leading portion 30min, and dyeing dyeing temperature in back segment 20min is 75 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810773030.4A CN109235075A (en) | 2018-07-14 | 2018-07-14 | A kind of scutellaria dyeing of terylene ribbon |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810773030.4A CN109235075A (en) | 2018-07-14 | 2018-07-14 | A kind of scutellaria dyeing of terylene ribbon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109235075A true CN109235075A (en) | 2019-01-18 |
Family
ID=65072643
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810773030.4A Pending CN109235075A (en) | 2018-07-14 | 2018-07-14 | A kind of scutellaria dyeing of terylene ribbon |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109235075A (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20050048299A (en) * | 2003-11-19 | 2005-05-24 | 대한민국(광주.전남지방중소기업청) | Dye having antivirus efficacy and dyeing tissue thereof |
| CN1712452A (en) * | 2005-07-21 | 2005-12-28 | 上海交通大学 | Production of Baical skullcap root plant dye |
| CN101955692A (en) * | 2010-08-10 | 2011-01-26 | 浙江理工大学 | Method for preparing pulpy disperse dye for low-temperature dyeing of terylene |
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2018
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Application publication date: 20190118 |