CN108978235B - Manufacturing method of anti-static high-temperature-resistant fabric - Google Patents
Manufacturing method of anti-static high-temperature-resistant fabric Download PDFInfo
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Abstract
The invention relates to a manufacturing method of an anti-static high-temperature-resistant fabric, which comprises the following steps: the method comprises the following steps: coating the high-density knitted fabric serving as base fabric with special anti-static high-temperature-resistant paint; step two: adding butanone, polyurethane, an accelerator and phosphate in a certain proportion into a container, fully mixing and uniformly stirring to prepare flame-retardant glue; spraying flame-retardant glue on the front and back sides of the curtain base cloth coated with the anti-static high-temperature-resistant coating; step three: and (4) washing, drying and baking the base fabric treated in the step (II) to obtain the anti-static high-temperature-resistant fabric. The special coating has good antistatic effect and excellent fireproof and high temperature resistant performance. Meanwhile, the knitted base fabric is coated, the problem of stressed deformation of the knitted fabric in the coating process is solved, and the produced coated fabric is good in flame retardant property and good in water washing resistance.
Description
Technical Field
The invention belongs to the field of textiles, and particularly relates to a manufacturing method of an anti-static high-temperature-resistant fabric.
Background
Static electricity, which is a static or non-flowing charge, is formed when the charge accumulates on an object or surface. For example, in winter in the north, people are easy to be charged with static electricity, and when people contact with other people or metal conductors, the phenomenon of discharge can occur. People can feel the acupuncture feeling of electric shock, and sparks can be seen at night, which is the reason that chemical fiber clothes and human bodies rub to bring positive static electricity to the human bodies. The persistent static electricity can cause the pH value of blood of a human body to be increased, the excretion amount of calcium in urine to be increased, the blood calcium to be reduced, and the adverse effects on the heart, the brain and the skin are caused.
Meanwhile, the industrial harm of static electricity is more serious:
(1) causing malfunction or malfunction of the electronic device and causing electromagnetic interference.
(2) Breakdown of integrated circuits and precision electronic components, or aging of components, lowering production yield.
(3) High-voltage electrostatic discharge causes electric shock, and personal safety is endangered.
(4) Explosion and fire are easily caused in production places of various flammable and explosive articles or dust and oil mist.
(5) Electronic industry: dust is adsorbed to cause pollution of integrated circuits and semiconductor elements, and the yield is greatly reduced.
(6) Film and plastics industries: the film or the film is rolled unevenly; the film and the CD plastic disc are stained with dust, which affects the quality.
(7) Paper making and printing industry: the paper is not rolled up neatly, the overprinting is inaccurate, the dirt absorption is serious, and even the paper is bonded, which affects the production.
(8) Textile industry: causing the damages of root filament fluttering, twisting and breaking, yarn entanglement and the like.
Especially in flammable and explosive working environment, and when processing and using places of electronic components work, the requirement on static electricity is extremely severe. At present, static electricity generated and carried by a human body is mainly controlled by antistatic clothes. However, the antistatic clothing in the present stage has a single function, and cannot meet the requirements of complex and severe working environments, such as high-temperature environments. In addition, the fabric is stiff and heavy, and the wearing comfort is poor.
Disclosure of Invention
The invention aims to overcome the defects in the prior art, and provides a manufacturing method of an anti-static high-temperature-resistant fabric, which comprises the following steps:
the method comprises the following steps: coating the high-density knitted fabric serving as base fabric with an antistatic high-temperature-resistant coating;
step two: adding butanone, polyurethane and phosphate in a certain proportion into a container, fully mixing and uniformly stirring to prepare flame-retardant glue; spraying flame-retardant glue on the front side of the curtain base cloth coated with the anti-static high-temperature-resistant coating; when the front surface of the base fabric is sprayed with the flame-retardant glue, the spraying pressure is 6-8Pa, the spraying time is 3-5s, and the dosage of the flame-retardant glue is 40-60g/m2(ii) a Spraying the flame-retardant glue on the back surface of the base cloth with the front surface sprayed with the flame-retardant glue for the second time, wherein the dosage of the flame-retardant glue is 120-150g/m2；
Step three: washing, drying and baking the base fabric treated in the step two to obtain the anti-static high-temperature-resistant fabric;
the preparation method of the antistatic high-temperature-resistant coating in the first step comprises the following steps:
a: taking 10 parts of bisphenol A type epoxy resin, 10 parts of epoxy-terminated modified polyurethane resin, 10 parts of polyester resin, 5 parts of diluent, 15 parts of flaky mica, 10 parts of titanium dioxide and the like in parts by weight, and stirring and mixing for 1 hour to obtain a mixture A;
b: respectively weighing 10 parts of ethyl acetate, 10 parts of n-butyl acetate, 5 parts of cyclohexanone, 15 parts of potassium titanate whiskers and 15 parts of zinc oxide whiskers in parts by weight, sequentially adding the materials into the mixture A in a stirring state, and continuing stirring for 1 hour after all the materials are added to obtain a mixture B;
c: respectively weighing 0.5 part of wear-resistant protective wax, 0.5 part of dispersant, 0.5 part of defoamer and 15 parts of cobalt blue in parts by weight, sequentially adding the materials into the mixture B, and fully stirring for about 30-60 minutes;
d: c, adding the mixture obtained in the step c into a three-roller grinding machine, fully grinding for 1 hour, and filtering by a filter screen of 400 meshes to obtain an antistatic high-temperature-resistant coating product;
the preparation method of the potassium titanate whisker comprises the following steps: weighing K according to a certain molar ratio2CO3、TiO2Adding the raw materials into a ball milling tank, adding agate balls, ball milling for 2 hours at the rotating speed of 500r/min, then placing the ball-milled mixture into a crucible, placing the crucible into a resistance furnace, heating to 900 ℃ by adopting a programmed heating mode, preserving the temperature for 2 hours, cooling to room temperature, crushing, and sieving to obtain the potassium titanate whisker.
Further, the length of the potassium titanate whisker is 10-30 μm.
Further, in the second step, when the front surface of the base fabric is sprayed with the flame-retardant glue, the dosage of the flame-retardant glue is 50g/m2；。
Further, in the second step, when the back surface of the base fabric is sprayed with the flame-retardant glue for the second time, the using amount of the flame-retardant glue is 140g/m2。
Compared with the prior art, the invention has the beneficial effects that:
(1) the antistatic coating is prepared by using a specific combination of conductive composite resin, namely the combination of bisphenol A epoxy resin, epoxy-terminated modified polyurethane resin and polyester resin, and simultaneously using potassium titanate whiskers and zinc oxide whiskers with excellent conductivity in the coating on the basis of the traditional conductive resin antistatic coating, so that organic/inorganic conductive materials in the coating are matched with each other, and the raw materials adopt specific proportions, so that the obtained coating has excellent antistatic property and good corrosion resistance;
(2) the fabric prepared by the preparation method has good flame-retardant and heat-insulating properties, the afterflame time and the smoldering time are 0s, and the damage length is 10.5 cm.
(3) The preparation method has wide adaptability. The knitted fabric can be used not only for knitted fabrics but also for woven fabrics, knitted fabrics and the like. Besides the finishing of cotton fabrics, the finishing of chemical fiber fabrics, blended fabrics and the like can also be carried out. The obtained fabric product takes the knitted fabric as the base fabric, and has soft hand feeling, good drapability and elasticity.
(4) The antistatic high-temperature-resistant heat-insulating coating adopted by the invention has good flexibility and strong adhesive force to fabrics, can be directly coated on various textiles and can prevent the textiles from mildewing.
Detailed Description
The technical scheme of the invention is further specifically described by the following embodiments.
Example 1:
a manufacturing method of an anti-static high-temperature-resistant fabric comprises the following steps:
the method comprises the following steps: coating the high-density knitted fabric serving as base fabric with an antistatic high-temperature-resistant coating;
step two: adding butanone, polyurethane and phosphate in a certain proportion into a container, fully mixing and uniformly stirring to prepare flame-retardant glue; spraying flame-retardant glue on the front side of the curtain base cloth coated with the anti-static high-temperature-resistant coating; when the front surface of the base fabric is sprayed with the flame-retardant glue, the spraying pressure is 6-8Pa, the spraying time is 3-5s, and the dosage of the flame-retardant glue is 40g/m2(ii) a Spraying the flame-retardant glue on the back surface of the base fabric with the front surface sprayed with the flame-retardant glue for the second time, wherein the using amount of the flame-retardant glue is 120g/m2；
Step three: washing, drying and baking the base fabric treated in the step two to obtain the anti-static high-temperature-resistant fabric;
the preparation method of the antistatic high-temperature-resistant coating in the first step comprises the following steps:
a: taking 10 parts of bisphenol A type epoxy resin, 10 parts of epoxy-terminated modified polyurethane resin, 10 parts of polyester resin, 5 parts of diluent, 15 parts of flaky mica, 10 parts of titanium dioxide and the like in parts by weight, and stirring and mixing for 1 hour to obtain a mixture A;
b: respectively weighing 10 parts of ethyl acetate, 10 parts of n-butyl acetate, 5 parts of cyclohexanone, 15 parts of potassium titanate whiskers and 15 parts of zinc oxide whiskers in parts by weight, sequentially adding the materials into the mixture A in a stirring state, and continuing stirring for 1 hour after all the materials are added to obtain a mixture B;
c: respectively weighing 0.5 part of wear-resistant protective wax, 0.5 part of dispersant, 0.5 part of defoamer and 15 parts of cobalt blue in parts by weight, sequentially adding the materials into the mixture B, and fully stirring for about 30-60 minutes;
d: c, adding the mixture obtained in the step c into a three-roller grinding machine, fully grinding for 1 hour, and filtering by a filter screen of 400 meshes to obtain an antistatic high-temperature-resistant coating product;
the preparation method of the potassium titanate whisker comprises the following steps: weighing K according to a certain molar ratio2CO3、TiO2Adding the raw materials into a ball milling tank, adding agate balls, ball milling for 2 hours at the rotating speed of 500r/min, then placing the ball-milled mixture into a crucible, placing the crucible into a resistance furnace, heating to 900 ℃ by adopting a programmed heating mode, preserving the temperature for 2 hours, cooling to room temperature, crushing, and sieving to obtain the potassium titanate whisker with the length of 10 mu m.
Example 2:
a manufacturing method of an anti-static high-temperature-resistant fabric comprises the following steps:
the method comprises the following steps: coating the high-density knitted fabric serving as base fabric with an antistatic high-temperature-resistant coating;
step two: adding butanone, polyurethane and phosphate in a certain proportion into a container, fully mixing and uniformly stirring to prepare flame-retardant glue; spraying flame-retardant glue on the front side of the curtain base cloth coated with the anti-static high-temperature-resistant coating; when the front surface of the base fabric is sprayed with the flame-retardant glue, the spraying pressure is 6-8Pa, the spraying time is 3-5s, and the dosage of the flame-retardant glue is 60g/m2(ii) a Spraying the flame-retardant glue on the back surface of the base fabric with the front surface sprayed with the flame-retardant glue for the second time, wherein the using amount of the flame-retardant glue is 150g/m2；
Step three: washing, drying and baking the base fabric treated in the step two to obtain the anti-static high-temperature-resistant fabric;
the preparation method of the antistatic high-temperature-resistant coating in the first step comprises the following steps:
a: taking 10 parts of bisphenol A type epoxy resin, 10 parts of epoxy-terminated modified polyurethane resin, 10 parts of polyester resin, 5 parts of diluent, 15 parts of flaky mica, 10 parts of titanium dioxide and the like in parts by weight, and stirring and mixing for 1 hour to obtain a mixture A;
b: respectively weighing 10 parts of ethyl acetate, 10 parts of n-butyl acetate, 5 parts of cyclohexanone, 15 parts of potassium titanate whiskers and 15 parts of zinc oxide whiskers in parts by weight, sequentially adding the materials into the mixture A in a stirring state, and continuing stirring for 1 hour after all the materials are added to obtain a mixture B;
c: respectively weighing 0.5 part of wear-resistant protective wax, 0.5 part of dispersant, 0.5 part of defoamer and 15 parts of cobalt blue in parts by weight, sequentially adding the materials into the mixture B, and fully stirring for about 30-60 minutes;
d: c, adding the mixture obtained in the step c into a three-roller grinding machine, fully grinding for 1 hour, and filtering by a filter screen of 400 meshes to obtain an antistatic high-temperature-resistant coating product;
the preparation method of the potassium titanate whisker comprises the following steps: weighing K according to a certain molar ratio2CO3、TiO2Adding the raw materials into a ball milling tank, adding agate balls, ball milling for 2 hours at the rotating speed of 500r/min, then placing the ball-milled mixture into a crucible, placing the crucible into a resistance furnace, heating to 900 ℃ by adopting a programmed heating mode, preserving the temperature for 2 hours, cooling to room temperature, crushing, and sieving to obtain the potassium titanate whisker with the length of 30 mu m.
Example 3:
a manufacturing method of an anti-static high-temperature-resistant fabric comprises the following steps:
the method comprises the following steps: coating the high-density knitted fabric serving as base fabric with an antistatic high-temperature-resistant coating;
step two: adding butanone, polyurethane and phosphate in a certain proportion into a container, fully mixing and uniformly stirring to prepare flame-retardant glue; spraying flame-retardant glue on the front side of the curtain base cloth coated with the anti-static high-temperature-resistant coating; when the front surface of the base fabric is sprayed with the flame-retardant glue, the spraying pressure is 6-8Pa, the spraying time is 3-5s, and the dosage of the flame-retardant glue is 50g/m2(ii) a Spraying the flame-retardant glue on the back surface of the base fabric with the front surface sprayed with the flame-retardant glue for the second time, wherein the using amount of the flame-retardant glue is 140g/m2；
Step three: washing, drying and baking the base fabric treated in the step two to obtain the anti-static high-temperature-resistant fabric;
the preparation method of the antistatic high-temperature-resistant coating in the first step comprises the following steps:
a: taking 10 parts of bisphenol A type epoxy resin, 10 parts of epoxy-terminated modified polyurethane resin, 10 parts of polyester resin, 5 parts of diluent, 15 parts of flaky mica, 10 parts of titanium dioxide and the like in parts by weight, and stirring and mixing for 1 hour to obtain a mixture A;
b: respectively weighing 10 parts of ethyl acetate, 10 parts of n-butyl acetate, 5 parts of cyclohexanone, 15 parts of potassium titanate whiskers and 15 parts of zinc oxide whiskers in parts by weight, sequentially adding the materials into the mixture A in a stirring state, and continuing stirring for 1 hour after all the materials are added to obtain a mixture B;
c: respectively weighing 0.5 part of wear-resistant protective wax, 0.5 part of dispersant, 0.5 part of defoamer and 15 parts of cobalt blue in parts by weight, sequentially adding the materials into the mixture B, and fully stirring for about 30-60 minutes;
d: c, adding the mixture obtained in the step c into a three-roller grinding machine, fully grinding for 1 hour, and filtering by a filter screen of 400 meshes to obtain an antistatic high-temperature-resistant coating product;
the preparation method of the potassium titanate whisker comprises the following steps: weighing K according to a certain molar ratio2CO3、TiO2Adding the raw materials into a ball milling tank, adding agate balls, ball milling for 2 hours at the rotating speed of 500r/min, putting the ball milled mixture into a crucible, putting the crucible into a resistance furnace, and adopting a programmed heating methodHeating to 900 deg.C, holding for 2 hr, cooling to room temperature, pulverizing, and sieving to obtain potassium titanate crystal whisker of 20 μm length.
The foregoing description has disclosed fully preferred embodiments of the present invention. It should be noted that those skilled in the art can make modifications to the embodiments of the present invention without departing from the scope of the appended claims. Accordingly, the scope of the appended claims is not to be limited to the specific embodiments described above.
Claims (1)
1. A manufacturing method of an anti-static high-temperature-resistant fabric is characterized by comprising the following steps: the method comprises the following steps:
the method comprises the following steps: taking the high-density curtain knitted fabric as base cloth, and coating the base cloth with antistatic high-temperature-resistant paint;
step two: adding butanone, polyurethane and phosphate in a certain proportion into a container, fully mixing and uniformly stirring to prepare flame-retardant glue; spraying flame-retardant glue on the front side of the curtain base cloth coated with the anti-static high-temperature-resistant coating; when the front surface of the base fabric is sprayed with the flame-retardant glue, the spraying pressure is 6-8Pa, the spraying time is 3-5s, and the dosage of the flame-retardant glue is 50g/m2(ii) a Spraying the flame-retardant glue on the back surface of the base fabric with the front surface sprayed with the flame-retardant glue for the second time, wherein the using amount of the flame-retardant glue is 140g/m2；
Step three: washing, drying and baking the base fabric treated in the step two to obtain the anti-static high-temperature-resistant fabric;
the preparation method of the antistatic high-temperature-resistant coating in the first step comprises the following steps:
a: taking 10 parts of bisphenol A type epoxy resin, 10 parts of epoxy-terminated modified polyurethane resin, 10 parts of polyester resin, 5 parts of diluent, 15 parts of flaky mica and 10 parts of titanium dioxide by weight parts, and stirring and mixing for 1 hour to obtain a mixture A;
b: respectively weighing 10 parts of ethyl acetate, 10 parts of n-butyl acetate, 5 parts of cyclohexanone, 15 parts of potassium titanate whiskers and 15 parts of zinc oxide whiskers in parts by weight, sequentially adding the materials into the mixture A in a stirring state, and continuing stirring for 1 hour after all the materials are added to obtain a mixture B;
c: respectively weighing 0.5 part of wear-resistant protective wax, 0.5 part of dispersant, 0.5 part of defoamer and 15 parts of cobalt blue in parts by weight, sequentially adding the materials into the mixture B, and fully stirring for 30-60 minutes;
d: c, adding the mixture obtained in the step c into a three-roller grinding machine, fully grinding for 1 hour, and filtering by a filter screen of 400 meshes to obtain an antistatic high-temperature-resistant coating product;
the preparation method of the potassium titanate whisker comprises the following steps: weighing K according to a certain molar ratio2CO3、TiO2Adding the raw materials into a ball milling tank, adding agate balls, ball milling for 2 hours at a rotating speed of 500r/min, then placing the ball-milled mixture into a crucible, placing the crucible into a resistance furnace, heating to 900 ℃ by adopting a programmed heating mode, preserving the temperature for 2 hours, cooling to room temperature, crushing, and sieving to obtain potassium titanate whiskers, wherein the length of the potassium titanate whiskers is about 10-30 mu m.
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| CN201810564061.9A CN108978235B (en) | 2015-07-29 | 2015-07-29 | Manufacturing method of anti-static high-temperature-resistant fabric |
| CN201510453571.5A CN105133165B (en) | 2015-07-29 | 2015-07-29 | A kind of production method of antistatic high temperature resistant fabric |
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| CN111893779B (en) * | 2020-07-23 | 2022-09-06 | 杭州众逸布业有限公司 | Three-proofing sofa fabric and preparation method thereof |
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| KR100597843B1 (en) * | 2005-03-28 | 2006-07-10 | 배효청 | Fire resistance velure and producing method of it's |
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| CN101358099A (en) * | 2008-09-09 | 2009-02-04 | 北京市射线应用研究中心 | Epoxy static conducting anti-corrosive paint |
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| CN108978235A (en) | 2018-12-11 |
| CN105133165B (en) | 2018-08-17 |
| CN105133165A (en) | 2015-12-09 |
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