CN108918387A - It is a kind of for detecting the impervious test method of mortar - Google Patents

It is a kind of for detecting the impervious test method of mortar Download PDF

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Publication number
CN108918387A
CN108918387A CN201810805615.XA CN201810805615A CN108918387A CN 108918387 A CN108918387 A CN 108918387A CN 201810805615 A CN201810805615 A CN 201810805615A CN 108918387 A CN108918387 A CN 108918387A
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Prior art keywords
mortar
test
impervious
sealant
specimen
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CN201810805615.XA
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CN108918387B (en
Inventor
马国栋
谢红
孟辉江
李幸展
郭丹丹
陈占虎
郝建江
冯晓烨
张茜
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Hebei Sankaishenfa Science & Technology Co Ltd
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Hebei Sankaishenfa Science & Technology Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/38Diluting, dispersing or mixing samples
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples
    • G01N2001/366Moulds; Demoulding

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  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Dispersion Chemistry (AREA)
  • Examining Or Testing Airtightness (AREA)
  • Sealing Material Composition (AREA)

Abstract

The present invention relates to a kind of for detecting the test method of mortar anti-permeability performance, it puts the mortar block to be measured conserved into standard laboratory and carries out standing and drying processing 0.5h, the inner wall of impervious test mould is coated uniformly on mixing sealant, mix sealant with a thickness of 1~2mm.Then mortar block press machine is pressed into impervious test mould and forms mortar specimen, make have colloid extrusion in the above and below gap of mortar specimen, as gap occurs re-starting coating operation in mortar specimen.Mortar specimen bottom surface after being pressed into mortar block is parallel with the bottom surface of impervious test mould, scrapes off the colloid squeezed out in the gap of mortar specimen above and below, carries out impermeability test after placing 2h in the lab.Mixing sealant is acetic acid silicone sealant and quick hardening sulphoaluminate cement by weight 2:1 is uniformly mixed to prepare.The present invention solves the problems, such as easy leak when detection High Voltage, optimizes detection operating process, improves detection effect and accuracy.

Description

It is a kind of for detecting the impervious test method of mortar
Technical field
The invention belongs to construction material technical field of performance test, are related to a kind of detection technique of mortar, and in particular to one Kind is for detecting the impervious test method of mortar.
Background technique
The anti-permeability performance of waterproof mortar drastically influences its using effect, resists to meet requirement to waterproof mortar Seeping performance test is particularly important.The impermeability pressure with waterproof performance mortar is generally all in 1.5MPa or more at present, according to To mortar specimen 7d impermeability pressure requirement >=1.5MPa in GB 23440-2009 standard, when detecting mortar specimen impermeability pressure, It needs that the painting of mortar block is first covered with one layer of rosin paraffin liquid or using butter and cement weight than 1:3 lotion is sealed, It places into impervious test mould and is fastened.The solidification in coating of rosin paraffin liquid method is difficult coating uniformly quickly, in operation, thick Degree is also difficult uniform.It is rigid contact between mortar specimen and impervious test mould, the ductility being pressurized after the hardening of rosin paraffin liquid is very Difference is easy to produce gap, and the paraffin after hardening is difficult to seal up irregular gap and (is generated due to the scrambling of mortar block Gap between impervious test mould) butter cement seal method firm time is long, 1d or more is generally required, and be extremely difficult to 1.5MPa When it is water-tight, hydraulic pressure Gao Shihui occurs spurting water column from leak between mortar block and impervious test mould, when serious.The prior art The bad control of paraffin temperature, the leakproofness of paraffin is poor, will leak at paraffin sealing when hydraulic pressure reaches 0.6MPa or so Water phenomenon, condenses into solid at once after being coated on test specimen because of paraffin, fragile material has been condensed into after being put on pressuring machine, There is no ductility after withstanding pressure, the sealing function to Anomalistic space cannot be played very well, be not able to satisfy actually detected mortar Impervious needs.
Summary of the invention
The present invention provides a kind of for detecting the impervious test method of mortar, and easy leak is asked when solving to detect High Voltage Topic, optimizing detection operating process improve detection effect and accuracy.
The technical scheme is that:For detecting the test method of mortar anti-permeability performance, the mortar to be measured that will conserve Block puts standard laboratory into and carries out standing and drying processing 0.5h, and the inner wall of impervious test mould is coated uniformly on mixing sealant, is mixed Close sealant with a thickness of 1~2mm.Then mortar block press machine is pressed into impervious test mould and forms mortar specimen, make mortar block Above and below gap in have colloid extrusion, as gap occurs re-starting coating operation in mortar specimen.After being pressed into mortar block Mortar specimen bottom surface it is parallel with the bottom surface of impervious test mould, scrape off the colloid squeezed out in the gap of mortar specimen above and below, testing Impervious experiment is carried out after placing 2h in room.
Mixing sealant is acetic acid silicone sealant and quick hardening sulphoaluminate cement by weight 2:1 is uniformly mixed to prepare. Impervious test mould is conical structure, and the back cut diameter of cone is 70mm, lower port diameter 80mm, is highly 30mm, uses steel plate Or aluminium sheet is made.
Impermeability test includes the following steps:
(1) ingredient, mixing mortar are carried out by standard requirements, impervious test mould is once filled after mixing thoroughly, on a vibration table molding vibration It is real, it is smoothed out after wiping extra slurry off, prepares 6 test specimens;
(2) 24 ± 2h of moisture-keeping maintaining in the environment of 20 ± 3 DEG C of temperature, relative humidity 90%~100%, is being put into 20 ± 2 DEG C maintenance pond in maintenance to 7d age, surface washing is clean;
(3) after dry tack free, mixing sealant is fitted into impervious test mould, can be carried out after sealant hardening to be mixed Impervious water permeabillity test;The water pressure test is carried out according to standard requirements, is gradually boosted during test:1. hydraulic pressure since 0.2MPa, Constant pressure 2h increases to 0.3MPa, increases hydraulic pressure 0.1MPa every 1h later;2. being forced into after 1.5MPa, constant pressure 1h is not permeable, stops Boosting;3. do not occur the maximum pressure value to seep water as test specimen impermeability pressure using 4 in every 6 test specimens, such as to 1.5MPa when have 4 The above test specimen keeps 1h not seep water, then maximum impermeability pressure >=1.5MPa.
The present invention is according to GB 23440-2009《Inorganic leak-stopping material》, prepare normal sand and meet GB 175-2007 42.5 grades of ordinary portland cements, to belong to 6 impervious test moulds, shake table, mortar mixer, mortars impervious for frustum of a cone band down payment Instrument and water.
The present invention utilizes acetic acid silicone sealant and quick hardening sulphoaluminate cement for detecting the impervious test method of mortar By weight 2:1 is made the inner wall that mixing sealant is coated uniformly on impervious test mould, solves easy leak when detection High Voltage Problem optimizes detection operating process, improves detection effect and accuracy.The present invention overcomes the prior arts cannot detect height The deficiency of hydraulic pressure avoids high-temperature heating compared with compared with rosin paraffin method, has easy to operate, Environmental Safety, sealing The advantages of complete and easy to clean is suitable for the experimental enviroment of 1.5MPa high pressure.
Detailed description of the invention
Fig. 1 is the mold schematic diagram for detecting mortar impermeability test;
Wherein:A-mortar specimen, b-mixing sealant, c-impervious test mould.
Specific embodiment
Below with reference to embodiment and attached drawing, the present invention is described in detail.The scope of protection of the present invention is not limited to the embodiment, Those skilled in the art make any change within the scope of the claims and also belong to the scope of protection of the invention.
The test method that the present invention is used to detect mortar anti-permeability performance is, first by acetic acid silicone sealant and fast hard sulfuric acid Salt cement is according to weight ratio 2:1 is uniformly mixed and made into mixing sealant.Accelerate hard sulfate cement in toward acetic acid silicone sealant It when material, is uniformly sprinkled upon on colloid, is added in two portions, put on environmentally friendly acid-proof gloves and grabbed repeatedly and hold operation, make fast hard sulfate Cement is uniformly mixed with acetic acid silicone sealant.The mortar block to be measured conserved is put into standard laboratory to carry out at standing and drying 0.5h is managed, mortar block surface Ming Shui is wiped.It is coated uniformly on the inner wall of impervious test mould c with mixing sealant b, mixes sealant With a thickness of 1mm.Then mortar block press machine is pressed into impervious test mould and forms mortar specimen 1, make the bottom surface of mortar specimen with The bottom surface of impervious test mould flushes.As shown in Figure 1, impervious test mould c is conical structure, the back cut diameter of cone is 70mm, under Mouth diameter is 80mm, is highly 30mm, is surrounded with steel plate.It is required that having colloid extrusion in the gap of the above and below of mortar specimen, such as Fruit, which has partial gap region, colloid extrusion, illustrates that colloid is not filled by full herein, and this occurs needs to re-start Coating operation, it is ensured that the bottom surface mortar specimen a of indentation mortar block is parallel with the bottom surface of impervious test mould c.It must not tilt and be higher by, scrape The colloid squeezed out in the gap of above and below is removed, pays attention to preventing colloid from coating in the top and bottom of mortar specimen, is coated onto accidentally if any colloid Surface is rooted out completely with pocket knife, leaks out screed.The colloid squeezed out in the gap of mortar specimen above and below is scraped off, after processing is clean Impervious experiment is carried out after placing 2h in the lab.
The step of impermeability test is:
(1) ingredient, mixing mortar are carried out by standard requirements, impervious test mould c is once filled after mixing thoroughly, is formed on a vibration table Jolt ramming smoothes out after wiping extra slurry off, prepares 6 test specimens;
(2) 24 ± 2h of moisture-keeping maintaining in the environment of 20 ± 3 DEG C of temperature, relative humidity 90%~100%, is being put into 20 ± 2 DEG C maintenance pond in maintenance to 7d age, surface washing is clean;
(3) after dry tack free, mixing sealant is fitted into impervious test mould c, sealant hardening to be mixed can be resisted Permeate water test;Hydraulic pressure is gradually boosted according to standard requirements:1. hydraulic pressure, since 0.2MPa, constant pressure 2h increases to 0.3MPa, Increase hydraulic pressure 0.1MPa every 1h later;2. fully meeting that 1.5MPa in standard criterion is non-leakage to be wanted to ensure to mix sealant It asks, constant pressure 1h is not permeable after test hydraulic pressure is enlarged to 1.8MPa, stops boosting;3. not seeped with 4 in every 6 test specimens The maximum pressure value of water is test specimen impermeability pressure, such as to 1.5MPa when there are 4 or more test specimens holding 1h not seep water, then it is maximum impervious Pressure >=1.5MPa.
After experiment, mortar block is tapped out from impervious test mould with hammer, with wallpaper knife cleaning iron mould inner wall Colloid.
Watch 1 is to mix sealant progress sand made of sulfate cement firmly with fast with acetic acid silicone sealant using the present invention Starch the result of anti-permeability performance detection test.It is mixed with paraffin to list the prior art convenient for comparing, in table 1 and is done with rosin resin Sealant and the data for making sealant progress mortar anti-permeability performance detection test with butter and cement mixing.Table 1 is the result shows that originally Invention with acetic acid silicone sealant and fast hard sulfate cement be mix sealant detection mortar anti-permeability performance test method it is excellent In the test method of the prior art.
Table 1:The impermeability pressure (MPa) of different sealing method
Impermeability pressure, MPa Paraffin and rosin resin Butter and cement Sealant and quick-hardening cement
0.5 Non- leak 5 pieces of leaks in 6 pieces Non- leak
0.6 2 pieces of leaks in 6 pieces 5 pieces of leaks in 6 pieces Non- leak
0.7 4 pieces of leaks in 6 pieces 6 pieces of whole leaks Non- leak
0.8 5 pieces of leaks in 6 pieces ---- Non- leak
1.0 6 pieces of whole leaks ---- Non- leak
1.5 ---- ---- Non- leak
1.8 ----- ---- Non- leak

Claims (4)

1. it is a kind of for detecting the test method of mortar anti-permeability performance, it is characterized in that:Put the mortar block to be measured conserved into mark Quasi-experiment room carries out standing and drying and handles 0.5h, and the inner wall of impervious test mould c, mixing sealing are coated uniformly on mixing sealant b Glue with a thickness of 1~2mm;Then mortar block press machine is pressed into impervious test mould and forms mortar specimen a, make mortar specimen There is colloid extrusion in the gap of above and below, as gap occurs re-starting coating operation in mortar specimen;After being pressed into mortar block Mortar specimen bottom surface is parallel with the bottom surface of impervious test mould, scrapes off the colloid squeezed out in the gap of test block above and below, in the lab Impervious experiment is carried out after placing 2h.
2. according to claim 1 for detecting the test method of mortar anti-permeability performance, it is characterized in that:The mixing sealant B is acetic acid silicone sealant and quick hardening sulphoaluminate cement by weight 2:1 is uniformly mixed to prepare.
3. according to claim 1 for detecting the test method of mortar anti-permeability performance, it is characterized in that:The impervious test mould c Back cut diameter for conical structure, cone is 70mm, lower port diameter 80mm, is highly 30mm, with steel plate or aluminium sheet system At.
4. according to claim 1 for detecting the test method of mortar anti-permeability performance, it is characterized in that:The impermeability test packet Include following steps:
(1) ingredient, mixing mortar are carried out by standard requirements, impervious test mould c are once filled after mixing thoroughly, forms jolt ramming on a vibration table, It is smoothed out after wiping extra slurry off, prepares 6 test specimens;
(2) 24 ± 2h of moisture-keeping maintaining in the environment of 20 ± 3 DEG C of temperature, relative humidity 90%~100%, places into 20 ± 2 DEG C It is to 7d age, surface washing is clean to conserve maintenance in pond;
(3) after dry tack free, mixing sealant is fitted into impervious test mould c, can be carried out after sealant hardening to be mixed impervious Water permeabillity test;The water pressure test is carried out according to standard requirements, is gradually boosted during test:1. hydraulic pressure is since 0.2MPa, constant pressure 2h increases to 0.3MPa, increases hydraulic pressure 0.1MPa every 1h later;2. being forced into after 1.5MPa, constant pressure 1h is not permeable, stops rising Pressure;3. do not occur the maximum pressure value to seep water as test specimen impermeability pressure using 4 in every 6 test specimens, such as to 1.5MPa when have 4 with Upper test specimen keeps 1h not seep water, then maximum impermeability pressure >=1.5MPa.
CN201810805615.XA 2018-07-20 2018-07-20 Test method for detecting impermeability of mortar Active CN108918387B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109883925A (en) * 2019-03-27 2019-06-14 武汉大学 The coarse crack of change aperture and preparation method thereof for visualized experiment
CN111471427A (en) * 2020-04-07 2020-07-31 衡水衡宝胶业有限公司 Preparation method of TPIN bi-component sealant
CN112834299A (en) * 2020-12-31 2021-05-25 中铁十八局集团有限公司 Sealing material based on fly ash machine-made sand mortar impermeability test and use method thereof
IT202000016993A1 (en) * 2020-07-13 2022-01-13 Alice Berto REINFORCED STRUCTURAL COMPONENT OR FLEXIBLE ROD

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109883925A (en) * 2019-03-27 2019-06-14 武汉大学 The coarse crack of change aperture and preparation method thereof for visualized experiment
CN109883925B (en) * 2019-03-27 2024-02-13 武汉大学 Variable-opening rough crack for visual experiment and manufacturing method thereof
CN111471427A (en) * 2020-04-07 2020-07-31 衡水衡宝胶业有限公司 Preparation method of TPIN bi-component sealant
IT202000016993A1 (en) * 2020-07-13 2022-01-13 Alice Berto REINFORCED STRUCTURAL COMPONENT OR FLEXIBLE ROD
WO2022013750A1 (en) * 2020-07-13 2022-01-20 Berto Alice Reinforced structural component or flexible tie rod
CN112834299A (en) * 2020-12-31 2021-05-25 中铁十八局集团有限公司 Sealing material based on fly ash machine-made sand mortar impermeability test and use method thereof

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