CN108913061A - A kind of luminous mural painting waterproof hot melt film and preparation method thereof - Google Patents
A kind of luminous mural painting waterproof hot melt film and preparation method thereof Download PDFInfo
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- CN108913061A CN108913061A CN201810899446.0A CN201810899446A CN108913061A CN 108913061 A CN108913061 A CN 108913061A CN 201810899446 A CN201810899446 A CN 201810899446A CN 108913061 A CN108913061 A CN 108913061A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J123/00—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers
- C09J123/02—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers not modified by chemical after-treatment
- C09J123/04—Homopolymers or copolymers of ethene
- C09J123/08—Copolymers of ethene
- C09J123/0846—Copolymers of ethene with unsaturated hydrocarbons containing other atoms than carbon or hydrogen atoms
- C09J123/0853—Vinylacetate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J161/00—Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
- C09J161/04—Condensation polymers of aldehydes or ketones with phenols only
- C09J161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/29—Laminated material
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/30—Adhesives in the form of films or foils characterised by the adhesive composition
- C09J7/35—Heat-activated
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2423/00—Presence of polyolefin
- C09J2423/04—Presence of homo or copolymers of ethene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2423/00—Presence of polyolefin
- C09J2423/10—Presence of homo or copolymers of propene
- C09J2423/106—Presence of homo or copolymers of propene in the substrate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2475/00—Presence of polyurethane
- C09J2475/006—Presence of polyurethane in the substrate
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a kind of luminous mural painting waterproof hot melt films and preparation method thereof, its hot melt adhesive film, including high transmittance film, EVA hot-melt adhesive film and TPU water permeable membrane, the high transmittance film and TPU water permeable membrane are two layers, and two layers of high transmittance film and TPU water permeable membrane are respectively distributed on the two sides outer wall of EVA hot-melt adhesive film, the preparation method of its hot melt adhesive film, include the following steps, it is sent into high-speed mixer after being weighed by above-mentioned raw material according to mass percent, it is stirred after heating, the raw material after stirring in step S1 is sent into hot melt adhesive machine, hot melt adhesive molten liquid is made.The present invention is added RA-2 light transmission agent by high definition film on the basis of original pp film and increases translucency, the distortion that will not seem is inserted in masking-out in mural painting, TPU water permeable membrane can improve its waterproofness, in preparation method, the mural painting that shines is reasonable with the material rate of waterproof hot melt film, technique for sticking is simple, and high comprehensive performance meets batch production requirements.
Description
Technical field
The present invention relates to waterproof hot melt technical field of membrane more particularly to a kind of luminous mural painting waterproof hot melt film and its
Preparation method.
Background technique
Hot melt adhesive film is a kind of with release paper or without the film class product of release paper, it is convenient to accomplished continuously or intermittently be grasped
Make, can be widely used for each kind fabric, paper, high molecular material and metal bonding, for the waterproof hot melt film in the mural painting that shines
It is that mural painting coat of paint or level fall off in order to prevent, guarantees its whole integrality.The transmitance of existing thermosol glue film is general,
Masking-out when on mural painting can because insufficient light seem be distorted it is more serious, while in the fabrication process due to match it is unreasonable,
The viscous stickiness that will cause hot melt adhesive film is poor.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of luminous mural painting waterproof hot melt film and its
Preparation method.
A kind of luminous mural painting waterproof hot melt film proposed by the present invention, including high transmittance film, EVA hot-melt adhesive film and TPU are saturating
Moisture film, the high transmittance film and TPU water permeable membrane are two layers, and two layers of high transmittance film and TPU water permeable membrane are respectively distributed to EVA hot-melt adhesive
On the two sides outer wall of film, the EVA hot-melt adhesive film is by EVA resin, SBS resin, terpene phenolic resin, polyethylene wax, neck benzene two
Formic acid dibutyl ester, 2,6- toluene di-tert-butyl phenol, calcium carbonate, glycidyl ether oxygen propyl trimethoxy silicane and gas phase dioxy
SiClx is made, and the permeable membrane structure of TPU is to be crosslinked '-diphenylmethane diisocyanate and toluene di-isocyanate(TDI) by chain extender
React the flexibility that obtained hard block and '-diphenylmethane diisocyanate, toluene di-isocyanate(TDI) and polyol reaction obtain
Segment is alternately constituted.
Preferably, resin based on the EVA resin, SBS resin are additional body resin, and terpene phenolic resin is thickening
Resin, polyethylene wax are viscosity modifier, and neck dibatyl phithalate is plasticizer, and 2,6- toluene di-tert-butyl phenols are antioxygen
Agent, calcium carbonate are filler, and glycidyl ether oxygen propyl trimethoxy silicane is coupling agent, and fumed silica is delustering agent.
Preferably, the EVA resin, SBS resin, terpene phenolic resin, polyethylene wax, neck dibatyl phithalate, 2,
The quality hundred of 6- toluene di-tert-butyl phenol, calcium carbonate, glycidyl ether oxygen propyl trimethoxy silicane and fumed silica
Divide than being respectively 35-45%, 3-6%, 25-35%, 3-6%, 3-6%, 2-4%, 19-25%, 0-1% and 0-1%.
Preferably, the high transmittance film is that PP film and RA-2 light transmission agent crosslinking are made, and RA-2 light transmission agent is crosslinked the knot of PP film
The light transmittance of brilliant conversion performance, PP film improves.
A kind of luminous mural painting production method of waterproof hot melt film, includes the following steps：
S1：It is sent into high-speed mixer after being weighed by above-mentioned raw material according to mass percent, is stirred after heating；
S2：Raw material after stirring in step S1 are sent into hot melt adhesive machine, hot melt adhesive molten liquid is made；
S3：Hot melt adhesive molten liquid obtained in step S2 is put into extrusion coated machine, EVA hot-melt adhesive film is made；
S4：High transmittance film is that PP film and RA-2 light transmission agent crosslinking are made, and RA-2 light transmission agent is crosslinked the crystallization conversion performance of PP film, right
Transparent filler parent granule, which is improved light transmittance, effect on thermal and other auxiliary agents, preferable synergistic effect, while having coupling to increase
It is molten, increase the functions such as lubrication；
S5：High transmittance film in S4 being attached on the outer wall of EVA hot-melt adhesive film, TPU water permeable membrane is attached on the outer wall of high definition film,
Finished film is made by hot pressing fitting；
S6：It is packed after finished film in S5 is integrated trimming.
Having the beneficial effect that in the present invention：By being provided with high definition film, RA- is added on the basis of original pp film in high definition film
2 light transmission agent, increase translucency, are inserted in masking-out the distortion that will not seem in mural painting, while being provided with TPU water permeable membrane to improve
Its waterproofness, in preparation method, shining, mural painting is reasonable with the material rate of waterproof hot melt film, and technique for sticking is simple, comprehensive
Function admirable meets batch production requirements.
Detailed description of the invention
Fig. 1 is a kind of luminous mural painting waterproof hot melt film the schematic diagram of the section structure proposed by the present invention；
Fig. 2 is a kind of flow chart of the preparation method of luminous mural painting waterproof hot melt film proposed by the present invention.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Referring to Fig.1, a kind of luminous mural painting waterproof hot melt film, including high transmittance film, EVA hot-melt adhesive film and TPU water permeable membrane,
High transmittance film and TPU water permeable membrane are two layers, and two layers of high transmittance film and TPU water permeable membrane are respectively distributed to the two sides of EVA hot-melt adhesive film
On outer wall, EVA hot-melt adhesive film by EVA resin, SBS resin, terpene phenolic resin, polyethylene wax, neck dibatyl phithalate, 2,
6- toluene di-tert-butyl phenol, calcium carbonate, glycidyl ether oxygen propyl trimethoxy silicane and fumed silica are made, TPU
Permeable membrane structure is embedding to be crosslinked the rigidity that '-diphenylmethane diisocyanate and toluene di-isocyanate(TDI) react by chain extender
Section and '-diphenylmethane diisocyanate, toluene di-isocyanate(TDI) with the soft segment that polyol reaction obtains replace composition.
In this waterproof hot melt film, resin based on EVA resin, SBS resin is additional body resin, terpene phenolic resin
For tackifying resin, polyethylene wax is viscosity modifier, and neck dibatyl phithalate is plasticizer, 2,6- toluene di-tert-butyl phenols
For antioxidant, calcium carbonate is filler, and glycidyl ether oxygen propyl trimethoxy silicane is coupling agent, and fumed silica is delustring
Agent, EVA resin, SBS resin, terpene phenolic resin, polyethylene wax, neck dibatyl phithalate, 2,6- di-t-butyl are to toluene
Phenol, calcium carbonate, glycidyl ether oxygen propyl trimethoxy silicane and fumed silica mass percent be respectively 35-45%,
3-6%, 25-35%, 3-6%, 3-6%, 2-4%, 19-25%, 0-1% and 0-1%, high transmittance film are PP film and RA-2 light transmission agent crosslinking system
At, and the crystallization conversion performance of RA-2 light transmission agent crosslinking PP film, the light transmittance of PP film improve.
Referring to Fig. 2, a kind of luminous mural painting production method of waterproof hot melt film includes the following steps：
S1：It is sent into high-speed mixer after being weighed by above-mentioned raw material according to mass percent, is stirred after heating；
S2：Raw material after stirring in step S1 are sent into hot melt adhesive machine, hot melt adhesive molten liquid is made；
S3：Hot melt adhesive molten liquid obtained in step S2 is put into extrusion coated machine, EVA hot-melt adhesive film is made；
S4：High transmittance film is that PP film and RA-2 light transmission agent crosslinking are made, and RA-2 light transmission agent is crosslinked the crystallization conversion performance of PP film, right
Transparent filler parent granule, which is improved light transmittance, effect on thermal and other auxiliary agents, preferable synergistic effect, while having coupling to increase
It is molten, increase the functions such as lubrication；
S5：High transmittance film in S4 being attached on the outer wall of EVA hot-melt adhesive film, TPU water permeable membrane is attached on the outer wall of high definition film,
Finished film is made by hot pressing fitting；
S6：It is packed after finished film in S5 is integrated trimming.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (5)
1. a kind of luminous mural painting waterproof hot melt film, including high transmittance film, EVA hot-melt adhesive film and TPU water permeable membrane, feature exist
In the high transmittance film and TPU water permeable membrane are two layers, and two layers of high transmittance film and TPU water permeable membrane are respectively distributed to EVA hot-melt adhesive film
Two sides outer wall on, the EVA hot-melt adhesive film by EVA resin, SBS resin, terpene phenolic resin, polyethylene wax, neck benzene diformazan
Dibutyl phthalate, 2,6- toluene di-tert-butyl phenol, calcium carbonate, glycidyl ether oxygen propyl trimethoxy silicane and gas phase titanium dioxide
Silicon is made, and the permeable membrane structure of TPU is to be crosslinked '-diphenylmethane diisocyanate by chain extender and toluene di-isocyanate(TDI) is anti-
The flexible chain that hard block and '-diphenylmethane diisocyanate, toluene di-isocyanate(TDI) and the polyol reaction that should be obtained obtain
Section is alternately constituted.
2. a kind of luminous mural painting waterproof hot melt film according to claim 1, which is characterized in that the EVA resin is
Matrix resin, SBS resin are additional body resin, and terpene phenolic resin is tackifying resin, and polyethylene wax is viscosity modifier, neck
Dibatyl phithalate is plasticizer, and 2,6- toluene di-tert-butyl phenols are antioxidant, and calcium carbonate is filler, glycidyl ether oxygen
Propyl trimethoxy silicane is coupling agent, and fumed silica is delustering agent.
3. a kind of luminous mural painting waterproof hot melt film according to claim 1, which is characterized in that the EVA resin,
SBS resin, terpene phenolic resin, polyethylene wax, neck dibatyl phithalate, 2,6- toluene di-tert-butyl phenol, calcium carbonate, contracting
The mass percent of the gentle aerosil of water glycerol ether oxygen propyl trimethoxy silicane is respectively 35-45%, 3-6%, 25-
35%, 3-6%, 3-6%, 2-4%, 19-25%, 0-1% and 0-1%.
4. a kind of luminous mural painting waterproof hot melt film according to claim 1, which is characterized in that the high transmittance film is PP
Film and RA-2 light transmission agent crosslinking are made, and the crystallization conversion performance of RA-2 light transmission agent crosslinking PP film, the light transmittance of PP film improve.
5. a kind of production method of luminous mural painting waterproof hot melt film, which is characterized in that include the following steps：
S1：It is sent into high-speed mixer after being weighed by above-mentioned raw material according to mass percent, is stirred after heating；
S2：Raw material after stirring in step S1 are sent into hot melt adhesive machine, hot melt adhesive molten liquid is made；
S3：Hot melt adhesive molten liquid obtained in step S2 is put into extrusion coated machine, EVA hot-melt adhesive film is made；
S4：High transmittance film is that PP film and RA-2 light transmission agent crosslinking are made, and RA-2 light transmission agent is crosslinked the crystallization conversion performance of PP film, right
Transparent filler parent granule, which is improved light transmittance, effect on thermal and other auxiliary agents, preferable synergistic effect, while having coupling to increase
It is molten, increase the functions such as lubrication；
S5：High transmittance film in S4 being attached on the outer wall of EVA hot-melt adhesive film, TPU water permeable membrane is attached on the outer wall of high definition film,
Finished film is made by hot pressing fitting；
S6：It is packed after finished film in S5 is integrated trimming.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810899446.0A CN108913061A (en) | 2018-08-09 | 2018-08-09 | A kind of luminous mural painting waterproof hot melt film and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810899446.0A CN108913061A (en) | 2018-08-09 | 2018-08-09 | A kind of luminous mural painting waterproof hot melt film and preparation method thereof |
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| CN108913061A true CN108913061A (en) | 2018-11-30 |
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| CN201810899446.0A Pending CN108913061A (en) | 2018-08-09 | 2018-08-09 | A kind of luminous mural painting waterproof hot melt film and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1648145A (en) * | 2004-01-30 | 2005-08-03 | 香港理工大学 | Water base block polyurethane, its preparing method and water-proof, heat insulation and wet permeable material made thereof |
| DE102007023425A1 (en) * | 2007-05-16 | 2008-11-20 | Henkel Ag & Co. Kgaa | Adhering labels on hollow container from e.g. plastic, comprises coating the label with a melt adhesive, adhering the coated label on the container, and filling the container with a filling material before or after the adhering process |
| CN204000466U (en) * | 2014-06-09 | 2014-12-10 | 湖南智谷景城环保装饰材料有限公司 | A kind of wallpaper |
| CN105017982A (en) * | 2015-07-16 | 2015-11-04 | 广东禹能建材科技股份有限公司 | Preparation method of non-asphalt multifunctional waterproof coiled material laminated adhesive |
| CN106273950A (en) * | 2016-08-12 | 2017-01-04 | 夏成余 | Advertisement special glue protecting film and preparation method thereof and automatic double surface gluer |
-
2018
- 2018-08-09 CN CN201810899446.0A patent/CN108913061A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1648145A (en) * | 2004-01-30 | 2005-08-03 | 香港理工大学 | Water base block polyurethane, its preparing method and water-proof, heat insulation and wet permeable material made thereof |
| DE102007023425A1 (en) * | 2007-05-16 | 2008-11-20 | Henkel Ag & Co. Kgaa | Adhering labels on hollow container from e.g. plastic, comprises coating the label with a melt adhesive, adhering the coated label on the container, and filling the container with a filling material before or after the adhering process |
| CN204000466U (en) * | 2014-06-09 | 2014-12-10 | 湖南智谷景城环保装饰材料有限公司 | A kind of wallpaper |
| CN105017982A (en) * | 2015-07-16 | 2015-11-04 | 广东禹能建材科技股份有限公司 | Preparation method of non-asphalt multifunctional waterproof coiled material laminated adhesive |
| CN106273950A (en) * | 2016-08-12 | 2017-01-04 | 夏成余 | Advertisement special glue protecting film and preparation method thereof and automatic double surface gluer |
Non-Patent Citations (1)
| Title |
|---|
| 郭志璜: "透明聚丙烯和透明改进剂", 《精细石油化工进展》 * |
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Application publication date: 20181130 |
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