CN108913028A - glaze and preparation method thereof - Google Patents
glaze and preparation method thereof Download PDFInfo
- Publication number
- CN108913028A CN108913028A CN201810737257.3A CN201810737257A CN108913028A CN 108913028 A CN108913028 A CN 108913028A CN 201810737257 A CN201810737257 A CN 201810737257A CN 108913028 A CN108913028 A CN 108913028A
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- China
- Prior art keywords
- glaze
- drier
- toner
- alkyd resin
- resin
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
- C09D191/005—Drying oils
Abstract
The present invention provides a kind of glazes, by weight percentage, including 6-10wt% alkyd resin, 11-20wt% alkane solvents, 42-52wt% linseed oil resin, 15-20wt% toner, 3-5wt% dispersing agent and 1.5-3wt% drier.Alkyd resin has good thixotropy, slipping and lubricity, can promote wiping and operability, and can toner sufficiently be soaked and be improved storage stability；Linseed oil resin smell is small, and alkyd resin, the interaction of linseed oil resin form one layer of bright film in wood product surface, to highlight the grain effect of wood surface；Toner can provide color effect, dispersing agent can adequately disperse toner, conducive to the uniformity of wood surface color, drier can promote drying property, the drying time of glaze is adjusted by adjusting the content of drier, solve the smell that occurs when NC glaze is used together with wood wax oil greatly, not environmentally, the problems such as room temperature lower drying time is long.
Description
Technical field
The present invention relates to glaze technical fields more particularly to a kind of glaze and preparation method thereof.
Background technique
Wood wax oil can fully penetrate into timber and make the surface of timber in open texture as a kind of environment friendly wood coatings
Effect, it is very popular due to wood wax oil, which is sprayed at different timber, can bring different true senses of touch, and also have
The advantages that not trace is overhauled in construction is simple, part.
To make the surface of woodwork coat color to enhance aesthetic effect, common glaze is mixed together with wood wax oil to be made
With.However, the existing dedicated glaze being used in mixed way that can match with wood wax oil is almost absent, usually select NC glaze with
Wood wax oil is used together, but NC glaze is non-drying type glaze, after being used together with wood wax oil, is not easy drying, and place
It for a long time there are also very heavy smell, causes serious injury to human body, the concept of this and wood wax oil environment-friendly type coating runs in the opposite direction.
Therefore, it is badly in need of inventing a kind of dedicated glaze product of wood wax oil, to overcome NC glaze to make together with wood wax oil
With and the smell that occurs it is big, not environmentally, room temperature lower drying time is long the problems such as.
Summary of the invention
The purpose of the present invention is to provide a kind of glazes and preparation method thereof, to overcome NC glaze together with wood wax oil
Using and the smell that occurs it is big, not environmentally, room temperature lower drying time is long the problems such as.
To achieve the above object, the present invention provides a kind of glazes, by weight percentage, including 6-10wt% alkyd
Resin, 11-20wt% alkane solvents, 42-52wt% linseed oil resin, 15-20wt% toner, 3-5wt% dispersing agent and
1.5-3wt% drier.
A kind of preparation method of glaze is additionally provided, is included the following steps：
(1) alkyd resin is soaked in handle in the alkane solvents of part and mixture A is made；
(2) linseed oil resin is added in mixture A after the completion of step (1), and carries out dispersion milled processed；
(3) dispersing agent and remainder alkane solvents are added after the completion of step (2), and carried out at mixing and dispersion
Reason；
(4) after the completion of step (3), toner is added and carries out dispersion and milled processed；
(5) after the completion of step (4), drier is added and carries out decentralized processing.
Compared with prior art, glaze of the invention contain alkyd resin, alkane solvents, linseed oil resin,
Toner, dispersing agent and drier.Wherein, alkyd resin has good thixotropy, slipping and lubricity, can promote wiping
And operability, and can toner sufficiently be soaked and be improved storage stability；Linseed oil resin smell is small, alkyd resin, Asia
The interaction of edestan oleoresin forms one layer of bright film in wood product surface, to highlight the grain effect of wood surface；
Toner can provide color effect, and dispersing agent can adequately disperse toner, conducive to the uniformity of wood surface color, urge dry
Agent can promote drying property, and the drying time of glaze is adjusted by adjusting the content of drier.
Specific embodiment
For the technology contents that the present invention will be described in detail, construction feature, it is described further below in conjunction with embodiment.
A kind of glaze, by weight percentage, including 6-10wt% alkyd resin, 11-20wt% alkane solvents,
42-52wt% linseed oil resin, 15-20wt% toner, 3-5wt% dispersing agent and 1.5-3wt% drier.Wherein, flax
Benevolence oleoresin can be 45wt%, 48wt%, 42wt%, 52wt%, 44wt%, 47wt%, 46wt%, and alkyd resin can be
6wt%, 10wt%, 7wt%, 8wt%, 6.5wt%, 9wt%, alkane solvents can be 11wt%, 20wt%, 12wt%,
14wt%, 15wt%, 17wt%, toner can be 15wt%, 20wt%, 16wt%, 17wt%, 18wt%, 19wt%, dispersion
Agent can be 3wt%, 5wt%, 4wt%, 4.5wt%, and drier can be 1.5wt%, 3wt%, 2wt%, 2.4wt%.It is right
Drying property and operability are taken into account in the selection of linseed oil, C10-C12 higher boiling can be selected in optional HSDB-512 type linseed oil
Alkane solvent specifically can be space and surpass (trader) ordor removing peace bar powder (reddish brown) as alkane solvent, the preferably organic toner of toner
750/ yellow toner or/black toner 598, the BYK-163 type dispersing agent of the optional Germany Bi Ke production of dispersing agent.Alkyd resin is excellent
It is selected as thixotropy alkyd resin, that is, the alkyd resin containing amide or polyamide structure, the operability of coating can be improved, had
Body can be the MH439 type product of WORLEE (manufacturer).
Preferably, drier is selected from one or both of organic amine drier and organic tin drier.Preferred type
Number be HL-903 organic amine drier, the organotin drier of model T-12.Organic amine drier and organic tin are urged
Dry agent can promote drying property, and the content that can adjust drier adjusts the drying time of glaze.
Preferably, further including 0.5-1wt% anti-settling agent.Anti-settling agent is polyamide-based anti-settling agent, preferably Supreme Being Si Balong
The polyamide-based anti-settling agent of 6900HV type, polyamide-based anti-settling agent can avoid toner precipitating, improve distribution of the toner in glaze
Uniformity.
Preferably, further including 2-5wt% anti skinning agent.The preferred methyl ethyl ketoxime of anti skinning agent, prevents production process high temperature
Cause glaze surface skining.
A kind of preparation method of glaze, includes the following steps：
(1) alkyd resin is soaked in handle in the alkane solvents of part and mixture A is made；
(2) linseed oil resin is added in mixture A after the completion of step (1), and carries out dispersion milled processed；
(3) dispersing agent and remainder alkane solvents are added after the completion of step (2), and carried out at mixing and dispersion
Reason；
(4) after the completion of step (3), toner is added and carries out dispersion and milled processed；
(5) after the completion of step (4), drier is added and carries out decentralized processing.Wherein, in step (1), the part of addition
The weight range that alkane solvents account for total alkane solvents can be 20-80wt%, preferably, alkyd resin is molten with alkanes
The weight ratio of agent is 1:1.
When also containing anti-settling agent and anti skinning agent in the formula of glaze, the preparation method of glaze includes following step
Suddenly：
(1) alkyd resin is soaked in handle in the alkane solvents of part and mixture A is made；
(2) linseed oil resin is added in mixture A after the completion of step (1), and carries out dispersion milled processed；
(3) dispersing agent and remainder alkane solvents are added after the completion of step (2), and carried out at mixing and dispersion
Reason；
(4) after the completion of step (3), toner is added and carries out dispersion and milled processed；
(5) after the completion of step (4), anti-settling agent, drier and anti skinning agent is added and carries out decentralized processing.
Preferably, the weight ratio of alkyd resin and alkane solvents is 1 in step (1):1 and immersion overnight.
Preferably, being ground to 15 μ of fineness < in step (2) and step (4).
It is described in detail below for glaze of the invention and preparation method thereof using embodiment, agents useful for same can
It is obtained from commercially available.
The glaze of embodiment 1-3 and comparative example 1-2 formula are as shown in table 1.
1. embodiment 1-3 of table and comparative example 1-2 glaze formula
The each component of embodiment 2-3 glaze formula is weighed, and is prepared by following glaze preparation method：
A kind of preparation method of glaze, includes the following steps：
(1) alkyd resin is mixed with the alkane solvents for accounting for alkane solvents total weight 30wt%, and carry out every
Mixture A is made in night immersion treatment；Wherein, the weight ratio of alkyd resin and alkane solvents is 1:1；
(2) linseed oil resin is added in mixture A after the completion of step (1), and is carried out at grinding after dispersing 30min
It manages to 15 μ of fineness <；
(3) after the completion of step (2), dispersing agent and residue 70wt% alkane solvents are added, and carry out mixing dispersion
10min；
(4) after the completion of step (3), toner is added and carries out dispersion milled processed to 15 μ of fineness <；
(5) after the completion of step (4), anti-settling agent, drier and anti skinning agent is added and carries out dispersion 20min；
(6) it is packed after taking sample test film qualified in step (5).
Embodiment 1, the preparation method of comparative example 1-2 are similar with embodiment 2-3, are free of when in embodiment 1, comparative example 1-2
There is certain group of timesharing, the component is not added in corresponding step in above-mentioned glaze preparation method.
The each component of embodiment 1-3 glaze formula is pressed to the glaze and comparative example of the preparation of above-mentioned glaze preparation method
1-2, NC glaze carry out smell and drying property test and grain effect characterization.
Smell test method：Curstomer's site operating method is simulated, the glaze and comparative example of packaged embodiment 1-3 are taken
1-2, NC glaze wipe respectively on solid wood material, after 24 hours dry, then seal box are respectively prepared, are then being opened with hand
Jog at mouthful, hears the smell of the gas given out；
Drying property is by standard GB/T/T1728-1979 method test；
Grain effect characterizing method：The glaze and comparative example 1-2, NC glaze of packaged embodiment 1-3 are taken, respectively
It wipes on solid wood material, after 24 hours dry, whether visual observations texture is smooth, natural.
The glaze and comparative example 1-2, NC glaze of 1-3 of embodiment of the present invention preparation carry out smell, drying property and texture
It is as a result as follows after measure of merit：
The glaze and comparative example 1-2, NC glaze the performance test results of 2. embodiment 1-3 of table preparation
| Smell | Drying time | Grain effect | |
| Embodiment 1 | It is small | 24h | It is smooth, natural |
| Embodiment 2 | Very little | 24h | It is smooth, natural |
| Embodiment 3 | Very little | 24h | It is smooth, natural |
| Comparative example 1 | It is small | 24h | It has some setbacks, is unnatural |
| Comparative example 2 | Greatly | 48h | It has some setbacks, is unnatural |
| NC glaze | Greatly | It does not do | It is smooth, natural |
It was found from 2 embodiment 1-3 of the table glaze prepared and comparative example 1-2, NC glaze the performance test results：
1. the glaze of embodiment 1-3 preparation is smaller than the smell of comparative example 2, NC glaze, this is because lattice of the invention
The raw materials such as linseed oil resin, alkane solvents that Li Si selects giving forth fragrance small, and during the preparation process without generating smell
Big substance；
2. the glaze of embodiment 1-3 preparation is shorter than the drying time of comparative example 2, NC glaze, this is because embodiment
1-3 has selected drying property and the appropriate linseed oil resin of operability, and is added to organic amine drier and/or organic
Tin class drier, organic amine drier and organic tin drier can promote the drying property of glaze, shorten drying time；
3. the grain effect of embodiment 1-3 is better than comparative example 1-2 and NC glaze, this is because alkyd resin, flaxseed
Oleoresin interaction forms one layer of bright film on solid wood material surface, to highlight the grain effect of wood surface.
Above disclosed is only the preferred embodiments of the application, and the interest field of the application cannot be limited with this,
Therefore according to equivalent variations made by the claim of this application, the range that the application is covered is belonged to.
Claims (10)
1. a kind of glaze, by weight percentage, which is characterized in that including 6-10wt% alkyd resin, 11-20wt% alkane
Class solvent, 42-52wt% linseed oil resin, 15-20wt% toner, 3-5wt% dispersing agent and 1.5-3wt% drier.
2. glaze according to claim 1, which is characterized in that the alkyd resin is thixotropy alkyd resin.
3. glaze according to claim 1, which is characterized in that the toner is organic toner.
4. glaze according to claim 1, which is characterized in that the drier is selected from organic amine drier and organic
One or both of tin class drier.
5. glaze according to claim 1, which is characterized in that further include 0.5-1wt% anti-settling agent.
6. glaze according to claim 5, which is characterized in that the anti-settling agent is polyamide-based anti-settling agent.
7. glaze according to claim 1, which is characterized in that further include 2-5wt% anti skinning agent.
8. a kind of preparation method of -7 any glazes according to claim 1, which is characterized in that include the following steps：
(1) alkyd resin is soaked in handle in the alkane solvents of part and mixture A is made；
(2) the linseed oil resin is added in the mixture A after the completion of step (1), and carries out dispersion milled processed；
(3) alkane solvents described in the dispersing agent and remainder are added after the completion of step (2), and is mixed and is divided
Dissipate processing；
(4) after the completion of step (3), the toner is added and carries out dispersion and milled processed；
(5) after the completion of step (4), the drier is added and carries out decentralized processing.
9. the preparation method of glaze according to claim 8, which is characterized in that alkyd resin described in step (1) with
The weight ratio of the alkane solvents is 1:1 and immersion overnight.
10. the preparation method of glaze according to claim 8, which is characterized in that grinding in step (2) and step (4)
To 15 μ of fineness <.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810737257.3A CN108913028A (en) | 2018-07-06 | 2018-07-06 | glaze and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810737257.3A CN108913028A (en) | 2018-07-06 | 2018-07-06 | glaze and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108913028A true CN108913028A (en) | 2018-11-30 |
Family
ID=64424942
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810737257.3A Pending CN108913028A (en) | 2018-07-06 | 2018-07-06 | glaze and preparation method thereof |
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| CN102408828A (en) * | 2011-09-29 | 2012-04-11 | 刘光君 | Nano silicon dioxide modified hard wood wax oil and preparation method thereof |
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Application publication date: 20181130 |
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