CN108892587A - A kind of selenium-enriched fertilizer of glycosidase containing nucleotide - Google Patents
A kind of selenium-enriched fertilizer of glycosidase containing nucleotide Download PDFInfo
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- CN108892587A CN108892587A CN201810926375.9A CN201810926375A CN108892587A CN 108892587 A CN108892587 A CN 108892587A CN 201810926375 A CN201810926375 A CN 201810926375A CN 108892587 A CN108892587 A CN 108892587A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B15/00—Organic phosphatic fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
Abstract
The present invention relates to a kind of selenium-enriched fertilizers of glycosidase containing nucleotide, are by following weight percent meter：Nucleotide 15~35%, glycosidase 8~10%, glucose 15~20%, glycerine 8~15%, sodium selenite 10~15%, rare earth 3~10% and surplus are made of water, total amount is 100%, wherein, first nucleotide, glycosidase are poured into and are placed in the water in reaction kettle, at 30-50 DEG C, glucose is added in stirring, after 2-4 hours, at 30-50 DEG C, sodium selenite is added in stirring, stirs 2 hours, and rare earth is added in 30-50 DEG C of stirring, after stirring 2~3 hours are sufficiently complexed, at 18-25 DEG C, glycerine is added in stirring for cooling, stirs 2-3 hours to obtain the final product；The method of the present invention is simple, abundant raw material, preparation easy to produce, and application is convenient, and effect is good, and nutrition is high, and crop good absorbing, quality are good, are the innovations on crops selenium-supply fertilizer, there is significant economic and social benefit.
Description
Technical field
The present invention relates to fertilizer, especially a kind of selenium-enriched fertilizer of glycosidase containing nucleotide.
Background technique
Selenium is one of the essential trace elements of the human body, with ability that is anti-oxidant and delaying senescence, but selenium element
Supplement, selenium element is not innately to be present in food, and current selenium-rich product is all by fertilising, and crop inhales during the growth process
It receives the fertilizer of selenium element and produces.Currently, southern area rice is low containing selenium, selenium deficiency assists human health prestige extremely serious.
Southern some places major part place be selenium deficiency area, liver cancer, lung cancer, intestinal cancer and breast cancer etc. with local people's diet selenium deficiency
It is related.So selenium-supply is of great significance for improving people's health level.According to statistics, 42, whole world countries and regions lack
Selenium.China there are about 2/3 degree selenium deficiency from different places, wherein 1/3 is serious Selenium deficiency area, shows according to investigations from northeast to southwest,
Yangtze River Delta soil selenium-containing amount is generally lower, is 0.20~0.40 micro- g kg.It can not grow selenium-rich in the soil of poor selenium
Food can not obtain enough selenium from common food.Crop can only obtain in the fertilizer containing selenium element.Because it can be to prevent
It treats constipation, enteritis, the carcinoma of the rectum, protects eyes, prevent heart disease and cancer, this has become the common recognition of people's health care.Selenium is not day
So existing in things, is to absorb the selenium in soil by crop to realize, crop will apply fertilizer, therefore, selenium-rich water-soluble fertilizer
Research has great importance, but so far there are no really the open of the good selenium-enriched fertilizer of effect is reported.
Summary of the invention
For above situation, for the defect for overcoming the prior art, the purpose of the present invention is just to provide a kind of containing nucleotide sugar
Glycosides enzyme selenium-enriched fertilizer, can effectively solve selenium be absorbed more directly, faster, be easier to conversion, utilization rate is higher, protects environment not dirty
The problem of dye.
The technical solution that the present invention solves is that a kind of selenium-enriched fertilizer of glycosidase containing nucleotide, is by following weight percent
Meter：Nucleotide 15~35%, glycosidase 8~10%, glucose 15~20%, glycerine 8~15%, sodium selenite 10~
15%, rare earth 3~10% and surplus are made of water, total amount 100%, wherein first pour into nucleotide, glycosidase and be placed in reaction
In water in kettle, at 30-50 DEG C, glucose is added in stirring, and after 2-4 hours, at 30-50 DEG C, sodium selenite is added in stirring,
Stirring 2 hours is added rare earth after stirring 2~3 hours are sufficiently complexed in 30-50 DEG C of stirring and cools down at 18-25 DEG C, and stirring adds
Enter glycerine, stir 2-3 hours to obtain the final product；The glycosidase is：Mannosidase, xylosidase, glucuronidase
One or more kinds of mixtures are made；The nucleotide is atriphos, uridine triphosphate, cytidine, three phosphorus
The mixture of the weight ratios such as one or more of sour guanosine.
The method of the present invention is simple, abundant raw materials, preparation easy to produce, and application is convenient, and effect is good, and nutrition is high, and crop absorbs
Well, quality is good, is the innovation on crops selenium-supply fertilizer, there is significant economic and social benefit.
Specific embodiment
It elaborates with reference to embodiments with concrete condition to a specific embodiment of the invention.
The present invention can be provided in specific implementation by following embodiment：
Embodiment 1
One kind selenium-enriched fertilizer of glycosidase containing nucleotide of the invention, is by following weight percent meter：Nucleotide 20~
30%, glycosidase 8.5~9%, glucose 16~18%, glycerine 10~12%, sodium selenite 11~13%, rare earth 5~8%
It is made with surplus of water, total amount 100%, wherein first nucleotide, glycosidase are poured into and are placed in the water in reaction kettle, in 30-
At 50 DEG C, glucose is added in stirring, and after 2-4 hours, at 30-50 DEG C, sodium selenite is added in stirring, is stirred 2-3 hours,
Rare earth is added in 30-50 DEG C of stirring, stirs 2~3 hours after being sufficiently complexed, cools down at 18-25 DEG C, and glycerine is added in stirring, stirs
Mix 2-3 hours to obtain the final product.
Embodiment 2
One kind selenium-enriched fertilizer of glycosidase containing nucleotide of the invention, is by following weight percent meter：Mannosidase
25%, glucose 9%, glycerine 17%, nucleotide 11%, sodium selenite 12%, rare earth 6% and surplus are made of water, wherein
First nucleotide, glycosidase are poured into and are placed in the water in reaction kettle, at 40 DEG C, glucose is added in stirring, after 3 hours, 40
At DEG C, stirring addition sodium selenite is stirred 2 hours, and rare earths are added in 40 DEG C of stirrings, stir 2.5 hours after being sufficiently complexed, cooling
At 21 DEG C, glycerine is added in stirring, stirs 2.5 hours to obtain the final product.
Embodiment 3
One kind selenium-enriched fertilizer of glycosidase containing nucleotide of the invention, is by following weight percent meter：Mannosidase
8%, glucose 8%, glycerine 10%, nucleotide 15%, sodium selenite 15%, rare earth 4% and surplus are made of water, wherein
First nucleotide, glycosidase are poured into and are placed in the water in reaction kettle, at 30 DEG C, glucose is added in stirring, after 2 hours, 30
At DEG C, stirring addition sodium selenite is stirred 2 hours, and rare earths are added in 30 DEG C of stirrings, stir 2 hours after being sufficiently complexed, cooling exists
At 185 DEG C, glycerine is added in stirring, stirs 2 hours to obtain the final product.
Embodiment 4
Present invention one kind selenium-enriched fertilizer of glycosidase containing nucleotide, is by following weight percent meter：Mannosidase
5%, xylosidase 5%, glucose 20%, glycerine 15%, nucleotide 15%, sodium selenite 10%, rare earth 10% and surplus
It is made of water, wherein first mannosidase, xylosidase, nucleotide are poured into and are placed in the water in reaction kettle, at 30 DEG C,
Glucose is added in stirring, and after 3 hours, at 40 DEG C, sodium selenite is added in stirring, is stirred 2 hours, is added in 40 DEG C of stirrings dilute
Soil is stirred 2.5 hours and is mixed, and at 22 DEG C, glycerine is added in stirring, stirs 2.5 hours to obtain the final product.
Embodiment 5
Present invention one kind selenium-enriched fertilizer of glycosidase containing nucleotide, is by following weight percent meter：Mannosidase
3%, xylosidase 3%, glucuronidase 3%, glucose 9%, glycerine 15%, nucleotide 15%, sodium selenite
15%, rare earth 8% and surplus are made of water, wherein first by mannosidase, xylosidase, glucuronidase, nucleotide
It pours into and is placed in the water in reaction kettle respectively, at 30 DEG C, glucose is added in stirring, and after 4 hours, at 50 DEG C, stirring is added
Sodium selenite stirs 2 hours, and rare earth is added in 50 DEG C of stirrings, stirs 3 hours and mixes, and at 18 DEG C, glycerine is added in stirring,
Stir 3 hours to obtain the final product.
Embodiment 6
Present invention one kind selenium-enriched fertilizer of glycosidase containing nucleotide, is by following weight percent meter：Adenosine triphosphate
Glycosides 6%, guanosine triphosphate 1%, uridine triphosphate 6%, cytidine 2%, mannosidase 5%, glucose 20%, the third three
Alcohol 15%, sodium selenite 15%, rare earth 5% and surplus are made of water, wherein first pour into nucleotide, glycosidase and be placed in reaction
In water in kettle, at 30 DEG C, glucose is added in stirring, and after 2 hours, at 40 DEG C, sodium selenite is added in stirring, and stirring 2 is small
When, rare earth is added in 40 DEG C of stirrings, stirs 3 hours after being sufficiently complexed, cools down at 20 DEG C, glycerine is added in stirring, and stirring 2 is small
When to obtain the final product.
Embodiment 7
Present invention one kind selenium-enriched fertilizer of glycosidase containing nucleotide, is by following weight percent meter：Atriphos
11%, uridine triphosphate 7%, cytidine 7%, mannosidase 2%, xylosidase 3%, glucuronidase 3%,
Glucose 12%, glycerine 15%, sodium selenite 10%, rare earth 10% and surplus are made of water, wherein first by nucleotide, sugar
Glycosides enzyme, which pours into, to be placed in the water in reaction kettle, and at 30 DEG C, glucose is added in stirring, and after 2 hours, at 50 DEG C, stirring is added
Sodium selenite stirs 2 hours, and rare earth is added in 50 DEG C of stirrings, stirs 3 hours after being sufficiently complexed, cools down at 20 DEG C, stirring is added
Glycerine stirs 2 hours to obtain the final product.
Component of the present invention is scientific and reasonable, and abundant raw material, preparation method is simple, easy to produce, and total content is up to 60-80%, makes
Good with effect, through on probation, content is high, enhances photosynthesis, improves enzymatic activity, easily absorbs, and crop product is had using healthy and safe
Significant economic and social benefit, and through site test and application, effect is very good, and relevant information is as follows：
Laboratory report：
The competition of food products market, mankind's dietary intake turn to " healthy epoch " from " quantity epoch ".Food
Safety, health is the important indicator of fruit quality.Under same weather conditions, the present invention is continuously from 2015-2017, and continuous 3
Year applies rice, peanut, wheat, fruit tree, tea tree, 10 mu of experimental plot, wherein 5 mu of contrast groups, and 5 mu of test group on probation, comparison
Group selenium-enriched fertilizer on the market, the test group present invention.
One, agricultural product selenium-rich situation
Cereal crops technique of enriched selenium is mature, can accurately reach 0.1mg/kg or more.
Two, increase production situation：For the general amount of increase in production of rice, wheat in 10%-18%, peanut generally increases production 10%-15%,
Fruit tree generally increases production 10%-15%.
1, it is passed through in Henan somewhere within 2015 and product of the present invention is used to rice, application method is：In tillering stage, the jointing stage,
Pustulation period respectively sprays once, increasing production of rice 17.28%.
2, it is passed through in Hunan Province two places within 2016 and product of the present invention is used to hybrid rice, application method is：In tillering stage,
Jointing stage, pustulation period respectively spray once, increase production 10.7% and 11.8% respectively.
3, product of the present invention is used to rice in Heilungkiang somewhere within 2017, application method is：In rice plant of tillering stage, jointing
Phase, pustulation period respectively spray once, and per mu yield reaches 640 kilograms.
4, product of the present invention is used to winter wheat (peaceful winter No. 10) in Ningxia somewhere within 2017, application method is：In wheat
Tillering stage, the jointing stage, the pustulation period respectively sprays once, increases production 11.18%-12.66%.
Three, degradation heavy metal situation
1, it is tested in somewhere hybrid rice early rice selenium-rich within 2016, lead, cadmium, mercury content decline in various degree：
Somewhere hybrid rice early rice selenium-rich test in 2016, lead, cadmium, mercury content decline in various degree：
2, the tea plantation of Henan in 2016 is tested using selenium-rich of the present invention, lead content decline 9.3%.
Four, amino acid content improves：The 11 kinds of amino acid content summations of somewhere rice test in 2015 improve 2.1%, wherein
Lysine increases by 5.5%, and cysteine increases by 5.3%.
Apple uses test report of the present invention：
Selenium element is improved in order to verify the present invention in apple, the application effect to the appearance and quality that change apple, simultaneously
Also scientific basis is provided to widely popularize product of the present invention, spy carries out the test of field collunarium, and test is summarized as follows now.
Experimental field：
Henan apple base, the Fuji apple of life in 8 years, management level are preferable.Soil selenium deficiency.
Planning experiment：
The present invention applies ground, and (12-15 day April) sprays 600 times of liquid of the present invention before spending respectively, (the May 3- that spends latter 7-10 days
7 days), (23-27 days May), expanding stage (12-15 days July), preceding 20 days of harvesting (September 24-27 day) are distinguished 400 liquid and are sprayed before bagging
It applies, compares field not Spraying Se-fertilizer.
Interpretation of result：
1. the present invention can effectively improve fruit-setting rate to spraying before spending, inflorescence fruit-setting rate improves 30% or more, and flower is beared fruit
Rate improves 23% or more.The blinds fresh weight on blade face is improved from blade face, the blinds fresh weight of long shoot respectively increases 20g, enhances
Photosynthesis, the spring tip also significantly improved stop long rate, stop long rate and improve 24%, can reduce the loss of nutrient, are conducive to spend
The formation of bud.
2. the present invention can improve the longitudinal and transverse demeter of fruit, be conducive to expanding for fruit, improve fruit shape index, complete red rate increases
26%, pericarp is bright and clean, and hardness obviously increases, and is conducive to store, and single fruit weight increases 89g/ mus, and the output of milk increases 726kg.It is better than
Compare field.
3. the apple selenium that the present invention uses is detected as 0.043mg/Kg, content meets national standard.Quality is greatly improved, fruit
Garden volume increase, increasing benefit are significant.
Product of the present invention is nontoxic, without hormone.Its non-toxic test situation is as follows：
One, test objective
Product of the present invention toxic effect situation by oral administration is understood by test.
Two, material and method
1, tested material：The present invention is brown liquid, specific gravity 1.2887.
2, experimental animal：SD rat 40, weight 182-196g provided by experimental animal center of henan province, male and female are each
Half, it is in a good state of health, and quarantine one week on this basis.
3, animal packet and dosage：Using HornShi method, with 2.15 multiple proportions relational design dosage groups.After experimental animal weighing
It is randomly divided into four groups, every group female, male each 5.
4, test operation step：Experimental animal fasting overnight, drug are made into suspension with distilled water, and stomach-filling amount presses 1.0ml/
100g weight, primary oral stomach-filling, is observed 2 weeks, and record animal shows situation.
5, evaluation of result：According to the animal dead situation of each dosage group of mouse female, great and mighty or powerful, using HornShi method find out LD50 and
Its 95% credibility interval.According to People's Republic of China's pesticide acute toxicity grading criteria (GB15670-1995), to tested
Object makes acute toxicity classification.
Three, test result
Dosage grouping and test result see the table below, because dosage 5000mg/kg weight group is female, mouse great and mighty or powerful is without death, therefore its
Remaining each group test does not carry out again.
From upper table confirm, mouse female, great and mighty or powerful by oral administration after without obvious poisoning symptom, rat is without death in the observation period.
Four, conclusion
Product of the present invention is greater than 5050mg/kg weight to male rat and female rats by oral administration, situation without exception, therefore root
According to National Standard of the People's Republic of China《Agriculture chemical registration toxicology test method》(GB15670-1995) pesticide acute oral in
Toxicity grading standard, it is safe and reliable the invention belongs to hypotoxicity or nontoxicity, improve soil, high yield good harvest, crops increase
10%-18% is produced, it is the big innovation on selenium-supply fertilizer that fruit tree fruit-setting rate, which improves 30% or more, and economic and social benefit is aobvious
It writes.
Claims (8)
1. a kind of selenium-enriched fertilizer of glycosidase containing nucleotide, it is characterized in that：It is by following weight percent meter：Nucleotide 15~
35%, glycosidase 8~10%, glucose 15~20%, glycerine 8~15%, sodium selenite 10~15%, rare earth 3~10% and surplus
It is made of water, total amount 100%, wherein first nucleotide, glycosidase are poured into and are placed in the water in reaction kettle, at 30-50 DEG C,
Glucose is added in stirring, and after 2-4 hours, at 30-50 DEG C, sodium selenite is added in stirring, stirs 2 hours, stirs at 30-50 DEG C
Addition rare earth is mixed, stirs 2~3 hours after being sufficiently complexed, cools down at 18-25 DEG C, glycerine is added in stirring, stirs 2-3 hours
To obtain the final product；The glycosidase is：Mannosidase, xylosidase, glucuronidase one or more kinds of mixtures
It is made；The nucleotide is one or both of atriphos, uridine triphosphate, cytidine, guanosine triphosphate
With the mixture of first-class weight ratio.
2. the selenium-enriched fertilizer of glycosidase containing nucleotide according to claim 1, it is characterized in that：It is by following weight percent meter
's：Nucleotide 20~30%, glycosidase 8.5~9%, glucose 16~18%, glycerine 10~12%, sodium selenite 11~13% are dilute
Soil 5~8% and surplus are made of water, total amount 100%, wherein nucleotide, glycosidase are first poured into the water being placed in reaction kettle
In, at 30-50 DEG C, glucose is added in stirring, and after 2-4 hours, at 30-50 DEG C, sodium selenite is added in stirring, stirs 2-3
Hour, rare earth is added in 30-50 DEG C of stirring, stirs 2~3 hours after being sufficiently complexed, cools down at 18-25 DEG C, stirring is added third
Triol stirs 2-3 hours to obtain the final product.
3. the selenium-enriched fertilizer of glycosidase containing nucleotide according to claim 1, it is characterized in that：It is by following weight percent meter
's：Mannosidase 25%, glucose 9%, glycerine 17%, nucleotide 11%, sodium selenite 12%, rare earth 6% and surplus are water system
At, wherein first nucleotide, glycosidase are poured into and are placed in the water in reaction kettle, at 40 DEG C, stirring addition glucose, 3 hours
Afterwards, at 40 DEG C, sodium selenite is added in stirring, is stirred 2 hours, and rare earth is added in 40 DEG C of stirrings, stirs 2.5 hours abundant networks
After conjunction, cool down at 21 DEG C, glycerine is added in stirring, stirs 2.5 hours to obtain the final product.
4. the selenium-enriched fertilizer of glycosidase containing nucleotide according to claim 1, it is characterized in that：It is by following weight percent meter
's：Mannosidase 8%, glucose 8%, glycerine 10%, nucleotide 15%, sodium selenite 15%, rare earth 4% and surplus are water system
At, wherein first nucleotide, glycosidase are poured into and are placed in the water in reaction kettle, at 30 DEG C, stirring addition glucose, 2 hours
Afterwards, at 30 DEG C, sodium selenite is added in stirring, is stirred 2 hours, and rare earth is added in 30 DEG C of stirrings, stirs sufficiently complexing in 2 hours
Afterwards, at 185 DEG C, glycerine is added in stirring for cooling, stirs 2 hours to obtain the final product.
5. the selenium-enriched fertilizer of glycosidase containing nucleotide according to claim 1, it is characterized in that：It is by following weight percent meter
's：Mannosidase 5%, xylosidase 5%, glucose 20%, glycerine 15%, nucleotide 15%, sodium selenite 10%, rare earth 10%
It is made with surplus of water, wherein first mannosidase, xylosidase, nucleotide are poured into and are placed in the water in reaction kettle, 30
At DEG C, stirring addition glucose, after 3 hours, at 40 DEG C, sodium selenite is added in stirring, is stirred 2 hours, is added in 40 DEG C of stirrings
Enter rare earth, stir 2.5 hours and mix, at 22 DEG C, glycerine is added in stirring, stirs 2.5 hours to obtain the final product.
6. the selenium-enriched fertilizer of glycosidase containing nucleotide according to claim 1, it is characterized in that：It is by following weight percent meter
's：Mannosidase 3%, xylosidase 3%, glucuronidase 3%, glucose 9%, glycerine 15%, nucleotide 15%, sub- selenium
Sour sodium 15%, rare earth 8% and surplus are made of water, wherein first by mannosidase, xylosidase, glucuronidase, nucleosides
Acid pours into respectively to be placed in the water in reaction kettle, and at 30 DEG C, glucose is added in stirring, and after 4 hours, at 50 DEG C, stirring adds
Enter sodium selenite, stir 2 hours, rare earths are added in 50 DEG C of stirrings, stirs 3 hours and mixes, at 18 DEG C, stirring addition the third three
Alcohol stirs 3 hours to obtain the final product.
7. the selenium-enriched fertilizer of glycosidase containing nucleotide according to claim 1, it is characterized in that：It is by following weight percent meter
's：Atriphos 6%, guanosine triphosphate 1%, uridine triphosphate 6%, cytidine 2%, mannosidase 5%, glucose
20%, glycerine 15%, sodium selenite 15%, rare earth 5% and surplus are made of water, wherein first pour into nucleotide, glycosidase and be placed in
In water in reaction kettle, at 30 DEG C, glucose is added in stirring, and after 2 hours, at 40 DEG C, sodium selenite, stirring is added in stirring
2 hours, rare earth is added in 40 DEG C of stirrings, stirs 3 hours after being sufficiently complexed, cools down at 20 DEG C, glycerine, stirring is added in stirring
2 hours to obtain the final product.
8. the selenium-enriched fertilizer of glycosidase containing nucleotide according to claim 1, it is characterized in that：It is by following weight percent meter
's：Atriphos 11%, uridine triphosphate 7%, cytidine 7%, mannosidase 2%, xylosidase 3%, glucuronic acid
Glycosides enzyme 3%, glucose 12%, glycerine 15%, sodium selenite 10%, rare earth 10% and surplus are made of water, wherein first by nucleotide,
Glycosidase, which pours into, to be placed in the water in reaction kettle, and at 30 DEG C, glucose is added in stirring, and after 2 hours, at 50 DEG C, stirring adds
Enter sodium selenite, stir 2 hours, 50 DEG C of stirrings are added rare earth and cool down at 20 DEG C after stirring 3 hours are sufficiently complexed, and stirring adds
Enter glycerine, stir 2 hours to obtain the final product.
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| CN112110766A (en) * | 2020-09-22 | 2020-12-22 | 烟台天晟农业科技有限公司 | Application of guanosine triphosphate in agriculture |
| CN114456007A (en) * | 2022-02-25 | 2022-05-10 | 郑州盛润生物质能源化工研究院 | Compound phosphorus-potassium coloring sugar-increasing fertilizer and preparation method thereof |
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