CN108864501A - A kind of antibacterial moisture-proof emgloves - Google Patents
A kind of antibacterial moisture-proof emgloves Download PDFInfo
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- CN108864501A CN108864501A CN201810812853.3A CN201810812853A CN108864501A CN 108864501 A CN108864501 A CN 108864501A CN 201810812853 A CN201810812853 A CN 201810812853A CN 108864501 A CN108864501 A CN 108864501A
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- parts
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- emgloves
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- antibacterial moisture
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L7/00—Compositions of natural rubber
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/16—Halogen-containing compounds
- C08K2003/162—Calcium, strontium or barium halides, e.g. calcium, strontium or barium chloride
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2296—Oxides; Hydroxides of metals of zinc
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of antibacterial moisture-proof emgloves, by the way that 3-6 parts of wheat bran albumen, 2-6 parts of Chloranthus glaber fiber, 4-8 parts of arghan, 10-14 parts of gelatin are added in the conventional formulation to emgloves, utilize the distinctive moisture absorption and restraining and sterilizing bacteria function of wheat bran albumen, three kinds of Chloranthus glaber fiber, arghan materials, with optimum proportion, it is added to preparing for emgloves to go in raw material and gelatin collective effect, the gloves prepared, compared with prior art：With more preferably moisture absorption moisture-proof function, bacteriostasis is obvious, and is easy to get using raw material, low in cost.
Description
Technical field
The present invention relates to the preparation fields of emgloves, more particularly to a kind of preparation method of antibacterial moisture-proof emgloves.
Background technique
Safety of the gloves due to barrier protection effect, can be good at protecting user, has been widely used
In the production and living of people.According to the difference of its purposes, medical gloves, industrial gloves and domestic purpose gloves can be divided into.Mesh
Before, the rubber gloves including medical is easy to dress when hand is dry, but is not easy when hand is moist or has water mark
Wearing；Especially through wearing after a period of time, hand is perspired, and gloves glue hand, will affect the wearing comfort of medical personnel.
Although there are the gloves of wet hand easy donning in foreign countries, but it is by deepening chlorination degree, in the side of internal layer plus hydrogel
Method, since chlorination is excessive, leverages the physical property and Storage period of gloves come what is realized.Gloves are due to its own substance
For the nutrition of bacterium, so easily causing the growth and procreation of bacterium or microorganism.Simultaneously because hand is perspired, can also increase
The breeding of refinement bacterium increases the danger of doctor and patient's infectious disease.Currently, usually being added into glove substrate a certain amount of
Antibacterial material or composition, but these substances itself and glove substrate material intermiscibility are poor, are easy dissolution, and antibacterial timeliness has
Limit or antibacterial ability itself be not strong, cannot effectively inhibit various pathogen.Some antibacterial materials are more toxic, and are had to human body latent
It is endangering.
Based on this, if a kind of emgloves for having both sweat absorption and moisture and bacteria resistance function can be provided, it will solve the above problems.
Summary of the invention
Goal of the invention：In order to solve the problems of prior art, the present invention provides one kind to have both sweat absorption and moisture, excellent
The antibacterial moisture-proof emgloves of different bacteriostasis property.
Technical solution：In order to achieve the above objectives, the technical scheme is that：A kind of antibacterial moisture-proof emgloves, including
It is following calculated by mass to prepare raw material：60-70 parts of natural rubber, 0.5-1.2 parts of sulphur, 0.5-0.8 parts of zinc oxide, potassium sulfate
0.5-1.5 parts, 4-8 parts of calcium chloride, 0.6-0.8 parts of N- ethyl, N-phenyl zinc dithiocarbamate, 0.2-0.5 parts of diphenylguanidine,
0.3-0.6 parts of hydroquinone dibenzyl ether, 0.3-0.6 parts of 2- sulfenyl benzimidazole, 4-6 parts of superfine silica gel powder, microcrystalline cellulose 4-6
Part, 60-80 parts of water；It further include 3-6 parts of wheat bran albumen, 2-6 parts of Chloranthus glaber fiber, 4-8 parts of arghan, 10-14 parts of gelatin.
Further, the extracting method of the wheat bran albumen is：10-20 times of lye is added into wheat bran, mentions
1.5h is taken, Extracting temperature is 60 DEG C, and protease is added afterwards, and enzyme-to-substrate ratio is 1%, continues to extract 1h, Extracting temperature is reduced to
It 50 DEG C, extracts pH and maintains 7.5.
Further, the extraction process of the wheat bran carries out in Vltrasonic device, and supersonic frequency is set as 50-
60Hz。
Further, the extracting method of the Chloranthus glaber fiber is：With 5:1 mass ratio takes Chloranthus glaber blade, careless coral
Coral root, clean crush mixed powder minces, to mixed powder mince it is middle 10-20 times of dehydrated alcohol is added, extraction time is
1.5h, Extracting temperature are 80 DEG C, and the rear acetic acid that liquor capacity 20% is added continues to extract 2h, and Extracting temperature is reduced to 60 DEG C.
Further, the extraction process of the Chloranthus glaber fiber carries out in Vltrasonic device, and supersonic frequency is set as 55-
65Hz。
Further, the extracting method of the arghan is：Pineapple leaves are taken, cleans and crushes, middle 10-20 times of addition
Dehydrated alcohol, extraction time 2.5h, Extracting temperature is 70 DEG C, and the rear hydrogen peroxide that liquor capacity 10% is added continues to extract
1h, Extracting temperature are reduced to 60 DEG C.
Further, the extraction process of the arghan carries out in Vltrasonic device, and supersonic frequency is set as 80-
90Hz。
Further, the gelatin is made using acid treatment.
Beneficial effect：The antibacterial moisture-proof emgloves of one kind provided by the present invention, compared with prior art：With more preferably
Moisture absorption moisture-proof function, bacteriostasis is obvious, and is easy to get using raw material, low in cost.
Specific embodiment
Below with reference to embodiment, invention is further described in detail：
Embodiment 1：
A kind of antibacterial moisture-proof emgloves calculated by mass prepares raw material including following：60 parts of natural rubber, sulphur
0.5 part, 0.5 part of zinc oxide, 0.5 part of potassium sulfate, 4 parts of calcium chloride, 0.6 part of N- ethyl, N-phenyl zinc dithiocarbamate, two
0.2 part of benzene guanidine, 0.3 part of hydroquinone dibenzyl ether, 0.3 part of 2- sulfenyl benzimidazole, 4 parts of superfine silica gel powder, 4 parts of microcrystalline cellulose,
60 parts of water；It further include 3 parts of wheat bran albumen, 2 parts of Chloranthus glaber fiber, 4 parts of arghan, 10 parts of gelatin.
Wherein, the extracting method of the wheat bran albumen is：10 times of lye is added into wheat bran, extracts 1.5h, mentions
Taking temperature is 60 DEG C, and protease is added afterwards, and enzyme-to-substrate ratio is 1%, continues to extract 1h, and Extracting temperature is reduced to 50 DEG C, extracts
PH maintains 7.5；The extraction process of the wheat bran carries out in Vltrasonic device, and supersonic frequency is set as 50Hz；The grass
The extracting method of coral fiber is：With 5:1 mass ratio takes Chloranthus glaber blade, Chloranthus glaber root, cleans and crushes to obtain co-grinding
Object, to mixed powder mince it is middle 10 times of dehydrated alcohol is added, extraction time 1.5h, Extracting temperature is 80 DEG C, and solution is added afterwards
The acetic acid of volume 20% continues to extract 2h, and Extracting temperature is reduced to 60 DEG C；The extraction process of the Chloranthus glaber fiber is filled in ultrasound
Middle progress is set, supersonic frequency is set as 55Hz；The extracting method of the arghan is：Take pineapple leaves, clean crush, in plus
Entering 10 times of dehydrated alcohol, extraction time 2.5h, Extracting temperature is 70 DEG C, the rear hydrogen peroxide that liquor capacity 10% is added, after
Continuous to extract 1h, Extracting temperature is reduced to 60 DEG C；The extraction process of the arghan carries out in Vltrasonic device, supersonic frequency
It is set as 80Hz；The gelatin is made using acid treatment.
Embodiment 2：
A kind of antibacterial moisture-proof emgloves calculated by mass prepares raw material including following：70 parts of natural rubber, sulphur
1.2 parts, 0.8 part of zinc oxide, 1.5 parts of potassium sulfate, 8 parts of calcium chloride, 0.8 part of N- ethyl, N-phenyl zinc dithiocarbamate, two
0.5 part of benzene guanidine, 0.6 part of hydroquinone dibenzyl ether, 0.6 part of 2- sulfenyl benzimidazole, 6 parts of superfine silica gel powder, 6 parts of microcrystalline cellulose,
60-80 parts of water；It further include 6 parts of wheat bran albumen, 6 parts of Chloranthus glaber fiber, 8 parts of arghan, 14 parts of gelatin.
Wherein, the extracting method of the wheat bran albumen is：20 times of lye is added into wheat bran, extracts 1.5h, mentions
Taking temperature is 60 DEG C, and protease is added afterwards, and enzyme-to-substrate ratio is 1%, continues to extract 1h, and Extracting temperature is reduced to 50 DEG C, extracts
PH maintains 7.5；The extraction process of the wheat bran carries out in Vltrasonic device, and supersonic frequency is set as 60Hz；The grass
The extracting method of coral fiber is：With 5:1 mass ratio takes Chloranthus glaber blade, Chloranthus glaber root, cleans and crushes to obtain co-grinding
Object, to mixed powder mince it is middle 20 times of dehydrated alcohol is added, extraction time 1.5h, Extracting temperature is 80 DEG C, and solution is added afterwards
The acetic acid of volume 20% continues to extract 2h, and Extracting temperature is reduced to 60 DEG C；The extraction process of the Chloranthus glaber fiber is filled in ultrasound
Middle progress is set, supersonic frequency is set as 65Hz；The extracting method of the arghan is：Take pineapple leaves, clean crush, in plus
Entering 20 times of dehydrated alcohol, extraction time 2.5h, Extracting temperature is 70 DEG C, the rear hydrogen peroxide that liquor capacity 10% is added, after
Continuous to extract 1h, Extracting temperature is reduced to 60 DEG C；The extraction process of the arghan carries out in Vltrasonic device, supersonic frequency
It is set as 90Hz；The gelatin is made using acid treatment.
Embodiment 3：
A kind of antibacterial moisture-proof emgloves calculated by mass prepares raw material including following：65 parts of natural rubber, sulphur
0.8 part, 0.6 part of zinc oxide, 0.9 part of potassium sulfate, 6 parts of calcium chloride, 0.7 part of N- ethyl, N-phenyl zinc dithiocarbamate, two
0.3 part of benzene guanidine, 0.5 part of hydroquinone dibenzyl ether, 0.4 part of 2- sulfenyl benzimidazole, 5 parts of superfine silica gel powder, 5 parts of microcrystalline cellulose,
70 parts of water；It further include 4 parts of wheat bran albumen, 4 parts of Chloranthus glaber fiber, 6 parts of arghan, 12 parts of gelatin.
Wherein, the extracting method of the wheat bran albumen is：15 times of lye is added into wheat bran, extracts 1.5h, mentions
Taking temperature is 60 DEG C, and protease is added afterwards, and enzyme-to-substrate ratio is 1%, continues to extract 1h, and Extracting temperature is reduced to 50 DEG C, extracts
PH maintains 7.5；The extraction process of the wheat bran carries out in Vltrasonic device, and supersonic frequency is set as 55Hz；The grass
The extracting method of coral fiber is：With 5:1 mass ratio takes Chloranthus glaber blade, Chloranthus glaber root, cleans and crushes to obtain co-grinding
Object, to mixed powder mince it is middle 15 times of dehydrated alcohol is added, extraction time 1.5h, Extracting temperature is 80 DEG C, and solution is added afterwards
The acetic acid of volume 20% continues to extract 2h, and Extracting temperature is reduced to 60 DEG C；The extraction process of the Chloranthus glaber fiber is filled in ultrasound
Middle progress is set, supersonic frequency is set as 60Hz；The extracting method of the arghan is：Take pineapple leaves, clean crush, in plus
Entering 15 times of dehydrated alcohol, extraction time 2.5h, Extracting temperature is 70 DEG C, the rear hydrogen peroxide that liquor capacity 10% is added, after
Continuous to extract 1h, Extracting temperature is reduced to 60 DEG C；The extraction process of the arghan carries out in Vltrasonic device, supersonic frequency
It is set as 85Hz；The gelatin is made using acid treatment.
Comparative example 1：
Remaining is identical as 3 embodiment of embodiment, formula be include following calculated by mass preparing raw material：Natural rubber
65 parts, 0.8 part of sulphur, 0.6 part of zinc oxide, 0.9 part of potassium sulfate, 6 parts of calcium chloride, N- ethyl, N-phenyl aminodithioformic acid
0.7 part of zinc, 0.3 part of diphenylguanidine, 0.5 part of hydroquinone dibenzyl ether, 0.4 part of 2- sulfenyl benzimidazole, 5 parts of superfine silica gel powder, crystallite
5 parts of cellulose, 70 parts of water.
Comparative example 2：
Remaining is identical as 3 embodiment of embodiment, formula be include following calculated by mass preparing raw material：Natural rubber
65 parts, 0.8 part of sulphur, 0.6 part of zinc oxide, 0.9 part of potassium sulfate, 6 parts of calcium chloride, N- ethyl, N-phenyl aminodithioformic acid
0.7 part of zinc, 0.3 part of diphenylguanidine, 0.5 part of hydroquinone dibenzyl ether, 0.4 part of 2- sulfenyl benzimidazole, 5 parts of superfine silica gel powder, crystallite
5 parts of cellulose, 70 parts of water；It further include 4 parts of wheat bran albumen, 12 parts of gelatin.
Comparative example 3：
Remaining is identical as 3 embodiment of embodiment, and formula includes following calculated by mass preparing raw material：Natural rubber 65
Part, 0.8 part of sulphur, 0.6 part of zinc oxide, 0.9 part of potassium sulfate, 6 parts of calcium chloride, N- ethyl, N-phenyl zinc dithiocarbamate
0.7 part, 0.3 part of diphenylguanidine, 0.5 part of hydroquinone dibenzyl ether, 0.4 part of 2- sulfenyl benzimidazole, 5 parts of superfine silica gel powder, crystallite fibre
5 parts, 70 parts of water of dimension element；It further include 4 parts of Chloranthus glaber fiber, 12 parts of gelatin.
Comparative example 4：
Remaining is identical as 3 embodiment of embodiment, and formula includes following calculated by mass preparing raw material：Natural rubber 65
Part, 0.8 part of sulphur, 0.6 part of zinc oxide, 0.9 part of potassium sulfate, 6 parts of calcium chloride, N- ethyl, N-phenyl zinc dithiocarbamate
0.7 part, 0.3 part of diphenylguanidine, 0.5 part of hydroquinone dibenzyl ether, 0.4 part of 2- sulfenyl benzimidazole, 5 parts of superfine silica gel powder, crystallite fibre
5 parts, 70 parts of water of dimension element；It further include 6 parts of arghan, 12 parts of gelatin.
Performance and take test：
It takes and carries out water suction suppression by emgloves prepared by traditional preparation methods by above-described embodiment 3 and comparative example 1-4 formula
Bacterium test.
The test of water absorption rate is the water absorption rate data in 5 minutes, 10 minutes, 20 minutes.
Antibacterial test is Escherichia coli, staphylococcus glucose bacterium uses 6 hours, 12 hours antibacterial percentage test numbers
According to.Concrete outcome is as shown in table 1：
The water suction bacteriostasis test of the emgloves of 1 embodiment 3 of table and comparative example 1-4
It can be seen that from upper table data, the embodiment of the present invention 3 joined wheat bran albumen, Chloranthus glaber fiber, arghan, bright
The antibacterial moisture-proof emgloves of glue preparation, the water absorption rate and bacteriostasis for having consumption reduction are simply added into one of which in contrast
Comparative example 2-4 water suction fungistatic effect not as good as embodiment 3, and the emgloves of the comparative example 1 of common material preparation, water suction
Property is poor, and the increase of bacteriostasis at any time reduces instead, it is easier to breed bacterium.
It should be pointed out that the above specific embodiment is only illustrative of the invention and is not intended to limit the scope of the invention,
After having read the present invention, those skilled in the art fall within power appended by the application to the modification of various equivalent forms of the invention
Benefit requires limited range.
Claims (8)
1. a kind of antibacterial moisture-proof emgloves, calculated by mass raw material is prepared including following：60-70 parts of natural rubber, sulphur
0.5-1.2 parts, 0.5-0.8 parts of zinc oxide, 0.5-1.5 parts of potassium sulfate, 4-8 parts of calcium chloride, N- ethyl, N-phenyl dithiocarbamates
0.6-0.8 parts of zinc formate, 0.2-0.5 parts of diphenylguanidine, 0.3-0.6 parts of hydroquinone dibenzyl ether, 2- sulfenyl benzimidazole 0.3-0.6
Part, 4-6 parts of superfine silica gel powder, 4-6 parts of microcrystalline cellulose, 60-80 parts of water；Characterized by further comprising 3-6 parts of wheat bran albumen, careless coral
2-6 parts of coral fiber, 4-8 parts of arghan, 10-14 parts of gelatin.
2. antibacterial moisture-proof emgloves according to claim 1, it is characterised in that：The extracting method of the wheat bran albumen
For：10-20 times of lye is added into wheat bran, extracts 1.5h, Extracting temperature is 60 DEG C, and protease, enzyme and bottom are added afterwards
Object ratio is 1%, continues to extract 1h, and Extracting temperature is reduced to 50 DEG C, extracts pH and maintains 7.5.
3. antibacterial moisture-proof emgloves according to claim 2, it is characterised in that：The extraction process of the wheat bran in
It is carried out in Vltrasonic device, supersonic frequency is set as 50-60Hz.
4. antibacterial moisture-proof emgloves according to claim 1, it is characterised in that：The extracting method of the Chloranthus glaber fiber
For：With 5:1 mass ratio takes Chloranthus glaber blade, Chloranthus glaber root, clean crush mixed powder minces, to mixed powder mince in plus
Entering 10-20 times of dehydrated alcohol, extraction time 1.5h, Extracting temperature is 80 DEG C, the rear acetic acid that liquor capacity 20% is added, after
Continuous to extract 2h, Extracting temperature is reduced to 60 DEG C.
5. antibacterial moisture-proof emgloves according to claim 4, it is characterised in that：The extraction process of the Chloranthus glaber fiber
It is carried out in Vltrasonic device, supersonic frequency is set as 55-65Hz.
6. antibacterial moisture-proof emgloves according to claim 1, it is characterised in that：The extracting method of the arghan
For：Pineapple leaves are taken, cleans and crushes, the middle dehydrated alcohol for being added 10-20 times, extraction time 2.5h, Extracting temperature is 70 DEG C, after
The hydrogen peroxide of liquor capacity 10% is added, continues to extract 1h, Extracting temperature is reduced to 60 DEG C.
7. antibacterial moisture-proof emgloves according to claim 6, it is characterised in that：The extraction process of the arghan
It is carried out in Vltrasonic device, supersonic frequency is set as 80-90Hz.
8. antibacterial moisture-proof emgloves according to claim 1, it is characterised in that：The gelatin uses acid treatment system
?.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810812853.3A CN108864501A (en) | 2018-07-23 | 2018-07-23 | A kind of antibacterial moisture-proof emgloves |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810812853.3A CN108864501A (en) | 2018-07-23 | 2018-07-23 | A kind of antibacterial moisture-proof emgloves |
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| CN108864501A true CN108864501A (en) | 2018-11-23 |
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| CN201810812853.3A Pending CN108864501A (en) | 2018-07-23 | 2018-07-23 | A kind of antibacterial moisture-proof emgloves |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1931909A (en) * | 2006-09-07 | 2007-03-21 | 暨南大学 | Composite material of modified micro plant fiber powder and natural rubber and its prepn process and application |
| CN106336536A (en) * | 2016-08-29 | 2017-01-18 | 樊之雄 | Antibacterial and sweat-absorbing medical rubber glove and preparing method thereof |
-
2018
- 2018-07-23 CN CN201810812853.3A patent/CN108864501A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1931909A (en) * | 2006-09-07 | 2007-03-21 | 暨南大学 | Composite material of modified micro plant fiber powder and natural rubber and its prepn process and application |
| CN106336536A (en) * | 2016-08-29 | 2017-01-18 | 樊之雄 | Antibacterial and sweat-absorbing medical rubber glove and preparing method thereof |
Non-Patent Citations (5)
| Title |
|---|
| 何建新: "《新型纤维材料学》", 31 July 2014 * |
| 北京橡胶工业研究院设计院: "《橡胶制品工艺学》", 31 December 1980 * |
| 徐东翔: "《植物资源化学》", 30 September 2004 * |
| 胡必杰等: "《SIFIC医院感染防控用品使用指引 2014-2015年》", 31 May 2014 * |
| 陈晓磊等: ""麦麸多肽抗氧化及吸湿保湿性能的测定"", 《齐鲁工业大学学报》 * |
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Application publication date: 20181123 |