CN108863520A - A kind of sugarcane special bio medicine fertilizer and preparation method thereof containing the paulownia dregs of rice - Google Patents
A kind of sugarcane special bio medicine fertilizer and preparation method thereof containing the paulownia dregs of rice Download PDFInfo
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- CN108863520A CN108863520A CN201810686572.8A CN201810686572A CN108863520A CN 108863520 A CN108863520 A CN 108863520A CN 201810686572 A CN201810686572 A CN 201810686572A CN 108863520 A CN108863520 A CN 108863520A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
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Abstract
The invention discloses a kind of sugarcane special bio medicine fertilizer and preparation method thereof containing the paulownia dregs of rice, the sugarcane special bio medicine fertilizer containing the paulownia dregs of rice are made of the raw material of following parts by weight：Chinese medicine slag 50-55, paulownia dregs of rice 18-20, modified alta-mud 20-25, peat soil 13-16, compound fertilizer feed powder 10-13, pesticide 0.2-0.4, triacontanol 0.04-0.08, lanthana 0.4-0.7, calcium oxide 16-19；The present invention passes through the improvement to raw materials for production, reasonable proportion, make it that can generate the ingredients such as antibacterial, insect prevention, organic-inorganic nutrient, positive growth factor when being applied to sugarcane, overcomes single existing pesticide-fertilizer product insect prevention and pesticide and fertilizer are without any sustained release performance, lasting period shorter defect；At low cost, nutrient validity period length, advantages of environment protection are also had both simultaneously.
Description
Technical field
The invention belongs to technical field of fertilizer, and in particular to a kind of sugarcane special bio medicine containing the paulownia dregs of rice is fertile and its prepares
Method.
Background technique
Sugarcane is most important sugar crop and energy crop, and China is the third-largest sugarcane production state.Insect pest is to influence me
One of state's sugarcane yield and the principal element of quality, including ground pest (such as snout moth's larva, aphid and thrips) and subterranean pest-insect is (such as
Chafer, longicorn, termite and root nematode etc.).With the significantly downslide of China's rural labor size of population, labor cost is not
It is disconnected soaring, with the continuous promotion of agricultural scale and Mechanization Level, gently simplify the demand administration fertilizer of product technology and equipment
Development bring major opportunity.Medicine fertilizer integration avoids during Pesticide use the influence that effect of meeting with fertilizer is subtracted each other,
So that pesticide and fertilizer can be used in the optimal application phase, fertilizer efficiency and drug effect are improved.
Currently, cane planting is most of also according to traditional fertilizer and pesticide separate administration mode, with random and
Blindness, time-consuming, waste of resource, and some pesticide-fertilizer products to circulate in the market are also that insect prevention is single, without simultaneous anti-ground
And subterranean pest-insect, and pesticide and fertilizer, without any sustained release performance, the lasting period is shorter.
Summary of the invention
Technical problem to be solved by the present invention lies in：Single existing pesticide-fertilizer product insect prevention can be overcome and pesticide and fertilizer
Material is without any sustained release performance, lasting period shorter defect.
The present invention solves above-mentioned technical problem using following technical scheme：
A kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, which is characterized in that be made of the raw material of following parts by weight：Chinese medicine
Slag 50-55, paulownia dregs of rice 18-20, modified alta-mud 20-25, peat soil 13-16, compound fertilizer feed powder 10-13, pesticide 0.2-0.4, three
Ten alkanol 0.04-0.08, lanthana 0.4-0.7, calcium oxide 16-19.
The Chinese medicine slag is honeysuckle residue, specially with the discarded spontaneous fermentation in distilled liquid of honeysuckle production process
Solid residue after one month.
The method for preparing modified bentonite is：
(1) it takes bentonite to be placed in program in Muffle furnace and is warming up to 800-900 DEG C, constant temperature calcining 2h, be ground to grain after cooling
Diameter is 200-300 mesh；
(2) 15 times of bentonite quality of water is added into the medical stone after step (1) calcination process and enters bentonite quality
0.2-0.4 times of sodium lignin sulfonate stirs to form mud in suspension, takes upper suspension in the centrifuge of 2000-4000r/min
Middle centrifugal treating 10min, vacuum filtration, is spray-dried to obtain the final product.
Compound fertilizer's feed powder is by urea, potassium dihydrogen phosphate, calcium nitrate, ammonium sulfate, borax, zinc sulfate=3.1: 2.5:
Compound at 1.7: 0.9: 0.3: 0.2.
The pesticide is phoxim granule, penoxsuam is compounded according to mass ratio 12: 1.
Further, a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, is made of the raw material of following parts by weight：In
The dregs of a decoction 53, the paulownia dregs of rice 19, modified alta-mud 23, peat soil 15, compound fertilizer's feed powder 12, pesticide 0.3, triacontanol 0.05, lanthana
0.6, calcium oxide 18.
Further, a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, which is characterized in that by following parts by weight
Raw material composition：Chinese medicine slag 50, the paulownia dregs of rice 18, modified alta-mud 20, peat soil 13, compound fertilizer's feed powder 10, pesticide 0.2, triacontanol
0.04, lanthana 0.4, calcium oxide 16.
Further, the preparation method of a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, includes the following steps：
(1) Chinese medicine slag is smashed to pieces with pulverizer, calcium oxide is added and carries out co-grinding, sieves with 100 mesh sieve to obtain organic fertilizer；
(2) by the paulownia dregs of rice, hot dipping mentions 2h in 50 DEG C of distilled water, carries out first time water and mentions, and gained filtrate is recycled in 50 DEG C
To doing, water extract A can be obtained；
(3) by the dregs of rice slag of step (2) first with the extraction of 70% ethyl alcohol, hot dipping mentions 2h and carries out second in 50 DEG C of distilled water
Secondary water mentions, and 50 DEG C of gained filtrate is recycled to dry, obtains water extract B；
(4) water extract A, water extract B are merged, addition pesticide, peat soil stir and evenly mix, and grind 1-2h, must sterilize mixing
Powder；
(5) by step (1) organic fertilizer, step (4) sterilization mixed powder, modified alta-mud, compound fertilizer's feed powder, triacontanol,
Air-flow crushing is carried out after lanthana mixing, further remixes uniformly, adds water to carry out kneading granulation, then fluidized drying, is sieved,
Underproof particle is crushed again, qualified particle is finished product.
The technology of the present invention beneficial effect：The present invention is being applied to it by the improvement to raw materials for production, reasonable proportion
The ingredients such as antibacterial, insect prevention, organic-inorganic nutrient, positive growth factor can be generated when sugarcane, overcome existing pesticide-fertilizer product insect prevention list
One and pesticide and fertilizer without any sustained release performance, lasting period shorter defect；Also have both simultaneously at low cost, nutrient validity period it is long,
Advantages of environment protection.
Organic fertilizer, honeysuckle residue are prepared by the way that a certain amount of calcium oxide is added into the discarded solid residue of honeysuckle
Middle main component is insoluble polysaccharide, is very weak acid, after strong alkaline substance CaO is added thereto, is reacted with the water in residue
Generate the alkaloid Ca (OH) of improvement acid soil2, insoluble polysaccharide contains multiple hydroxyls, can form calcium composition with polysaccharide and exist
Ca(OH)2In a highly dispersed state, good air permeability is conducive to microbe survival in biological organic fertilizer on surface.
The paulownia dregs of rice are first carried out to first time water to mention, carry out second of water again after then extracting its dregs of rice slag using 70% ethyl alcohol
It mentions, then stirs and evenly mixs to obtain sterilization mixed powder with pesticide, peat soil, insect prevention range is wide, has to above and below ground pest and preferably goes out
Kill effect.
Specific embodiment
For convenient for those skilled in the art understand that technical solution of the present invention, does further technical solution of the present invention
It is bright.
Embodiment one
A kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, which is characterized in that be made of the raw material of following parts by weight：Chinese medicine
Slag 53, the paulownia dregs of rice 19, modified alta-mud 23, peat soil 15, compound fertilizer's feed powder 12, pesticide 0.3, triacontanol 0.05, lanthana
0.6, calcium oxide 18.
The Chinese medicine slag is honeysuckle residue, specially with the discarded spontaneous fermentation in distilled liquid of honeysuckle production process
Solid residue after one month.
The method for preparing modified bentonite is：
(1) it takes bentonite to be placed in program in Muffle furnace and is warming up to 850 DEG C, constant temperature calcining 2h, being ground to partial size after cooling is
250 mesh；
(2) 15 times of bentonite quality of water is added into the medical stone after step (1) calcination process and enters bentonite quality
0.3 times of sodium lignin sulfonate stirs to form mud in suspension, takes upper suspension centrifugal treating in the centrifuge of 3000r/min
10min, vacuum filtration, is spray-dried to obtain the final product.
Compound fertilizer's feed powder is by urea, potassium dihydrogen phosphate, calcium nitrate, ammonium sulfate, borax, zinc sulfate=3.1: 2.5:
Compound at 1.7: 0.9: 0.3: 0.2.
The pesticide is phoxim granule, penoxsuam is compounded according to mass ratio 12: 1.
Further, the preparation method of a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, includes the following steps：
(1) Chinese medicine slag is smashed to pieces with pulverizer, calcium oxide is added and carries out co-grinding, sieves with 100 mesh sieve to obtain organic fertilizer；
(2) by the paulownia dregs of rice, hot dipping mentions 2h in 50 DEG C of distilled water, carries out first time water and mentions, and gained filtrate is recycled in 50 DEG C
To doing, water extract A can be obtained；
(3) by the dregs of rice slag of step (2) first with the extraction of 70% ethyl alcohol, hot dipping mentions 2h and carries out second in 50 DEG C of distilled water
Secondary water mentions, and 50 DEG C of gained filtrate is recycled to dry, obtains water extract B；
(4) water extract A, water extract B are merged, addition pesticide, peat soil stir and evenly mix, and grind 1-2h, must sterilize mixing
Powder；
(5) by step (1) organic fertilizer, step (4) sterilization mixed powder, modified alta-mud, compound fertilizer's feed powder, triacontanol,
Air-flow crushing is carried out after lanthana mixing, further remixes uniformly, adds water to carry out kneading granulation, then fluidized drying, is sieved,
Underproof particle is crushed again, qualified particle is finished product.
Embodiment two
A kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, which is characterized in that be made of the raw material of following parts by weight：Chinese medicine
Slag 50, the paulownia dregs of rice 18, modified alta-mud 20, peat soil 13, compound fertilizer's feed powder 10, pesticide 0.2, triacontanol 0.04, lanthana
0.4, calcium oxide 16.
The Chinese medicine slag is honeysuckle residue, specially with the discarded spontaneous fermentation in distilled liquid of honeysuckle production process
Solid residue after one month.
The method for preparing modified bentonite is：
(1) it takes bentonite to be placed in program in Muffle furnace and is warming up to 800 DEG C, constant temperature calcining 2h, being ground to partial size after cooling is
200 mesh；
(2) 15 times of bentonite quality of water is added into the medical stone after step (1) calcination process and enters bentonite quality
0.2 times of sodium lignin sulfonate stirs to form mud in suspension, takes upper suspension centrifugal treating in the centrifuge of 2000r/min
10min, vacuum filtration, is spray-dried to obtain the final product.
Compound fertilizer's feed powder is by urea, potassium dihydrogen phosphate, calcium nitrate, ammonium sulfate, borax, zinc sulfate=3.1: 2.5:
Compound at 1.7: 0.9: 0.3: 0.2.
The pesticide is phoxim granule, penoxsuam is compounded according to mass ratio 12: 1.
Further, the preparation method of a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, includes the following steps：
(1) Chinese medicine slag is smashed to pieces with pulverizer, calcium oxide is added and carries out co-grinding, sieves with 100 mesh sieve to obtain organic fertilizer；
(2) by the paulownia dregs of rice, hot dipping mentions 2h in 50 DEG C of distilled water, carries out first time water and mentions, and gained filtrate is recycled in 50 DEG C
To doing, water extract A can be obtained；
(3) by the dregs of rice slag of step (2) first with the extraction of 70% ethyl alcohol, hot dipping mentions 2h and carries out second in 50 DEG C of distilled water
Secondary water mentions, and 50 DEG C of gained filtrate is recycled to dry, obtains water extract B；
(4) water extract A, water extract B are merged, addition pesticide, peat soil stir and evenly mix, and grind 1-2h, must sterilize mixing
Powder；
(5) by step (1) organic fertilizer, step (4) sterilization mixed powder, modified alta-mud, compound fertilizer's feed powder, triacontanol,
Air-flow crushing is carried out after lanthana mixing, further remixes uniformly, adds water to carry out kneading granulation, then fluidized drying, is sieved,
Underproof particle is crushed again, qualified particle is finished product.
Embodiment three
A kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, which is characterized in that be made of the raw material of following parts by weight：Chinese medicine
Slag 55, the paulownia dregs of rice 20, modified alta-mud 25, peat soil 16, compound fertilizer's feed powder 13, pesticide 0.4, triacontanol 0.08, lanthana
0.7, calcium oxide 19.
The Chinese medicine slag is honeysuckle residue, specially with the discarded spontaneous fermentation in distilled liquid of honeysuckle production process
Solid residue after one month.
The method for preparing modified bentonite is：
(1) it takes bentonite to be placed in program in Muffle furnace and is warming up to 900 DEG C, constant temperature calcining 2h, being ground to partial size after cooling is
300 mesh；
(2) 15 times of bentonite quality of water is added into the medical stone after step (1) calcination process and enters bentonite quality
0.4 times of sodium lignin sulfonate stirs to form mud in suspension, takes upper suspension centrifugal treating in the centrifuge of 4000r/min
10min, vacuum filtration, is spray-dried to obtain the final product.
Compound fertilizer's feed powder is by urea, potassium dihydrogen phosphate, calcium nitrate, ammonium sulfate, borax, zinc sulfate=3.1: 2.5:
Compound at 1.7: 0.9: 0.3: 0.2.
The pesticide is phoxim granule, penoxsuam is compounded according to mass ratio 12: 1.
Further, the preparation method of a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, includes the following steps：
(1) Chinese medicine slag is smashed to pieces with pulverizer, calcium oxide is added and carries out co-grinding, sieves with 100 mesh sieve to obtain organic fertilizer；
(2) by the paulownia dregs of rice, hot dipping mentions 2h in 50 DEG C of distilled water, carries out first time water and mentions, and gained filtrate is recycled in 50 DEG C
To doing, water extract A can be obtained；
(3) by the dregs of rice slag of step (2) first with the extraction of 70% ethyl alcohol, hot dipping mentions 2h and carries out second in 50 DEG C of distilled water
Secondary water mentions, and 50 DEG C of gained filtrate is recycled to dry, obtains water extract B；
(4) water extract A, water extract B are merged, addition pesticide, peat soil stir and evenly mix, and grind 1-2h, must sterilize mixing
Powder；
(5) by step (1) organic fertilizer, step (4) sterilization mixed powder, modified alta-mud, compound fertilizer's feed powder, triacontanol,
Air-flow crushing is carried out after lanthana mixing, further remixes uniformly, adds water to carry out kneading granulation, then fluidized drying, is sieved,
Underproof particle is crushed again, qualified particle is finished product.
Claims (10)
1. a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice, which is characterized in that be made of the raw material of following parts by weight：Chinese medicine slag
50-55, paulownia dregs of rice 18-20, modified alta-mud 20-25, peat soil 13-16, compound fertilizer feed powder 10-13, pesticide 0.2-0.4,30
Alkanol 0.04-0.08, lanthana 0.4-0.7, calcium oxide 16-19.
2. a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice according to claim 1, which is characterized in that the Chinese medicine
Slag is honeysuckle residue, specially residual with the solid behind discarded spontaneous fermentation one month in distilled liquid of honeysuckle production process
Slag.
3. a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice according to claim 1, which is characterized in that the modification
Preparation method for bentonite is：
(1) it takes bentonite to be placed in program in Muffle furnace and is warming up to 800-900 DEG C, constant temperature calcining 2h, being ground to partial size after cooling is
200-300 mesh；
(2) 15 times of bentonite quality of water is added into the medical stone after step (1) calcination process and enters bentonite quality 0.2-
0.4 times of sodium lignin sulfonate stirs to form mud in suspension, take upper suspension in the centrifuge of 2000-4000r/min from
The heart handles 10min, and vacuum filtration is spray-dried to obtain the final product.
4. a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice according to claim 1, which is characterized in that described is compound
Fertilizer powder is by urea, potassium dihydrogen phosphate, calcium nitrate, ammonium sulfate, borax, zinc sulfate=3.1: 2.5: 1.7: 0.9: 0.3: 0.2 is multiple
With forming.
5. a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice according to claim 1, which is characterized in that the pesticide
It is compounded for phoxim granule, penoxsuam according to mass ratio 12: 1.
6. a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice according to claim 1, which is characterized in that by following weight
The raw material composition of part：Chinese medicine slag 53, the paulownia dregs of rice 19, modified alta-mud 23, peat soil 15, compound fertilizer's feed powder 12, pesticide 0.3,30
Alkanol 0.05, lanthana 0.6, calcium oxide 18.
7. a kind of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice according to claim 1, which is characterized in that by following weight
The raw material composition of part：Chinese medicine slag 50, the paulownia dregs of rice 18, modified alta-mud 20, peat soil 13, compound fertilizer's feed powder 10, pesticide 0.2,30
Alkanol 0.04, lanthana 0.4, calcium oxide 16.
8. a kind of preparation method of the sugarcane special bio medicine fertilizer containing the paulownia dregs of rice described in -7 any one according to claim 1,
It is characterized by comprising the following steps：
(1) Chinese medicine slag is smashed to pieces with pulverizer, calcium oxide is added and carries out co-grinding, sieves with 100 mesh sieve to obtain organic fertilizer；
(2) paulownia dregs of rice progress first time water is mentioned, gained filtrate is recycled to dry water extract A；
(3) it by the dregs of rice slag of step (2) first with the extraction of 70% ethyl alcohol, then carries out second of water and mentions, gained filtrate is recycled to dry, obtain
Water extract B；
(4) water extract A, water extract B are merged, addition pesticide, peat soil stir and evenly mix, and grind 1-2h, obtain sterilization mixed powder；
(5) step (1) organic fertilizer, step (4) are sterilized into mixed powder, modified alta-mud, compound fertilizer's feed powder, triacontanol, oxidation
Air-flow crushing is carried out after lanthanum mixing, further remixes uniformly, adds water to carry out kneading granulation, then fluidized drying, is sieved, it will not
Qualified particle crushes again, and qualified particle is finished product.
9. a kind of preparation method of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice according to claim 8, which is characterized in that
By the paulownia dregs of rice, hot dipping mentions 2h in 50 DEG C of distilled water in the step (2), gained filtrate is recycled in 50 DEG C dry, can be obtained
Water extract A.
10. a kind of preparation method of sugarcane special bio medicine fertilizer containing the paulownia dregs of rice according to claim 8, feature exist
In, hot dipping mentions 2h in 50 DEG C of distilled water when second of water mentions in the step (3), 50 DEG C of gained filtrate are recycled to it is dry,
Obtain water extract B.
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Cited By (1)
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| CN112335693A (en) * | 2020-11-03 | 2021-02-09 | 中国科学院地理科学与资源研究所 | Special plant source composite pesticide for green tea trees and preparation method thereof |
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Application publication date: 20181123 |