CN108852905A - A kind of preparation method of the hand cleanser of effect stability - Google Patents
A kind of preparation method of the hand cleanser of effect stability Download PDFInfo
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- CN108852905A CN108852905A CN201810743196.1A CN201810743196A CN108852905A CN 108852905 A CN108852905 A CN 108852905A CN 201810743196 A CN201810743196 A CN 201810743196A CN 108852905 A CN108852905 A CN 108852905A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8129—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses a kind of preparation methods of the hand cleanser of effect stability, include the following steps：（1）The preparation of antibacterial load-carrying additive,（2）Raw material weigh it is spare,（3）Finished product preparation.Present invention improves the preparation method of hand cleanser, rationally, simple process is easy to promote and utilize for the collocation of each step, and hand cleanser decontamination obtained, bacteria-eliminating efficacy are good, and safe and harmless using stay in grade, the market competitiveness is strong, great application value.
Description
Technical field
The present invention relates to a kind of hand cleanser, and in particular to a kind of preparation method of the hand cleanser of effect stability.
Background technique
The 80's of 20th century, hand cleanser start to move towards family by hotel, the hotel in west, and gradually ripe for everybody
Know, has worldwide obtained relatively broad popularization as a result,.1999, " ancestral's silk " hand cleanser entered Chinese market, beat
The blank in Chinese hand cleanser market is broken.It has passed through the development of more than ten years, hand cleanser has become widely known, at for people's lives
In requirement.Currently, hand cleanser in the market is many kinds of, but with environmentally protective, bactericidal effect is good, stability in use is strong
It is less.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of preparation method of the hand cleanser of effect stability is provided.
The present invention is achieved by the following technical solutions：
A kind of preparation method of the hand cleanser of effect stability, includes the following steps：
（1）The preparation of antibacterial load-carrying additive：
A. by formaldehyde and ammeline according to mass ratio 1：1.4 ~ 1.7 mixed after be put into reaction kettle, it is then added
Mixture A is obtained after the boric acid of gross mass 2.0 ~ 2.6%, 0.4 ~ 0.45% ferrocene, is then adjusted to the pH value of mixture A
8.0 ~ 8.5, heating keep reaction kettle in temperature be 38 ~ 42 DEG C, and with 350 ~ 380 revs/min of revolving speed stir process 32 ~
It is spare after 37min；
B. be added into operation a treated reaction kettle 6 ~ 8% polyvinyl alcohol of mixture A gross mass, 2 ~ 3% ethyl acetate,
2.5 ~ 3.5% sodium chloride, 30 ~ 35% essential oil, 3 ~ 5% chitosan, 1 ~ 2% sodium pyrophosphate, temperature is then risen to 48 ~ 52
DEG C, to be taken out after 500 ~ 550 revs/min of 47 ~ 51min of revolving speed stir process, then the deionization with 100 ~ 110 times of its gross mass
It is spare that water obtains mixture B after mixing jointly；
C. bentonite is put into hydrochloric acid solution after 3 ~ 5min of immersion treatment and is taken out, then placed into sodium hydroxide solution
It is taken out after 4 ~ 6min of immersion treatment, it is spare after finally being rinsed with deionized water to neutrality；
D. will operation c treated that bentonite is put into calcining furnace carries out calcination processing, taken out after 1 ~ 2h spare；
E. will be in operation d treated bentonite the is immersed in operation resulting mixture B of b, ultrasonic vibration filters after handling 4 ~ 6h,
Finally the bentonite filtered out is put into drying box after being dried 5 ~ 7h and is taken out, it is spare to obtain antibacterial load-carrying additive；
（2）Raw material weighs spare：
It is spare that following substance is weighed by corresponding parts by weight：4 ~ 7 parts of dodecyldimethylamine oxide, 1 ~ 2 part of laruyl alcohol oleate,
2 ~ 4 parts of glycerol, 1 ~ 3 part of Cocoamidopropyl betaine, 2 ~ 4 parts of hydroxyethyl celluloses, 1.5 ~ 2.5 parts of single dodecyl phosphoric acid
Ester, 1 ~ 2 part of ceteth, 3 ~ 5 parts of steps（1）Antibacterial load-carrying additive obtained, 95 ~ 100 parts of water；
（3）Finished product preparation：
By step（2）Weighed all raw materials are put into agitator tank jointly, get product hand cleanser after high-speed stirred is uniform.
Further, step（1）Operating polyvinyl alcohol described in b is low molecular weight low viscosity polyvinyl alcohol, viscosity
It is 4.5 ~ 6.0, average molecular weight is 15000 ~ 17000.
Further, step（1）Operating essential oil described in b is by peppermint oil dementholized, tea tree ethereal oil according to weight ratio 1:2~3
It mixes.
Further, step（1）The mass fraction for operating hydrochloric acid in hydrochloric acid solution described in c is 4 ~ 6%, the hydrogen
The mass fraction of sodium hydroxide is 5 ~ 8% in sodium hydroxide solution.
Further, step（1）Temperature when operating calcination processing described in d in control calcining furnace is 880 ~ 920 DEG C.
Further, step（1）The frequency of ultrasonic wave is 380 ~ 420kHz when operating the processing of ultrasonic vibration described in e,
Temperature when the described drying process in control drying box is 88 ~ 93 DEG C.
Further, step（3）Described in high-speed stirred processing when speed of agitator be 2000 ~ 2400 revs/min.
Commercially available hand cleanser type is more, and in order to assign hand cleanser antibacterial functions, it is living that antibacterial is added usually into hand cleanser
Property ingredient, is mostly artificial synthesized chemicals, but such components are larger for skin irritatin, safety is poor, to this people
The natural components such as addition Chinese medical extract, essential oil are attempted, are achieved good results, but such components are easy inactivation, Ye Jibao
Deposit the time soon, stability is bad.In addition, the detergency ability of existing hand cleanser is also not satisfactory.In this regard, the present invention provides
A kind of preparation method of hand cleanser effectively improves the synthesis of hand cleanser using quality, is added to a kind of antibacterial wherein preparing
Load-carrying additive ingredient is made of the substance modification based on bentonite, wherein first having carried out soda acid immersion to bentonite, having forged
Burning processing, effectively improves bentonitic specific surface area and adsorption capacity, improves its surface reaction activity, and it is subsequent to be conducive to its
Processing operation, it is last that immersion modification carried out to bentonite with the mixture B of formulated again, mixture B be it is a kind of with
Formaldehyde, ammeline are main polymeric material, in alkaline environment, the catalytic action through boric acid, ferrocene, and sodium chloride, shell
Glycan is composite modified, the ingredients such as cooperation polyvinyl alcohol, based on the resin of formation generated with formaldehyde, ammeline reaction
A kind of low-molecular-weight resin solution that amine-aldehyde-phenol polymer makes, small molecule particle penetrate into bentonitic interlayer, with
Bentonite forms a kind of compound ingredient, can cooperate and essential oil is fixed in bentonite, enhance the stability of essential oil,
People wash by rubbing with the hands in use, the release of essential oil effective component is realized bacteria-eliminating efficacy by bentonite lamella sliding, while passing through mixture B
Modified bentonite has very strong adsorption binding energy power to little particle dirt, enhances the clean effect of hand cleanser, cooperates
Remaining material composition is used in conjunction with, and improves the use quality of hand cleanser well.
The present invention has the following advantages that compared with prior art：
Present invention improves the preparation method of hand cleanser, rationally, simple process is easy to promote and utilize, is made for each step collocation
Hand cleanser decontamination, bacteria-eliminating efficacy it is good, safe and harmless using stay in grade, the market competitiveness is strong, great application value.
Specific embodiment
Embodiment 1
A kind of preparation method of the hand cleanser of effect stability, includes the following steps：
（1）The preparation of antibacterial load-carrying additive：
A. by formaldehyde and ammeline according to mass ratio 1：1.4 mixed after be put into reaction kettle, its total matter is then added
Mixture A is obtained after measuring 2.0% boric acid, 0.4% ferrocene, the pH value of mixture A is then adjusted to 8.0, heating keeps anti-
Answering the temperature in kettle is 38 DEG C, and with spare after 350 revs/min of revolving speed stir process 32min；
B. 6% polyvinyl alcohol of mixture A gross mass, 2% ethyl acetate, 2.5% is added into operation a treated reaction kettle
Sodium chloride, 30% essential oil, 3% chitosan, 1% sodium pyrophosphate, temperature is then risen to 48 DEG C, with 500 revs/min
Taken out after revolving speed stir process 47min, then with 100 times of its gross mass of deionized water jointly after mixing mixture B is standby
With；
C. bentonite is put into hydrochloric acid solution after immersion treatment 3min and is taken out, then placed into sodium hydroxide solution and soak
It is taken out after bubble processing 4min, it is spare after finally being rinsed with deionized water to neutrality；
D. will operation c treated that bentonite is put into calcining furnace carries out calcination processing, taken out after 1h spare；
E. it will be filtered after ultrasonic vibration processing 4h, most in operation d treated bentonite the is immersed in operation resulting mixture B of b
The bentonite filtered out is put into drying box afterwards after being dried 5h and is taken out, it is spare to obtain antibacterial load-carrying additive；
（2）Raw material weighs spare：
It is spare that following substance is weighed by corresponding parts by weight：4 parts of dodecyldimethylamine oxide, 1 part of laruyl alcohol oleate, 2 parts
Glycerol, 1 part of Cocoamidopropyl betaine, 2 parts of hydroxyethyl celluloses, 1.5 parts of single dodecyl phosphates, 1 part of cetanol
Polyethers, 3 parts of steps（1）Antibacterial load-carrying additive obtained, 95 parts of water；
（3）Finished product preparation：
By step（2）Weighed all raw materials are put into agitator tank jointly, get product hand cleanser after high-speed stirred is uniform.
Further, step（1）Operating polyvinyl alcohol described in b is low molecular weight low viscosity polyvinyl alcohol, viscosity
It is 4.5, average molecular weight 15000.
Further, step（1）Operating essential oil described in b is by peppermint oil dementholized, tea tree ethereal oil according to weight ratio 1:2 is mixed
It closes.
Further, step（1）The mass fraction for operating hydrochloric acid in hydrochloric acid solution described in c is 4%, the hydrogen-oxygen
The mass fraction for changing sodium hydroxide in sodium solution is 5%.
Further, step（1）Temperature when operating calcination processing described in d in control calcining furnace is 880 DEG C.
Further, step（1）The frequency of ultrasonic wave is 380kHz when operating the processing of ultrasonic vibration described in e, described
Drying process when control drying box in temperature be 88 DEG C.
Further, step（3）Described in high-speed stirred processing when speed of agitator be 2000 revs/min.
Embodiment 2
A kind of preparation method of the hand cleanser of effect stability, includes the following steps：
（1）The preparation of antibacterial load-carrying additive：
A. by formaldehyde and ammeline according to mass ratio 1：1.6 mixed after be put into reaction kettle, its total matter is then added
Mixture A is obtained after measuring 2.3% boric acid, 0.42% ferrocene, the pH value of mixture A is then adjusted to 8.3, heating keeps anti-
Answering the temperature in kettle is 40 DEG C, and with spare after 370 revs/min of revolving speed stir process 35min；
B. 7% polyvinyl alcohol of mixture A gross mass, 2.5% ethyl acetate, 3% is added into operation a treated reaction kettle
Sodium chloride, 32% essential oil, 4% chitosan, 1.5% sodium pyrophosphate, temperature is then risen to 50 DEG C, with 530 revs/min
Revolving speed stir process 49min after take out, then with 105 times of its gross mass of deionized water jointly after mixing mixture B
It is spare；
C. bentonite is put into hydrochloric acid solution after immersion treatment 4min and is taken out, then placed into sodium hydroxide solution and soak
It is taken out after bubble processing 5min, it is spare after finally being rinsed with deionized water to neutrality；
D. will operation c treated that bentonite is put into calcining furnace carries out calcination processing, taken out after 1.5h spare；
E. it will be filtered after ultrasonic vibration processing 5h, most in operation d treated bentonite the is immersed in operation resulting mixture B of b
The bentonite filtered out is put into drying box afterwards after being dried 6h and is taken out, it is spare to obtain antibacterial load-carrying additive；
（2）Raw material weighs spare：
It is spare that following substance is weighed by corresponding parts by weight：6 parts of dodecyldimethylamine oxide, 1.5 parts of laruyl alcohol oleates, 3
Part glycerol, 2 parts of Cocoamidopropyl betaines, 3 parts of hydroxyethyl celluloses, 2 parts of single dodecyl phosphates, 1.5 parts of spermaceti
Alcohol polyethers, 4 parts of steps（1）Antibacterial load-carrying additive obtained, 98 parts of water；
（3）Finished product preparation：
By step（2）Weighed all raw materials are put into agitator tank jointly, get product hand cleanser after high-speed stirred is uniform.
Further, step（1）Operating polyvinyl alcohol described in b is low molecular weight low viscosity polyvinyl alcohol, viscosity
It is 5.6, average molecular weight 16000.
Further, step（1）Operating essential oil described in b is by peppermint oil dementholized, tea tree ethereal oil according to weight ratio 1:2.5
It mixes.
Further, step（1）The mass fraction for operating hydrochloric acid in hydrochloric acid solution described in c is 5%, the hydrogen-oxygen
The mass fraction for changing sodium hydroxide in sodium solution is 7%.
Further, step（1）Temperature when operating calcination processing described in d in control calcining furnace is 900 DEG C.
Further, step（1）The frequency of ultrasonic wave is 400kHz when operating the processing of ultrasonic vibration described in e, described
Drying process when control drying box in temperature be 90 DEG C.
Further, step（3）Described in high-speed stirred processing when speed of agitator be 2200 revs/min.
Embodiment 3
A kind of preparation method of the hand cleanser of effect stability, includes the following steps：
（1）The preparation of antibacterial load-carrying additive：
A. by formaldehyde and ammeline according to mass ratio 1：1.7 mixed after be put into reaction kettle, its total matter is then added
Mixture A is obtained after measuring 2.6% boric acid, 0.45% ferrocene, the pH value of mixture A is then adjusted to 8.5, heating keeps anti-
Answering the temperature in kettle is 42 DEG C, and with spare after 380 revs/min of revolving speed stir process 37min；
B. 8% polyvinyl alcohol of mixture A gross mass, 3% ethyl acetate, 3.5% is added into operation a treated reaction kettle
Sodium chloride, 35% essential oil, 5% chitosan, 2% sodium pyrophosphate, temperature is then risen to 52 DEG C, with 550 revs/min
Taken out after revolving speed stir process 51min, then with 110 times of its gross mass of deionized water jointly after mixing mixture B is standby
With；
C. bentonite is put into hydrochloric acid solution after immersion treatment 5min and is taken out, then placed into sodium hydroxide solution and soak
It is taken out after bubble processing 6min, it is spare after finally being rinsed with deionized water to neutrality；
D. will operation c treated that bentonite is put into calcining furnace carries out calcination processing, taken out after 2h spare；
E. it will be filtered after ultrasonic vibration processing 6h, most in operation d treated bentonite the is immersed in operation resulting mixture B of b
The bentonite filtered out is put into drying box afterwards after being dried 7h and is taken out, it is spare to obtain antibacterial load-carrying additive；
（2）Raw material weighs spare：
It is spare that following substance is weighed by corresponding parts by weight：7 parts of dodecyldimethylamine oxide, 2 parts of laruyl alcohol oleates, 4 parts
Glycerol, 3 parts of Cocoamidopropyl betaines, 4 parts of hydroxyethyl celluloses, 2.5 parts of single dodecyl phosphates, 2 parts of cetanols
Polyethers, 5 parts of steps（1）Antibacterial load-carrying additive obtained, 100 parts of water；
（3）Finished product preparation：
By step（2）Weighed all raw materials are put into agitator tank jointly, get product hand cleanser after high-speed stirred is uniform.
Further, step（1）Operating polyvinyl alcohol described in b is low molecular weight low viscosity polyvinyl alcohol, viscosity
It is 6.0, average molecular weight 17000.
Further, step（1）Operating essential oil described in b is by peppermint oil dementholized, tea tree ethereal oil according to weight ratio 1:3 is mixed
It closes.
Further, step（1）The mass fraction for operating hydrochloric acid in hydrochloric acid solution described in c is 6%, the hydrogen-oxygen
The mass fraction for changing sodium hydroxide in sodium solution is 8%.
Further, step（1）Temperature when operating calcination processing described in d in control calcining furnace is 920 DEG C.
Further, step（1）The frequency of ultrasonic wave is 420kHz when operating the processing of ultrasonic vibration described in e, described
Drying process when control drying box in temperature be 93 DEG C.
Further, step（3）Described in high-speed stirred processing when speed of agitator be 2400 revs/min.
Comparative example 1
This comparative example 1 compared with Example 2, in step（2）Raw material weighs in spare, with etc. mass parts common bentonite
（Immersion treatment has been carried out by the corresponding essential oil of embodiment 2 in advance）Step of replacing（1）Antibacterial load-carrying additive ingredient obtained,
Method and step in addition to this is all the same.
Comparative example 2
This comparative example 2 compared with Example 2, in step（2）Raw material weighs in spare, eliminates step（1）It is obtained anti-
Bacterium load-carrying additive ingredient, instead directly it is added to step（1）Essential oil in antibacterial load-carrying additive obtained at
Point, method and step in addition to this is all the same.
In order to compare effect of the present invention, according to professional standard QB/T2850-2007 antibacterial bacteriostatic type detergent, to above-mentioned reality
It applies the corresponding hand cleanser obtained of example 2, comparative example 1, comparative example 2 and carries out fungistatic effect test, activity is
1wt%, action time are 20 minutes, and specific correlation data is as shown in table 1 below：
Table 1
The hand cleanser made from the method for the present invention it can be seen from upper table 1 has very strong bacteriostasis, and use value is high.
In order to further compare the stability of hand cleanser of the present invention, above-described embodiment 2, comparative example 1, comparison are implemented
The corresponding obtained hand cleanser of example 2 is put into glass dish, places one month in atmospheric environment, during which daily stir process one
It is secondary, 30s is stirred every time, and finally to treated, hand cleanser is tested according to the method described above, specific correlation data such as the following table 2 institute
Show：
Table 2
The hand cleanser made from the method for the present invention it can be seen from upper table 2 is exposed in air to be still able to maintain for a long time to be resisted well
Bacterium using effect, high stability, great application value.
Claims (7)
1. a kind of preparation method of the hand cleanser of effect stability, which is characterized in that include the following steps：
（1）The preparation of antibacterial load-carrying additive：
A. by formaldehyde and ammeline according to mass ratio 1：1.4 ~ 1.7 mixed after be put into reaction kettle, it is then added
Mixture A is obtained after the boric acid of gross mass 2.0 ~ 2.6%, 0.4 ~ 0.45% ferrocene, is then adjusted to the pH value of mixture A
8.0 ~ 8.5, heating keep reaction kettle in temperature be 38 ~ 42 DEG C, and with 350 ~ 380 revs/min of revolving speed stir process 32 ~
It is spare after 37min；
B. be added into operation a treated reaction kettle 6 ~ 8% polyvinyl alcohol of mixture A gross mass, 2 ~ 3% ethyl acetate,
2.5 ~ 3.5% sodium chloride, 30 ~ 35% essential oil, 3 ~ 5% chitosan, 1 ~ 2% sodium pyrophosphate, temperature is then risen to 48 ~ 52
DEG C, to be taken out after 500 ~ 550 revs/min of 47 ~ 51min of revolving speed stir process, then the deionization with 100 ~ 110 times of its gross mass
It is spare that water obtains mixture B after mixing jointly；
C. bentonite is put into hydrochloric acid solution after 3 ~ 5min of immersion treatment and is taken out, then placed into sodium hydroxide solution
It is taken out after 4 ~ 6min of immersion treatment, it is spare after finally being rinsed with deionized water to neutrality；
D. will operation c treated that bentonite is put into calcining furnace carries out calcination processing, taken out after 1 ~ 2h spare；
E. will be in operation d treated bentonite the is immersed in operation resulting mixture B of b, ultrasonic vibration filters after handling 4 ~ 6h,
Finally the bentonite filtered out is put into drying box after being dried 5 ~ 7h and is taken out, it is spare to obtain antibacterial load-carrying additive；
（2）Raw material weighs spare：
It is spare that following substance is weighed by corresponding parts by weight：4 ~ 7 parts of dodecyldimethylamine oxide, 1 ~ 2 part of laruyl alcohol oleate,
2 ~ 4 parts of glycerol, 1 ~ 3 part of Cocoamidopropyl betaine, 2 ~ 4 parts of hydroxyethyl celluloses, 1.5 ~ 2.5 parts of single dodecyl phosphoric acid
Ester, 1 ~ 2 part of ceteth, 3 ~ 5 parts of steps（1）Antibacterial load-carrying additive obtained, 95 ~ 100 parts of water；
（3）Finished product preparation：
By step（2）Weighed all raw materials are put into agitator tank jointly, get product hand cleanser after high-speed stirred is uniform.
2. a kind of preparation method of the hand cleanser of effect stability according to claim 1, which is characterized in that step（1）Behaviour
Making polyvinyl alcohol described in b is low molecular weight low viscosity polyvinyl alcohol, and viscosity is 4.5 ~ 6.0, average molecular weight 15000
~17000。
3. a kind of preparation method of the hand cleanser of effect stability according to claim 1, which is characterized in that step（1）Behaviour
Making essential oil described in b is by peppermint oil dementholized, tea tree ethereal oil according to weight ratio 1:2 ~ 3 mix.
4. a kind of preparation method of the hand cleanser of effect stability according to claim 1, which is characterized in that step（1）Behaviour
The mass fraction for making hydrochloric acid in hydrochloric acid solution described in c is 4 ~ 6%, the quality of sodium hydroxide in the sodium hydroxide solution
Score is 5 ~ 8%.
5. a kind of preparation method of the hand cleanser of effect stability according to claim 1, which is characterized in that step（1）Behaviour
Temperature when making calcination processing described in d in control calcining furnace is 880 ~ 920 DEG C.
6. a kind of preparation method of the hand cleanser of effect stability according to claim 1, which is characterized in that step（1）Behaviour
The frequency of ultrasonic wave is 380 ~ 420kHz when making the processing of ultrasonic vibration described in e, and when described drying process controls drying box
Interior temperature is 88 ~ 93 DEG C.
7. a kind of preparation method of the hand cleanser of effect stability according to claim 1, which is characterized in that step（3）In
The speed of agitator when high-speed stirred is handled is 2000 ~ 2400 revs/min.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112680285A (en) * | 2020-12-29 | 2021-04-20 | 上海塞寇文化传播有限公司 | Preparation method of environment-friendly cleaning agent with strong decontamination effect |
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