CN108827831A - Oscillatory type viscosity apparatus and its Detection Method of Liquid Viscosity - Google Patents

Oscillatory type viscosity apparatus and its Detection Method of Liquid Viscosity Download PDF

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Publication number
CN108827831A
CN108827831A CN201810578002.7A CN201810578002A CN108827831A CN 108827831 A CN108827831 A CN 108827831A CN 201810578002 A CN201810578002 A CN 201810578002A CN 108827831 A CN108827831 A CN 108827831A
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viscosity
spring plate
sensor
distance
vibration spring
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黄宇宁
叶辉煌
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Ye Yaojian
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Shenzhen Hongshu Technology Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/10Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
    • G01N11/16Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by measuring damping effect upon oscillatory body

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Abstract

A kind of oscillatory type viscosity apparatus and its Detection Method of Liquid Viscosity, wherein, oscillatory type viscosity apparatus includes fixing piece, vibration spring plate, distance-sensor, on the fixing piece of the close free end between the fixing end and free end of the vibration spring plate, after the predetermined displacement close to the distance-sensor of the free end of the vibration spring plate, it triggers distance-sensor and changes into another working condition from a kind of working condition, and issue electric signal;Driving device, including driving circuit and driving main body, the driving circuit are controlled by the controller, and provide predetermined resonant frequency signal to the driving main body;Temperature detection device is kept for the interval time of constant, collection distance-sensor the electric signal of driving device vibration frequency and the temperature data of sample with the distance-sensor, driving device and the controller of connection for the temperature detection of sample.The present invention has will not be by electromagnetic interference, the stable advantage of test result.

Description

Oscillatory type viscosity apparatus and its Detection Method of Liquid Viscosity
Technical field
The present invention relates to a kind of oscillatory type viscosity apparatus and its Detection Method of Liquid Viscosity.
Background technique
Viscosity is to indicate liquid in flowing, and the interior physical quantity to rub occurs for liquid internal, is the energy of liquid resistance deformation Power is for identifying certain finished products or semi-finished product important indicator.
In Practical Project and industrial production, it is often necessary to the viscosity of liquid is detected, to guarantee optimal process operation environment And product quality, to improve productivity effect.By the liquid viscosity in measurement process, the number of available fluid stream behavior According to for predicting that the technology controlling and process of Product Process process, the operability of transporting and product when in use have important finger Lead value.
Viscosimeter (Viscosimeter) is used to measure the instrument of the viscosity of liquid.Viscosimeter mainly has capillary viscosity Meter, rotational viscometer and vibrating type viscometer three categories.Wherein, the working principle of vibrating type viscometer is:It is intracorporal in liquid It will receive the inhibition of liquid when object vibration, the size of this effect is related with the viscosity of liquid.Common oscillatory type viscosity Meter is equipped with an elastic slice.When by pulsed current excitation, elastic slice generates mechanical oscillation.When elastic slice is immersed in sample, bullet The amplitude of piece is related with the viscosity of sample and density.In the case where known density, viscosity can be acquired from the frequency data measured Numerical value.
A kind of vibrating type viscometer disclosed in Chinese patent literature CN102183440A is exactly this kind of product, it includes level The fixing end of vibration device, the horizontal vibration device is fixed on bracket, and free end is equipped with sensing chip;Vibration device by Excitation identical with its resonance frequency, sensing chip vibrate the viscous drag that will receive liquid in a liquid;One detection device is used Movement velocity when vibrating vibration device becomes electric signal and sends controller to, and changing excitation density by control algolithm makes The vibration velocity is kept constant, then can measure viscous drag, and then calculate viscosity.The detection device of the vibrating type viscometer For electromagnetic detection mode, including detection coil and signal processing circuit;Detection coil is fixed on the other side of the permanent magnet, when When permanent magnet is moved with horizontal vibration device, induced voltage is generated in detection coil, realizes horizontal vibration device movement speed To the conversion of electric signal.This vibrating type viscometer has two groups of coils, one group of powered coil, and powered coil generates magnetic field excitation sense Piece is answered to vibrate, another group of coil is detection coil, and induction is located at the induction that the permanent magnet on sensing chip generates in detection coil Then induced voltage transformed value is again viscosity by voltage transformation value, this vibrating type viscometer is due to there are two groups of coils, two groups Coil generates two magnetic fields, can usually generate interference between two magnetic fields, and makes measurement result unstable.
Summary of the invention
In order to overcome the above problem, the present invention provides one kind will not be by electromagnetic interference, and the stable oscillatory type of test result is viscous Spend instrument and its Detection Method of Liquid Viscosity.
The technical scheme is that:A kind of vibrating type viscometer is provided, by controller control while automatic measurement liquid Viscosity and temperature, including following components:
For fixing the fixing piece of driving device;
The vibration spring plate made of ferrimagnet, described vibration spring plate one end are fixedly connected with the fixing piece, the vibration The elastic slice other end is free end;
Distance-sensor, on the fixing piece of the close free end between the fixing end and free end of the vibration spring plate, when Distance-sensor is triggered from a kind of work shape after the close predetermined displacement of the distance-sensor in the free end of the vibration spring plate State changes into another working condition, and issues electric signal;
Driving device, including driving circuit and driving main body, the driving circuit are controlled by the controller, mention to the driving main body For predetermined resonant frequency signal;
Temperature detection device, including temp probe and processing circuit, temp probe are used for the temperature detection of sample, processing electricity The simulation signal for the temperature that road will test is changed into digital signal;
With the distance-sensor, driving device and the controller of connection, holding driving device vibration frequency is constant, collects distance Inductor triggering moment, so that the time difference of electric signal is issued at the beginning of calculating elastic slice starting of oscillation to distance-sensor, with And the temperature data of sample.
As improvement of the present invention, the invention also includes be used to stablize the vibration spring plate made of ferrimagnet The baffle of vibration, the baffle and the vibration spring plate are arranged in parallel, and the baffle is located at the separate institute of the vibration spring plate The side of fixing piece is stated, at least one end of the baffle is fixedly connected with the fixing piece.
As improvement of the present invention, the driving main body includes iron core and driving coil;After the driving coil is powered Magnetic field is generated, vibration spring plate is vibrated.
As improvement of the present invention, the fixing piece is a box body, and the vibration spring plate is located on the lateral wall of box body, At least described driving main body and the distance-sensor are located in box, the driving main body and described distance-sensor one end part Ground stretches out in outside box body, and corresponding with the position of the vibration spring plate.
As improvement of the present invention, protection circuit is parallel between the disengaging both ends of the driving coil.
As improvement of the present invention, there are also range sensor protective covers for 3 outside of range sensor.Range sensor It is embedded into protective cover, first is that playing protection waterproof action, two can also play the role of fixation spring tab displacement.
As improvement of the present invention, the invention also includes the container for containing solvent and executing agency, the executing agencies When the viscosity of fluid to be measured is greater than predetermined value, the solvent in container is blended into fluid to be measured according to the instruction of controller.
The present invention also provides a kind of Detection Method of Liquid Viscosity, include the following steps,
S1, under the control of the controller, driving circuit provide the square-wave pulse signal of preset frequency to driving coil;
S2, pulse signal make driving coil generate magnetic field identical with preset frequency;
S3, the magnetic field suction vibration spring plate deformation, it is mobile to distance-sensor, when the free end of the vibration spring plate is to described Distance-sensor triggers distance-sensor from a kind of working condition and changes into another working condition after predetermined displacement, and Electric signal is issued to controller;
S4, controller control the driving coil power-off, and the vibration spring plate restores reset condition;In cycles;Controller root The time difference for issuing electric signal at the beginning of according to vibration spring plate starting of oscillation to distance-sensor, find out the viscosity of liquid.
As improvement of the present invention, the invention also includes S5, temperature-compensating step, controller is according to temp probe institute The temperature for the current environment measured is compared with environment temperature when calibration, because temperature will affect the magnetic force size of coil, And then influence the viscosity number of measurement.It is modified according to viscosity of the comparison result to the liquid that S4 step is found out.
It further include S6, viscosity-adjusting agent step after S4 or S5 step as improvement of the present invention, controller is according to working as Preceding viscosity or revised actual viscosity are held when the viscosity of fluid to be measured is greater than predetermined viscosity value according to the instruction of controller Solvent is blended into fluid to be measured by row mechanism, to adjust actual viscosity.
The present invention has will not be by electromagnetic interference, the stable advantage of test result.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of embodiment of the invention.
Fig. 2 is the protection electrical block diagram of Fig. 1.
Fig. 3 is method frame structure schematic diagram of the invention.
Specific embodiment
A specific embodiment of the invention is described in further detail with reference to the accompanying drawing.
The working principle of the invention is:
When to the rectangular pulse signal of driving coil input preset frequency, driving coil is due to that electric must can generate magnetic field, magnetic field To attract vibration spring plate deformation, vibration spring plate can be mobile to distance-sensor, when the free end of the vibration spring plate is to described Distance-sensor triggers distance-sensor from a kind of working condition and changes into another working condition after predetermined displacement, and Electric signal is issued to controller, controller controls driving coil and powers off at once.Vibration spring plate restores reset condition.In cycles, Vibrate vibration spring plate always.Controller according to vibration spring plate starting of oscillation at the beginning of to distance-sensor issue electric signal when Between it is poor, find out the viscosity of liquid;When detection, environment temperature and temperature when calibration have the temperature difference, also need to the viscosity of measurement into Row amendment.
According to the definition of viscosity, it is defined as a pair of of parallel-plate, area A is filled with certain liquid between dr, plate;The present is to upper Plate applies a thrust F, power needed for making it generate a velocity variations degree.Since the viscosity of liquid transmits this power layer by layer, each layer Also corresponding sports, one velocity gradient dv/dr of formation claim shear rate to liquid, and F/A is known as shear stress.Shear rate and shearing There is following relationship between stress:
(F/A)=η(dv/dr)Formula one
η is viscosity, and F is the thrust applied onboard, and A is the area of plate, and dv/dr is the speed increment in unit length, i.e., Dv is speed increment, and dr is displacement increment.
In the present invention, apply thrust onboard:
F=F1-F2 formula two
F1 is magnetic force, and F2 is the elastic force of elastic slice.
Speed increment in unit length:
(dv/dr)=V/S=1/t formula three
V is the average speed of elastic slice, and S is elastic slice displacement, and t is the time of elastic slice movement.
To sum up:η=(F1-F2)* t/A formula four
F1 is magnetic force in formula, and F2 is elastic force, and t is elastic slice run duration, and A is elastic slice area.F1, F2, A are invariant, it is seen that Liquid viscosity is directly proportional to the run duration of elastic slice, as long as detecting that elastic slice run duration can find out the viscosity of liquid.
When viscosity sensor is put into a kind of normal fluid, time t0 at this time can detecte out, viscosity at this time can be used Flow cup measures.So as to obtain(F1-F2)The value of/A.
When being put into fluid to be measured, the time t of liquid can be detected out, can be calculated separately by the formula of bringing into four A kind of viscosity of liquid.
When viscosity apparatus immerse liquid in when, due to liquid viscosity difference, thus at the beginning of vibration spring plate starting of oscillation to away from The time for issuing electric signal from inductor also can be different, by detection vibration spring plate starting of oscillation at the beginning of sent out to distance-sensor The time difference of electric signal can measure the viscosity of liquid out.
Referring to Figure 1 and Fig. 2, Fig. 1 and Fig. 2 disclose be a kind of vibrating type viscometer, by controller control simultaneously it is automatic Measure the viscosity and temperature of liquid, including following components:
For fixing the fixing piece 1 of driving device 4;
Vibration spring plate 2 made of ferrimagnet, described 2 one end 21 of vibration spring plate is fixedly connected with the fixing piece 1, described 2 other end of vibration spring plate is free end 22;Ferrimagnet in the present embodiment can be iron, cobalt or nickel and its iron cobalt or nickel Alloy material, especially steel disc or teleoseal piece;
Distance-sensor 3, the fixing piece 1 of the close free end 22 between the fixing end and free end of the vibration spring plate 2 On, when the free end 22 of the vibration spring plate 2 to the distance-sensor 3 close to predetermined displacement after, triggering distance-sensor 3 from A kind of working condition changes into another working condition, and issues electric signal;Distance-sensor 3 in the present invention can be close Switch or range sensor, when the free end of vibration spring plate 2 22 to the distance-sensor 3 close to predetermined displacement after, triggering away from From inductor 3 from pass, or the variation from closing to opening is reached, so that distance-sensor 3 be made to generate an electric signal, electric signal quilt It is conveyed to controller 6;
Driving device 4, including driving circuit 41 and driving main body 42, the driving circuit 41 is controlled by controller 6, to the drive Dynamic main body 42 provides predetermined resonant frequency signal;Resonant frequency signal is generally square-wave pulse signal;
Temperature detection device 5, including temp probe 51 and processing circuit 52, temp probe 51 both can be used for the temperature of sample Degree detection, also can detecte the temperature of coil.The simulation signal for the temperature that processing circuit 52 will test is changed into digital signal;
With the distance-sensor 3, driving device 4 and the controller 6 connecting, constant, the receipts of 4 vibration frequency of driving device are kept Collect the triggering moment of the electric signal of distance-sensor 3 and the temperature data of sample.Controller 6 in the present embodiment is by model The chip and base peripheral circuit of stm8s105 is constituted.
Preferably, the invention also includes the baffles vibrated made of ferrimagnet for stablizing the vibration spring plate 2 7, the baffle 7 is arranged in parallel with the vibration spring plate 2, and the baffle 7 is located at the separate fixation of the vibration spring plate 2 The side of part 1, at least one end of the baffle 7 are fixedly connected with the fixing piece 1.The baffle 7 plays protection vibration spring plate 2 and stable vibration elastic slice 2 effect, i.e., when driving coil 422 power off after, vibration spring plate 2 can stop in time.
Preferably, the driving main body 42 includes iron core 421 and driving coil 422;The driving coil 422 produces after being powered Magnetisation field vibrates vibration spring plate 2.The shape of the iron core 421 can be U-shaped, and the driving coil 422 can be divided into 2 On a two poles for being respectively wound around U-iron core, it is also possible to an independent driving coil 422 and is wrapped in U-iron core On the pole of the free end 22 of elastic slice 2;
Preferably, the fixing piece 1 is a box body, and the vibration spring plate 2 is located on the lateral wall of box body, at least described driving master Body 42 and the distance-sensor 3 are located in box, and the driving main body 42 and 3 one end of the distance-sensor partly stretch out in Outside box body, and it is corresponding with the position of the vibration spring plate 2.
Preferably, protection circuit 8 is parallel between the disengaging both ends of the driving coil 422.Protection circuit 8 can join See Fig. 2, the first voltage-stabiliser tube D1 and the second voltage-stabiliser tube D2 in circuit is protected to play the induced electricity to driving coil 422 after a loss of power The effect discharged, while immediate stability elastic slice can be played the role of after power-off.Third voltage-stabiliser tube D3, the 4th voltage-stabiliser tube D4, the 5th voltage-stabiliser tube D5 and the 6th voltage-stabiliser tube D6 play the role of the electric signal that stabilizing distance inductor 3 is inputted to controller 6.
Preferably, there are also range sensor protective covers for 3 outside of range sensor.Range sensor is embedded into protective cover Interior, first is that playing protection waterproof action, two can also play the role of fixation spring tab displacement.
Preferably, the invention also includes the container for containing solvent and executing agency, the executing agency is in fluid to be measured When viscosity is greater than predetermined value, the solvent in container is blended into fluid to be measured according to the instruction of controller 6.
Fig. 3 is referred to, the present invention also provides a kind of Detection Method of Liquid Viscosity, include the following steps,
S1, under the control of controller 6, driving circuit 42 to driving coil 422 provide preset frequency pulse signal;
S2, pulse signal make driving coil 422 generate magnetic field identical with preset frequency;
S3,2 deformation of magnetic field suction vibration spring plate, it is mobile to distance-sensor 3, when the free end 22 of the vibration spring plate 2 To the distance-sensor 3 after predetermined displacement, distance-sensor 3 is triggered from a kind of working condition and changes into another work State, and electric signal is issued to controller 6;Ferrimagnet in the present embodiment can be iron, cobalt or nickel and its iron, cobalt or The alloy material of nickel, especially steel disc or teleoseal piece;Distance-sensor 3 in the present invention can be close to switch or away from From sensor, when the free end of vibration spring plate 2 22 to the distance-sensor 3 close to predetermined displacement after, trigger distance-sensor 3 It is closed from reaching, or the variation from closing to opening, so that distance-sensor 3 be made to generate an electric signal, electric signal is fed to control Device 6 processed;
S4, the driving coil 422 power off, and the vibration spring plate 2 restores reset condition;In cycles;Controller 6 is according to vibration The time difference for issuing electric signal at the beginning of 2 starting of oscillation of elastic slice to distance-sensor 3, find out the viscosity of liquid.
As improvement of the present invention, the invention also includes S5, temperature-compensating step, controller 6 is according to temp probe 51 Measured current environmental temperature is compared with environment temperature when calibration, is repaired to the viscosity for the liquid that S4 step is found out Just.
It further include S6, viscosity-adjusting agent step after S4 or S5 step as improvement of the present invention, controller 6 is according to working as Preceding viscosity or revised actual viscosity are held when the viscosity of fluid to be measured is greater than predetermined viscosity value according to the instruction of controller 6 Solvent is blended into fluid to be measured by row mechanism, to adjust actual viscosity.
Obviously, various changes and modifications can be made to the invention without departing from essence of the invention by those skilled in that art Mind and range.In this way, if these modifications and changes of the present invention belongs to the range of the claims in the present invention and its equivalent technologies Within, then the invention is also intended to include including these modification and variations.

Claims (8)

1. a kind of vibrating type viscometer, by controller control while the viscosity and temperature of automatic measurement liquid, including following components:
For fixing driving device(4)Fixing piece(1);It is characterized in that,
The vibration spring plate made of ferrimagnet(2), the vibration spring plate(2)One end(21)With the fixing piece(1)It is fixed Connection, the vibration spring plate(2)The other end is free end(22);
Distance-sensor(3), it is located at the vibration spring plate(2)Fixing end and free end between close free end(22)Consolidate Determine part(1)On, when the vibration spring plate(2)Free end(22)To the distance-sensor(3)After predetermined displacement, triggering Distance-sensor(3)Another working condition is changed into from a kind of working condition, and issues electric signal;
Driving device(4), including driving circuit(41)With driving main body(42), the driving circuit(41)By controller(5)Control System, to the driving main body(42)Predetermined resonant frequency signal is provided;
Temperature detection device(5), including temp probe(51)And processing circuit(52), temp probe(51)For sample Temperature detection, processing circuit(52)The simulation signal for the temperature that will test is changed into digital signal;
With the distance-sensor(3), driving device(4)With the controller of connection(6), keep driving device(4)Vibration frequency Constant, collection distance-sensor(3)Triggering moment, at the beginning of starting of oscillation to distance-sensor issue electric signal time The temperature data of difference and sample.
2. the vibrating type viscometer according to claim 1, which is characterized in that further include being used made of ferrimagnet In stablizing the vibration spring plate(2)The baffle of vibration(7), the baffle(7)With the vibration spring plate(2)Parallel arrangement, and institute State baffle(7)Positioned at the vibration spring plate(2)Far from the fixing piece(1)Side, the baffle(7)At least one end with The fixing piece(1)It is fixedly connected.
3. according to claim 1 or vibrating type viscometer described in 2, which is characterized in that the driving main body(42)Including iron core (421)And driving coil(422);The driving coil(422)Magnetic field is generated after energization, makes vibration spring plate(2)Vibration.
4. vibrating type viscometer according to claim 3, which is characterized in that in the driving coil(422)Disengaging two Protection circuit is parallel between end(8).
5. vibrating type viscometer according to claim 1 or 2, which is characterized in that further include containing the container of solvent and holding Row mechanism, the executing agency is when the viscosity of fluid to be measured is greater than predetermined value, according to controller(6)Instruction will be in container Solvent is blended into fluid to be measured.
6. a kind of Detection Method of Liquid Viscosity, it is characterised in that:Include the following steps,
S1, in controller(6)Control under, driving circuit(42)To driving coil(422)The square-wave pulse of preset frequency is provided Signal;
S2, pulse signal make driving coil(422)Generate magnetic field identical with preset frequency;
S3, the magnetic field suction vibration spring plate(2)Deformation, to distance-sensor(3)It is mobile, when the vibration spring plate(2)From By holding(22)To the distance-sensor(3)After predetermined displacement, distance-sensor is triggered(3)Change from a kind of working condition For another working condition, and to controller(6)Issue electric signal;
S4, controller control the driving coil(422)Power-off, the vibration spring plate(2)Restore reset condition;In cycles; Controller(6)According to vibration spring plate(2)Distance-sensor is arrived at the beginning of starting of oscillation(3)It the time difference for issuing electric signal, finds out The viscosity of liquid.
7. Detection Method of Liquid Viscosity according to claim 6, it is characterised in that:It further include S5, temperature-compensating step, Controller(6)According to temp probe(51)Temperature go out the current environment measured temperature, with calibration when environment temperature carry out Comparison is modified according to viscosity of the comparison result to the liquid that S4 step is found out.
8. Detection Method of Liquid Viscosity described according to claim 6 or 7, it is characterised in that:It is also wrapped after S4 or S5 step It includes, S6, viscosity-adjusting agent step, controller(6)It is big in the viscosity of fluid to be measured according to actual viscosity or revised actual viscosity When predetermined viscosity value, according to controller(6)Command execution unit solvent is blended into fluid to be measured, it is current viscous to adjust Degree.
CN201810578002.7A 2018-06-07 2018-06-07 Oscillatory type viscosity apparatus and its Detection Method of Liquid Viscosity Withdrawn CN108827831A (en)

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CN111504854A (en) * 2020-04-13 2020-08-07 中国矿业大学 Temperature difference type measuring device and method for viscosity of Newton fluid

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CA1224060A (en) * 1985-03-15 1987-07-14 Paul Beaudoin Vibrating needle viscosity meter
JPH03123839A (en) * 1989-10-06 1991-05-27 Kobe Steel Ltd Method for immersing vibrating piece of vibrating viscometer
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ITMI942479A1 (en) * 1994-12-07 1996-06-07 Selectra S R L DEVICE AND PROCEDURE FOR MEASUREMENT AND CONTROL OF THE SPEED OF A LIQUID
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111504854A (en) * 2020-04-13 2020-08-07 中国矿业大学 Temperature difference type measuring device and method for viscosity of Newton fluid
CN111504854B (en) * 2020-04-13 2021-12-31 中国矿业大学 Temperature difference type measuring device and method for viscosity of Newton fluid

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