CN108812933A - A kind of Fatsia japonica seed nutrient blend oil and its preparation process - Google Patents

A kind of Fatsia japonica seed nutrient blend oil and its preparation process Download PDF

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Publication number
CN108812933A
CN108812933A CN201810526384.9A CN201810526384A CN108812933A CN 108812933 A CN108812933 A CN 108812933A CN 201810526384 A CN201810526384 A CN 201810526384A CN 108812933 A CN108812933 A CN 108812933A
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oil
fatsia japonica
japonica seed
fatsia
nutrient blend
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蒋新龙
蒋益花
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Zhejiang Shuren University
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Zhejiang Shuren University
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/007Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A23D9/04Working-up

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

A kind of Fatsia japonica seed nutrient blend oil and its preparation process, belong to edible oil and its processing technique field.It is characterized in that being process by the material component of following parts by weight:9-15 parts of Fatsia japonica seed oil, 40-50 parts of peanut oil, 12-16 parts of linseed oil, 25-34 parts of corn oil.In 35~40 DEG C of thermostatic tank, Fatsia japonica seed oil, peanut oil, linseed oil, corn oil are sequentially added, 30~60min is mixed to full and uniform, obtained Fatsia japonica seed nutrient blend oil.Fatsia japonica seed nutrient blend oil provided by the invention, on the one hand ω -3 rich in is polyene unsaturated fatty acid and ω -6 is polyene unsaturated fatty acid, and ratio is reasonable, the two can be absorbed by human body equilibrium, it is throughout the year edible to enhance eater's constitution and intelligence, prevent the generation of cardiovascular and cerebrovascular disease.On the other hand, the raw material of selection, preparation process are simple, and production cost is low, convenient.

Description

A kind of Fatsia japonica seed nutrient blend oil and its preparation process
Technical field
The present invention relates to edible oil and its processing technique fields, reconcile in particular to a kind of Fatsia japonica seed nutrition Oil and its preparation process.
Background technique
Edible oil is also referred to as " edible oil ", refers to animal or vegetable fat used in production food products, due to original Expect that reasons, the common edible oils such as source, processing technology and quality are mostly vegetable fat.Vegetable fat is divided into nonessential rouge again Fat acid and essential fatty acid.Non-essential fatty acid includes saturated fatty acid and monounsaturated fatty acids (oleic acid), mainly contains this The grease of class fatty acid has palm oil, rapeseed oil, sesame oil, olive oil etc..This kind of fatty acid can be in human body by carbohydrate With protein Synthesis, so not being the fatty acid of intake needed by human.A large amount of thermal energy can be discharged when they are oxidized, such as Intake is excessive to easily lead to the diseases such as fat, hyperlipidemia and cardiovascular and cerebrovascular embolism, should control intake.Essential fatty acid includes ω -3 It is polyene unsaturated fatty acid, alpha-linolenic acid and ω -6 is polyene unsaturated fatty acid-linoleic acid.
Wherein, it is to perfect brain neuron, enhancing intelligence to the main function of human health that ω -3, which is polyene unsaturated fatty acid, Power and memory prevent cardiovascular and cerebrovascular disease, can change human body words spoken by an actor from offstage cell state, mitigating inflammation and allergy, raising body Immunoregulation capability, additionally it is possible to inhibit to promote the formation of cancer substance, the generation etc. of pre- anti-cancer.ω -6 is polyene unsaturated fatty acid Main function to human body is prevention and cure of cardiovascular disease.ω -6 is polyene unsaturated fatty acid in edible oil and fat such as soybean oil, flower Exist in the form of linoleic in oil generation, corn oil, sunflower oil, linseed oil etc.;ω -3 is polyene unsaturated fatty acid flat Content is few in normal food, and most people also just lacks the intake of this respect.
Fatsia japonica is Araliaceae Fatsia evergreen shrubs, originates in China Taiwan and Japan, now on the south the Yangtze river basin Area is widely distributed.Its root, leaf, flower and seed all have certain medical value, and many scholars are to ingredient therein and its mention Taking technique is studied.Currently, about the research of Fatsia japonica seed oil, there is not been reported, and the present inventor passes through to Fatsia japonica The Study on extraction and Fatsia japonica seed oil analysis of physical and chemical property of seed oil.The result shows that under Optimizing Technical, it is octagonal The oil yield of golden disk seed oil is up to 35.55%.Analysis of physical and chemical property, acid value (KOH) 2.88mg/g of Fatsia japonica seed oil, is lower than 3.00mg/g meets edible vegetable oil national standard;Peroxide value 6.63mmol/kg is lower than edible vegetable oil national standard;Iodine Value 97.23g/100g, belongs to nondrying oil, illustrates that Fatsia japonica seed oil degree of unsaturation is lower;Relative density 0.8928, it is made The Fatsia japonica seed oil obtained is the light yellow liquid of clear.Judge from the physical and chemical index of measurement, Fatsia japonica seed oil reaches Edible vegetable oil national standard.
In addition, analyzing Fatsia japonica seed oil fatty acid composition and content, detected altogether in Fatsia japonica seed oil 15 kinds of fatty acid, main component is oleic acid (87.02%), linoleic acid (7.00%), cis- 10- pentadecylenic acid (3.08%), stearic Sour (0.86%), 4 kinds of primary fat acid contents account for 97.96%, and wherein unsaturated fatty acid relative amount is 97.10%, especially Based on oleic acid.Oleic acid antioxidative stabilizer is good, helps to reduce low density lipoprotein cholesterol content in blood of human body, simultaneously High-density Lipoprotein-cholesterol is maintained, has effects that nutrition and health care and medication, oleic acid is called " safe fats by nutrition circle Acid ", how much is the content of oleic acid, is the important symbol for evaluating edible oil quality.Therefore, Fatsia japonica seed oil can be used as hyperlipidemia, Coronary atherosclerosis, cardiovascular patient long-term Dietotherapy health oil product, it is edible to can be used as high quality food oil source and functionality Oil development and utilization.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of Fatsia japonica seed nutrient blend oil and its preparation process, Fatty acid proportion is reasonable, meets the ratio of ω -6 and omega-3 polyunsaturated fatty acids in (4~6): in 1 range, especially containing 40% or more essential fatty acid-linoleic acid plus linolenic acid, be suitble to Chinese residents, can make Chinese residents to fat intake more Rationally, in addition, having for the generation for reducing the diseases such as hyperlipidemia, coronary atherosclerosis, angiocarpy, hypertension very heavy The meaning wanted.
In order to solve the above technical problems, the technical solution adopted by the present invention is that:A kind of Fatsia japonica seed nutrition reconciliation is provided Oil, it is characterised in that be process according to the material component of following parts by weight:
The preparation method of the Fatsia japonica seed oil is as follows:
S1:Fatsia japonica seed obtains Fatsia japonica seed powder after sorting, decladding, drying, crushing, being screened to 40~60 mesh;
S2:According to Fatsia japonica seed silty amount g:Extraction solvent volume ml is 1:The solid-liquid ratio of (8~10) is to Fatsia japonica Extraction solvent is added in seed powder;
S3:Sonication assisted treatment, handles 25~40min of time, decompression filters, concentration is made by 40~50 DEG C for the treatment of temperature Obtain Fatsia japonica seed oil.
Preferably, in the preparation method step S2 of Fatsia japonica seed oil, Extraction solvent is n-hexane, petroleum ether, acetone, nothing Any one in water-ethanol.
Preferably, in the preparation method step S3 of Fatsia japonica seed oil, 180~250W of power of ultrasonic treatment.
The various fatty acid that fat is formed in the Fatsia japonica seed nutrient blend oil account for the mass percent of total fatty acids Content is respectively:Saturated fatty acid 13.8~17.2%, monounsaturated fatty acids 40.7~43.7%, ω -3 linolenic acid 5.9~ 7.9%, ω -6 linoleic acid 32.5~35.0%, and total polyunsaturated fatty acid is 40.1~43.5%.
A kind of preparation process of Fatsia japonica seed nutrient blend oil, which is characterized in that the technique concrete operations are as follows:? In 35~40 DEG C of thermostatic tank, Fatsia japonica seed oil, peanut oil, linseed oil, corn oil are sequentially added, it is mixed 30~ 60min is made Fatsia japonica seed nutrient blend oil, then carries out tinning to full and uniform.
Compared with prior art, the beneficial effects of the present invention are:
1, exploitation Fatsia japonica seed oil is as raw material, on the one hand, Fatsia japonica seed oil making technology is simple, production cost It is low, no chemical solvent residual, edible safety.On the other hand, Fatsia japonica seed oil is in the base for reaching edible vegetable oil national standard On plinth, main component is based on unsaturated fatty acid, especially based on oleic acid.Oleic acid antioxidative stabilizer is good, helps to drop Low density lipoprotein cholesterol content in low blood of human body, while High-density Lipoprotein-cholesterol is maintained, there is nutrition to protect Strong and medication effect.Therefore, Fatsia japonica seed oil can be used as hyperlipidemia, coronary atherosclerosis, angiocarpy, hypertensive patient Long-term Dietotherapy health oil product, for reducing hyperlipidemia, coronary atherosclerosis, the generation of angiocarpy, the diseases such as hypertension It has a very important significance.
2, raw material peanut oil, linseed oil, corn oil are common vegetable oil, there is mature preparation process at present, It is readily available in the market, price material benefit.Wherein, saturated fatty acid (S), monounsaturated fatty acids (M), more insatiable hungers in peanut oil With fatty acid (P) ratio closest to 1:1.93:2.55, and be polyene unsaturated fatty acid there are also ω -6 abundant;Wherein, flax Containing more rich ω -3 in seed oil is polyene unsaturated fatty acid, thus the available equilibrium of the two, so that ω -6/ ω -3 exists (4~6):In 1 range, meet the World Health Organization, FAO (Food and Agriculture Organization of the United Nation) and Chinese nutrition to Chinese residents fat and rouge The recommended intake and recommendation ratio of fat acid.Wherein, corn oil is rich in the necessary vitamin E of human body and unsaturated fatty acid, contains For amount up to 80% or more, predominantly linoleic plus oleic acid, Linoleic acid accounts for 50% or more of grease total amount, has prevention and improves Artery sclerosis reduces the effects of heart disease occurs.
3, Fatsia japonica seed nutrient blend oil preparation process is simple, production cost is low, it is important that the Fatsia japonica of selection Seed oil, peanut oil, linseed oil, 4 vegetable oil of corn oil have respective unique nutritional ingredient, reconcile by a certain percentage, make The Fatsia japonica seed nutrient blend oil ω -3 rich in obtained is polyene unsaturated fatty acid and ω -6 is polyenoid unsaturated lipid Fat acid, and ratio is reasonable, the two can be absorbed by human body equilibrium, and it is throughout the year edible to enhance eater's constitution and intelligence, prevent heart and brain The generation of vascular diseases.
Specific embodiment
The present invention is further described through combined with specific embodiments below.
Embodiment one:
In 35 DEG C of thermostatic tanks, Fatsia japonica seed oil 10Kg, linseed oil 15Kg, corn oil 25Kg, peanut are sequentially added Oily 50Kg is mixed 30min to full and uniform, Fatsia japonica seed nutrient blend oil is made, then carries out tinning.
Wherein, the preparation process of Fatsia japonica seed oil is as follows:
S1:Fatsia japonica seed obtains Fatsia japonica seed powder after sorting, decladding, drying, crushing, being screened to 40~60 mesh;
S2:According to Fatsia japonica seed silty amount g:Extraction solvent volume ml is 1:9.6 solid-liquid ratio is to Fatsia japonica seed powder Middle addition Extraction solvent;
S3:Ultrasonic treatment, 48 DEG C of temperature, time 30min, decompression filters, obtained Fatsia japonica seed oil is concentrated.
In the preparation method step S2 of the Fatsia japonica seed oil, Extraction solvent is petroleum ether.
In the preparation method step S3 of the Fatsia japonica seed oil, ultrasonic power 200W.
Fatyy acids are carried out to obtained Fatsia japonica seed nutrient blend oil, various fatty acid account for the matter of total fatty acids Measuring degree is respectively:ω -3 linolenic acid 7.3%, ω -6 linoleic acid 33.4%, monounsaturated fatty acids 42.4%, saturation Fatty acid 16.4%, wherein:The ratio of ω -3/ ω -6 is 1: 4.6, in the range of 1: 4-6, polyunsaturated fatty acid gross mass Percentage composition is 41.2%.
Embodiment two:
In 35 DEG C of thermostatic tanks, Fatsia japonica seed oil 10Kg, linseed oil 12Kg, corn oil 28Kg, peanut are sequentially added Oily 50Kg is mixed 35min to full and uniform, Fatsia japonica seed nutrient blend oil is made, then carries out tinning.
Wherein, the preparation process of Fatsia japonica seed oil is as follows:
S1:Fatsia japonica seed obtains Fatsia japonica seed powder after sorting, decladding, drying, crushing, being screened to 40~60 mesh;
S2:According to Fatsia japonica seed silty amount g:Extraction solvent volume ml is 1:8.5 solid-liquid ratio is to Fatsia japonica seed powder Middle addition Extraction solvent;
S3:Sonication assisted treatment, handles time 25min by 42 DEG C for the treatment of temperature, and decompression filters, octagonal gold is made in concentration Disk seed oil.
In the preparation method step S2 of the Fatsia japonica seed oil, Extraction solvent is n-hexane.
In the preparation method step S3 of the Fatsia japonica seed oil, ultrasonic power 220W.
Fatyy acids are carried out to obtained Fatsia japonica seed nutrient blend oil, various fatty acid account for the matter of total fatty acids Measuring degree is respectively:ω -3 linolenic acid 5.9%, ω -6 linoleic acid 34.4%, monounsaturated fatty acids 42.6%, saturation Fatty acid 16.6%, wherein:The ratio of ω -3/ ω -6 is 1: 5.8, in the range of 1: 4-6, polyunsaturated fatty acid gross mass Percentage composition is 40.8%.
Embodiment three:
In 37 DEG C of thermostatic tanks, Fatsia japonica seed oil 12Kg, linseed oil 12Kg, corn oil 30Kg, peanut are sequentially added Oily 46Kg is mixed 45min to full and uniform, Fatsia japonica seed nutrient blend oil is made, then carries out tinning.
Wherein, the preparation process of Fatsia japonica seed oil is as follows:
S1:Fatsia japonica seed obtains Fatsia japonica seed powder after sorting, decladding, drying, crushing, being screened to 40~60 mesh;
S2:According to Fatsia japonica seed silty amount g:Extraction solvent volume ml is 1:9.1 solid-liquid ratio is to Fatsia japonica seed powder Middle addition Extraction solvent;
S3:Sonication assisted treatment, handles time 40min by 48 DEG C for the treatment of temperature, and decompression filters, octagonal gold is made in concentration Disk seed oil.
In the preparation method step S2 of the Fatsia japonica seed oil, Extraction solvent is acetone.
In the preparation method step S3 of the Fatsia japonica seed oil, ultrasonic power 180W.
Fatyy acids are carried out to obtained Fatsia japonica seed nutrient blend oil, various fatty acid account for the matter of total fatty acids Measuring degree is respectively:ω -3 linolenic acid 5.9%, ω -6 linoleic acid 34.2%, monounsaturated fatty acids 43.2%, saturation Fatty acid 16.7%, wherein:The ratio of ω -3/ ω -6 is 1: 5.8, in the range of 1: 4-6, polyunsaturated fatty acid gross mass Percentage composition is 40.4%.
Example IV:
In 37 DEG C of thermostatic tanks, Fatsia japonica seed oil 10Kg, linseed oil 16Kg, corn oil 34Kg, peanut are sequentially added Oily 40Kg is mixed 50min to full and uniform, Fatsia japonica seed nutrient blend oil is made, then carries out tinning.
Wherein, the preparation process of Fatsia japonica seed oil is as follows:
S1:Fatsia japonica seed obtains Fatsia japonica seed powder after sorting, decladding, drying, crushing, being screened to 40~60 mesh;
S2:According to Fatsia japonica seed silty amount g:Extraction solvent volume ml is 1:10 solid-liquid ratio is into Fatsia japonica seed powder Extraction solvent is added;
S3:Sonication assisted treatment, handles time 38min by 45 DEG C for the treatment of temperature, and decompression filters, octagonal gold is made in concentration Disk seed oil.
In the preparation method step S2 of the Fatsia japonica seed oil, Extraction solvent is dehydrated alcohol.
In the preparation method step S3 of the Fatsia japonica seed oil, ultrasonic power 200W.
Fatyy acids are carried out to obtained Fatsia japonica seed nutrient blend oil, various fatty acid account for the matter of total fatty acids Measuring degree is respectively:ω -3 linolenic acid 7.9%, ω -6 linoleic acid 34.6%, monounsaturated fatty acids 40.7%, saturation Fatty acid 16.3%, wherein:The ratio of ω -3/ ω -6 is 1: 4.4, in the range of 1: 4-6, polyunsaturated fatty acid gross mass Percentage composition is 43.0%.
Embodiment five:
In 40 DEG C of thermostatic tanks, Fatsia japonica seed oil 15Kg, linseed oil 16Kg, corn oil 29Kg, peanut are sequentially added Oily 40Kg is mixed 55min to full and uniform, Fatsia japonica seed nutrient blend oil is made, then carries out tinning.
Wherein, the preparation process of Fatsia japonica seed oil is as follows:
S1:Fatsia japonica seed obtains Fatsia japonica seed powder after sorting, decladding, drying, crushing, being screened to 40~60 mesh;
S2:According to Fatsia japonica seed silty amount g:Extraction solvent volume ml is 1:8.9 solid-liquid ratio is to Fatsia japonica seed powder Middle addition Extraction solvent;
S3:Sonication assisted treatment, handles time 40min by 50 DEG C for the treatment of temperature, and decompression filters, octagonal gold is made in concentration Disk seed oil.
In the preparation method step S2 of the Fatsia japonica seed oil, Extraction solvent is petroleum ether.
In the preparation method step S3 of the Fatsia japonica seed oil, ultrasonic power 220W.
Fatyy acids are carried out to obtained Fatsia japonica seed nutrient blend oil, various fatty acid account for the matter of total fatty acids Measuring degree is respectively:ω -3 linolenic acid 7.8%, ω -6 linoleic acid 32.4%, monounsaturated fatty acids 43.7%, saturation Fatty acid 15.6%, wherein:The ratio of ω -3/ ω -6 is 1: 4.2, in the range of 1: 4-6, polyunsaturated fatty acid gross mass Percentage composition is 40.7%.
Embodiment six:
In 40 DEG C of thermostatic tanks, Fatsia japonica seed oil 9Kg, linseed oil 14Kg, corn oil 32Kg, peanut oil are sequentially added 60min is mixed in 45Kg, and Fatsia japonica seed nutrient blend oil is made, then carries out tinning.
Wherein, the preparation process of Fatsia japonica seed oil is as follows:
S1:Fatsia japonica seed obtains Fatsia japonica seed powder after sorting, decladding, drying, crushing, being screened to 40~60 mesh;
S2:According to Fatsia japonica seed silty amount g:Extraction solvent volume ml is 1:9.6 solid-liquid ratio is to Fatsia japonica seed powder Middle addition Extraction solvent;
S3:Sonication assisted treatment, handles time 37min by 45 DEG C for the treatment of temperature, and decompression filters, octagonal gold is made in concentration Disk seed oil.
In the preparation method step S2 of the Fatsia japonica seed oil, Extraction solvent is n-hexane.
In the preparation method step S3 of the Fatsia japonica seed oil, ultrasonic power 250W.
Fatyy acids are carried out to obtained Fatsia japonica seed nutrient blend oil, various fatty acid account for the matter of total fatty acids Measuring degree is respectively:ω -3 linolenic acid 6.9%, ω -6 linoleic acid 35.0%, monounsaturated fatty acids 41.1%, saturation Fatty acid 16.6%, wherein:The ratio of ω -3/ ω -6 is 1: 5.1, in the range of 1: 4-6, polyunsaturated fatty acid gross mass Percentage composition is 42.3%.
Above-mentioned embodiment is only a preferred solution of the present invention, not the present invention is made in any form Limitation, there are also other variations and modifications on the premise of not exceeding the technical scheme recorded in the claims.

Claims (6)

1. a kind of Fatsia japonica seed nutrient blend oil, which is characterized in that the ready-mixed oil is added by the material component of following parts by weight Work forms:
2. a kind of Fatsia japonica seed nutrient blend oil according to claim 1, which is characterized in that the Fatsia japonica seed oil Preparation method is as follows:
S1:Fatsia japonica seed obtains Fatsia japonica seed powder after sorting, decladding, drying, crushing, being screened to 40~60 mesh;
S2:According to Fatsia japonica seed silty amount g:Extraction solvent volume ml is 1:The solid-liquid ratio of (8~10) is to Fatsia japonica seed powder Middle addition Extraction solvent;
S3:Sonication assisted treatment, handles 25~40min of time by 40~50 DEG C for the treatment of temperature, then filters through decompression, concentration Fatsia japonica seed oil is made.
3. a kind of Fatsia japonica seed nutrient blend oil according to claim 2, which is characterized in that in the step S2, extract Solvent is any one in n-hexane, petroleum ether, acetone and dehydrated alcohol.
4. a kind of Fatsia japonica seed nutrient blend oil according to claim 2, which is characterized in that in the step S3, ultrasound The power of wave is 180~250W.
5. a kind of Fatsia japonica seed nutrient blend oil according to claim 1, which is characterized in that the Fatsia japonica seed nutrition The various fatty acid that fat is formed in ready-mixed oil account for the mass percentage contents of total fatty acids and are respectively:Saturated fatty acid 13.8~ 17.2%, monounsaturated fatty acids 40.7~43.7%, ω -3 linolenic acid 5.9~7.9%, ω -6 linoleic acid 32.5~ 35.0%, and total polyunsaturated fatty acid is 40.1~43.5%.
6. a kind of preparation process of Fatsia japonica seed nutrient blend oil, feature described according to claim 1~any one of 5 It is, the technique concrete operations are as follows:In 35~40 DEG C of thermostatic tank, Fatsia japonica seed oil, peanut oil, Asia are sequentially added Flaxseed oil, corn oil are mixed 30~60min to full and uniform, Fatsia japonica seed nutrient blend oil are made, is then filled Tank.
CN201810526384.9A 2018-05-29 2018-05-29 A kind of Fatsia japonica seed nutrient blend oil and its preparation process Pending CN108812933A (en)

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Application publication date: 20181116