CN108786168A - A kind of pharmaceutical purpose vaporation-type crystallization kettle - Google Patents
A kind of pharmaceutical purpose vaporation-type crystallization kettle Download PDFInfo
- Publication number
- CN108786168A CN108786168A CN201810603914.5A CN201810603914A CN108786168A CN 108786168 A CN108786168 A CN 108786168A CN 201810603914 A CN201810603914 A CN 201810603914A CN 108786168 A CN108786168 A CN 108786168A
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- CN
- China
- Prior art keywords
- fixed
- shell
- funnel
- support plate
- heat conducting
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0018—Evaporation of components of the mixture to be separated
- B01D9/0031—Evaporation of components of the mixture to be separated by heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
Abstract
The invention discloses a kind of pharmaceutical purpose vaporation-type crystallization kettles,Including shell,Heat conducting pipe,Crystal slab,Screw rod and support plate,The upper surface of the shell is provided with evaporation mouth,The support plate is located at the middle part of evaporation mouth,And threaded hole is provided in the middle part of support plate,The both sides of the support plate are respectively and fixedly provided with connecting rod,And the one end of connecting rod far from support plate is fixed on the shell,It is fixed with funnel below the shell,The lower end of the funnel is fixed with condensate outlet,It is fixed with partition board among the position that the funnel and shell overlap,Six the second through-holes are evenly provided on the partition board,The upper end of the heat conducting pipe is set as sealing end,The present invention is provided with heat conducting pipe,Steam enters after funnel the inside for entering heat conducting pipe by the second through-hole and open end again,Heat conducting pipe is by the heat transfer of steam to Pharmaceutical solutions,Six heat conducting pipes can be heated uniformly to solution,So that solution is heated evenly,Crystallization rate is fast.
Description
Technical field
The present invention relates to pharmaceutical technology field, specifically a kind of pharmaceutical purpose vaporation-type crystallization kettle.
Background technology
It needs to use crystallization kettle, vaporation-type crystallization kettle among pharmacy procedure to be heating evaporation solvent, makes solution by insatiable hunger
With become being saturated, continue to evaporate, superfluous solute will be in that crystal is precipitated, and be evaporative crystallization, and existing vaporation-type crystallization kettle
Usually be provided with interlayer on the inner wall of crystallization kettle, be passed through steam inside interlayer, interlayer by the heat transfer of steam to solution,
Such mode can cause solution uneven heating even, and crystallization rate is slow.
Invention content
The purpose of the present invention is to provide a kind of pharmaceutical purpose vaporation-type crystallization kettles, to solve the problems of the prior art.
To achieve the above object, the present invention provides the following technical solutions：A kind of pharmaceutical purpose vaporation-type crystallization kettle, including it is outer
The upper surface of shell, heat conducting pipe, crystal slab, screw rod and support plate, the shell is provided with evaporation mouth, and the support plate is located at evaporation
The middle part of mouth, and threaded hole is provided in the middle part of support plate, the both sides of the support plate are respectively and fixedly provided with connecting rod, and connecting rod is remote
One end from support plate is fixed on the shell, funnel is fixed with below the shell, the lower end of the funnel is fixed with condensation
Liquid exports, and is fixed with partition board among the position that the funnel and shell overlap, six second are evenly provided on the partition board
The upper end of through-hole, the heat conducting pipe is set as sealing end, and the lower end of heat conducting pipe is set as open end, and the open end is fixed on
The top of crystal slab, and the fixation of open end and the second through-hole be connected to, the crystal slab are located at the top of partition board, and on crystal slab and
Vertically corresponding position is both provided with first through hole to second through-hole, and intensive mesh, the crystal are provided on the crystal slab
Screw rod is fixed with by bearing among the upper surface of plate, and the upper end of screw rod passes through threaded hole.
Preferably, the upper end of the screw rod, which is fixed with, changes hands, and the outer surface changed hands is fixed with Anti-slip cover.
Preferably, the both sides of the funnel fixation is communicated with steam pipe, and steam pipe is connect with external steam generator.
Preferably, the lower section both sides of the funnel are respectively and fixedly provided with support leg, and rubber pad is fixed with below support leg.
Preferably, the side-lower fixation of the shell is communicated with serum outlet, and lid is threaded on serum outlet
Son.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention is provided with heat conducting pipe, and steam enters after funnel again
Enter the inside of heat conducting pipe by the second through-hole and open end, by the heat transfer of steam to Pharmaceutical solutions, six are led heat conducting pipe
Heat pipe can be heated uniformly to solution, so that solution is heated evenly, crystallization rate is fast；Provided with screw rod, pass through
It rotates counterclockwise and changes hands, screw rod is moved upwards in threaded hole inner rotation, screw rod, to which crystal slab moves upwards, until crystal
Plate reaches the position of evaporation mouth, and staff can collect from the position of evaporation mouth by the crystal on crystal slab at this time, go out
Material is convenient.
Description of the drawings
Fig. 1 is the dimensional structure diagram of the present invention.
Fig. 2 is the vertical view of crystal slab of the present invention.
Fig. 3 is the vertical view of partition board of the present invention.
Fig. 4 is the face upwarding stereogram of heat conducting pipe of the present invention.
In figure：1, it changes hands；2, evaporation mouth；3, connecting rod；4, shell；5, heat conducting pipe；51, open end；52, sealing end；6,
First through hole；7, steam pipe；8, condensate outlet；9, funnel；10, partition board；11, crystal slab；12, screw rod；13, threaded hole；14,
Mesh；15, the second through-hole；16, serum outlet；17, support leg；18, support plate.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Please refer to Fig.1~4, in the embodiment of the present invention, a kind of pharmaceutical purpose vaporation-type crystallization kettle, including shell 4, heat conducting pipe 5,
The side-lower fixation of crystal slab 11, screw rod 12 and support plate 18, shell 4 is communicated with serum outlet 16, and on serum outlet 16
It is threaded with lid, serum outlet 16 discharges for paddle liquid, and the upper surface of shell 4 is provided with evaporation mouth 2,2 conduct of evaporation mouth
Boil-off gas outflux, support plate 18 is located at the middle part of evaporation mouth 2, and the middle part of support plate 18 is provided with threaded hole 13, support
The both sides of plate 18 are respectively and fixedly provided with connecting rod 3, and connecting rod 3 is used for fixed support plate 18, and support plate 18 has been used to support screw rod 12, and
The one end of connecting rod 3 far from support plate 18 is fixed on shell 4, and the lower section of shell 4 is fixed with funnel 9, and funnel 9 is steamed for collecting
The condensed liquid of vapour, the both sides of funnel 9 are fixed to be communicated with steam pipe 7, and steam pipe 7 is steamed for 5 inside injection of heat conductive pipes
Vapour, and steam pipe 7 is connect with external steam generator, the lower section both sides of funnel 9 are respectively and fixedly provided with support leg 17, and support leg 17 is used for
Shell 4 is supported, and the lower section of support leg 17 is fixed with rubber pad, the lower end of funnel 9 is fixed with condensate outlet 8, condensate liquid
Outlet 8 discharges for condensate liquid, partition board 10 is fixed among the position that funnel 9 is overlapped with shell 4, partition board 10 is for installing heat conduction
Pipe 5 is evenly provided with six the second through-holes 15 on partition board 10, and the second through-hole 15 enters the channel of heat conducting pipe 5 as steam, leads
The upper end of heat pipe 5 is set as sealing end 52, and the lower end of heat conducting pipe 5 is set as open end 51, and open end 51 is fixed on crystal slab
11 top, and open end 51 is connected to the fixation of the second through-hole 15, crystal slab 11 is located at the top of partition board 10, and on crystal slab 11
It is both provided with first through hole 6 with 15 vertical corresponding position of the second through-hole, first through hole 6 is used for across heat conducting pipe 5, crystal slab 11
On be provided with intensive mesh 14, mesh 14 stays crystal on crystal slab 11, the upper surface of crystal slab 11 for filtering out slurries
Centre is fixed with screw rod 12 by bearing, and the upper end of screw rod 12 passes through threaded hole 13, and the upper end of screw rod 12, which is fixed with, changes hands 1,
And change hands 1 outer surface and be fixed with Anti-slip cover, changing hands 1 can make screw rod 12 in 13 inner rotation of threaded hole, to make
It obtains screw rod 12 to move up and down, so that crystal slab 11 moves up and down.
The present invention operation principle be：The inside that the Pharmaceutical solutions that crystallize will be needed to pour into from evaporation mouth 2 shell 4, Xiang Zheng
Steam pipe 7 is passed through steam, and steam enters after funnel 9 inside for entering heat conducting pipe 5 by the second through-hole 15 and open end 51 again, heat conduction
Pipe 5 is by the heat transfer of steam to Pharmaceutical solutions, and the gas of the evaporation of the solvent of Pharmaceutical solutions, evaporation is flowed out from evaporation mouth 2, solution
Become being saturated from unsaturation, superfluous solute will be precipitated, and the crystal of precipitation stays on crystal slab 11, by turning counterclockwise
So that screw rod 12 is in 13 inner rotation of threaded hole, screw rod 12 moves upwards hand 1, to which crystal slab 11 moves upwards, crystal slab 11
When moving upwards, mesh 14 filters out during first through hole 6 is slided on heat conducting pipe 5, while crystal slab 11 moves upwards
Remaining solvent stays in solute on crystal slab 11, until crystal slab 11 reaches the position of evaporation mouth 2, staff can at this time
To collect the crystal on crystal slab 11 from the position of evaporation mouth 2, the lid on serum outlet 16 is opened, solvent can be from
Serum outlet 16 flows out, and enters the inside of funnel 9 after the steam condensation inside heat conducting pipe 5, then is flowed by condensate outlet 8
Go out.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
Claims (5)
1. a kind of pharmaceutical purpose vaporation-type crystallization kettle, including shell (4), heat conducting pipe (5), crystal slab (11), screw rod (12) and support
Plate (18), it is characterised in that：The upper surface of the shell (4) is provided with evaporation mouth (2), and the support plate (18) is located at evaporation mouth
(2) middle part, and threaded hole (13) is provided in the middle part of support plate (18), the both sides of the support plate (18) are respectively and fixedly provided with connection
Bar (3), and the one end of connecting rod (3) far from support plate (18) is fixed on shell (4), is fixed with below the shell (4)
Funnel (9), the lower end of the funnel (9) are fixed with condensate outlet (8), in the position that the funnel (9) overlaps with shell (4)
Between be fixed with partition board (10), be evenly provided with six the second through-holes (15) on the partition board (10), the heat conducting pipe (5) it is upper
End is set as sealing end (52), and the lower end of heat conducting pipe (5) is set as open end (51), and the open end (51) is fixed on crystal
The top of plate (11), and open end (51) are connected to the second through-hole (15) fixation, the crystal slab (11) is located at partition board (10)
Top, and corresponding position vertical with the second through-hole (15) is both provided with first through hole (6), the crystal slab on crystal slab (11)
(11) it is provided with intensive mesh (14) on, screw rod (12) is fixed with by bearing among the upper surface of the crystal slab (11),
And the upper end of screw rod (12) passes through threaded hole (13).
2. a kind of pharmaceutical purpose vaporation-type crystallization kettle according to claim 1, it is characterised in that：The upper end of the screw rod (12)
It is fixed with and changes hands (1), and the outer surface for changing hands (1) is fixed with Anti-slip cover.
3. a kind of pharmaceutical purpose vaporation-type crystallization kettle according to claim 1, it is characterised in that：The both sides of the funnel (9)
Fixation is communicated with steam pipe (7), and steam pipe (7) is connect with external steam generator.
4. a kind of pharmaceutical purpose vaporation-type crystallization kettle according to claim 1, it is characterised in that：The lower section of the funnel (9)
Both sides are respectively and fixedly provided with support leg (17), and are fixed with rubber pad below support leg (17).
5. a kind of pharmaceutical purpose vaporation-type crystallization kettle according to claim 1, it is characterised in that：The side of the shell (4)
Lower section is fixed and is communicated with serum outlet (16), and is threaded with lid on serum outlet (16).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810603914.5A CN108786168A (en) | 2018-06-12 | 2018-06-12 | A kind of pharmaceutical purpose vaporation-type crystallization kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810603914.5A CN108786168A (en) | 2018-06-12 | 2018-06-12 | A kind of pharmaceutical purpose vaporation-type crystallization kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108786168A true CN108786168A (en) | 2018-11-13 |
Family
ID=64085572
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810603914.5A Withdrawn CN108786168A (en) | 2018-06-12 | 2018-06-12 | A kind of pharmaceutical purpose vaporation-type crystallization kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108786168A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4156459A (en) * | 1976-05-17 | 1979-05-29 | Hisaka Works Ltd. | Plate type evaporator |
| CN203525332U (en) * | 2013-10-12 | 2014-04-09 | 象山医疗精密仪器有限公司 | Medicine concentration and evaporation device |
| CN104436725A (en) * | 2014-12-04 | 2015-03-25 | 重庆云升食品饮料有限公司 | Food concentration evaporator |
| CN205886247U (en) * | 2016-07-21 | 2017-01-18 | 四川康而好动物药业有限公司 | Medicine enrichment facility |
| CN205995076U (en) * | 2016-08-30 | 2017-03-08 | 赣州卓越再生资源综合利用有限公司 | A kind of evaporating, concentrating and crystallizing kettle |
| CN206746030U (en) * | 2017-04-07 | 2017-12-15 | 新泰市佳禾生物科技有限公司 | A kind of equipment for amino acid evaporative crystallization |
| CN107854860A (en) * | 2017-11-28 | 2018-03-30 | 佛山科学技术学院 | A kind of industrial chemicals rapid crystallization equipment |
-
2018
- 2018-06-12 CN CN201810603914.5A patent/CN108786168A/en not_active Withdrawn
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4156459A (en) * | 1976-05-17 | 1979-05-29 | Hisaka Works Ltd. | Plate type evaporator |
| CN203525332U (en) * | 2013-10-12 | 2014-04-09 | 象山医疗精密仪器有限公司 | Medicine concentration and evaporation device |
| CN104436725A (en) * | 2014-12-04 | 2015-03-25 | 重庆云升食品饮料有限公司 | Food concentration evaporator |
| CN205886247U (en) * | 2016-07-21 | 2017-01-18 | 四川康而好动物药业有限公司 | Medicine enrichment facility |
| CN205995076U (en) * | 2016-08-30 | 2017-03-08 | 赣州卓越再生资源综合利用有限公司 | A kind of evaporating, concentrating and crystallizing kettle |
| CN206746030U (en) * | 2017-04-07 | 2017-12-15 | 新泰市佳禾生物科技有限公司 | A kind of equipment for amino acid evaporative crystallization |
| CN107854860A (en) * | 2017-11-28 | 2018-03-30 | 佛山科学技术学院 | A kind of industrial chemicals rapid crystallization equipment |
Non-Patent Citations (1)
| Title |
|---|
| 刘银等: "《固体废弃物资源化工程设计概论》", 31 January 2017 * |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20181113 |