CN112121451A - Distillation still with liquid level meter - Google Patents

Distillation still with liquid level meter Download PDF

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Publication number
CN112121451A
CN112121451A CN202010907151.0A CN202010907151A CN112121451A CN 112121451 A CN112121451 A CN 112121451A CN 202010907151 A CN202010907151 A CN 202010907151A CN 112121451 A CN112121451 A CN 112121451A
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CN
China
Prior art keywords
fixedly connected
cauldron
pipe
kettle
liquid level
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010907151.0A
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Chinese (zh)
Inventor
刘林
陈伟
蒋伟
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Hunan Hengxing Environmental Protection Technology Development Co ltd
Original Assignee
Hunan Hengxing Environmental Protection Technology Development Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Hunan Hengxing Environmental Protection Technology Development Co ltd filed Critical Hunan Hengxing Environmental Protection Technology Development Co ltd
Priority to CN202010907151.0A priority Critical patent/CN112121451A/en
Publication of CN112121451A publication Critical patent/CN112121451A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/02Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42Regulation; Control

Abstract

The invention provides a distillation kettle with a liquid level meter, and relates to the technical field of distillation. This stills with level gauge, including the cauldron body, the surface of the cauldron body is provided with the support frame, the surface of the cauldron body and the top fixedly connected with ring gear that is located the support frame, at the bottom of the lower fixed surface of the cauldron body is connected with the cauldron, the inside fixedly connected with discharging pipe at the bottom of the cauldron, the one end fixedly connected with valve at the bottom of the cauldron is kept away from to the discharging pipe, the lower fixed surface at the bottom of the cauldron is connected with the heat insulating board, the lower surface of heat insulating board is provided with vibrating motor, the last fixed surface of the cauldron body is connected with the cauldron top, the lower fixed surface at the cauldron top is. Through shock dynamo, rotating electrical machines, can make the cauldron body carry out reciprocal rotation and vibrations, hinder solid and the internal wall of cauldron, the contact for a long time at the bottom of the cauldron to melt, hug closely at the bottom of inner wall, cauldron, influence stills next use, it is comparatively convenient to clear up inside moreover.

Description

Distillation still with liquid level meter
Technical Field
The invention relates to the technical field of distillation, in particular to a distillation kettle with a liquid level meter.
Background
A distillation still relates to a still used for distillation in chemical production. The distillation kettle is designed for mainly solving the problem that the existing distillation kettle needs to be overhauled and cleaned intermittently when materials contain solid matters and high-boiling-point matters in the production process, and has the function of vaporizing distilled liquid and providing necessary ascending steam quantity in a tower. The distillation still has jacket type, coil type and tube type. The jacketed type distillation still and the coil type distillation still are mostly used for large-scale production due to small heating area.
Present stills are for separating solid thing and the high boiling point thing in Liao, but when it separates, need heat wherein, make low boiling point thing separate, but in the heating process, solid particle is along with going on of heating, precipitate for it pastes cauldron internal wall or cauldron bottom, cause the influence to the heating, and inconvenient clearance, when distilling, when liquid is less, mostly be high boiling point and solid, continue to distill, the repayment is lower, and waste resources.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a distillation still with a liquid level meter, and solves the problems that solid particles are easy to adhere to the interior of the distillation still and are difficult to clean.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: a distillation kettle with a liquid level meter comprises a kettle body, wherein a support frame is arranged on the outer surface of the kettle body, a toothed ring is fixedly connected on the outer surface of the kettle body and positioned above the support frame, a kettle bottom is fixedly connected to the lower surface of the kettle body, a discharge pipe is fixedly connected inside the kettle bottom, one end, away from the kettle bottom, of the discharge pipe is fixedly connected with a valve, a heat insulation plate is fixedly connected to the lower surface of the kettle bottom, a vibration motor is arranged on the lower surface of the heat insulation plate, a kettle top is fixedly connected to the upper surface of the kettle body, a liquid level detection head is fixedly connected to the lower surface of the kettle top, a liquid level display instrument is fixedly connected to the upper surface of the kettle top, a feed pipe is arranged inside the kettle top, a gas outlet is fixedly connected to the right side of the feed pipe, a temperature sensor is arranged, the utility model discloses a solar water heater, including a support frame, a gas outlet, a connecting pipe, a condenser pipe, a right flank fixedly connected with inlet tube, the left surface fixedly connected with outlet pipe of condenser pipe, the one end fixedly connected with runner pipe of connecting pipe is kept away from to the connecting pipe, the inside of condenser pipe is provided with the steam pipe, the inside of condenser pipe just is located the steam pipe, the right flank fixedly connected with inlet tube of condenser pipe, the left surface fixedly connected with outlet pipe of condenser pipe, the one end fixedly connected with runner pipe of connecting pipe is kept away from to the condenser pipe, the last fixed surface of support.
Preferably, the cauldron body includes first insulating layer, the inside fixedly connected with first heat preservation of first insulating layer, the inside fixedly connected with on first heat preservation heats the layer, the inside fixedly connected with heat-conducting layer on layer heats.
Preferably, the kettle bottom comprises a second heat insulation layer, a second heat insulation layer is fixedly connected to the lower surface of the second heat insulation layer, and the inner structure of the kettle top is the same as that of the kettle bottom.
Preferably, the first heat insulation layer is made of glass fibers, the first heat preservation layer is made of a polyurethane material, and heating wires are arranged inside the heating layer.
Preferably, the gear is meshed with the gear ring, the rotating motor is a swing motor, and sealing structures are arranged at the connecting parts of the kettle bottom, the kettle top and the kettle body.
Preferably, the liquid level detection head is in signal connection with the liquid level display instrument, and the vibration motor is fixedly connected with the support frame.
Preferably, the steam pipe has a serpentine shape, is arranged obliquely downward, and has an inclination angle of 10 ° to 20 °.
Preferably, the one end that the cauldron top was kept away from to the inlet pipe is provided with the cock body, the upper surface of cauldron top and the right side that is located liquid level display appearance are provided with pressure measurement appearance, and the bottom extends to the inside of the cauldron body, the lower fixed surface of support frame is connected with the supporting legs.
The working principle is as follows: through pouring into cauldron body 1 from inlet pipe 15 with the distilled raw materials that will need, heat through layer 103 heats, open vibrating motor 7 and rotating electrical machines 10 simultaneously, vibrate and rotate cauldron body 1, make inside liquid be in the mobile state, avoid solid particle to be in same position for a long time, thereby paste the inner wall, the material of distilling out passes through gas outlet 17 and reachs in condenser pipe 20, carry out the condensation, then flow, detect inside temperature through temperature sensor 18, be convenient for control the distillation order of material, detect the inside liquid level through liquid level detection head 13 simultaneously, when the stock is less, early warning is carried out, avoid the waste of energy.
(III) advantageous effects
The invention provides a distillation still with a liquid level meter. The method has the following beneficial effects:
1. according to the invention, the kettle body can be rotated and vibrated in a reciprocating manner through the vibration motor and the rotating motor, so that the solid is prevented from contacting with the inner wall of the kettle body and the kettle bottom for a long time, the solid is melted and clings to the inner wall and the kettle bottom, the next use of the distillation kettle is influenced, and the cleaning of the internal residues is more convenient.
2. According to the invention, the liquid level detection head and the temperature sensor are arranged, so that the liquid level of the residual liquid in the kettle body can be conveniently detected, the situation that the residual low-boiling-point substances in the kettle body are small and much waste is avoided, and meanwhile, the temperature can be conveniently controlled and the substances with different boiling points can be distinguished through the temperature sensor.
3. The steam pipe is bent and inclined, so that the condensation time is prolonged conveniently, and the condensation effect is better.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of the internal structure of the present invention;
FIG. 3 is a schematic view of the structure of FIG. 2 at A according to the present invention;
FIG. 4 is a schematic view of the structure of the kettle of the present invention;
FIG. 5 is a schematic view of the bottom structure of the reactor of the present invention.
Wherein, 1, a kettle body; 101. a first insulating layer; 102. a first insulating layer; 103. heating the layer; 104. a heat conductive layer; 2. a support frame; 3. the bottom of the kettle; 301. a second insulating layer; 302. a second thermal insulation layer; 4. the kettle top; 5. a discharge pipe; 6. a valve; 7. a vibration motor; 8. a heat insulation plate; 9. a toothed ring; 10. a rotating electric machine; 11. a connecting shaft; 12. a gear; 13. a liquid level detection head; 14. a liquid level display; 15. a feed pipe; 16. supporting legs; 17. an air outlet; 18. a temperature sensor; 19. a connecting pipe; 20. a condenser tube; 21. a steam pipe; 22. a water outlet pipe; 23. a water inlet pipe; 24. a flow-through tube; 25. a cold water pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
as shown in fig. 1-5, an embodiment of the present invention provides a distillation kettle with a liquid level meter, comprising a kettle body 1, a place for distillation, a support frame 2 arranged on the outer surface of the kettle body 1 for supporting the distillation kettle body, a toothed ring 9 fixedly connected to the outer surface of the kettle body 1 and above the support frame 2 for transmitting power to rotate the kettle body 1, a kettle bottom 3 fixedly connected to the lower surface of the kettle body 1, a discharge pipe 5 fixedly connected to the interior of the kettle bottom 3 for discharging high boiling point materials and solid particles, a valve 6 fixedly connected to one end of the discharge pipe 5 far from the kettle bottom 3 for controlling the discharge of the discharge pipe 5, a thermal insulation board 8 fixedly connected to the lower surface of the kettle bottom 3 for isolating the heat of the kettle bottom 3, a vibration motor 7 arranged on the lower surface of the thermal insulation board 8 for vibrating the kettle body 1 to prevent the solid from contacting the kettle bottom 3 for a long time, thereby bonding, a kettle top 4 fixedly connected to the, the lower surface of the kettle top 4 is fixedly connected with a liquid level detection head 13, the liquid level inside the kettle body 1 is detected, the upper surface of the kettle top 4 is fixedly connected with a liquid level display instrument 14 for displaying the liquid level, the inside of the kettle top 4 is provided with a feeding pipe 15 for entering distilled liquid, the inside of the kettle top 4 is fixedly connected with a gas outlet 17 positioned at the right side of the feeding pipe 15, the outlet of the low boiling point liquid after vaporization is formed, the inside of the gas outlet 17 is provided with a temperature sensor 18 for measuring the gas temperature after the liquid is discharged out, the liquid distillation with different boiling points is convenient to control, the outer surface of the gas outlet 17 is provided with a connecting pipe 19, one end of the connecting pipe 19 far away from the gas outlet 17 is fixedly connected with a condensing pipe 20 for distilling the gas, the inside of the condensing pipe 20 is provided with a steam pipe 21 for entering the steam, be convenient for carry out the condensation, condenser pipe 20's right flank fixedly connected with inlet tube 23, get into from low, condenser pipe 20's left flank fixedly connected with outlet pipe 22, go out from the eminence, it is more smooth and easy to make the condensation, condenser pipe 20 keeps away from the one end fixedly connected with runner pipe 24 of connecting pipe 19, liquid after the condensation, circulate, the last fixed surface of support frame 2 is connected with rotating electrical machines 10, provide the rotatory power of ring gear 9, rotating electrical machines 10's output fixedly connected with connecting axle 11, rotating electrical machines 10's one end fixedly connected with gear 12 is kept away from to connecting axle 11, transmit rotary power and give ring gear 9.
The kettle body 1 comprises a first heat insulation layer 101, so that the internal heat is not transferred out of the kettle body 1, a first heat preservation layer 102 is fixedly connected inside the first heat insulation layer 101, the internal heat of the kettle body 1 is kept, the utilization rate is high, a heating layer 103 is fixedly connected inside the first heat preservation layer 102, the kettle body 1 is heated, a heat conduction layer 104 is fixedly connected inside the heating layer 103, the heat is transferred, the kettle bottom 3 comprises a second heat insulation layer 301, a second heat insulation layer 302 is fixedly connected to the lower surface of the second heat insulation layer 301, the internal structure of the kettle top 4 is the same as that of the kettle bottom 3, the first heat insulation layer 101 is made of glass fiber and has a good heat insulation effect, the first heat insulation layer 102 is made of polyurethane material and has a good heat insulation effect, heating wires are arranged inside the heating layer 103 and are convenient to heat, a gear 12 is meshed with a gear ring 9, and a rotary motor 10 is a swing motor, can circulate and swing, vibrate internal liquid production, 3 at the bottom of the cauldron, cauldron top 4 all is provided with seal structure with the junction of the cauldron body 1, keep the leakproofness of the cauldron body 1, liquid level detection head 13 and liquid level display instrument 14 signal connection, be convenient for learn liquid level data, shock dynamo 7 and support frame 2 fixed connection, the shape of steam pipe 21 is snakelike, extension condenser pipe 20, steam pipe 21 slope is arranged downwards, and inclination is 10 ~ 20, the one end that inlet pipe 15 kept away from cauldron top 4 is provided with the cock body, cauldron body 1 seals up, the upper surface of cauldron top 4 and the right side that is located liquid level display instrument 14 are provided with pressure detector, detect 1 internal pressure of the cauldron body, and the bottom extends to the inside of the cauldron body 1, the lower fixed surface of support frame 2 is connected with supporting legs 16, strutting arrangement.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (8)

1. The utility model provides a stills with level gauge, includes the cauldron body (1), its characterized in that: the device is characterized in that a support frame (2) is arranged on the outer surface of the kettle body (1), a toothed ring (9) is fixedly connected to the outer surface of the kettle body (1) and positioned above the support frame (2), a kettle bottom (3) is fixedly connected to the lower surface of the kettle body (1), a discharge pipe (5) is fixedly connected to the inner portion of the kettle bottom (3), a valve (6) is fixedly connected to one end, away from the kettle bottom (3), of the discharge pipe (5), a heat insulation plate (8) is fixedly connected to the lower surface of the kettle bottom (3), a vibration motor (7) is arranged on the lower surface of the heat insulation plate (8), a kettle top (4) is fixedly connected to the upper surface of the kettle body (1), a liquid level detection head (13) is fixedly connected to the lower surface of the kettle top (4), a liquid level display instrument (14) is fixedly connected to the upper surface of the kettle top (, the inner part of the kettle top (4) is fixedly connected with a gas outlet (17) on the right side of the inlet pipe (15), a temperature sensor (18) is arranged inside the gas outlet (17), a connecting pipe (19) is arranged on the outer surface of the gas outlet (17), a condensing pipe (20) is fixedly connected with one end of the connecting pipe (19) far away from the gas outlet (17), a steam pipe (21) is arranged inside the condensing pipe (20), a cold water pipe (25) is arranged inside the condensing pipe (20) and outside the steam pipe (21), a water inlet pipe (23) is fixedly connected with the right side surface of the condensing pipe (20), a water outlet pipe (22) is fixedly connected with the left side surface of the condensing pipe (20), a circulation pipe (24) is fixedly connected with one end of the condensing pipe (20) far away from the connecting pipe (19), and a rotating motor (10) is fixedly connected with the upper, the output end of the rotating motor (10) is fixedly connected with a connecting shaft (11), and one end, far away from the rotating motor (10), of the connecting shaft (11) is fixedly connected with a gear (12).
2. The retort according to claim 1, comprising a liquid level meter, wherein: the kettle body (1) comprises a first heat insulation layer (101), a first heat insulation layer (102) is fixedly connected to the inside of the first heat insulation layer (101), a heating layer (103) is fixedly connected to the inside of the first heat insulation layer (102), and a heat conduction layer (104) is fixedly connected to the inside of the heating layer (103).
3. The retort according to claim 1, comprising a liquid level meter, wherein: the cauldron bottom (3) includes second heat preservation (301), the lower surface fixedly connected with second insulating layer (302) of second heat preservation (301), the inner structure of cauldron top (4) is the same with the inner structure of cauldron bottom (3).
4. The retort according to claim 2, comprising a liquid level meter, wherein: the first heat insulation layer (101) is made of glass fibers, the first heat preservation layer (102) is made of polyurethane, and heating wires are arranged inside the heating layer (103).
5. The retort according to claim 1, comprising a liquid level meter, wherein: the gear (12) is meshed with the gear ring (9), the rotating motor (10) is a swing motor, and sealing structures are arranged at the connecting parts of the kettle bottom (3), the kettle top (4) and the kettle body (1).
6. The retort according to claim 1, comprising a liquid level meter, wherein: the liquid level detection head (13) is in signal connection with the liquid level display instrument (14), and the vibration motor (7) is fixedly connected with the support frame (2).
7. The retort according to claim 1, comprising a liquid level meter, wherein: the steam pipe (21) is in a snake shape, the steam pipe (21) is arranged in an inclined downward mode, and the inclined angle ranges from 10 degrees to 20 degrees.
8. The retort according to claim 1, comprising a liquid level meter, wherein: the one end that cauldron top (4) were kept away from in inlet pipe (15) is provided with the cock body, the right side that the upper surface of cauldron top (4) just is located liquid level display appearance (14) is provided with pressure measurement appearance, and the bottom extends to the inside of cauldron body (1), the lower fixed surface of support frame (2) is connected with supporting legs (16).
CN202010907151.0A 2020-09-02 2020-09-02 Distillation still with liquid level meter Pending CN112121451A (en)

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CN202010907151.0A CN112121451A (en) 2020-09-02 2020-09-02 Distillation still with liquid level meter

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Application Number Priority Date Filing Date Title
CN202010907151.0A CN112121451A (en) 2020-09-02 2020-09-02 Distillation still with liquid level meter

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113350817A (en) * 2021-05-28 2021-09-07 张成龙 Evaporation kettle with regulation and control injection function

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0406093A1 (en) * 1989-06-27 1991-01-02 Societe Nationale Elf Aquitaine (Production) Laboratory distillation apparatus
CN201634658U (en) * 2010-02-26 2010-11-17 湖北中烟工业有限责任公司 High-efficient essential oil production equipment
CN205886262U (en) * 2016-08-01 2017-01-18 扬州日发干燥工程有限公司 Drying device
CN206027142U (en) * 2016-07-02 2017-03-22 南昌绿捷日化有限公司 Concentrated crystallizer of high -efficient material
CN209237376U (en) * 2018-10-24 2019-08-13 什邡开源环保科技有限公司 It is a kind of can serialization distillation distilling apparatus
CN209756175U (en) * 2018-09-27 2019-12-10 汪明新 High-efficient equipment that draws of spices
CN210215295U (en) * 2019-05-10 2020-03-31 金溪县鑫润香料实业有限公司 Eucalyptol rectifying device
CN210313612U (en) * 2019-05-21 2020-04-14 浙江浙能技术研究院有限公司 High salt waste water flue gas drying treatment device that contains

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0406093A1 (en) * 1989-06-27 1991-01-02 Societe Nationale Elf Aquitaine (Production) Laboratory distillation apparatus
CN201634658U (en) * 2010-02-26 2010-11-17 湖北中烟工业有限责任公司 High-efficient essential oil production equipment
CN206027142U (en) * 2016-07-02 2017-03-22 南昌绿捷日化有限公司 Concentrated crystallizer of high -efficient material
CN205886262U (en) * 2016-08-01 2017-01-18 扬州日发干燥工程有限公司 Drying device
CN209756175U (en) * 2018-09-27 2019-12-10 汪明新 High-efficient equipment that draws of spices
CN209237376U (en) * 2018-10-24 2019-08-13 什邡开源环保科技有限公司 It is a kind of can serialization distillation distilling apparatus
CN210215295U (en) * 2019-05-10 2020-03-31 金溪县鑫润香料实业有限公司 Eucalyptol rectifying device
CN210313612U (en) * 2019-05-21 2020-04-14 浙江浙能技术研究院有限公司 High salt waste water flue gas drying treatment device that contains

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113350817A (en) * 2021-05-28 2021-09-07 张成龙 Evaporation kettle with regulation and control injection function
CN113350817B (en) * 2021-05-28 2022-06-21 黄山市鼎利新材料有限公司 Evaporation kettle with regulation and control injection function

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Application publication date: 20201225

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