CN108764443A - A kind of movable type river and lake is desilted and dredged the counting device in sludge sample processing device - Google Patents
A kind of movable type river and lake is desilted and dredged the counting device in sludge sample processing device Download PDFInfo
- Publication number
- CN108764443A CN108764443A CN201810493700.7A CN201810493700A CN108764443A CN 108764443 A CN108764443 A CN 108764443A CN 201810493700 A CN201810493700 A CN 201810493700A CN 108764443 A CN108764443 A CN 108764443A
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- Prior art keywords
- stirring
- sample
- gear
- tower reactor
- control system
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Classifications
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- G—PHYSICS
- G06—COMPUTING; CALCULATING OR COUNTING
- G06M—COUNTING MECHANISMS; COUNTING OF OBJECTS NOT OTHERWISE PROVIDED FOR
- G06M1/00—Design features of general application
- G06M1/27—Design features of general application for representing the result of count in the form of electric signals, e.g. by sensing markings on the counter drum
- G06M1/272—Design features of general application for representing the result of count in the form of electric signals, e.g. by sensing markings on the counter drum using photoelectric means
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/70—Spray-mixers, e.g. for mixing intersecting sheets of material
- B01F25/72—Spray-mixers, e.g. for mixing intersecting sheets of material with nozzles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/25—Mixers with loose mixing elements, e.g. loose balls in a receptacle
- B01F33/251—Mixers with loose mixing elements, e.g. loose balls in a receptacle using balls as loose mixing element
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/286—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
Abstract
A kind of mobile river and lake of disclosure of the invention is desilted and dredged the counting device in sludge sample processing device.It pops one's head in equipped with spare Laser Measuring circle in conversion head horizontal direction, spare Laser Measuring circle probe is identical as Laser Measuring circle sonde configuration, and Laser Measuring circle probe and spare Laser Measuring circle probe are Demountable;The rotary shaft top is equipped with gearbox, and transmission internal is equipped with deboost axle, and deboost axle engages connection with rotation shaft gear;Upper part of gear box is equipped with electric rotating machine, and electric rotating machine engages connection with deceleration shaft gear;Gearbox bottom is equipped with temperature sensor, velocity sensor;Electric rotating machine drives the probe rotation of Laser Measuring circle by deboost axle, rotary shaft, to exchange the operating angle of Laser Measuring circle probe;Temperature sensor, velocity sensor positioned at gearbox bottom are in real time monitored the object state on workbench.The device intelligence degree is high, and stability is high, small to sample impact force, ensures that sample is without damage, high yield rate.
Description
Technical field
It desilts and dredges sludge sample processing device field the invention belongs to river and lake, and in particular to a kind of movable type river and lake dredging
Counting device in Dredged Sludge sample processing device.
Background technology
Counter function in the prior art is single, inconvenient objective record and storage count results, let alone will be individual
Count information collating sort is set by individual character and reports statistics platform positioned at high in the clouds, simultaneously because original fixed form is led
It causes that receiving is being needed to place when not used, when use is found out again, for there is the operating personnel for needing tally function at any time as day
It is very inconvenient for the personage of Chang Zuoye, it cannot start with work for counting at any time, and non-regular guest is easy to be lost.
Invention content
It desilts and dredges sludge sample processing device in order to solve the above technical problem, the present invention provides a kind of mobile river and lake
In counting device, the fixed frame 2 be stainless steel rectangular structure, thickness is between 3cm~4cm;The shock-absorbing foot pad 1
Quantity is four, is respectively and fixedly installed to 2 bottom four corners of fixed frame.
Further, what this section was told about is heretofore described 3 structure of pushing mechanism.The slideway 3-2 passes through slideway
Fixed block 3-1 is fixedly connected with support platform 5;The cross sections the slideway 3-2 are in " Ω " shape, and slideway 3-2 quantity is 2;Institute
It states sliding block 3-3 and slideway 3-2 to be slidably connected, the ends sliding block 3-3 are provided with slide motor 3-8, slide motor 3-8 driving sliding blocks 3-
3 slide on slideway 3-2;The speed regulating motor 3-4 is variable-frequency motor, and speed regulating motor 3-4 pedestals are welded and fixed with sliding block 3-3.
Further, what this section was told about is heretofore described 7 structure of rolling cutter.Driven wheel 7-1 positioned at one end,
It connect with external cutter motor, meanwhile, driven wheel 7-1 is fixedly connected with transmission shaft 7-9;It is equipped on the inside of driven wheel 7-1
Back-up roller bearing 7-4, the back-up roller bearing 7-4 quantity are 2, are located at the both ends of transmission shaft 7-9;The transmission shaft 7-
9 hollow structures are internally provided with transformer 7-2, heating tube 7-5, water inlet pipe 7-7;Water inlet pipe 7-7 is parallel to transmission shaft 7-9, water inlet
The quantity of pipe 7-7 is 3, and water inlet pipe 7-7 is connected to water inlet port 7-8, and water inlet port 7-8 is connected to external pump.
Further, what this section was told about is heretofore described slideway 3-2 refrigerating device inside structures.Positioned at side
It is connected to heat-exchanging chamber 3-2-3 by coolant liquid entrance 3-2-1, and is located under heat-exchanging chamber 3-2-3 by coolant liquid entrance 3-2-1
Portion, low level;It is described that the tops heat-exchanging chamber 3-2-3, a high position are located at by coolant liquid outlet 3-2-7, and by coolant liquid export 3-2-7 and
Heat-exchanging chamber 3-2-3 connections;The heat-exchange tube 3-2-2 is located in the middle part of heat-exchanging chamber 3-2-3, the hollow knots of heat-exchange tube 3-2-2
The quantity of structure, heat-exchange tube 3-2-2 is 20, the more vertical equidistant arrangements of heat-exchange tube 3-2-2;The both ends heat-exchange tube 3-2-2
Be respectively equipped with buffered room 3-2-5, the both ends heat-exchange tube 3-2-2 respectively with the buffered room 3-2- that is located at its upper and lower ends
5 connections.
Further, what this section was told about is heretofore described medicament mixing device 3-2-8 structures.Medicine positioned at one end
Enter pipe 3-2-8-9 equipped with diluent on the right side of agent import 3-2-8-1, medicament inlet 3-2-8-1, diluent enters pipe 3-2-8-9
One end is connected to external diluent bottle, and it is open that diluent, which enters the pipe 3-2-8-9 other ends, and is inserted into diffusion horn mouth 3-
Inside 2-8-7;It is equipped with decentralized network 3-2-8-8 in the middle part of diffusion horn mouth 3-2-8-7, is holey, vertical display;Diffusion
Horn mouth 3-2-8-7 is flared structure, and horn mouth 3-2-8-7 heavy calibers end and osculum are spread in heavy caliber end towards right side
The diameter ratio at diameter end is 3:1;The diffusant jet pipe 3-2-8-2 is located on the right side of diffusion horn mouth 3-2-8-7, is hollow ring
Pipe structure, the ring pipe right lateral surface of diffusant jet pipe 3-2-8-2 are equipped with a large amount of through-holes, diffusant one end jet pipe 3-2-8-2 with
Diffusant enters pipe 3-2-8-3 connections.
Further, what this section was told about is heretofore described promotion disk brake apparatus 3-9 structures.On central axes
Speed regulating motor transmission shaft 3-10, be surrounded by friction plate 3-9-6, friction plate 3-9-6 quantity is 4,4 friction plate 3-9-
6 wrap up speed regulating motor transmission shaft 3-10 wherein, and the periphery of friction plate 3-9-6 is equipped with brake caliper 3-9-4, brake caliper 3-
9-4 is cyclic annular, is divided into pintongs, and friction plate 3-9-6 is fixed on the inside of brake caliper 3-9-4;It is equipped with and dissipates on the left of brake caliper 3-9-4
Hot-air fan 3-9-5, radiator fan 3-9-5 are brake caliper 3-9-4 coolings.
Further, what this section was told about is heretofore described 4 structure of sample clamp.The gear wheel 4-4 is arranged in
Inside service chamber 4-2, gear wheel 4-4 is interior tooth type hollow structure, and interior teeth are located in gear wheel 4-4 internal circumferences, canine tooth
It is outer toothing to take turns and be equipped with central gear 4-5 and handgrip gear 4-6, central gear 4-5, handgrip gear 4-6 in 4-4;In described
Heart gear 4-5 is located at the central axes gear wheel 4-4, central gear 4-5 be surrounded by handgrip gear 4-6, gear wheel 4-4, in
Heart gear 4-5, handgrip gear 4-6 three engage connection.
Further, what this section was told about is heretofore described lap count 4-7 structures.Laser Measuring positioned at bottom
Circle probe 4-7-1, surface further includes secondary light source 4-7-8 and Laser emission receiver 4-7-9, the Laser emission receiver
4-7-9 is located at Laser Measuring circle probe 4-7-1 bottom centre, direction is aimed downwardly, and Laser emission receiver 4-7-9 is surrounded by auxiliary
It is 12 to help light source 4-7-8, secondary light source 4-7-8, and secondary light source 4-7-8 is LE light sources;The conversion head 4-7-2 is located at laser
The rotary shaft 4-7-7 on the top of survey circle probe 4-7-1, conversion head 4-7-2 and top is rotatablely connected, meanwhile, Laser Measuring circle probe
4-7-1 is fixedly connected with the rotary shaft 4-7-7 on top;It is equipped with spare Laser Measuring circle probe 4- in conversion head 4-7-2 horizontal directions
7-11, quantity are 4, and spare Laser Measuring circle probe 4-7-11 is identical as Laser Measuring circle probe 4-7-1 structures, and Laser Measuring circle is visited
Head 4-7-1 and spare Laser Measuring circle probe 4-7-11 is Demountable.
Further, what this section was told about is heretofore described sample handgrip 4-3 structures.The sample cell 4-3-2 cloth
The tops arm 4-3-1 are placed in, sample cell 4-3-2 is circular groove, and diameter is 8cm~12cm;The banjo traction splint
4-3-3 quantity is three, and circumference is equally distributed on around sample cell 4-3-2, and the ends banjo traction splint 4-3-3 are equipped with anti-skidding guarantor
Protection pad and sample clamping degree inductor 4-3-4.
Further, the rotary shaft 4-7-7 is molded by high molecular material pressing mold, the constituent of rotary shaft 4-7-7 and
Manufacturing process is as follows:
One, rotary shaft 4-7-7 constituents:
339.2~564.8 parts of lake water of meter purification in parts by weight, N- methyl-1s, 1,2,2,3,3,4,4,5,5,5- ten one fluoro-
131.5~173.6 parts of 1- pentanes sulfonamide, 134.2~243.1 parts of 1- (methoxy) -4- methylbenzenes, 4- (methyl mercapto) fourth
130.4~147.4 parts of aldehyde, 133.1~190.3 parts of rutile, bis- [2- (2- the acrylic)] phenol of 4,4'- (1- methyl ethylidene)
With 136.9~197.5 parts of the polymer of (chloromethyl) ethylene oxide, 138.7~193.3 parts of silver nano-particle, polymerization oxidation
1,1,2,3,3,3,131.1~173.6 parts of-hexafluoro -1- propylene, the polymer of formaldehyde and dicyanodiamide and ethylenediamine sulfate
133.6~173.5 parts, 133.9~156.6 parts of alkali formula aphthenic acids zinc salt, methyl ethyl ketoxime sealing end [2,4,6- tri- oxygen triazine -1,
3,5 (2H, 4H, 6H)-three base] three 122.5~158.8 parts of (cyclohexyl) isocyanates, 121.2~164.8 parts of 7- methyl octanals,
130.8~175.4 parts of (2E)-formic acid -2- hexen-1-ols ester, 140.3~184.3 parts of the polymer of polyurethane, mass concentration are
163.4~217.8 parts of the rosolic acid cetyl ester of 130mg/L~397mg/L;
Two, the manufacturing process of rotary shaft 4-7-7, comprises the steps of:
1st step:In tower reactor is found in stirring, it is added and purifies lake water and N- methyl-1s, 1,2,2,3,3,4,4,5,5,5- ten
One fluoro -1- pentane sulfonamide starts the blender in the vertical tower reactor of stirring, and setting speed is 132rpm~178rpm,
Start the steam oil heater in the vertical tower reactor of stirring, so that temperature is risen to 147.2 DEG C~148.8 DEG C, 1- (methoxies are added
Ylmethyl) -4- methylbenzenes stir evenly, and carry out reaction 124.5~135.6 minutes, and 4- (methyl mercapto) butyraldehyde is added, is passed through flow
For 123.5m3/ min~164.4m3The helium of/min 124.5~135.6 minutes;It is added in tower reactor is found in stirring later
Rutile, the steam oil heater being again started up in the vertical tower reactor of stirring, makes temperature rise to 164.2 DEG C~197.1 DEG C,
4,4'- (1- methyl ethylidene) bis- [2- (2- acrylic)] phenol and (chloromethyl) ring is added in heat preservation 124.4~135.4 minutes
The polymer of oxidative ethane, the pH value that solution in tower reactor is found in adjustment stirring are 4.1~8.3, keep the temperature 124.1~364.1 points
Clock;
2nd step:Separately take silver nano-particle, by silver nano-particle power be 6.64KW~12.08KW under ultrasonication 0.130
After~1.197 hours;Silver nano-particle is added to another stirring to stand in tower reactor, addition mass concentration is 134mg/
The 1 of the polymerization oxidation of L~364mg/L, 1,2,3,3,3,-hexafluoro -1- propylene disperses silver nano-particle, and it is vertical tower anti-to start stirring
The steam oil heater in device is answered, makes solution temperature between 45 DEG C~89 DEG C, starts stirring and stands stirring in tower reactor
Machine is mixed, and with 4 × 102Rpm~8 × 102The speed of rpm stirs, and adjusts pH value between 4.5~8.8, and insulated and stirred 130~
197 minutes;Stop reaction later and stand 6.64 × 10~12.08 × 10 minutes, removes impurity;Formaldehyde and two is added in suspension
The polymer of cyano diamides and ethylenediamine sulfate, adjustment pH value form sediment and are washed with purification lake water between 1.5~2.8
It is de-, by centrifuge in rotating speed 4.192 × 103Rpm~9.643 × 103Solid content is obtained under rpm, 2.407 × 102DEG C~
3.642×102It is dry at a temperature of DEG C, 0.192 × 10 is crossed after grinding3~1.643 × 103Mesh sieves, spare;
3rd step:Another silver nano-particle after taking alkali formula aphthenic acids zinc salt and the processing of the 2nd step, uses the small angle of glancing incidence after mixing
Gamma-rays diffusing reflection irradiation is spent, the energy of glancing incidence low-angle gamma-rays diffusing reflection irradiation is 121.2MeV~149.8MeV, agent
Amount is 169.2kGy~209.8kGy, irradiation time is 133.2~158.8 minutes, obtains the alkali formula zinc naphthenate of character change
Salt and silver nano-particle mixture;Alkali formula aphthenic acids zinc salt and silver nano-particle mixture are placed in another stirring and stand tower reaction
In device, start the steam oil heater in the vertical tower reactor of stirring, 132.8 DEG C~178.4 DEG C of set temperature starts stirring
Blender in vertical tower reactor, rotating speed are 124rpm~519rpm, and pH is adjusted between 4.3~8.3, dehydration 133.3~
147.3 minute, spare;
4th step:The alkali formula aphthenic acids zinc salt and silver nano-particle mixture that the character that 3rd step is obtained changes, it is dense to add to quality
[- three base of tri- oxygen triazines -1,3,5 (2H, 4H, 6H) of 2,4,6-] three that the methyl ethyl ketoxime that degree is 134mg/L~364mg/L blocks
In (cyclohexyl) isocyanates, cocurrent add to the 1st step stirring stand tower reactor in, flow acceleration be 269mL/min~
997mL/min;Start stirring and found tower reactor blender, setting speed is 138rpm~178rpm;Stirring 4~8 minutes;Again
7- methyl octanals are added, starts the steam oil heater in the vertical tower reactor of stirring, is warming up to 168.4 DEG C~205.8 DEG C,
PH is adjusted between 4.4~8.8, and it is 123.118m to be passed through helium ventilatory capacity3/ min~164.273m3/ min, heat preservation are stood
158.2~188.8 minutes;It is again started up stirring and founds tower reactor blender, rotating speed is 133rpm~178rpm, is added
(2E)-formic acid -2- hexen-1-ol esters, and pH is adjusted between 4.4~8.8, heat preservation stands 157.5~197.6 minutes;
5th step:Start the blender in the vertical tower reactor of stirring, setting speed is 130rpm~197rpm, and it is vertical to start stirring
Steam oil heater in tower reactor sets stirring and founds temperature in tower reactor as 1.287 × 102DEG C~2.32
×102DEG C, the polymer of polyurethane is added, reacts 124.2~135.1 minutes;Rosolic acid cetyl ester is added later, starts
The steam oil heater in tower reactor is found in stirring, set temperature in the vertical tower reactor of stirring as 208.4 DEG C~
264.4 DEG C, pH is adjusted between 4.1~8.1, and pressure is 1.3MPa~1.31MPa, and the reaction time is 0.4~0.9 hour;It
After be depressurized to normal pressure, be cooled to 124.2 DEG C~135.1 DEG C and discharge into molding press to get to rotary shaft 4-7-7;The silver nanoparticle
The grain size of particle is 138 μm~148 μm.
Further, a kind of mobile river and lake is desilted and dredged the work side of the counting device in sludge sample processing device
Method, this method include following steps:
1st step:Object to be cut is encased in the sample cell 4-3-2 on sample handgrip 4-3 by treatment process, control system 6
Banjo traction splint 4-3-3 work is controlled, process object is clamped;Sample clamping degree inductor 4-3-4 monitors process object in real time
Clamping degree, when sample clamping degree inductor 4-3-4 detects that process object clamping degree reaches default value M, sample clamps
Feedback signal is sent to control system 6 by degree inductor 4-3-4, and control system 6 controls banjo traction splint 4-3-3 and is stopped;
2nd step:At the same time, control system 6 starts the slide motor 3-8 of the ends sliding block 3-3, in the case where slide motor 3-8 drives,
Sliding block 3-3 does sliding motion along slideway 3-2, pushes disk 3-7 to be leaned on to the sample for being fixed on the ends sample handgrip 4-3 to drive
Closely;When pushing disk 3-7 apart from sample 3cm~5cm, control system 6 stops slide motor 3-8 work, while controlling hydraulic cylinder
3-6 works;Under hydraulic cylinder 3-6 drivings, push disk 3-7 slowly close to sample, until pushing disk 3-7 front end blades and processing
Object end face is in contact;
3rd step:Control system 6 starts the electric rotating machine 4- in speed regulating motor 3-4 and sample clamp 4 in pushing mechanism 3 simultaneously
1;Under speed regulating motor 3-4 drivings, disk 3-7 is pushed to do circular motion clockwise;Under the driving of electric rotating machine 4-1 motors, sample
Handgrip 4-3 does counterclockwise circular motion by handgrip gear 4-6;
4th step:In electric rotating machine 4-1 rotary courses, lap count 4-7 monitors electric rotating machine 4-1 rotating cycles in real time;When
When lap count 4-7 detects that electric rotating machine 4-1 rotating cycles reach default value R, lap count 4-7 is by feedback letter
It number is sent to control system 6, control system 6 controls electric rotating machine 4-1 and is stopped;
5th step:In the speed regulating motor 3-4 courses of work, when the timer in control system 6 works to speed regulating motor 3-4
Between carry out timing;When timer, which adds up timing time, reaches default value T, control system 6 stops speed regulating motor 3-4;
6th step:Control system 6 controls banjo traction splint 4-3-3 and unclamps, and the sample handled well enters subsequent processing.
A kind of mobile river and lake of the present invention is desilted and dredged the counting device in sludge sample processing device, the device
Intelligence degree is high, and time intelligence is controllable, counts quality and is substantially improved, and stability is high, and the speed of service is fast, is rushed to other equipment
It is small to hit power, work efficiency is high.
Description of the drawings
Fig. 1 is the counting device that a kind of heretofore described mobile river and lake is desilted and dredged in sludge sample processing device
Schematic diagram.
Fig. 2 is heretofore described 3 structural schematic diagram of pushing mechanism.
Fig. 3 is 7 structural schematic diagram of heretofore described rolling cutter.
Fig. 4 is in the present invention for the cooling device structural schematic diagram of slideway 3-2 settings.
Fig. 5 is heretofore described medicament mixing device 3-2-8 structural schematic diagrams.
Fig. 6 is heretofore described promotion disk brake apparatus 3-9 structural schematic diagrams.
Fig. 7 is heretofore described 4 structural schematic diagram of sample clamp.
Fig. 8 is heretofore described lap count 4-7 structural schematic diagrams.
Fig. 9 is heretofore described sample handgrip 4-3 structural schematic diagrams.
Figure 10 is heretofore described rotary shaft 4-7-7 material wear-resistant rates with usage time variation diagram.
Specific implementation mode
It desilts and dredges sludge sample process to a kind of mobile river and lake provided by the invention with reference to the accompanying drawings and examples
Counting device in equipment is further described.
As shown in Figure 1, being that a kind of heretofore described mobile river and lake is desilted and dredged in sludge sample processing device
Counting device schematic diagram.The support platform 5 is rectangle galvanized sheet, and support platform 5 is fixedly mounted on 2 top of fixed frame;Institute
It states pushing mechanism 3 and is arranged in 5 side of support platform;The sample clamp 4 is arranged in 5 other side of support platform;The control system
System 6 is fixedly mounted on fixed frame 2;The rolling cutter 7 is located at 3 left side of pushing mechanism, the two connection.
As shown in Fig. 2, being heretofore described 3 structural schematic diagram of pushing mechanism.The speed regulating motor transmission shaft 3-10
One end is connect with speed regulating motor 3-4, and the other end passes through fuel tank 3-5, pushes disk brake apparatus 3-9, hydraulic cylinder 3-6 and push disk 3-
7 are fixedly connected, and speed regulating motor 3-4, which drives, pushes disk 3-7 rotations;The fuel tank 3-5 is connected to the one end hydraulic cylinder 3-6 conduit;Institute
State the hydraulic cylinder 3-6 other ends pushes disk 3-7 to connect with detachable;The promotion disk brake apparatus 3-9, which is located at, pushes disk 3-7 and liquid
Cylinder pressure 3-6 is between the two;The speed regulating motor 3-4, hydraulic cylinder 3-6, disk 3-7 central axis are pushed in the same horizontal line, pushed away
Moving plate 3-7 is connect with rolling cutter 7, pushes disk 3-7 that rolling cutter 7 is driven to rotate;3-6 points of the speed regulating motor 3-4, hydraulic cylinder
It is not connected by conducting wire and the control of control system 6;The slide motor 3-8 is connected by conducting wire and the control of control system 6.
As shown in figure 3, being 7 structural schematic diagram of heretofore described rolling cutter.The peripheries water inlet pipe 7-7 are equipped with heating tube 7-
5, heating tube 7-5 helical structures, one end heating tube 7-5 is connected to by conducting wire with transformer 7-2, and the other end of transformer 7-2 is logical
It crosses conducting wire to be electrically connected with external city, heating tube 7-5 implements heating to water inlet pipe 7-7, and transformer 7-2 implements to adjust to heating temperature
Section;Outside transmission shaft 7-9 be equipped with cutting edge 7-3, cutting edge 7-3 quantity be 4,4 cutting edge 7-3 angularly, central shaft
Symmetric mode is fixed on transmission shaft 7-9;It is equipped with cutting edge nozzle 7-6, the one end cutting edge nozzle 7-6 in the roots cutting edge 7-3
Open design is simultaneously directed toward cutting edge 7-3 knife faces, and the cutting edge nozzle 7-6 other ends are connected to water inlet pipe 7-7;Driven wheel 7-1 passes through
Transmission shaft 7-9 drives cutting edge 7-3 rotations, cutting edge 7-3 to implement equidistant cutting to material;Meanwhile cutting edge nozzle 7-6 is to cutting
Blade 7-3 knife faces implement cleaning.
As shown in figure 4, being the cooling device structural schematic diagram being arranged for slideway 3-2 in the present invention.The heat-exchanging chamber 3-
2-3 is separated by the partition board 3-2-4 and buffered room 3-2-5 of upper and lower ends;Superposed buffered room 3-2-5,
Top is equipped with refrigerant inlet 3-2-6, and the buffered room 3-2-5 on top is connected to refrigerant inlet 3-2-6, is located at the buffering of lower part
Its bottom process chamber 3-2-5 is equipped with refrigerant exit 3-2-9, the buffered room 3-2-5 of lower part and the refrigerant exit 3-2-9 of bottom
Connection;The medicament mixing device 3-2-8 is connected to heat-exchanging chamber 3-2-3;Refrigerant enters buffered from refrigerant inlet 3-2-6
Room 3-2-5, and then enter inside heat-exchange tube 3-2-2, by heat absorption caused by heat-exchange tube 3-2-2, and from refrigerant
Export 3-2-9 outflows;Heat-exchanging chamber 3-2-3 is entered from by coolant liquid entrance 3-2-1 by coolant liquid, transfers heat to heat exchange
Pipe 3-2-2, and from by coolant liquid outlet 3-2-7 outflows;Meanwhile external agent is controllably added by medicament mixing device 3-2-8
Enter to inside heat-exchanging chamber 3-2-3, is reacted with by coolant liquid.
As shown in figure 5, being heretofore described medicament mixing device 3-2-8 structural schematic diagrams.The buffer subsystem 3-2-
8-4 is located at diffusant and enters on the right side of pipe 3-2-8-3, and buffer subsystem 3-2-8-4 is holey, vertical display;The agitation ball 3-2-
8-5 is located on the right side of buffer subsystem 3-2-8-4, and agitation ball 3-2-8-5 is macromolecule thin-walled hollow structure, stirs ball 3-2-8-5 materials
Density is less than the density of water, and agitation ball 3-2-8-5 quantity is 50~100, and the single ball 3-2-8-5 mass that stirs is less than 10
Gram, between multiple agitation ball 3-2-8-5 are limited at buffer subsystem 3-2-8-4 and stablize net 3-2-8-6, the agitation ball 3-2-8-
5 be scattered distribution, and gap mutual agitation ball 3-2-8-5 is more than 5cm;The stable net 3-2-8-6 is located at agitation ball 3-
On the right side of 2-8-5, it is holey, vertical display to stablize net 3-2-8-6;Medicament enters from medicament inlet 3-2-8-1, with diluent
The diluent sprayed into pipe 3-2-8-9 meets, will be dilute under the action of decentralized network 3-2-8-8, diffusion horn mouth 3-2-8-7
Agent is released further to disperse and mix with medicament;Diffusant enters pipe 3-2-8-3 by diffusant and is sprayed from diffusant jet pipe 3-2-8-2
Go out, buffer subsystem 3-2-8-4 implements buffering to the diffusant of ejection, and enters together with medicament, diluent and be located at buffer subsystem 3-2-
Agitation ball 3-2-8-5 action spaces between 8-4 and stable net 3-2-8-6, in the case where stirring ball 3-2-8-5 agitaions, diffusion
Agent, diluent, medicament are sufficiently mixed, and mixture is discharged from agent outlet 3-2-8-10.
As shown in fig. 6, being heretofore described promotion disk brake apparatus 3-9 structural schematic diagrams.Outside brake caliper 3-9-4
It encloses equipped with braking hauling rope 3-9-3, braking hauling rope 3-9-3 is around brake caliper 3-9-4 surroundings, and the two is hinged;Braking is led
The other end of straw line 3-9-3 is connect with haulage gear 3-9-2;It is equipped with brake cooling system 3-9- on the tops brake caliper 3-9-4
1, the two is connected by conduit;Haulage gear 3-9-2 rotations, tightening braking hauling rope 3-9-3, and then pass through brake caliper 3-9-
4 are tightly attached to 4 friction plate 3-9-6 on speed regulating motor transmission shaft 3-10, and speed regulating motor transmission shaft 3-10 is made to stop operating;With this
Meanwhile the heat that friction plate 3-9-6 is generated by friction, pass through the brake cooling system 3-9-1 bands being connect with brake caliper 3-9-4
It walks.
As shown in fig. 7, being heretofore described 4 structural schematic diagram of sample clamp.The handgrip gear 4-6 quantity is three
It is a, it is circumferentially symmetrical around central gear 4-5;The electric rotating machine 4-1 is fixedly mounted on the sides service chamber 4-2, rotation
Motor 4-1 is drivingly connected with central gear 4-5;The sample handgrip 4-3 is arranged in the other sides service chamber 4-2, sample handgrip 4-3
One end is fixedly connected with handgrip gear 4-6;The lap count 4-7 is fixedly connected on electric rotating machine 4-1 turntables;The rotation
Rotating motor 4-1, lap count 4-7 are connected by conducting wire and the control of control system 6 respectively;Electric rotating machine 4-1 drives centre tooth
4-5 rotations are taken turns, and then three, periphery handgrip gear 4-6 is driven to do revolution motion, while three handgrips along gear wheel 4-4 interior tooths
Gear 4-6 is also done rotation movement, and handgrip gear 4-6 drives sample revolution and rotation by sample handgrip 4-3.
As shown in figure 8, being heretofore described lap count 4-7 structural schematic diagrams.The tops the rotary shaft 4-7-7
Equipped with gearbox 4-7-5, gearbox 4-7-5 is internally provided with deboost axle 4-7-3, and deboost axle 4-7-3 is nibbled with rotary shaft 4-7-7 gears
Close connection;The tops gearbox 4-7-5 are equipped with electric rotating machine 4-7-10, and electric rotating machine 4-7-10 is engaged with deboost axle 4-7-3 gears
Connection;The bottoms gearbox 4-7-5 are equipped with temperature sensor 4-7-4, velocity sensor 4-7-6;Electric rotating machine 4-7-10 is by subtracting
Fast axis 4-7-3, rotary shaft 4-7-7 drive the probe 4-7-1 rotations of Laser Measuring circle, to exchange the work of Laser Measuring circle probe 4-7-1
Angle;At the same time, it is located at temperature sensor 4-7-4, the velocity sensor 4-7-6 of the bottoms gearbox 4-7-5 in real time to work
Object state on platform 4 is monitored.
As shown in figure 9, being heretofore described sample handgrip 4-3 structural schematic diagrams.Banjo traction splint 4-3-3 driving electricity
Machine, sample clamping degree inductor 4-3-4 are connected by conducting wire and the control of control system 6 respectively.It is provided in the control system 6
Timer, the timer are connect with speed regulating motor 3-4 actuating coil polygon control surveys.
A kind of mobile river and lake of the present invention is desilted and dredged the work of the counting device in sludge sample processing device
Process is:
1st step:Object to be cut is encased in the sample cell 4-3-2 on sample handgrip 4-3 by treatment process, control system 6
Banjo traction splint 4-3-3 work is controlled, process object is clamped;Sample clamping degree inductor 4-3-4 monitors process object in real time
Clamping degree, when sample clamping degree inductor 4-3-4 detects that process object clamping degree reaches default value M, sample clamps
Feedback signal is sent to control system 6 by degree inductor 4-3-4, and control system 6 controls banjo traction splint 4-3-3 and is stopped;
2nd step:At the same time, control system 6 starts the slide motor 3-8 of the ends sliding block 3-3, in the case where slide motor 3-8 drives,
Sliding block 3-3 does sliding motion along slideway 3-2, pushes disk 3-7 to be leaned on to the sample for being fixed on the ends sample handgrip 4-3 to drive
Closely;When pushing disk 3-7 apart from sample 3cm~5cm, control system 6 stops slide motor 3-8 work, while controlling hydraulic cylinder
3-6 works;Under hydraulic cylinder 3-6 drivings, push disk 3-7 slowly close to sample, until pushing disk 3-7 front end blades and processing
Object end face is in contact;
3rd step:Control system 6 starts the electric rotating machine 4- in speed regulating motor 3-4 and sample clamp 4 in pushing mechanism 3 simultaneously
1;Under speed regulating motor 3-4 drivings, disk 3-7 is pushed to do circular motion clockwise;Under the driving of electric rotating machine 4-1 motors, sample
Handgrip 4-3 does counterclockwise circular motion by handgrip gear 4-6;
4th step:In electric rotating machine 4-1 rotary courses, lap count 4-7 monitors electric rotating machine 4-1 rotating cycles in real time;When
When lap count 4-7 detects that electric rotating machine 4-1 rotating cycles reach default value R, lap count 4-7 is by feedback letter
It number is sent to control system 6, control system 6 controls electric rotating machine 4-1 and is stopped;
5th step:In the speed regulating motor 3-4 courses of work, when the timer in control system 6 works to speed regulating motor 3-4
Between carry out timing;When timer, which adds up timing time, reaches default value T, control system 6 stops speed regulating motor 3-4;
6th step:Control system 6 controls banjo traction splint 4-3-3 and unclamps, and the sample handled well enters subsequent processing.
The embodiment of the manufacturing process of rotary shaft 4-7-7 of the present invention below, embodiment be in order to further illustrate
Present disclosure, but should not be construed as limiting the invention.Without departing from the spirit and substance of the case in the present invention, to this
It changes and replaces made by inventive method, step or condition, all belong to the scope of the present invention.
Unless otherwise specified, the conventional means that technological means used in embodiment is well known to those skilled in the art.
The content that following embodiment further illustrates the present invention, as rotary shaft 4-7-7, it is the important set of the present invention
Part increases the service life of integral device due to its presence, it plays pass for the safety of integral device, even running
Key acts on.For this purpose, by it is following be embodiment, further verify rotary shaft 4-7-7 of the present invention, what is shown is higher than
The physical characteristic of other related patents.
Embodiment 1
Rotary shaft 4-7-7 of the present invention is prepared according to the following steps, and is counted in parts by weight:
1st step:In tower reactor is found in stirring, it is added and purifies 339.2 parts of lake water and N- methyl-1s, 1,2,2,3,3,4,4,5,
5,5- ten one 131.5 parts of fluoro -1- pentanes sulfonamide start stirring and found blender in tower reactor, and setting speed is
132rpm starts the steam oil heater in the vertical tower reactor of stirring, so that temperature is risen to 147.2 DEG C, 1- (methoxyl groups are added
Methyl) 134.2 parts of -4- methylbenzenes stir evenly, and carry out reaction 124.5 minutes, and 130.4 parts of 4- (methyl mercapto) butyraldehyde is added, lead to
Inbound traffics are 123.5m3The helium of/min 124.5 minutes;133.1 parts of rutile is added in tower reactor is found in stirring later,
The steam oil heater being again started up in the vertical tower reactor of stirring, makes temperature rise to 164.2 DEG C, keeps the temperature 124.4 minutes, add
Enter 136.9 parts of the polymer of 4,4'- (1- methyl ethylidene) bis- [2- (2- acrylic)] phenol and (chloromethyl) ethylene oxide, adjusts
The pH value that solution in tower reactor is found in whole stirring is 4.1, keeps the temperature 124.1 minutes;
2nd step:138.7 parts of silver nano-particle separately is taken, ultrasonication 0.130 is small in the case where power is 6.64KW by silver nano-particle
Shi Hou;Silver nano-particle is added to another stirring to stand in tower reactor, the polymeric oxygen that mass concentration is 134mg/L is added
1,1,2,3,3,3 changed, 131.1 parts of dispersion silver nano-particles of-hexafluoro -1- propylene, starts the steaming in the vertical tower reactor of stirring
Vapour formula oil heater makes solution temperature at 45 DEG C, starts the blender in the vertical tower reactor of stirring, and with 4 × 102Rpm's
Speed stirs, and adjustment pH value is 4.5, insulated and stirred 130 minutes;Stop reaction later and stand 6.64 × 10 minutes, removes impurity;
Suspension is added to 133.6 parts of the polymer of formaldehyde and dicyanodiamide and ethylenediamine sulfate, adjustment pH value is formed 1.5
Sediment purification lake water elution, by centrifuge in rotating speed 4.192 × 103Solid content is obtained under rpm, 2.407 × 102℃
At a temperature of it is dry, 0.192 × 10 is crossed after grinding3Mesh sieves, spare;
3rd step:Another silver nano-particle after taking alkali formula aphthenic acids zinc salt 133.9 and the processing of the 2nd step, uses glancing incidence after mixing
Low-angle gamma-rays diffusing reflection irradiates, and the energy of glancing incidence low-angle gamma-rays diffusing reflection irradiation is 121.2MeV, dosage is
169.2kGy, irradiation time are 133.2 minutes, obtain the alkali formula aphthenic acids zinc salt and silver nano-particle mixture of character change;
Alkali formula aphthenic acids zinc salt and silver nano-particle mixture are placed in another stirring to stand in tower reactor, it is vertical tower anti-to start stirring
The steam oil heater in device, 132.8 DEG C of set temperature is answered to start the blender in the vertical tower reactor of stirring, rotating speed is
124rpm, pH are adjusted to 4.3, are dehydrated 133.3 minutes, spare;
4th step:The alkali formula aphthenic acids zinc salt and silver nano-particle mixture that the character that 3rd step is obtained changes, it is dense to add to quality
[- three base of tri- oxygen triazines -1,3,5 (2H, 4H, 6H) of 2,4,6-] three (cyclohexyl) that the methyl ethyl ketoxime that degree is 134mg/L blocks are different
In 122.5 parts of cyanate, the stirring that cocurrent adds to the 1st step is stood in tower reactor, flow acceleration 269mL/min;Startup is stirred
Mix vertical tower reactor blender, setting speed 138rpm;Stirring 4 minutes;121.2 parts of 7- methyl octanals are added, are started
The steam oil heater in tower reactor is found in stirring, is warming up to 168.4 DEG C, pH is adjusted to 4.4, is passed through helium ventilatory capacity and is
123.118m3/ min, heat preservation stand 158.2 minutes;It is again started up to stir and founds tower reactor blender, rotating speed 133rpm,
130.8 parts of (2E)-formic acid -2- hexen-1-ols ester is added, and pH is made to be adjusted to 4.4, heat preservation stands 157.5 minutes;
5th step:Start the blender in the vertical tower reactor of stirring, setting speed 130rpm starts stirring and stands tower reaction
Steam oil heater in device sets stirring and founds temperature in tower reactor as 1.287 × 102DEG C, polyurethane is added
140.3 parts of polymer reacts 124.2 minutes;The rosolic acid cetyl ester 163.4 that mass concentration is 130mg/L is added later
Part, start stirring and found steam oil heater in tower reactor, set temperature in the vertical tower reactor of stirring as 208.4
DEG C, pH is adjusted to 4.1, and pressure 1.3MPa, the reaction time is 0.4 hour;It is depressurized to normal pressure later, is cooled to 124.2 DEG C and goes out
Expect into molding press to get to rotary shaft 4-7-7;
The grain size of the silver nano-particle is 138 μm.
Embodiment 2
Rotary shaft 4-7-7 of the present invention is prepared according to the following steps, and is counted in parts by weight:
1st step:In tower reactor is found in stirring, it is added and purifies 564.8 parts of lake water and N- methyl-1s, 1,2,2,3,3,4,4,5,
5,5- ten one 173.6 parts of fluoro -1- pentanes sulfonamide start stirring and found blender in tower reactor, and setting speed is
178rpm starts the steam oil heater in the vertical tower reactor of stirring, so that temperature is risen to 148.8 DEG C, 1- (methoxyl groups are added
Methyl) 243.1 parts of -4- methylbenzenes stir evenly, and carry out reaction 135.6 minutes, and 147.4 parts of 4- (methyl mercapto) butyraldehyde is added, lead to
Inbound traffics are 164.4m3The helium of/min 135.6 minutes;190.3 parts of rutile is added in tower reactor is found in stirring later,
The steam oil heater being again started up in the vertical tower reactor of stirring, makes temperature rise to 197.1 DEG C, keeps the temperature 135.4 minutes, add
Enter 197.5 parts of the polymer of 4,4'- (1- methyl ethylidene) bis- [2- (2- acrylic)] phenol and (chloromethyl) ethylene oxide, adjusts
The pH value that solution in tower reactor is found in whole stirring is 8.3, keeps the temperature 364.1 minutes;
2nd step:Separately take 193.3 parts of silver nano-particle, by silver nano-particle power be 12.08KW under ultrasonication 1.197
After hour;Silver nano-particle is added to another stirring to stand in tower reactor, the polymerization that mass concentration is 364mg/L is added
The 1,1,2,3,3,3 of oxidation, 173.6 parts of dispersion silver nano-particles of-hexafluoro -1- propylene, starts stirring and stands in tower reactor
Steam oil heater makes solution temperature between 89 DEG C, starts stirring and founds blender in tower reactor, and with 8 ×
102The speed of rpm stirs, and adjustment pH value is 8.8, insulated and stirred 197 minutes;Stop reaction later and stand 12.08 × 10 minutes,
Remove impurity;Suspension is added to 173.5 parts of the polymer of formaldehyde and dicyanodiamide and ethylenediamine sulfate, adjustment pH value exists
2.8, sediment purification lake water elution is formed, solid content is obtained at 9.643 × 103rpm of rotating speed by centrifuge,
3.642×102It is dry at a temperature of DEG C, 1.643 × 103 mesh sieve is crossed after grinding, it is spare;
3rd step:It is another take 156.6 parts of alkali formula aphthenic acids zinc salt and the 2nd step to handle after silver nano-particle, after mixing use plunder into
Low-angle gamma-rays diffusing reflection irradiation is penetrated, the energy of glancing incidence low-angle gamma-rays diffusing reflection irradiation is 149.8MeV, dosage is
209.8kGy, irradiation time are 158.8 minutes, obtain the alkali formula aphthenic acids zinc salt and silver nano-particle mixture of character change;
Alkali formula aphthenic acids zinc salt and silver nano-particle mixture are placed in another stirring to stand in tower reactor, it is vertical tower anti-to start stirring
The steam oil heater in device, 178.4 DEG C of set temperature is answered to start the blender in the vertical tower reactor of stirring, rotating speed is
519rpm, pH are adjusted to 8.3, are dehydrated 147.3 minutes, spare;
4th step:The alkali formula aphthenic acids zinc salt and silver nano-particle mixture that the character that 3rd step is obtained changes, it is dense to add to quality
[- three base of tri- oxygen triazines -1,3,5 (2H, 4H, 6H) of 2,4,6-] three (cyclohexyl) that the methyl ethyl ketoxime that degree is 364mg/L blocks are different
In 158.8 parts of cyanate, the stirring that cocurrent adds to the 1st step is stood in tower reactor, flow acceleration 997mL/min;Startup is stirred
Mix vertical tower reactor blender, setting speed 178rpm;Stirring 8 minutes;164.8 parts of 7- methyl octanals are added, are started
The steam oil heater in tower reactor is found in stirring, is warming up to 205.8 DEG C, pH is adjusted to 8.8, is passed through helium ventilatory capacity and is
164.273m3/min heat preservation stands 188.8 minutes;It is again started up to stir and founds tower reactor blender, rotating speed 178rpm,
175.4 parts of (2E)-formic acid -2- hexen-1-ols ester is added, and pH is made to be adjusted to 8.8, heat preservation stands 197.6 minutes;
5th step:Start the blender in the vertical tower reactor of stirring, setting speed 197rpm starts stirring and stands tower reaction
Steam oil heater in device sets stirring and founds temperature in tower reactor as 2.32 × 102DEG C, the poly- of polyurethane is added
184.3 parts of object is closed, is reacted 135.1 minutes;217.8 parts of the rosolic acid cetyl ester that mass concentration is 397mg/L is added later,
Start stirring and found steam oil heater in tower reactor, set the temperature in the vertical tower reactor of stirring as 264.4 DEG C,
PH is adjusted to 8.1, and pressure 1.31MPa, the reaction time is 0.9 hour;It is depressurized to normal pressure later, is cooled to 135.1 DEG C of dischargings
Enter molding press to get to rotary shaft 4-7-7;
The grain size of the silver nano-particle is 148 μm.
Embodiment 3
Rotary shaft 4-7-7 of the present invention is prepared according to the following steps, and is counted in parts by weight:
1st step:In tower reactor is found in stirring, it is added and purifies 339.9 parts of lake water and N- methyl-1s, 1,2,2,3,3,4,4,5,
5,5- ten one 131.9 parts of fluoro -1- pentanes sulfonamide start stirring and found blender in tower reactor, and setting speed is
132rpm starts the steam oil heater in the vertical tower reactor of stirring, so that temperature is risen to 147.9 DEG C, 1- (methoxyl groups are added
Methyl) 134.9 parts of -4- methylbenzenes stir evenly, and carry out reaction 124.9 minutes, and 130.9 parts of 4- (methyl mercapto) butyraldehyde is added, lead to
The helium that inbound traffics are 123.9m3/min 124.9 minutes;133.9 parts of rutile is added in tower reactor is found in stirring later,
The steam oil heater being again started up in the vertical tower reactor of stirring, makes temperature rise to 164.9 DEG C, keeps the temperature 124.9 minutes, add
Enter 136.9 parts of the polymer of 4,4'- (1- methyl ethylidene) bis- [2- (2- acrylic)] phenol and (chloromethyl) ethylene oxide, adjusts
The pH value that solution in tower reactor is found in whole stirring is 4.9, keeps the temperature 124.9 minutes;
2nd step:Separately take 138.9 parts of silver nano-particle, by silver nano-particle power be 6.649KW under ultrasonication 0.1309
After hour;Silver nano-particle is added to another stirring to stand in tower reactor, it is the poly- of 134.9mg/L that mass concentration, which is added,
The 1,1,2,3,3,3 of oxidation is closed, 131.9 parts of dispersion silver nano-particles of-hexafluoro -1- propylene start stirring and stand in tower reactor
Steam oil heater, make solution temperature at 45.9 DEG C, start stirring and found blender in tower reactor, and with 4.9 ×
102The speed of rpm stirs, and adjustment pH value is 4.9, insulated and stirred 130.9 minutes;Stop reaction later and stands 6.64 × 10 points
Clock removes impurity;Suspension is added to 133.9 parts of the polymer of formaldehyde and dicyanodiamide and ethylenediamine sulfate, adjusts pH
Value forms sediment purification lake water elution, solid content is obtained at 4.192 × 103rpm of rotating speed by centrifuge 1.9,
2.407×102It is dry at a temperature of DEG C, 0.192 × 103 mesh sieve is crossed after grinding, it is spare;
3rd step:Another silver nano-particle after taking alkali formula aphthenic acids zinc salt 133.9 and the processing of the 2nd step, uses glancing incidence after mixing
Low-angle gamma-rays diffusing reflection irradiates, and the energy of glancing incidence low-angle gamma-rays diffusing reflection irradiation is 121.9MeV, dosage is
169.9kGy, irradiation time are 133.9 minutes, obtain the alkali formula aphthenic acids zinc salt and silver nano-particle mixture of character change;
Alkali formula aphthenic acids zinc salt and silver nano-particle mixture are placed in another stirring to stand in tower reactor, it is vertical tower anti-to start stirring
The steam oil heater in device, 132.9 DEG C of set temperature is answered to start the blender in the vertical tower reactor of stirring, rotating speed is
124rpm, pH are adjusted to 4.9, are dehydrated 133.9 minutes, spare;
4th step:The alkali formula aphthenic acids zinc salt and silver nano-particle mixture that the character that 3rd step is obtained changes, it is dense to add to quality
[- three base of tri- oxygen triazines -1,3,5 (2H, 4H, 6H) of 2,4,6-] three (cyclohexyl) that the methyl ethyl ketoxime that degree is 134.9mg/L blocks
In 122.9 parts of isocyanates, the stirring that cocurrent adds to the 1st step is stood in tower reactor, flow acceleration 269.9mL/min;It opens
Tower reactor blender, setting speed 138rpm are found in dynamic stirring;Stirring 4.9 minutes;Add 7- methyl octanals 121.9
Part, start the steam oil heater in the vertical tower reactor of stirring, is warming up to 168.9 DEG C, pH is adjusted to 4.9, is passed through helium
Ventilatory capacity is 123.9m3/min, and heat preservation stands 158.9 minutes;It is again started up stirring and founds tower reactor blender, rotating speed is
130.9 parts of (2E)-formic acid -2- hexen-1-ols ester is added in 133rpm, and pH is made to be adjusted to 4.9, and heat preservation stands 157.9 points
Clock;
5th step:Start the blender in the vertical tower reactor of stirring, setting speed 130rpm starts stirring and stands tower reaction
Steam oil heater in device sets stirring and founds temperature in tower reactor as 1.287 × 102DEG C, polyurethane is added
140.9 parts of polymer reacts 124.9 minutes;The rosolic acid cetyl ester 163.4 that mass concentration is 130mg/L is added later
Part, start stirring and found steam oil heater in tower reactor, set temperature in the vertical tower reactor of stirring as 208.9
DEG C, pH is adjusted to 4.9, and pressure 1.3MPa, the reaction time is 0.41 hour;It is depressurized to normal pressure later, is cooled to 124.9 DEG C and goes out
Expect into molding press to get to rotary shaft 4-7-7;
The grain size of the silver nano-particle is 138 μm.
Reference examples
Reference examples are tested for the property experiment using the rotary shaft of certain commercially available brand.
Embodiment 4
The rotary shaft that Examples 1 to 3 and reference examples are obtained is tested for the property experiment, mechanical strength is carried after test
The parameters such as the rate of liter, compression strength enhancing rate, anti-yield strength enhancing rate, wear rate enhancing rate are analyzed.Data analysis such as table 1
It is shown.
As seen from Table 1, rotary shaft 4-7-7 of the present invention, mechanical strength enhancing rate, resist compression strength enhancing rate
Yield strength enhancing rate, wear rate enhancing rate are above the product of prior art production.
In addition, as shown in Figure 10, rotary shaft 4-7-7 of the present invention is carried out with reference examples, with usage time
Change test data statistics.Find out in figure, Examples 1 to 3 is substantially better than the prior art and gives birth in test data technical indicator
The product of production.
Claims (10)
- A kind of counting device 1. movable type river and lake is desilted and dredged in sludge sample processing device, including:Shock-absorbing foot pad (1), Gu Determine frame (2), pushing mechanism (3), sample clamp (4), support platform (5), control system (6), rolling cutter (7);Its feature It is, the fixed frame (2) is stainless steel rectangular structure, and thickness is between 3cm~4cm;Shock-absorbing foot pad (1) quantity It is four, is respectively and fixedly installed to fixed frame (2) bottom four corners;The support platform (5) is rectangle galvanized sheet, support platform (5) it is fixedly mounted on above fixed frame (2);The pushing mechanism (3) is arranged in support platform (5) side;The specimen holder Tool (4) is arranged in support platform (5) other side;The control system (6) is fixedly mounted on fixed frame (2);The rolling cutter (7) is located on the left of pushing mechanism (3), the two connection;Sample clamp (4) is equipped with lap count (4-7);The lap count (4-7) includes:Laser Measuring circle is popped one's head in (4-7-1), conversion head (4-7-2), deboost axle (4-7-3), Temperature sensor (4-7-4), gearbox (4-7-5), velocity sensor (4-7-6), rotary shaft (4-7-7), secondary light source (4-7- 8), Laser emission receiver (4-7-9), electric rotating machine (4-7-10), spare Laser Measuring circle pop one's head in (4-7-11);Laser Measuring circle positioned at bottom is popped one's head in (4-7-1), and surface further includes secondary light source (4-7-8) and Laser emission receiver (4-7-9), the Laser emission receiver (4-7-9) is located at Laser Measuring circle probe (4-7-1) bottom centre, direction is shone downwards It penetrates, Laser emission receiver (4-7-9) is surrounded by secondary light source (4-7-8), and secondary light source (4-7-8) is 12, fill-in light Source (4-7-8) is LE light sources;The conversion head (4-7-2) is located at the top of Laser Measuring circle probe (4-7-1), conversion head (4-7- 2) it is rotatablely connected with the rotary shaft on top (4-7-7), meanwhile, the rotary shaft (4-7-7) of Laser Measuring circle probe (4-7-1) and top It is fixedly connected;Spare Laser Measuring circle is equipped in conversion head (4-7-2) horizontal direction to pop one's head in (4-7-11), quantity is 4, spare Laser Measuring circle (4-7-11) and Laser Measuring circle probe (4-7-1) structure of popping one's head in is identical, and Laser Measuring circle is popped one's head in (4-7-1) and spare sharp Flash ranging circle pops one's head in (4-7-11) as Demountable;Rotary shaft (4-7-7) top is equipped with gearbox (4-7-5), speed change Case (4-7-5) is internally provided with deboost axle (4-7-3), and deboost axle (4-7-3) engages connection with rotary shaft (4-7-7) gear;Speed change The top case (4-7-5) is equipped with electric rotating machine (4-7-10), and electric rotating machine (4-7-10) engages company with deboost axle (4-7-3) gear It connects;The bottom gearbox (4-7-5) is equipped with temperature sensor (4-7-4), velocity sensor (4-7-6);Electric rotating machine (4-7-10) drives Laser Measuring circle probe (4-7-1) to turn by deboost axle (4-7-3), rotary shaft (4-7-7) It is dynamic, to exchange the operating angle of Laser Measuring circle probe (4-7-1);At the same time, the temperature for being located at the bottom gearbox (4-7-5) passes Sensor (4-7-4), velocity sensor (4-7-6) are in real time monitored the object state on workbench (4).
- Counting device 2. a kind of mobile river and lake according to claim 1 is desilted and dredged in sludge sample processing device, It is characterized in that, the pushing mechanism (3) includes:Slideway fixed block (3-1), slideway (3-2), sliding block (3-3), speed regulating motor (3-4), fuel tank (3-5), hydraulic cylinder (3-6) push disk (3-7), slide motor (3-8) to push disk brake apparatus (3-9), adjust Speed motor transmission shaft (3-10);Wherein, the slideway (3-2) is fixedly connected by slideway fixed block (3-1) with support platform (5);The slideway (3-2) Cross section is in " Ω " shape, and slideway (3-2) quantity is 2;The sliding block (3-3) is slidably connected with slideway (3-2), sliding block (3- 3) end is provided with slide motor (3-8), and slide motor (3-8) driving sliding block (3-3) slides on slideway (3-2);The tune Speed motor (3-4) is variable-frequency motor, and speed regulating motor (3-4) pedestal is welded and fixed with sliding block (3-3);Described speed regulating motor transmission shaft one end (3-10) is connect with speed regulating motor (3-4), and the other end passes through fuel tank (3-5), pushes Disk brake apparatus (3-9), hydraulic cylinder (3-6) are fixedly connected with disk (3-7) is pushed, and speed regulating motor (3-4), which drives, pushes disk (3-7) Rotation;The fuel tank (3-5) is connected to the one end hydraulic cylinder (3-6) conduit;Hydraulic cylinder (3-6) other end is pushed with detachable Disk (3-7) connects;The promotion disk brake apparatus (3-9), which is located at, pushes disk (3-7) and hydraulic cylinder (3-6) between the two;It is described Speed regulating motor (3-4), pushes disk (3-7) central axis in the same horizontal line at hydraulic cylinder (3-6), pushes disk (3-7) and rolls Cutter (7) connects, and pushes disk (3-7) that rolling cutter (7) is driven to rotate;The speed regulating motor (3-4), hydraulic cylinder (3-6) are connected by conducting wire and control system (6) control respectively;The slide motor (3-8) is connected by conducting wire and control system (6) control.
- Counting device 3. a kind of mobile river and lake according to claim 2 is desilted and dredged in sludge sample processing device, It is characterized in that, the rolling cutter (7) includes:Driven wheel (7-1), transformer (7-2), cutting edge (7-3), back-up roller bearing (7-4), heating tube (7-5), cutting edge nozzle (7-6), water inlet pipe (7-7) are intake port (7-8), transmission shaft (7-9);Driven wheel (7-1) positioned at one end is connect with external cutter motor, meanwhile, driven wheel (7-1) and transmission shaft (7- 9) it is fixedly connected;Back-up roller bearing (7-4) is equipped on the inside of driven wheel (7-1), back-up roller bearing (7-4) quantity is 2, It is located at the both ends of transmission shaft (7-9);Transmission shaft (7-9) hollow structure, is internally provided with transformer (7-2), heating tube (7-5), water inlet pipe (7-7);Water inlet pipe (7-7) is parallel to transmission shaft (7-9), and the quantity of water inlet pipe (7-7) is 3, water inlet pipe (7-7) is connected to water inlet port (7-8), and water inlet port (7-8) is connected to external pump;Water inlet pipe (7-7) periphery is equipped with heating It manages (7-5), heating tube (7-5) helical structure, heating tube one end (7-5) is connected to by conducting wire with transformer (7-2), transformer The other end of (7-2) is electrically connected by conducting wire with external city, and heating tube (7-5) is implemented to heat to water inlet pipe (7-7), transformer (7-2) implements to adjust to heating temperature;Cutting edge (7-3) is equipped with outside transmission shaft (7-9), cutting edge (7-3) quantity is 4 A, 4 cutting edges (7-3) are angularly, mode substantially symmetrical about its central axis is fixed on transmission shaft (7-9);It is set in the root cutting edge (7-3) There are cutting edge nozzle (7-6), cutting edge nozzle (7-6) open at one end to design and be directed toward cutting edge (7-3) knife face, cutting edge nozzle (7-6) other end is connected to water inlet pipe (7-7);Driven wheel (7-1) drives cutting edge (7-3) to rotate by transmission shaft (7-9), and cutting edge (7-3) equidistantly cuts material implementation It cuts;Meanwhile cutting edge nozzle (7-6) is implemented to clean to cutting edge (7-3) knife face.
- Counting device 4. a kind of mobile river and lake according to claim 3 is desilted and dredged in sludge sample processing device, It is characterized in that, slideway (3-2) is equipped with cooling device, cooling device includes:By coolant liquid entrance (3-2-1), heat-exchange tube (3- 2-2), heat-exchanging chamber (3-2-3), partition board (3-2-4), buffered room (3-2-5), refrigerant inlet (3-2-6) are gone out by coolant liquid Mouth (3-2-7), medicament mixing device (3-2-8), refrigerant exit (3-2-9);It is connected to heat-exchanging chamber (3-2-3) by coolant liquid entrance (3-2-1) positioned at side, and by coolant liquid entrance (3-2-1) Positioned at the lower part heat-exchanging chamber (3-2-3), low level;It is described by coolant liquid outlet (3-2-7) be located at the top heat-exchanging chamber (3-2-3), A high position, and be connected to heat-exchanging chamber (3-2-3) by coolant liquid outlet (3-2-7);The heat-exchange tube (3-2-2) is located at heat exchange In the middle part of room (3-2-3), the quantity of heat-exchange tube (3-2-2) hollow structure, heat-exchange tube (3-2-2) is 20, more heat exchanges Manage (3-2-2) vertical equidistant arrangement;The both ends heat-exchange tube (3-2-2) are respectively equipped with buffered room (3-2-5), heat-exchange tube The both ends (3-2-2) are connected to the buffered room (3-2-5) for being located at its upper and lower ends respectively;The heat-exchanging chamber (3-2-3) is logical It crosses partition board (3-2-4) and the buffered room (3-2-5) of upper and lower ends separates;Superposed buffered room (3-2-5), Top is equipped with refrigerant inlet (3-2-6), and the buffered room (3-2-5) on top is connected to refrigerant inlet (3-2-6), is located at lower part Its bottom buffered room (3-2-5) be equipped with refrigerant exit (3-2-9), the buffered room (3-2-5) of lower part and bottom Refrigerant exit (3-2-9) is connected to;The medicament mixing device (3-2-8) is connected to heat-exchanging chamber (3-2-3).
- Counting device 5. a kind of mobile river and lake according to claim 4 is desilted and dredged in sludge sample processing device, It is characterized in that, the medicament mixing device (3-2-8) is L-type pipe structure, both ends perforation, medicament mixing device (3-2-8) packet It includes:Medicament inlet (3-2-8-1), diffusant jet pipe (3-2-8-2), diffusant enter pipe (3-2-8-3), buffer subsystem (3-2-8-4), Stir ball (3-2-8-5), stablize net (3-2-8-6), diffusion horn mouth (3-2-8-7), decentralized network (3-2-8-8), diluent into Enter pipe (3-2-8-9), agent outlet (3-2-8-10);Medicament inlet (3-2-8-1) positioned at one end, medicament inlet (3-2-8-1) right side enter pipe (3-2-8- equipped with diluent 9), diluent enters pipe one end (3-2-8-9) and is connected to external diluent bottle, and diluent enters pipe (3-2-8-9) other end To be open, and it is internal to be inserted into diffusion horn mouth (3-2-8-7);Decentralized network (3- is equipped in the middle part of diffusion horn mouth (3-2-8-7) 2-8-8), it is holey, vertical display;It is flared structure to spread horn mouth (3-2-8-7), and heavy caliber end direction is right Side, the diameter ratio for spreading horn mouth (3-2-8-7) heavy caliber end and small-caliber end is 3:1;The diffusant jet pipe (3-2-8-2) It is hollow ring pipe structure on the right side of diffusion horn mouth (3-2-8-7), the ring pipe of diffusant jet pipe (3-2-8-2) is right Side surface is equipped with a large amount of through-holes, and diffusant jet pipe one end (3-2-8-2) enters pipe (3-2-8-3) with diffusant and is connected to;The buffering Net (3-2-8-4) is located at diffusant and enters on the right side of pipe (3-2-8-3), and buffer subsystem (3-2-8-4) is holey, vertical display;Institute Agitation ball (3-2-8-5) to be stated to be located on the right side of buffer subsystem (3-2-8-4), agitation ball (3-2-8-5) is macromolecule thin-walled hollow structure, The density that ball (3-2-8-5) material density is less than water is stirred, agitation ball (3-2-8-5) quantity is 50~100, single to stir Ball (3-2-8-5) quality is less than 10 grams, and multiple agitation balls (3-2-8-5) are limited at buffer subsystem (3-2-8-4) and stablize net (3- Between 2-8-6), the agitation ball (3-2-8-5) is scattered distribution, and the mutual gap of agitation ball (3-2-8-5) is more than 5cm;For the stable net (3-2-8-6) on the right side of agitation ball (3-2-8-5), stable net (3-2-8-6) is holey, vertically It puts;Medicament enters from medicament inlet (3-2-8-1), and the diluent that pipe (3-2-8-9) ejection is entered with diluent meets, and is dividing Under the action of dissipating net (3-2-8-8), diffusion horn mouth (3-2-8-7), diluent is further disperseed and is mixed with medicament;Diffusant enters pipe (3-2-8-3) by diffusant and is sprayed from diffusant jet pipe (3-2-8-2), and buffer subsystem (3-2-8-4) is right The diffusant of ejection implements buffering, and enters together with medicament, diluent and be located at buffer subsystem (3-2-8-4) and stablize net (3-2- Agitation ball (3-2-8-5) action space between 8-6), in the case where stirring ball (3-2-8-5) agitaion, diffusant, diluent, Medicament is sufficiently mixed, and mixture is discharged from agent outlet (3-2-8-10).
- Counting device 6. a kind of mobile river and lake according to claim 5 is desilted and dredged in sludge sample processing device, It is characterized in that, the promotion disk brake apparatus (3-9) includes:Brake cooling system (3-9-1), haulage gear (3-9-2), system Dynamic hauling rope (3-9-3), brake caliper (3-9-4), radiator fan (3-9-5), friction plate (3-9-6);Speed regulating motor transmission shaft (3-10) on central axes is surrounded by friction plate (3-9-6), friction plate (3-9-6) Quantity is 4, and 4 friction plates (3-9-6) wrap up speed regulating motor transmission shaft (3-10) wherein, outside friction plate (3-9-6) It encloses and is equipped with brake caliper (3-9-4), brake caliper (3-9-4) is cyclic annular, is divided into pintongs, and friction plate (3-9-6) is fixed on braking clamp The inside of disk (3-9-4);Radiator fan (3-9-5) is equipped on the left of brake caliper (3-9-4), radiator fan (3-9-5) is braking Chuck (3-9-4) cools down;Brake caliper (3-9-4) periphery is equipped with braking hauling rope (3-9-3), brakes hauling rope (3-9-3) ring Around brake caliper (3-9-4) surrounding, and the two is hinged;The other end and haulage gear (3-9-2) for braking hauling rope (3-9-3) connect It connects;It is equipped with brake cooling system (3-9-1) on the top brake caliper (3-9-4), the two is connected by conduit;Haulage gear (3-9-2) is tightened brake caliper (3-9-4) by braking hauling rope (3-9-3), promotes friction plate (3-9- 6) generation friction brake force is closely encircled to speed regulating motor transmission shaft (3-10), the heat that friction generates passes through radiator fan (3-9-5), brake cooling system (3-9-1) take away heat.
- Counting device 7. a kind of mobile river and lake according to claim 6 is desilted and dredged in sludge sample processing device, It is characterized in that, the sample clamp (4) includes:Electric rotating machine (4-1), service chamber (4-2), sample handgrip (4-3), gear wheel (4-4), central gear (4-5), handgrip gear (4-6), lap count (4-7);Wherein, the gear wheel (4-4) is arranged in Service chamber (4-2) is internal, and gear wheel (4-4) is interior tooth type hollow structure, and interior teeth are located at gear wheel (4-4) internal circumference On, central gear (4-5) and handgrip gear (4-6), central gear (4-5), handgrip gear (4-6) are equipped in gear wheel (4-4) For outer toothing;The central gear (4-5) is located at the central axes gear wheel (4-4), is surrounded by and grabs in central gear (4-5) Hand gear (4-6), gear wheel (4-4), central gear (4-5), handgrip gear (4-6) three engage connection;The handgrip gear (4-6) quantity is three, circumferentially symmetrical around central gear (4-5);The electric rotating machine (4-1) is fixedly mounted on inspection The side case (4-2) is repaiied, electric rotating machine (4-1) is drivingly connected with central gear (4-5);The sample handgrip (4-3) is arranged in inspection The other side case (4-2) is repaiied, sample handgrip one end (4-3) is fixedly connected with handgrip gear (4-6);The lap count (4-7) It is fixedly connected on electric rotating machine (4-1) turntable;The electric rotating machine (4-1), lap count (4-7) are connected by conducting wire and control system (6) control respectively;Electric rotating machine (4-1) drives central gear (4-5) to rotate, and then drives three, periphery handgrip gear (4-6) along canine tooth Wheel (4-4) interior tooth does revolution motion, while three handgrip gears (4-6) also do rotation movement, and handgrip gear (4-6) passes through sample Handgrip (4-3) drives sample revolution and rotation.
- Counting device 8. a kind of mobile river and lake according to claim 7 is desilted and dredged in sludge sample processing device, It is characterized in that, the sample handgrip (4-3) includes:Arm (4-3-1), sample cell (4-3-2), banjo traction splint (4-3-3), Sample clamping degree inductor (4-3-4);Wherein, the sample cell (4-3-2) is arranged in the top arm (4-3-1), sample cell (4- 3-2) it is circular groove, diameter is 8cm~12cm;Banjo traction splint (4-3-3) quantity is three, and circumference is equidistant It is distributed in around sample cell (4-3-2), the end banjo traction splint (4-3-3) is equipped with antiskid protection pad and the induction of sample clamping degree Device (4-3-4);Banjo traction splint (4-3-3) driving motor, sample clamping degree inductor (4-3-4) pass through conducting wire and control system respectively (6) control connection;Timer is provided in the control system (6), the timer connects with speed regulating motor (3-4) actuating coil polygon control survey It connects.
- Counting device 9. a kind of mobile river and lake according to claim 8 is desilted and dredged in sludge sample processing device, It is characterized in that, the rotary shaft (4-7-7) is molded by high molecular material pressing mold, the constituent of rotary shaft (4-7-7) is as follows:339.2~564.8 parts of lake water of meter purification in parts by weight, N- methyl-1s, 1,2,2,3,3,4,4,5,5,5- ten one fluoro- 131.5~173.6 parts of 1- pentanes sulfonamide, 134.2~243.1 parts of 1- (methoxy) -4- methylbenzenes, 4- (methyl mercapto) fourth 130.4~147.4 parts of aldehyde, 133.1~190.3 parts of rutile, bis- [2- (2- the acrylic)] phenol of 4,4'- (1- methyl ethylidene) With 136.9~197.5 parts of the polymer of (chloromethyl) ethylene oxide, 138.7~193.3 parts of silver nano-particle, polymerization oxidation 1,1,2,3,3,3,131.1~173.6 parts of-hexafluoro -1- propylene, the polymer of formaldehyde and dicyanodiamide and ethylenediamine sulfate 133.6~173.5 parts, 133.9~156.6 parts of alkali formula aphthenic acids zinc salt, methyl ethyl ketoxime sealing end [2,4,6- tri- oxygen triazine -1, 3,5 (2H, 4H, 6H)-three base] three 122.5~158.8 parts of (cyclohexyl) isocyanates, 121.2~164.8 parts of 7- methyl octanals, 130.8~175.4 parts of (2E)-formic acid -2- hexen-1-ols ester, 140.3~184.3 parts of the polymer of polyurethane, mass concentration are 163.4~217.8 parts of the rosolic acid cetyl ester of 130mg/L~397mg/L.
- Counting device 10. a kind of mobile river and lake according to claim 9 is desilted and dredged in sludge sample processing device, It is characterized in that, the manufacturing process of rotary shaft (4-7-7), comprises the steps of:1st step:In tower reactor is found in stirring, it is added and purifies lake water and N- methyl-1s, 1,2,2,3,3,4,4,5,5,5- ten One fluoro -1- pentane sulfonamide starts the blender in the vertical tower reactor of stirring, and setting speed is 132rpm~178rpm, Start the steam oil heater in the vertical tower reactor of stirring, so that temperature is risen to 147.2 DEG C~148.8 DEG C, 1- (methoxies are added Ylmethyl) -4- methylbenzenes stir evenly, and carry out reaction 124.5~135.6 minutes, and 4- (methyl mercapto) butyraldehyde is added, is passed through flow For 123.5m3/ min~164.4m3The helium of/min 124.5~135.6 minutes;It is added in tower reactor is found in stirring later Rutile, the steam oil heater being again started up in the vertical tower reactor of stirring, makes temperature rise to 164.2 DEG C~197.1 DEG C, 4,4'- (1- methyl ethylidene) bis- [2- (2- acrylic)] phenol and (chloromethyl) ring is added in heat preservation 124.4~135.4 minutes The polymer of oxidative ethane, the pH value that solution in tower reactor is found in adjustment stirring are 4.1~8.3, keep the temperature 124.1~364.1 points Clock;2nd step:Separately take silver nano-particle, by silver nano-particle power be 6.64KW~12.08KW under ultrasonication 0.130 After~1.197 hours;Silver nano-particle is added to another stirring to stand in tower reactor, addition mass concentration is 134mg/ The 1 of the polymerization oxidation of L~364mg/L, 1,2,3,3,3,-hexafluoro -1- propylene disperses silver nano-particle, and it is vertical tower anti-to start stirring The steam oil heater in device is answered, makes solution temperature between 45 DEG C~89 DEG C, starts stirring and stands stirring in tower reactor Machine is mixed, and with 4 × 102Rpm~8 × 102The speed of rpm stirs, and adjusts pH value between 4.5~8.8, and insulated and stirred 130~ 197 minutes;Stop reaction later and stand 6.64 × 10~12.08 × 10 minutes, removes impurity;Formaldehyde and two is added in suspension The polymer of cyano diamides and ethylenediamine sulfate, adjustment pH value form sediment and are washed with purification lake water between 1.5~2.8 It is de-, by centrifuge in rotating speed 4.192 × 103Rpm~9.643 × 103Solid content is obtained under rpm, 2.407 × 102DEG C~ 3.642×102It is dry at a temperature of DEG C, 0.192 × 10 is crossed after grinding3~1.643 × 103Mesh sieves, spare;3rd step:Another silver nano-particle after taking alkali formula aphthenic acids zinc salt and the processing of the 2nd step, uses the small angle of glancing incidence after mixing Gamma-rays diffusing reflection irradiation is spent, the energy of glancing incidence low-angle gamma-rays diffusing reflection irradiation is 121.2MeV~149.8MeV, agent Amount is 169.2kGy~209.8kGy, irradiation time is 133.2~158.8 minutes, obtains the alkali formula zinc naphthenate of character change Salt and silver nano-particle mixture;Alkali formula aphthenic acids zinc salt and silver nano-particle mixture are placed in another stirring and stand tower reaction In device, start the steam oil heater in the vertical tower reactor of stirring, 132.8 DEG C~178.4 DEG C of set temperature starts stirring Blender in vertical tower reactor, rotating speed are 124rpm~519rpm, and pH is adjusted between 4.3~8.3, dehydration 133.3~ 147.3 minute, spare;4th step:The alkali formula aphthenic acids zinc salt and silver nano-particle mixture that the character that 3rd step is obtained changes, it is dense to add to quality [- three base of tri- oxygen triazines -1,3,5 (2H, 4H, 6H) of 2,4,6-] three that the methyl ethyl ketoxime that degree is 134mg/L~364mg/L blocks In (cyclohexyl) isocyanates, cocurrent add to the 1st step stirring stand tower reactor in, flow acceleration be 269mL/min~ 997mL/min;Start stirring and found tower reactor blender, setting speed is 138rpm~178rpm;Stirring 4~8 minutes;Again 7- methyl octanals are added, starts the steam oil heater in the vertical tower reactor of stirring, is warming up to 168.4 DEG C~205.8 DEG C, PH is adjusted between 4.4~8.8, and it is 123.118m to be passed through helium ventilatory capacity3/ min~164.273m3/ min, heat preservation are stood 158.2~188.8 minutes;It is again started up stirring and founds tower reactor blender, rotating speed is 133rpm~178rpm, is added (2E)-formic acid -2- hexen-1-ol esters, and pH is adjusted between 4.4~8.8, heat preservation stands 157.5~197.6 minutes;5th step:Start the blender in the vertical tower reactor of stirring, setting speed is 130rpm~197rpm, and it is vertical to start stirring Steam oil heater in tower reactor sets stirring and founds temperature in tower reactor as 1.287 × 102DEG C~2.32 ×102DEG C, the polymer of polyurethane is added, reacts 124.2~135.1 minutes;Rosolic acid cetyl ester is added later, starts The steam oil heater in tower reactor is found in stirring, set temperature in the vertical tower reactor of stirring as 208.4 DEG C~ 264.4 DEG C, pH is adjusted between 4.1~8.1, and pressure is 1.3MPa~1.31MPa, and the reaction time is 0.4~0.9 hour;It After be depressurized to normal pressure, be cooled to 124.2 DEG C~135.1 DEG C and discharge into molding press to get to rotary shaft (4-7-7);The grain size of the silver nano-particle is 138 μm~148 μm;A kind of movable type river and lake is desilted and dredged the working method of the counting device in sludge sample processing device, this method include with Under several steps:1st step:Object to be cut is encased in the sample cell (4-3-2) on sample handgrip (4-3) by treatment process, control system (6) control banjo traction splint (4-3-3) of uniting works, and process object is clamped;Sample clamping degree inductor (4-3-4) monitors in real time Clamping degree is dealt with objects, when sample clamping degree inductor (4-3-4) detects that process object clamping degree reaches default value M When, feedback signal is sent to control system (6) by sample clamping degree inductor (4-3-4), and control system (6) controls finger traction Folder (4-3-3) is stopped;2nd step:At the same time, control system (6) starts the slide motor (3-8) of the end sliding block (3-3), in slide motor (3- 8) under driving, sliding block (3-3) does sliding motion along slideway (3-2), pushes disk (3-7) to being fixed on sample handgrip to drive The sample of the end (4-3) is close;When pushing disk (3-7) apart from sample 3cm~5cm, control system (6) stops slide motor (3-8) works, while controlling hydraulic cylinder (3-6) work;Under hydraulic cylinder (3-6) driving, disk (3-7) is pushed slowly to be leaned on to sample Closely, until disk (3-7) front end blade is pushed to be in contact with process object end face;3rd step:Control system (6) while starting the rotation in speed regulating motor (3-4) and sample clamp (4) in pushing mechanism (3) Rotating motor (4-1);Under speed regulating motor (3-4) driving, disk (3-7) is pushed to do circular motion clockwise;At electric rotating machine (4-1) Under motor driving, sample handgrip (4-3) does counterclockwise circular motion by handgrip gear (4-6);4th step:In electric rotating machine (4-1) rotary course, lap count (4-7) monitors electric rotating machine (4-1) rotation in real time The number of turns;When lap count (4-7) detects that electric rotating machine (4-1) rotating cycle reaches default value R, lap count Feedback signal is sent to control system (6) by (4-7), and control system (6) control electric rotating machine (4-1) is stopped;5th step:In speed regulating motor (3-4) course of work, it is located at the timer in control system (6) to speed regulating motor (3-4) Working time carries out timing;When timer, which adds up timing time, reaches default value T, control system (6) stops speed governing electricity Machine (3-4);6th step:Control system (6) controls banjo traction splint (4-3-3) and unclamps, and the sample handled well enters subsequent processing.
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