CN108752096A - A kind of wheat water-soluble fertilizer containing amino acid and preparation method thereof - Google Patents
A kind of wheat water-soluble fertilizer containing amino acid and preparation method thereof Download PDFInfo
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- CN108752096A CN108752096A CN201810599341.3A CN201810599341A CN108752096A CN 108752096 A CN108752096 A CN 108752096A CN 201810599341 A CN201810599341 A CN 201810599341A CN 108752096 A CN108752096 A CN 108752096A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
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- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
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Abstract
The invention discloses a kind of wheat water-soluble fertilizers containing amino acid and preparation method thereof, include the raw material of following parts by weight：3.6-4.8 parts of 6-8.8 parts of oyster shell whiting, 16.5-22.4 parts of kelp residue, 4.5-7.6 parts of fructus hippophae, 20-26 parts of residue of monosodium glutamate, 6.6-8.4 parts of triethanolamine, 12-18.5 parts of phoenix tree leaf, 18-24.7 parts of vegetable protein, 5-7.5 parts of duckweed and Rhizoma Atractylodis Macrocephalae.Raw material sources of the present invention are extensive, by the way that fructus hippophae is decocted to obtain fructus hippophae decoction liquor, Rhizoma Atractylodis Macrocephalae is subjected to overcritical titanium dioxide, Rhizoma Atractylodis Macrocephalae extract liquor is obtained by extraction, remaining dhdps enzyme solution is obtained into enzymolysis product, again by different product mixing granulations, the finished product of preparation can reduce insect pest rate, disease rate and the lodging rate of wheat, improve the yield of wheat.
Description
Technical field
The present invention relates to wheat planting field, specifically a kind of wheat water-soluble fertilizer containing amino acid.
Background technology
Wheat is the general designation of wheat system plant, is monocotyledon, is a kind of grass family planted extensively all over the world
The caryopsis of plant, wheat is one of staple food of the mankind, and the foods such as bread, steamed bun, biscuit, noodles can be made after wearing into flour；Hair
It can be made into beer, alcohol, white wine (such as vodka), or raw matter fuel after ferment.Wheat is rich in starch, protein, fat, mineral
Matter, calcium, iron, thiamine, riboflavin, niacin, vitamin A and vitamin C etc..Wheat is one of three big cereal, is almost eaten entirely
With China is one of the country that wheat is planted in the world earliest.
Different degrees of a variety of physiological disturbances can occur in growth course for wheat, cause under wheat yield and quality
Drop, people can reduce the physiological disturbance of wheat using a variety of fertilizer.Amino acid water soluble fertilizer is that one kind containing amino acid
The new-type fertilizer of substance and a kind of multifunctional fertilizers, can reduce physiological disturbance, but currently without for wheat
Amino acid water soluble fertilizer.
Invention content
The purpose of the present invention is to provide a kind of wheat water-soluble fertilizers containing amino acid, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides the following technical solutions：
A kind of wheat water-soluble fertilizer containing amino acid, includes the raw material of following parts by weight：6-8.8 parts of oyster shell whiting, kelp residue
16.5-22.4 parts, 4.5-7.6 parts of fructus hippophae, 20-26 parts of residue of monosodium glutamate, 6.6-8.4 parts of triethanolamine, 12-18.5 parts of phoenix tree leaf,
3.6-4.8 parts of 18-24.7 parts of vegetable protein, 5-7.5 parts of duckweed and Rhizoma Atractylodis Macrocephalae.
As a further solution of the present invention：Oyster shell whiting is to be crushed after shell is calcined 10-13 hours at 460-580 degrees Celsius
It is obtained to 80-100 mesh.
As a further solution of the present invention：Vegetable protein include in soybean protein, zein and rice protein extremely
Few one kind.
As a further solution of the present invention：The length of kelp residue is 2.4-6.8mm, and the length of residue of monosodium glutamate is 0.6-
2.5mm。
The preparation method of wheat water-soluble fertilizer containing amino acid, is as follows：
Step 1, is broken to 50-80 mesh by seabuckthorn fruit powder and is added in the deionized water of 4-6 times of its weight and decoct 2-4 times,
Decoction liquor is filtered and merged, sea-buckthorn pomace and fructus hippophae decoction liquor are obtained；
Rhizoma Atractylodis Macrocephalae is freeze-dried 125-170 minutes at subzero 12 to subzero 4 degrees Celsius and is crushed to 60-80 by step 2
Rhizoma Atractylodis Macrocephalae powder is used supercritical carbon dioxide extracting, obtains Rhizoma Atractylodis Macrocephalae extract liquor by mesh；
Step 3 mixes sea-buckthorn pomace, kelp residue, residue of monosodium glutamate, triethanolamine, phoenix tree leaf, vegetable protein and duckweed simultaneously
And it is crushed to 150-200 mesh, then mix and be fitted into fermentation tank with the water of 19-28 times of its weight, adjust the pH value of fermentation tank
And protease is added, fermentation tank is kept for 15-22 days under 30-40 degrees Celsius, obtains enzymolysis product；
Oyster shell whiting is added in fructus hippophae decoction liquor and ultrasonic disperse is uniform, obtains the first mixture by step 4；
Rhizoma Atractylodis Macrocephalae extract liquor, enzymolysis product and the first mixture are mixed evenly step 5, are pressed into granular straight
Diameter is the fertilizer of 0.65-1.36mm and is dried to the mass fraction of water not higher than 3% to get to finished product.
As a further solution of the present invention：The power of ultrasonic disperse is 90-120W.
As a further solution of the present invention：The decoction temperature of fructus hippophae is 76-85 degrees Celsius in step 1, fructus hippophae
Decocting time is 80-105 minutes, and mixing velocity is 360-450rpm in step 5.
Compared with prior art, the beneficial effects of the invention are as follows：Raw material sources of the present invention are extensive, by carrying out fructus hippophae
Decoction obtains fructus hippophae decoction liquor, and Rhizoma Atractylodis Macrocephalae, which is carried out overcritical titanium dioxide, is obtained by extraction Rhizoma Atractylodis Macrocephalae extract liquor, by remaining dhdps enzyme
Solution obtains enzymolysis product, then by different product mixing granulations, the finished product of preparation can reduce the insect pest rate of wheat, disease rate and
Lodging rate improves the yield of wheat.
Specific implementation mode
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of wheat water-soluble fertilizer containing amino acid, includes the raw material of following parts by weight：6 parts of oyster shell whiting, kelp residue 16.5
Part, 4.5 parts of fructus hippophae, 20 parts of residue of monosodium glutamate, 6.6 parts of triethanolamine, 12 parts of phoenix tree leaf, 18 parts of vegetable protein, 5 parts of duckweed and Rhizoma Atractylodis Macrocephalae
3.6 part.Vegetable protein uses zein.
The preparation method of wheat water-soluble fertilizer containing amino acid, is as follows：
Step 1, is broken to 60 mesh by seabuckthorn fruit powder and is added in the deionized water of 5 times of its weight and decoct 3 times, and filtering is simultaneously
And merge decoction liquor, obtain sea-buckthorn pomace and fructus hippophae decoction liquor；
Rhizoma Atractylodis Macrocephalae is freeze-dried 150 minutes at subzero 8 degrees Celsius and is crushed to 70 mesh, Rhizoma Atractylodis Macrocephalae powder is used by step 2
Supercritical carbon dioxide extracting obtains Rhizoma Atractylodis Macrocephalae extract liquor；
Step 3 mixes sea-buckthorn pomace, kelp residue, residue of monosodium glutamate, triethanolamine, phoenix tree leaf, vegetable protein and duckweed simultaneously
And 160 mesh are crushed to, then mix and be fitted into fermentation tank with the water of 23 times of its weight, adjust the pH value of fermentation tank and addition
Protease, fermentation tank are kept for 19 days under 36 degrees Celsius, obtain enzymolysis product；
Oyster shell whiting is added in fructus hippophae decoction liquor and ultrasonic disperse is uniform by step 4, and the power of ultrasonic disperse is
105W obtains the first mixture；
Rhizoma Atractylodis Macrocephalae extract liquor, enzymolysis product and the first mixture are mixed evenly step 5, are pressed into granular straight
Diameter is the fertilizer of 0.65-1.08mm and is dried to the mass fraction of water not higher than 3% to get to finished product.
Embodiment 2
A kind of wheat water-soluble fertilizer containing amino acid, includes the raw material of following parts by weight：6.7 parts of oyster shell whiting, kelp residue
19.4 parts, it is 5.5 parts of fructus hippophae, 23.7 parts of residue of monosodium glutamate, 7.5 parts of triethanolamine, 14.6 parts of phoenix tree leaf, 20.6 parts of vegetable protein, floating
3.9 parts of 5.8 parts of duckweed and Rhizoma Atractylodis Macrocephalae.Oyster shell whiting is to be crushed to 90 mesh after shell is calcined 12 hours at 520 degrees Celsius to obtain.Kelp residue
Length is 4.3mm, and the length of residue of monosodium glutamate is 1.25mm.
The preparation method of wheat water-soluble fertilizer containing amino acid, is as follows：
Step 1, is broken to 60 mesh by seabuckthorn fruit powder and is added in the deionized water of 4 times of its weight and decoct 4 times, fructus hippophae
Decoction temperature be 79 degrees Celsius, the decocting time of fructus hippophae is 95 minutes, filters and merges decoction liquor, obtain sea-buckthorn pomace
With fructus hippophae decoction liquor；
Rhizoma Atractylodis Macrocephalae is freeze-dried 150 minutes at subzero 6 degrees Celsius and is crushed to 60 mesh, Rhizoma Atractylodis Macrocephalae powder is used by step 2
Supercritical carbon dioxide extracting obtains Rhizoma Atractylodis Macrocephalae extract liquor；
Step 3 mixes sea-buckthorn pomace, kelp residue, residue of monosodium glutamate, triethanolamine, phoenix tree leaf, vegetable protein and duckweed simultaneously
And 180 mesh are crushed to, then mix and be fitted into fermentation tank with the water of 25 times of its weight, adjust the pH value of fermentation tank and addition
Protease, fermentation tank are kept for 20 days under 33 degrees Celsius, obtain enzymolysis product；
Oyster shell whiting is added in fructus hippophae decoction liquor and ultrasonic disperse is uniform, obtains the first mixture by step 4；
Rhizoma Atractylodis Macrocephalae extract liquor, enzymolysis product and the first mixture are mixed evenly step 5 with the speed of 390rpm, pressure
The fertilizer of granular a diameter of 0.84mm is made and is dried to the mass fraction of water not higher than 3% to get to finished product.
Embodiment 3
A kind of wheat water-soluble fertilizer containing amino acid, includes the raw material of following parts by weight：8.4 parts of oyster shell whiting, kelp residue
21.5 parts, it is 6.8 parts of fructus hippophae, 24.3 parts of residue of monosodium glutamate, 8.1 parts of triethanolamine, 17.6 parts of phoenix tree leaf, 24.3 parts of vegetable protein, floating
4.5 parts of 7.2 parts of duckweed and Rhizoma Atractylodis Macrocephalae.Oyster shell whiting is to be crushed to 90 mesh after shell is calcined 10 hours at 480 degrees Celsius to obtain.Vegetable protein
Mixture including soybean protein and rice protein.
The preparation method of wheat water-soluble fertilizer containing amino acid, is as follows：
Step 1, is broken to 70 mesh by seabuckthorn fruit powder and is added in the deionized water of 6 times of its weight and decoct 3 times, and filtering is simultaneously
And merge decoction liquor, obtain sea-buckthorn pomace and fructus hippophae decoction liquor；
Rhizoma Atractylodis Macrocephalae is freeze-dried 160 minutes at subzero 10 degrees Celsius and is crushed to 60 mesh, Rhizoma Atractylodis Macrocephalae powder is used by step 2
Supercritical carbon dioxide extracting obtains Rhizoma Atractylodis Macrocephalae extract liquor；
Step 3 mixes sea-buckthorn pomace, kelp residue, residue of monosodium glutamate, triethanolamine, phoenix tree leaf, vegetable protein and duckweed simultaneously
And 190 mesh are crushed to, then mix and be fitted into fermentation tank with the water of 25 times of its weight, adjust the pH value of fermentation tank and addition
Protease, fermentation tank are kept for 21 days under 33 degrees Celsius, obtain enzymolysis product；
Oyster shell whiting is added in fructus hippophae decoction liquor and ultrasonic disperse is uniform by step 4, and the power of ultrasonic disperse is
105W obtains the first mixture；
Rhizoma Atractylodis Macrocephalae extract liquor, enzymolysis product and the first mixture are mixed evenly step 5, are pressed into granular straight
Diameter is the fertilizer of 0.65-1.36mm and is dried to the mass fraction of water not higher than 3% to get to finished product.
Embodiment 4
A kind of wheat water-soluble fertilizer containing amino acid, includes the raw material of following parts by weight：8.8 parts of oyster shell whiting, kelp residue
22.4 parts, 7.6 parts of fructus hippophae, 26 parts of residue of monosodium glutamate, 8.4 parts of triethanolamine, 18.5 parts of phoenix tree leaf, 24.7 parts of vegetable protein, duckweed
7.5 parts and 4.8 parts of Rhizoma Atractylodis Macrocephalae.Oyster shell whiting is to be crushed to 100 mesh after shell is calcined 13 hours at 580 degrees Celsius to obtain.Vegetable protein
Include the mixture of soybean protein, zein and rice protein.The length of kelp residue is 5.6mm, and the length of residue of monosodium glutamate is
1.7mm。
The preparation method of wheat water-soluble fertilizer containing amino acid, is as follows：
Step 1, is broken to 70 mesh by seabuckthorn fruit powder and is added in the deionized water of 6 times of its weight and decoct 4 times, fructus hippophae
Decoction temperature be 84 degrees Celsius, the decocting time of fructus hippophae is 98 minutes, filters and merges decoction liquor, obtain sea-buckthorn pomace
With fructus hippophae decoction liquor；
Rhizoma Atractylodis Macrocephalae is freeze-dried 125 minutes at subzero 12 degrees Celsius and is crushed to 80 mesh, Rhizoma Atractylodis Macrocephalae powder is used by step 2
Supercritical carbon dioxide extracting obtains Rhizoma Atractylodis Macrocephalae extract liquor；
Step 3 mixes sea-buckthorn pomace, kelp residue, residue of monosodium glutamate, triethanolamine, phoenix tree leaf, vegetable protein and duckweed simultaneously
And 200 mesh are crushed to, then mix and be fitted into fermentation tank with the water of 26 times of its weight, adjust the pH value of fermentation tank and addition
Protease, fermentation tank are kept for 21 days under 36 degrees Celsius, obtain enzymolysis product；
Oyster shell whiting is added in fructus hippophae decoction liquor and ultrasonic disperse is uniform by step 4, and the power of ultrasonic disperse is
110W obtains the first mixture；
Rhizoma Atractylodis Macrocephalae extract liquor, enzymolysis product and the first mixture are mixed evenly step 5 with the rotating speed of 420rpm, pressure
The fertilizer of granular a diameter of 0.95mm is made and is dried to the mass fraction of water not higher than 3% to get to finished product.
Comparative example 1
Except without fructus hippophae and duckweed, remaining raw material and preparation method are same as Example 1.
Comparative example 2
Using existing wheat fertilizer as a comparison case 2.
6 groups of wheatland for selecting same condition, 1-6 is respectively used to by the product of the product of embodiment 1-4 and comparative example 1-2
The wheat planting of group, embodiment 1-4 are respectively used to the wheat of 1-4 groups, and comparative example 1-2 is respectively used to the wheat of 5-6 groups, and every group is adopted
Fertilizer amount is identical, observes and records the upgrowth situation of wheat, the results are shown in Table 1.
Table 1
From table 1 it follows that being much higher than using comparative example in per mu yield using the 1-4 groups of embodiment 1-4 products
The 5-6 groups of 1-2 products are below use pair using the 1-4 groups of embodiment 1-4 products on insect pest rate, disease rate and lodging rate
The 5-6 groups of ratio 1-2 products, are also beneficial to the volume increase of wheat.
The present invention obtains fructus hippophae decoction liquor by being decocted fructus hippophae, by Rhizoma Atractylodis Macrocephalae using supercritical carbon dioxide into
Rhizoma Atractylodis Macrocephalae extract liquor is obtained by extraction in row, is digested to obtain enzymolysis product by vegetable protein, duckweed etc., then by enzymolysis product, sea-buckthorn
The finished product of the mixing granulations such as fruit decoction liquor, preparation can reduce insect pest rate, disease rate and the lodging rate of wheat, improve per mu yield
Amount, protease digests vegetable protein can provide sufficient nutrition at various amino acid for wheat, also improve the production of wheat
Amount.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (7)
1. a kind of wheat water-soluble fertilizer containing amino acid, which is characterized in that include the raw material of following parts by weight：Oyster shell whiting 6-8.8
Part, 16.5-22.4 parts of kelp residue, 4.5-7.6 parts of fructus hippophae, 20-26 parts of residue of monosodium glutamate, 6.6-8.4 parts of triethanolamine, phoenix tree leaf
3.6-4.8 parts of 12-18.5 parts, 18-24.7 parts of vegetable protein, 5-7.5 parts of duckweed and Rhizoma Atractylodis Macrocephalae.
2. wheat according to claim 1 water-soluble fertilizer containing amino acid, which is characterized in that the oyster shell whiting is that shell exists
460-580 degrees Celsius of calcining is crushed to 80-100 mesh and obtains after 10-13 hours.
3. wheat according to claim 1 water-soluble fertilizer containing amino acid, which is characterized in that the vegetable protein includes big
At least one of legumin, zein and rice protein.
4. wheat according to claim 1 water-soluble fertilizer containing amino acid, which is characterized in that the length of the kelp residue is
The length of 2.4-6.8mm, residue of monosodium glutamate are 0.6-2.5mm.
5. a kind of preparation method of wheat water-soluble fertilizer containing amino acid as described in claim 1-4 is any, which is characterized in that
It is as follows：
Step 1, is broken to 50-80 mesh by seabuckthorn fruit powder and is added in the deionized water of 4-6 times of its weight and decoct 2-4 times, filters
And merges decoction liquor, obtain sea-buckthorn pomace and fructus hippophae decoction liquor；
Rhizoma Atractylodis Macrocephalae is freeze-dried 125-170 minutes at subzero 12 to subzero 4 degrees Celsius and is crushed to 60-80 mesh by step 2, will
Rhizoma Atractylodis Macrocephalae powder uses supercritical carbon dioxide extracting, obtains Rhizoma Atractylodis Macrocephalae extract liquor；
Step 3, by the mixing of sea-buckthorn pomace, kelp residue, residue of monosodium glutamate, triethanolamine, phoenix tree leaf, vegetable protein and duckweed and powder
Be broken to 150-200 mesh, then mix and be fitted into fermentation tank with the water of 19-28 times of its weight, adjust the pH value of fermentation tank and
Protease is added, fermentation tank is kept for 15-22 days under 30-40 degrees Celsius, obtains enzymolysis product；
Oyster shell whiting is added in fructus hippophae decoction liquor and ultrasonic disperse is uniform, obtains the first mixture by step 4；
Rhizoma Atractylodis Macrocephalae extract liquor, enzymolysis product and the first mixture are mixed evenly step 5, are pressed into granular a diameter of
The fertilizer of 0.65-1.36mm and the mass fraction of water is dried to not higher than 3% to get to finished product.
6. the preparation method of wheat according to claim 5 water-soluble fertilizer containing amino acid, which is characterized in that the ultrasound
The power of dispersion is 90-120W.
7. the preparation method of wheat according to claim 5 or 6 water-soluble fertilizer containing amino acid, which is characterized in that described
The decoction temperature of fructus hippophae is 76-85 degrees Celsius in step 1, and the decocting time of fructus hippophae is 80-105 minutes, is mixed in step 5
Sum velocity is 360-450rpm.
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