CN108744570A - A kind of distillation equipment for Chemical Manufacture of environmental protection - Google Patents
A kind of distillation equipment for Chemical Manufacture of environmental protection Download PDFInfo
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- CN108744570A CN108744570A CN201810636471.XA CN201810636471A CN108744570A CN 108744570 A CN108744570 A CN 108744570A CN 201810636471 A CN201810636471 A CN 201810636471A CN 108744570 A CN108744570 A CN 108744570A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/02—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/42—Regulation; Control
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The present invention provides a kind of distillation equipment for Chemical Manufacture of environmental protection, including installation pedestal, one level of support bar, distillation reactor main body, discharging of waste liquid pipe, two level supporting rod, wasted nickel catalyst exhaust pipe device, multi-functional water supply case apparatus, thermometric condenser tube structure, diversion mixing impeller structure, chamber structure is heated, item is observed, depending on legendary venomous insect, distillate collecting pipe, production liquid delivery pipe, electric control box, top supporting frame, steam outlet pipe, storage tank and finished product return duct.Gas detecting instrument of the present invention, the setting of three-limb tube and gas treatment connecting tube are conducive to be detected exhaust gas according to the difference of Chemical Manufacture product, carry out classification processing for testing result, play the effect of environmental protection；The setting of agitating shaft, diversion rod and paddle is conducive to be stirred the industrial chemicals in reaction, industrial chemicals is allow to be heated evenly, and improves the efficiency of distillation, shortens distillation time.
Description
Technical field
The invention belongs to chemical industry distillation equipment technical fields more particularly to a kind of distillation for Chemical Manufacture of environmental protection to set
It is standby.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, it is different using each component boiling point in mixing liquid or liquid-solid system,
So that low boiling component is evaporated, then condense to detach the unit process of entire component, is two kinds of unit operations of evaporation and condensation
Joint.With other separation means, such as extraction, filtering for crystallizing compare, its advantage is that without the use of system components with
Outer other solvents, to ensure that new impurity will not be introduced.The relationship of the mankind and chemical industry is very close, spreads to the side of life
Aspect face.In the modern life, it almost all be unable to do without chemical products whenever and wherever possible, from material lifes such as food, clothing, housing and transportation to text
Change the cultural lives such as art, amusement, chemical products is required for service for it.
China Patent Publication No. is CN107596717A, and invention and created name is that a kind of distillation for Chemical Manufacture is set
Standby, cavity, pre-add heat pipe go out sap cavity layer, distillation case and feed liquor cavity layer, and the cavity is arranged in device housings inside top, institute
The escape pipe that array distribution is equipped at the top of feed liquor cavity layer is stated, escape pipe upper end is connected to cavity, and feed liquor cavity layer is each side equipped with
One liquid-feeding tube, is provided with inner tube on the pre-add heat pipe, and inner tube outer cover is equipped with outer tube, inner tube and outer tube it
Between be equipped with heater strip, inner tube is internally provided with shaft, it is described go out sap cavity layer bottom be equipped with the aeration head of array distribution, the distillation
Case is internally provided with liquid collecting cavity, and the third connecting tube of array distribution is equipped on the right side of liquid collecting cavity, shunting is connected on the right side of third connecting tube
Distillation cascade, shunting distillation cascade lower end are equipped with heating plate.But the distillation equipment of existing Chemical Manufacture there is also exhaust gas without
Detection direct emission causes not environmentally, and condensation uses water service efficiency is low and stirring is insufficient so that the problem that distillation time is long.
Therefore, a kind of distillation equipment for Chemical Manufacture of environmental protection of invention is very necessary.
Invention content
In order to solve the above technical problem, the present invention provides a kind of distillation equipments for Chemical Manufacture of environmental protection, with solution
The distillation equipment exhaust gas of certainly existing Chemical Manufacture not after testing direct emission cause not environmentally, condensation with water service efficiency it is low and
Stir insufficient problem for so that distillation time is long.A kind of distillation equipment for Chemical Manufacture of environmental protection, including installation base
Seat, one level of support bar, distillation reactor main body, discharging of waste liquid pipe, two level supporting rod, wasted nickel catalyst exhaust pipe device are multi-functional
Water supply case apparatus, thermometric condenser tube structure, diversion mixing impeller structure heat chamber structure, observe item, depending on legendary venomous insect, distillate collecting pipe,
Production liquid delivery pipe, electric control box, top supporting frame, steam outlet pipe, storage tank and finished product return duct, the level-one branch
Strut one end is bolted to the lower surface corner location of distillation reactor main body, the upper surface of the other end and installation pedestal respectively
It is bolted；The discharging of waste liquid pipe screw thread is connected to the lower surface centre position of distillation reactor main body；The two level
Supporting rod one end is bolted to the lower surface corner location of storage tank, the upper surface bolt company of the other end and installation pedestal respectively
It connects；The wasted nickel catalyst exhaust pipe device is mounted on the left upper portion position of distillation reactor main body；The multi-functional confession
Cistern device is mounted on the upper surface centre position of installation pedestal；The thermometric condenser tube structure and multi-functional water supply case apparatus
It is connected；The diversion mixing impeller structure is plugged on the upper inside centre position of distillation reactor main body；The heating
Chamber structure is bolted to the inside of distillation reactor main body；The observation item longitudinally inlays the front surface interposition of storage tank
It sets；The lower end that distillate collecting pipe is threaded in depending on legendary venomous insect；The distillate collecting pipe and thermometric condenser tube structure
It is connected；The production liquid delivery pipe is threaded in the lower right side position of storage tank；The electric control box spiral shell
Nail is connected to the left lower position of distillation reactor main body；The top supporting frame is bolted distillation reactor master respectively
At left and right sides of body upper surface；The steam outlet pipe is threaded in the upper surface right positions of distillation reactor main body；It is described
Finished product return duct threaded one end be connected to the upper surface centre position of storage tank, the other end is threaded in the following table regarding legendary venomous insect
Face；The wasted nickel catalyst exhaust pipe device includes exhaust pipe, gas detecting instrument, three-limb tube, solenoid valve and is manually controlled
Valve, the gas detecting instrument are threaded in the upper surface right positions of exhaust pipe；The three-limb tube is threadedly coupled
In the left position of exhaust pipe；The solenoid valve is embedded in the inside upper left side of three-limb tube；The hand control valve
It is threaded in the lower surface right positions of three-limb tube.
Preferably, the multi-functional water supply case apparatus includes water feeding tank, water circulating pump, interconnecting tube, water inlet pipe, note
Enter pipe, return pipe and external connecting pipe, the water circulating pump is bolted to the inside lower right side of water feeding tank；The inside
Connecting tube longitudinal screw is connected to the upper surface of water circulating pump；The water inlet pipe longitudinally runs through the upper surface right lateral position of water feeding tank
It sets and is threadedly coupled with interconnecting tube；The injection pipe is threaded in the upper surface centre position of water feeding tank；Described returns
Water pipe threaded one end is connected to the upper surface leftward position of water feeding tank, and the other end is threaded in the lower surface of external connecting pipe.
Preferably, the thermometric condenser tube structure includes condenser pipe, cooling cylinder, steam pipeline, sealing ring, two level temperature
Degree meter and condensation return pipt, the condenser pipe are wrapped in the outer surface centre position of steam pipeline；The cooling cylinder cover
It is connected on the outer surface of condenser pipe；The intersection in steam pipeline and cooling cylinder is arranged in the sealing ring；The two level temperature
Degree meter screw is connected to the front surface lower left side of cooling cylinder；The lower surface that the condensation return pipt is threaded in cooling cylinder is left
Side position.
Preferably, the diversion mixing impeller structure includes distillation stirring motor, hanging ring, agitating shaft, level-one casing, water conservancy diversion
Bar, two level casing and paddle, the hanging ring are threaded in the upper surface centre position of distillation stirring motor；Described stirs
Axis shaft coupling is mixed to be connected on the output shaft of distillation stirring motor；The level-one casing is socketed in the outer surface top of agitating shaft
Position；The diversion rod is respectively welded at the left and right sides centre position of level-one casing；The two level casing, which is socketed in, to be stirred
Mix the outer surface lower position of axis；The paddle is respectively welded at the left and right sides centre position of two level casing.
Preferably, the heating chamber structure includes heating cabinet, heater strip, fixed link, level-one thermometer, pressure detection
Meter, reaction kettle filling tube and heating rod, the heating cabinet integrated setting is in the inside of distillation reactor main body；Described adds
Heated filament is welded in the gap that heating cabinet is formed with distillation reactor main body；The fixed link is respectively welded at distillation reactor
Two up and down at left and right sides of body inner surface；The front surface that the level-one thermometer screw is connected to distillation reactor main body is right
Upside；The pressure detection meter screw is connected to the front surface upper left side of distillation reactor main body；The reaction kettle material feeding
Pipe is welded on the upper surface leftward position of distillation reactor main body；The heating rod longitudinal measure is in the outside of fixed link.
Preferably, the condensation return pipt is threadedly coupled setting with external connecting pipe；The water inlet pipe and cooling cylinder
It is threadedly coupled setting.
Preferably, the left end of the steam pipeline is threadedly coupled setting with steam outlet pipe；The steam pipeline
Right end be threadedly coupled setting with distillate collecting pipe.
Preferably, the intersection of the agitating shaft and level-one casing and two level casing is respectively arranged with clamping screw；Institute
The agitating shaft stated longitudinally runs through the upper surface centre position of distillation reactor main body；The agitating shaft and distillation reactor main body
Intersection be provided with gasket；The top supporting frame is bolted to the left and right sides lower part of distillation stirring motor respectively
Position.
Preferably, the heating rod specifically uses stainless steel heating rod；The heater strip is specifically added using stainless steel
Heated filament.
Preferably, the water inlet pipe is connected by condenser pipe with condensation return pipt.
Preferably, the water feeding tank is bolted setting with installation pedestal；The water feeding tank is arranged in one level of support
Between bar and two level supporting rod.
Preferably, the left side centre position of the external connecting pipe is threaded with cleaning pipe；The cleaning pipe
Left end is threaded with nozzle；The nozzle is arranged in the inside upper right side of distillation reactor main body；The cleaning pipe spiral shell
Line is connected to distillation reactor main body right upper portion position；The upper surface right positions of the cleaning pipe are threaded with control
Valve.
Preferably, the distillation reactor main body inside cleaning pipe and return pipe and water feeding tank by being connected to.
Preferably, the exhaust pipe is connected to setting with distillation reactor main body；The exhaust pipe and distillation reactor
Main body screw connects.
Preferably, the lower-left end of the three-limb tube is threaded with gas treatment connecting tube；, described three lead to
The left upper end taken over is threaded with air scoop.
Preferably, the air scoop and gas treatment connecting tube are connected by exhaust pipe and distillation reactor body interior
It is logical.
Preferably, the outer surface top of the injection pipe is threaded with protective cover.
Preferably, the discharging of waste liquid pipe is connected to distillation reactor body interior；A left side for the discharging of waste liquid pipe
Upper lateral part position is threaded with control valve.
Preferably, the leftward position in installation pedestal is arranged in the one level of support bar；The two level supporting rod setting
In the right positions of installation pedestal.
Preferably, the upper surface of the production liquid delivery pipe is provided with control valve；The production liquid delivery pipe
Setting is connected to storage tank.
Preferably, the steam outlet pipe is connected to distillation reactor body interior；The steam outlet pipe passes through steam
Delivery pipe and distillate collecting pipe, which pass through inside legendary venomous insect and finished product return duct and storage tank, to be connected to.
Preferably, the distillation reactor main body specifically uses carbon steel reaction kettle；Described regards legendary venomous insect specifically using stainless
Steel is straight-through to regard legendary venomous insect.
Preferably, the solenoid valve, water circulating pump, heater strip, heating rod and distillation stirring motor are electrically connected
Electric control box.
Preferably, the gas detecting instrument specifically uses the detector of model PT40；The level-one thermometer and
The thermometer of WSS-401 is respectively adopted in two level thermometer；The pressure detection meter specifically uses the pressure gauge of model Y100.
Compared with prior art, beneficial effects of the present invention are：
1. in the present invention, the gas detecting instrument, the setting of three-limb tube and gas treatment connecting tube is conducive to according to change
The difference of work production product is detected exhaust gas, carries out classification processing for testing result, plays the effect of environmental protection.
2. in the present invention, the setting of the cleaning pipe and nozzle is conducive to carry out distillation reactor body interior clear
It washes, increases the use function of water feeding tank.
3. in the present invention, the condenser pipe, the setting of cooling cylinder and condensation return pipt is conducive to will go into steam defeated
The distillation steam of pipe is sent, it is cooling to condense into liquid, improve working efficiency.
4. in the present invention, the setting of the two level thermometer is conducive to detect the temperature in cooling cylinder at any time, ensure cold
Solidifying operation carries out at a suitable temperature, convenient that water circulating pump is adjusted.
5. in the present invention, the agitating shaft, the setting of diversion rod and paddle is conducive to the industrial chemicals in reaction
It is stirred, industrial chemicals is allow to be heated evenly, improve the efficiency of distillation, shorten distillation time.
6. in the present invention, the setting of the level-one casing and two level casing is conducive to the difference according to reaction raw materials, adjust
The quantity of diversion rod and paddle is saved, stirring requirements of one's work are met.
7. in the present invention, the setting of the heater strip and heating rod is conducive to the industrial chemicals of distillation reactor main body
Difference carry out selection heating, meet the needs of distillation procedure.
8. in the present invention, the setting of the level-one thermometer and pressure detection meter is conducive to distillation reactor inside
Temperature and pressure be detected, ensure distillation procedure carried out in safely controllable range.
9. in the present invention, the observation item and the setting regarding legendary venomous insect are conducive to the amount of storage to distillate finished product and distillation
It is observed at liquid situation, the convenient control to distillation procedure.
10. in the present invention, the setting of the hanging ring is conducive to the installation and removal for facilitating distillation stirring motor.
Description of the drawings
Fig. 1 is the structural schematic diagram of the present invention.
Fig. 2 is the structural schematic diagram of the wasted nickel catalyst exhaust pipe device of the present invention.
Fig. 3 is the structural schematic diagram of the multi-functional water supply case apparatus of the present invention.
Fig. 4 is the structural schematic diagram of the thermometric condenser tube structure of the present invention.
Fig. 5 is the structural schematic diagram of the diversion mixing impeller structure of the present invention.
Fig. 6 is the structural schematic diagram of the heating chamber structure of the present invention.
In figure：
1, installation pedestal；2, one level of support bar；3, distillation reactor main body；4, discharging of waste liquid pipe；5, two level supporting rod；6, exhaust gas
Detect exhaust pipe device；61, exhaust pipe；62, gas detecting instrument；63, three-limb tube；631, gas treatment connecting tube；632,
Air scoop；64, solenoid valve；65, hand control valve；7, multi-functional water supply case apparatus；71, water feeding tank；72, water circulating pump；73, interior
Portion's connecting tube；74, water inlet pipe；75, injection pipe；76, return pipe；77, external connecting pipe；771, cleaning pipe；772, nozzle；8, it surveys
Warm condenser tube structure；81, condenser pipe；82, cooling cylinder；83, steam pipeline；84, sealing ring；85, two level thermometer；86, cold
Solidifying return pipe；9, diversion mixing impeller structure；91, stirring motor is distilled；92, hanging ring；93, agitating shaft；94, level-one casing；95, it leads
Flow post；96, two level casing；97, paddle；10, chamber structure is heated；101, heating cabinet；102, heater strip；103, fixed link；
104, level-one thermometer；105, pressure detection meter；106, reaction kettle filling tube；107, heating rod；11, item is observed；12, legendary venomous insect is regarded；
13, distillate collecting pipe；14, production liquid delivery pipe；15, electric control box；16, top supporting frame；17, steam outlet pipe；18,
Storage tank；19, finished product return duct.
Specific implementation mode
The present invention is described further below in conjunction with attached drawing：
Embodiment：
As shown in attached drawing 1 to attached drawing 6
The present invention provides a kind of distillation equipment for Chemical Manufacture of environmental protection, including installation pedestal 1, one level of support bar 2, distillation
Reactor main body 3, discharging of waste liquid pipe 4, two level supporting rod 5, wasted nickel catalyst exhaust pipe device 6, multi-functional water supply case apparatus 7 are surveyed
Warm condenser tube structure 8, diversion mixing impeller structure 9 heat chamber structure 10, observe item 11, depending on legendary venomous insect 12, distillate collecting pipe 13, at
Product liquid discharge pipe 14, electric control box 15, top supporting frame 16, steam outlet pipe 17, storage tank 18 and finished product return duct 19, institute
2 one end of one level of support bar stated is bolted to the lower surface corner location of distillation reactor main body 3, the other end and installation respectively
The upper surface of pedestal 1 is bolted；The discharging of waste liquid pipe 4 is threaded among the lower surface of distillation reactor main body 3
Position；Described 5 one end of two level supporting rod is bolted to the lower surface corner location of storage tank 18, the other end and installation respectively
The upper surface of pedestal 1 is bolted；The wasted nickel catalyst exhaust pipe device 6 is mounted on the left side of distillation reactor main body 3
Portion position；The multi-functional water supply case apparatus 7 is mounted on the upper surface centre position of installation pedestal 1；The thermometric condensation
Pipe structure 8 is connected with multi-functional water supply case apparatus 7；The diversion mixing impeller structure 9 is plugged on distillation reactor main body 3
Upper inside centre position；The heating chamber structure 10 is bolted to the inside of distillation reactor main body 3；The observation
The longitudinal front surface centre position for inlaying storage tank 18 of item 11；Described is threaded in depending on legendary venomous insect 12 under distillate collecting pipe 13
End；The distillate collecting pipe 13 is connected with thermometric condenser tube structure 8；The production liquid delivery pipe 14 is threadedly coupled
In the lower right side position of storage tank 18；15 screw of electric control box is connected under the left side of distillation reactor main body 3
Portion position；The top supporting frame 16 is bolted respectively at left and right sides of 3 upper surface of distillation reactor main body；The steam
Outlet pipe 17 is threaded in the upper surface right positions of distillation reactor main body 3；19 threaded one end of finished product return duct connects
It is connected on the upper surface centre position of storage tank 18, the other end is threaded in regarding the lower surface of legendary venomous insect 12；The wasted nickel catalyst row
Tracheae device 6 includes exhaust pipe 61, gas detecting instrument 62, three-limb tube 63, solenoid valve 64 and hand control valve 65, described
Gas detecting instrument 62 is threaded in the upper surface right positions of exhaust pipe 61；63 row of being threaded in of three-limb tube
The left position of tracheae 61；The solenoid valve 64 is embedded in the inside upper left side of three-limb tube 63；Described manually controls
Valve 65 is threaded in the lower surface right positions of three-limb tube 63.
In above-described embodiment, specifically, the multi-functional water supply case apparatus 7 includes water feeding tank 71, water circulating pump 72 is interior
Portion's connecting tube 73, water inlet pipe 74, injection pipe 75, return pipe 76 and external connecting pipe 77, the water circulating pump 72 are bolted
In the inside lower right side of water feeding tank 71；73 longitudinal screw of interconnecting tube is connected to the upper surface of water circulating pump 72；Institute
The longitudinal upper surface right positions through water feeding tank 71 of water inlet pipe 74 stated are threadedly coupled with interconnecting tube 73；The injection
Pipe 75 is threaded in the upper surface centre position of water feeding tank 71；76 threaded one end of return pipe is connected to water feeding tank 71
Upper surface leftward position, the other end are threaded in the lower surface of external connecting pipe 77.
In above-described embodiment, specifically, the thermometric condenser tube structure 8 includes condenser pipe 81, cooling cylinder 82, steam is defeated
Pipe 83, sealing ring 84, two level thermometer 85 and condensation return pipt 86, the condenser pipe 81 is sent to be wrapped in steam pipeline 83
Outer surface centre position；The cooling cylinder 82 covers the outer surface for being connected on condenser pipe 81；The sealing ring 84 is arranged in steam
The intersection of delivery pipe 83 and cooling cylinder 82；85 screw of two level thermometer is connected to the front surface lower-left of cooling cylinder 82
Side；The condensation return pipt 86 is threaded in the lower surface leftward position of cooling cylinder 82.
In above-described embodiment, specifically, the diversion mixing impeller structure 9 includes distillation stirring motor 91, hanging ring 92 stirs
Axis 93, level-one casing 94, diversion rod 95, two level casing 96 and paddle 97 are mixed, the hanging ring 92 is threaded in distillation and stirs
Mix the upper surface centre position of motor 91；93 shaft coupling of agitating shaft is connected on the output shaft of distillation stirring motor 91；
The level-one casing 94 is socketed in the outer surface upper position of agitating shaft 93；The diversion rod 95 is respectively welded at level-one set
The left and right sides centre position of pipe 94；The two level casing 96 is socketed in the outer surface lower position of agitating shaft 93；Described
Paddle 97 is respectively welded at the left and right sides centre position of two level casing 96.
In above-described embodiment, specifically, the heating chamber structure 10 includes heating cabinet 101, heater strip 102, fixed link
103, level-one thermometer 104, pressure detection meter 105, reaction kettle filling tube 106 and heating rod 107, the heating cabinet 101 1
Body is arranged in the inside of distillation reactor main body 3；The heater strip 102 is welded on heating cabinet 101 and distillation reactor master
In the gap that body 3 is formed；The fixed link 103 is respectively welded at 3 inner surface of the distillation reactor main body left and right sides or more two
Portion；104 screw of level-one thermometer is connected to the front surface upper right side of distillation reactor main body 3；The pressure detection
Count the front surface upper left side that 105 screws are connected to distillation reactor main body 3；The reaction kettle filling tube 106 is welded on distillation
The upper surface leftward position of reactor main body 3；107 longitudinal measure of heating rod is in the outside of fixed link 103.
In above-described embodiment, specifically, the condensation return pipt 86 is threadedly coupled setting with external connecting pipe 77；It is described
Water inlet pipe 74 be threadedly coupled setting with cooling cylinder 82.
In above-described embodiment, specifically, the left end of the steam pipeline 83 is threadedly coupled setting with steam outlet pipe 17；
The right end of the steam pipeline 83 is threadedly coupled setting with distillate collecting pipe 13.
In above-described embodiment, specifically, the intersection of the agitating shaft 93 and level-one casing 94 and two level casing 96 is punished
Clamping screw is not provided with it；The longitudinal upper surface centre position for running through distillation reactor main body 3 of the agitating shaft 93；Described
Agitating shaft 93 and the intersection of distillation reactor main body 3 are provided with gasket；The top supporting frame 16 is bolted respectively
In the left and right sides lower position of distillation stirring motor 91.
In above-described embodiment, specifically, the heating rod 107 specifically uses stainless steel heating rod；The heater strip
102 specifically use stainless steel heater strip.
In above-described embodiment, specifically, the water inlet pipe 74 is connected by condenser pipe 81 with condensation return pipt 86.
In above-described embodiment, specifically, the water feeding tank 71 is bolted setting with installation pedestal 1；The water supply
Case 71 is arranged between one level of support bar 2 and two level supporting rod 5.
In above-described embodiment, specifically, the left side centre position of the external connecting pipe 77 is threaded with cleaning pipe
771；The left end of the cleaning pipe 771 is threaded with nozzle 772；The nozzle 772 is arranged in distillation reactor main body 3
Inside upper right side；The cleaning pipe 771 is threaded in 3 right upper portion position of distillation reactor main body；The cleaning
The upper surface right positions of pipe 771 are threaded with control valve.
In above-described embodiment, specifically, the distillation reactor main body 3 passes through cleaning pipe 771 and return pipe 76 and confession
71 inside connection of water tank.
In above-described embodiment, specifically, the exhaust pipe 61 is connected to setting with distillation reactor main body 3；The row
Tracheae 61 is threadedly coupled with distillation reactor main body 3.
In above-described embodiment, specifically, the lower-left end of the three-limb tube 63 is threaded with gas treatment connection
Pipe 631；, the left upper end of the three-limb tube 63 is threaded with air scoop 632.
In above-described embodiment, specifically, the air scoop 632 and gas treatment connecting tube 631 by exhaust pipe 61 with
The 3 inside connection of distillation reactor main body.
In above-described embodiment, specifically, the outer surface top of the injection pipe 75 is threaded with protective cover.
In above-described embodiment, specifically, the discharging of waste liquid pipe 4 is connected to 3 inside of distillation reactor main body；Described
The left upper portion position of discharging of waste liquid pipe 4 is threaded with control valve.
In above-described embodiment, specifically, the leftward position in installation pedestal 1 is arranged in the one level of support bar 2；Described
The right positions in installation pedestal 1 are arranged in two level supporting rod 5.
In above-described embodiment, specifically, the upper surface of the production liquid delivery pipe 14 is provided with control valve；Described
Production liquid delivery pipe 14 is connected to setting with storage tank 18.
In above-described embodiment, specifically, the steam outlet pipe 17 is connected to 3 inside of distillation reactor main body；Described
Steam outlet pipe 17 is by steam pipeline 83 and distillate collecting pipe 13 by regarding legendary venomous insect 12 and finished product return duct 19 and storage tank 18
Inside connection.
In above-described embodiment, specifically, the distillation reactor main body 3 specifically uses carbon steel reaction kettle；Described regards
Legendary venomous insect 12 specifically regards legendary venomous insect using stainless steel is straight-through.
In above-described embodiment, specifically, the solenoid valve 64, water circulating pump 72, heater strip 102, heating rod 107 and steaming
It evaporates stirring motor 91 and electric control box 15 is electrically connected.
In above-described embodiment, specifically, the gas detecting instrument 62 specifically uses the detector of model PT40；It is described
Level-one thermometer 104 and two level thermometer 85 thermometer of WSS-401 is respectively adopted；The pressure detection meter 105 is specific
Using the pressure gauge of model Y100.
Operation principle
In the use of the present invention, by reaction kettle filling tube 106 heating cabinet 101 will be put into for the industrial chemicals of distillation procedure
It is interior, heating rod 107 and heater strip 102 are started by electric control box 15, play the role of heating industrial chemicals；By electrical
Control cabinet 15 starts the rotation that distillation stirring motor 91 drives agitating shaft 93, to drive 97 turns of diversion rod 95 and paddle
It is dynamic, to play the role of stirring to industrial chemicals, accelerates the progress of distillation procedure, improve distillation efficiency, shorten distillation time；
The steam that distillation generates is entered by steam outlet pipe 17 in steam pipeline 83；Start water circulating pump by electric control box 15
72, the cooling water in water feeding tank 71 is pumped to through interconnecting tube 73 in water inlet pipe 74, and then is entered in condenser pipe 81, is risen
To the effect to steam condensation cooling；After the condensed return pipe of cooling water 86 confession is flowed back into from return pipe 76 through external connecting pipe 77
In water tank 71, the needs for meeting condensation operation are recycled；Condensed liquid is flowed into distillate collecting pipe 13 regarding legendary venomous insect 12
It is interior, and then flow into finished product return duct 19, hence into in storage tank 18, complete the needs of distillation procedure；In distillation process
The exhaust gas of middle generation passes through the detection of gas detecting instrument 62, is excluded out of air scoop 632 through three-limb tube 63 after qualified, if
Detect it is unqualified handled with 631 connection processing equipment of gas treatment connecting tube after discharge, achieve the purpose that environmental protection；It is distilling
In the process, by level-one thermometer 104 and pressure detection meter 105,3 internal temperature of distillation reactor main body and pressure are observed at any time
Situation of change, ensure distillation procedure carried out in safely controllable range；Residue after distillation passes through discharging of waste liquid pipe 4
It is discharged, and the control valve for opening the setting of 771 upper surface of cleaning pipe is rinsed.
Using technical solutions according to the invention or those skilled in the art under the inspiration of technical solution of the present invention,
Similar technical solution is designed, and reaches above-mentioned technique effect, is to fall into protection scope of the present invention.
Claims (10)
1. a kind of distillation equipment for Chemical Manufacture of environmental protection, which is characterized in that the distillation for Chemical Manufacture of the environmental protection
Equipment includes installation pedestal（1）, one level of support bar（2）, distillation reactor main body（3）, discharging of waste liquid pipe（4）, two level supporting rod
（5）, wasted nickel catalyst exhaust pipe device（6）, multi-functional water supply case apparatus（7）, thermometric condenser tube structure（8）, diversion mixing leaf knot
Structure（9）, heat chamber structure（10）, observe item（11）, depending on legendary venomous insect（12）, distillate collecting pipe（13）, production liquid delivery pipe（14）,
Electric control box（15）, top supporting frame（16）, steam outlet pipe（17）, storage tank（18）With finished product return duct（19）, described
One level of support bar（2）One end is bolted to distillation reactor main body respectively（3）Lower surface corner location, the other end with installation
Pedestal（1）Upper surface be bolted；The discharging of waste liquid pipe（4）It is threaded in distillation reactor main body（3）Following table
Face centre position；The two level supporting rod（5）One end is bolted to storage tank respectively（18）Lower surface corner location, separately
One end and installation pedestal（1）Upper surface be bolted；The wasted nickel catalyst exhaust pipe device（6）Mounted on distillation reactor
Main body（3）Left upper portion position；The multi-functional water supply case apparatus（7）Mounted on installation pedestal（1）Upper surface among
Position；The thermometric condenser tube structure（8）With multi-functional water supply case apparatus（7）It is connected；The diversion mixing impeller structure
（9）It is plugged on distillation reactor main body（3）Upper inside centre position；The heating chamber structure（10）It is bolted to steaming
Evaporate reactor main body（3）Inside；The observation item（11）Inlay storage tank in longitudinal direction（18）Front surface centre position；It is described
Regard legendary venomous insect（12）It is threaded in distillate collecting pipe（13）Lower end；The distillate collecting pipe（13）With thermometric condenser pipe
Structure（8）It is connected；The production liquid delivery pipe（14）It is threaded in storage tank（18）Lower right side position；It is described
Electric control box（15）Screw is connected to distillation reactor main body（3）Left lower position；The top supporting frame
（16）It is bolted distillation reactor main body respectively（3）At left and right sides of upper surface；The steam outlet pipe（17）It is threaded in
Distillation reactor main body（3）Upper surface right positions；The finished product return duct（19）Threaded one end is connected to storage tank
（18）Upper surface centre position, the other end is threaded in regarding legendary venomous insect（12）Lower surface；The wasted nickel catalyst exhaust pipe dress
It sets（6）Including exhaust pipe（61）, gas detecting instrument（62）, three-limb tube（63）, solenoid valve（64）And hand control valve（65）,
The gas detecting instrument（62）It is threaded in exhaust pipe（61）Upper surface right positions；The three-limb tube（63）
It is threaded in exhaust pipe（61）Left position；The solenoid valve（64）It is embedded in three-limb tube（63）Inside upper left
Side；The hand control valve（65）It is threaded in three-limb tube（63）Lower surface right positions.
2. the distillation equipment for Chemical Manufacture of environmental protection as described in claim 1, which is characterized in that the multi-functional confession
Cistern device（7）Including water feeding tank（71）, water circulating pump（72）, interconnecting tube（73）, water inlet pipe（74）, injection pipe（75）,
Return pipe（76）And external connecting pipe（77）, the water circulating pump（72）It is bolted to water feeding tank（71）Inside bottom right
Side；The interconnecting tube（73）Longitudinal screw is connected to water circulating pump（72）Upper surface；The water inlet pipe（74）It is vertical
To through water feeding tank（71）Upper surface right positions and interconnecting tube（73）It is threadedly coupled；The injection pipe（75）Screw thread
It is connected to water feeding tank（71）Upper surface centre position；The return pipe（76）Threaded one end is connected to water feeding tank（71）It is upper
Surface leftward position, the other end are threaded in external connecting pipe（77）Lower surface.
3. the distillation equipment for Chemical Manufacture of environmental protection as described in claim 1, which is characterized in that the thermometric condensation
Pipe structure（8）Including condenser pipe（81）, cooling cylinder（82）, steam pipeline（83）, sealing ring（84）, two level thermometer（85）With
Condensation return pipt（86）, the condenser pipe（81）It is wrapped in steam pipeline（83）Outer surface centre position；Described is cold
Solidifying case（82）Cover is connected on condenser pipe（81）Outer surface；The sealing ring（84）It is arranged in steam pipeline（83）And cooling cylinder
（82）Intersection；The two level thermometer（85）Screw is connected to cooling cylinder（82）Front surface lower left side；Described is cold
Solidifying return pipe（86）It is threaded in cooling cylinder（82）Lower surface leftward position.
4. the distillation equipment for Chemical Manufacture of environmental protection as described in claim 1, which is characterized in that the diversion mixing
Impeller structure（9）Including distilling stirring motor（91）, hanging ring（92）, agitating shaft（93）, level-one casing（94）, diversion rod（95）, two
Grade casing（96）And paddle（97）, the hanging ring（92）It is threaded in distillation stirring motor（91）Upper surface interposition
It sets；The agitating shaft（93）Shaft coupling is connected to distillation stirring motor（91）Output shaft on；The level-one casing（94）
It is socketed in agitating shaft（93）Outer surface upper position；The diversion rod（95）It is respectively welded at level-one casing（94）Left and right
Both sides centre position；The two level casing（96）It is socketed in agitating shaft（93）Outer surface lower position；The paddle
（97）It is respectively welded at two level casing（96）Left and right sides centre position.
5. the distillation equipment for Chemical Manufacture of environmental protection as described in claim 1, which is characterized in that the heating cabinet knot
Structure（10）Including heating cabinet（101）, heater strip（102）, fixed link（103）, level-one thermometer（104）, pressure detection meter
（105）, reaction kettle filling tube（106）And heating rod（107）, the heating cabinet（101）Integrated setting is in distillation reactor
Main body（3）Inside；The heater strip（102）It is welded on heating cabinet（101）With distillation reactor main body（3）The gap of formation
It is interior；The fixed link（103）It is respectively welded at distillation reactor main body（3）Two up and down at left and right sides of inner surface；Described
Level-one thermometer（104）Screw is connected to distillation reactor main body（3）Front surface upper right side；The pressure detection meter
（105）Screw is connected to distillation reactor main body（3）Front surface upper left side；The reaction kettle filling tube（106）It is welded on
Distillation reactor main body（3）Upper surface leftward position；The heating rod（107）Longitudinal measure is in fixed link（103）It is outer
Side.
6. the distillation equipment for Chemical Manufacture of environmental protection as claimed in claim 3, which is characterized in that the steam conveying
Pipe（83）Left end and steam outlet pipe（17）It is threadedly coupled setting；The steam pipeline（83）Right end and distillate collect
Pipe（13）It is threadedly coupled setting.
7. the distillation equipment for Chemical Manufacture of environmental protection as claimed in claim 4, which is characterized in that the agitating shaft
（93）With level-one casing（94）With two level casing（96）Intersection be respectively arranged with clamping screw；The agitating shaft（93）It is vertical
To through distillation reactor main body（3）Upper surface centre position；The agitating shaft（93）With distillation reactor main body（3）'s
Intersection is provided with gasket；The top supporting frame（16）It is bolted to distillation stirring motor respectively（91）Left and right two
Side lower part position.
8. the distillation equipment for Chemical Manufacture of environmental protection as described in claim 1, which is characterized in that the water feeding tank
（71）With installation pedestal（1）It is bolted setting；The water feeding tank（71）It is arranged in one level of support bar（2）With two level supporting rod
（5）Between.
9. the distillation equipment for Chemical Manufacture of environmental protection as claimed in claim 2, which is characterized in that the external connection
Pipe（77）Left side centre position be threaded with cleaning pipe（771）；The cleaning pipe（771）Left end be threaded with spray
Head（772）；The nozzle（772）It is arranged in distillation reactor main body（3）Inside upper right side；The cleaning pipe（771）
It is threaded in distillation reactor main body（3）Right upper portion position；The cleaning pipe（771）Upper surface right positions screw thread
It is connected with control valve.
10. the distillation equipment for Chemical Manufacture of environmental protection as described in claim 1, which is characterized in that the exhaust pipe
（61）With distillation reactor main body（3）Connection setting；The exhaust pipe（61）With distillation reactor main body（3）It is threadedly coupled.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810636471.XA CN108744570A (en) | 2018-06-20 | 2018-06-20 | A kind of distillation equipment for Chemical Manufacture of environmental protection |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810636471.XA CN108744570A (en) | 2018-06-20 | 2018-06-20 | A kind of distillation equipment for Chemical Manufacture of environmental protection |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108744570A true CN108744570A (en) | 2018-11-06 |
Family
ID=63979156
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810636471.XA Pending CN108744570A (en) | 2018-06-20 | 2018-06-20 | A kind of distillation equipment for Chemical Manufacture of environmental protection |
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| CN (1) | CN108744570A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109663552A (en) * | 2018-12-27 | 2019-04-23 | 潘伟 | A kind of fixed-bed reactor preparing 9-Fluorenone |
| CN109806828A (en) * | 2019-02-27 | 2019-05-28 | 黄山天马新材料科技有限公司 | A kind of organo silane coupling agent reaction kettle |
| CN110960878A (en) * | 2019-11-22 | 2020-04-07 | 耒阳金悦科技发展有限公司 | Environment-friendly distillation equipment for chemical production |
| CN112717837A (en) * | 2021-03-23 | 2021-04-30 | 江苏国胶新材料有限公司 | High-purity isooctyl ester apparatus for producing with stirring structure |
| CN112755570A (en) * | 2021-01-05 | 2021-05-07 | 张淑侠 | Diethyl toluene diamine hydrolysis solvent distillation recovery unit |
| CN112933643A (en) * | 2021-02-23 | 2021-06-11 | 杨奉辛 | Intelligent rectifying still |
| CN113842855A (en) * | 2021-09-01 | 2021-12-28 | 齐齐哈尔大学 | Chemical raw material separation tower |
| CN114570319A (en) * | 2022-03-23 | 2022-06-03 | 扬州市职业大学(扬州开放大学) | A reation kettle for dimethyl disulfide production |
| CN114768290A (en) * | 2022-04-21 | 2022-07-22 | 郑州要来生物科技有限公司 | Process and device for extracting effective components of kaffir lily by steam distillation method |
| CN115745834A (en) * | 2022-11-29 | 2023-03-07 | 安徽海顺化工有限公司 | Production process of p-chlorobenzene acetonitrile |
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| CN110960878A (en) * | 2019-11-22 | 2020-04-07 | 耒阳金悦科技发展有限公司 | Environment-friendly distillation equipment for chemical production |
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| CN112755570A (en) * | 2021-01-05 | 2021-05-07 | 张淑侠 | Diethyl toluene diamine hydrolysis solvent distillation recovery unit |
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| CN112717837A (en) * | 2021-03-23 | 2021-04-30 | 江苏国胶新材料有限公司 | High-purity isooctyl ester apparatus for producing with stirring structure |
| CN113842855A (en) * | 2021-09-01 | 2021-12-28 | 齐齐哈尔大学 | Chemical raw material separation tower |
| CN114570319A (en) * | 2022-03-23 | 2022-06-03 | 扬州市职业大学(扬州开放大学) | A reation kettle for dimethyl disulfide production |
| CN114570319B (en) * | 2022-03-23 | 2023-09-29 | 扬州市职业大学(扬州开放大学) | Reaction kettle for producing dimethyl disulfide |
| CN114768290A (en) * | 2022-04-21 | 2022-07-22 | 郑州要来生物科技有限公司 | Process and device for extracting effective components of kaffir lily by steam distillation method |
| CN115745834A (en) * | 2022-11-29 | 2023-03-07 | 安徽海顺化工有限公司 | Production process of p-chlorobenzene acetonitrile |
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Application publication date: 20181106 |
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