CN114768290A - Process and device for extracting effective components of kaffir lily by steam distillation method - Google Patents
Process and device for extracting effective components of kaffir lily by steam distillation method Download PDFInfo
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- CN114768290A CN114768290A CN202210422235.4A CN202210422235A CN114768290A CN 114768290 A CN114768290 A CN 114768290A CN 202210422235 A CN202210422235 A CN 202210422235A CN 114768290 A CN114768290 A CN 114768290A
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- kaffir lily
- clivia miniata
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- 238000000034 method Methods 0.000 title claims abstract description 55
- 238000001256 steam distillation Methods 0.000 title claims abstract description 32
- 230000008569 process Effects 0.000 title claims abstract description 21
- 240000004550 Hesperantha coccinea Species 0.000 title abstract 4
- 238000006243 chemical reaction Methods 0.000 claims abstract description 70
- 238000005520 cutting process Methods 0.000 claims abstract description 68
- 239000007788 liquid Substances 0.000 claims abstract description 58
- 238000003756 stirring Methods 0.000 claims abstract description 42
- 241000755729 Clivia Species 0.000 claims description 56
- 241000755724 Clivia miniata Species 0.000 claims description 55
- 238000010438 heat treatment Methods 0.000 claims description 26
- 238000004140 cleaning Methods 0.000 claims description 18
- 239000002699 waste material Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 238000001035 drying Methods 0.000 claims description 12
- 239000011259 mixed solution Substances 0.000 claims description 12
- 238000009833 condensation Methods 0.000 claims description 9
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- 238000005406 washing Methods 0.000 claims description 9
- 239000004480 active ingredient Substances 0.000 claims description 7
- 238000005485 electric heating Methods 0.000 claims description 6
- 238000002791 soaking Methods 0.000 claims description 6
- 238000011084 recovery Methods 0.000 claims description 5
- 238000009826 distribution Methods 0.000 abstract description 3
- 238000000605 extraction Methods 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 description 5
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- XGVJWXAYKUHDOO-UHFFFAOYSA-N galanthidine Natural products C1CN2CC3=CC=4OCOC=4C=C3C3C2C1=CC(O)C3O XGVJWXAYKUHDOO-UHFFFAOYSA-N 0.000 description 1
- 208000006454 hepatitis Diseases 0.000 description 1
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- XGVJWXAYKUHDOO-DANNLKNASA-N lycorine Chemical compound C1CN2CC3=CC=4OCOC=4C=C3[C@H]3[C@H]2C1=C[C@H](O)[C@H]3O XGVJWXAYKUHDOO-DANNLKNASA-N 0.000 description 1
- KQAOMBGKIWRWNA-UHFFFAOYSA-N lycorine Natural products OC1C=C2CCN3C2C(C1O)c4cc5OCOc5cc34 KQAOMBGKIWRWNA-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/38—Steam distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
- B01D29/03—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements self-supporting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C18/00—Disintegrating by knives or other cutting or tearing members which chop material into fragments
- B02C18/06—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
- B02C18/08—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within vertical containers
- B02C18/12—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within vertical containers with drive arranged below container
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C18/00—Disintegrating by knives or other cutting or tearing members which chop material into fragments
- B02C18/06—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
- B02C18/16—Details
- B02C18/18—Knives; Mountings thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C18/00—Disintegrating by knives or other cutting or tearing members which chop material into fragments
- B02C18/06—Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
- B02C18/16—Details
- B02C18/24—Drives
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- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention relates to a process and a device for extracting effective components of kaffir lily by a steam distillation method, and the process and the device comprise a bottom plate, a reaction tank and a stirring structure, wherein the stirring structure is arranged at the top of the reaction tank, the inner side of the reaction tank is provided with a heat control structure, the left side of the reaction tank is provided with a cutting structure, the top of the bottom plate is provided with a liquid supply structure, and the top of the bottom plate is provided with a collection structure; the stirring structure includes that fixed rotation connects at the inside first rotation pole of retort, the outside fixedly connected with annular distribution's of first rotation pole puddler, the top fixedly connected with guard box of retort, the first motor of interior roof fixedly connected with of guard box, accuse hot structure includes the three temperature sensor of fixed mounting at retort left side wall, the ring channel has been seted up to the inside of retort. The process and the device for extracting the effective components of the kaffir lily by the steam distillation method can improve the extraction efficiency of the effective components of the kaffir lily.
Description
1. Device of kaffir lily active ingredient is drawed to steam distillation method, its characterized in that: the reaction tank comprises a bottom plate (1), a reaction tank (2) and a stirring structure (200), wherein the stirring structure (200) is arranged at the top of the reaction tank (2), a heat control structure (300) is arranged on the inner side of the reaction tank (2), a cutting structure (400) is arranged on the left side of the reaction tank (2), a liquid supply structure (500) is arranged at the top of the bottom plate (1), and a collection structure (600) is arranged at the top of the bottom plate (1);
the stirring structure (200) comprises a first rotating rod (201) fixedly and rotatably connected inside the reaction tank (2), stirring rods (202) distributed in an annular shape are fixedly connected to the outer side of the first rotating rod (201), a protection box (203) is fixedly connected to the top of the reaction tank (2), and a first motor (204) is fixedly connected to the inner top wall of the protection box (203);
the heat control structure (300) comprises three temperature sensors (301) fixedly mounted on the left side wall of the reaction tank (2), an annular groove (302) is formed in the reaction tank (2), an electric heating plate (303) is fixedly connected to the inner side of the annular groove (302), and a control panel (304) is fixedly connected to the front side of the reaction tank (2);
cutting structure (400) include fixed mounting at left cutting case (401) of retort (2), the inboard rotation of cutting case (401) is connected with second dwang (402), cutting knife (403) that the outside fixedly connected with annular of second dwang (402) distributes, the positive fixedly connected with headstock (404) of cutting case (401).
2. The device for extracting effective components of kaffir lily by using the steam distillation method as claimed in claim 1, is characterized in that: the liquid supply structure (500) comprises a liquid supply box (501) fixedly mounted at the top of the bottom plate (1), the top of the bottom plate (1) is fixedly connected with a pump body (502), and the bottom of the reaction tank (2) is communicated with a liquid return pipe (505).
3. The device for extracting effective components of kaffir lily by using the steam distillation method as claimed in claim 2, is characterized in that: the bottom fixedly connected with waste liquid case (503) of recovery tube (505), the inboard fixedly connected with filter screen (504) of waste liquid case (503).
4. The device for extracting effective components of kaffir lily by the steam distillation method according to claim 1, which is characterized in that: collect structure (600) including four pillar (601) of fixed mounting at bottom plate (1) top, four fixedly connected with condensing box (602) between the top of pillar (601), cavity (603) have been seted up to condensing box (602) inside.
5. The device for extracting effective components of kaffir lily by using the steam distillation method as claimed in claim 4, is characterized in that: the bottom of the condensing box (602) is fixedly connected with a collecting pipe (604), and the bottom of the collecting pipe (604) is fixedly connected with a collecting box (605).
6. The device for extracting effective components of kaffir lily by using the steam distillation method as claimed in claim 4, is characterized in that: the right side of the reaction tank (2) is fixedly connected with a circulating pipe, the right end of the circulating pipe is communicated with a cavity (603) in the condensation box (602), and the top of the circulating pipe is fixedly connected with a third control valve.
7. The process for extracting effective components of clivia miniata by using the steam distillation method as claimed in claim 1, is characterized by comprising the following steps:
1) selecting 10kg of clivia miniata, soaking and cleaning for 5-10 minutes, after cleaning, washing the clivia miniata for 1-2 minutes, drying the cleaned clivia miniata for 3-5 minutes, and drying the surface of the clivia miniata;
2) placing the clivia miniata obtained in the step 1) into a cutting device for cutting, wherein the cutting length is 3-5cm, after the cutting is finished, placing the clivia miniata into a reaction tank, adding a mixed solution, submerging the clivia miniata by the added mixed solution, and heating at the same time; the heating temperature is 65-80 ℃, and the heating time is 15-20 minutes;
3) stirring the clivia miniata which is being heated in the step 2) for 1-2 minutes at a stirring interval of 10-15 minutes for 3-5 times;
4) condensing the hot steam generated in the step 3), wherein the temperature of cold water is 20-25 ℃, and the flow rate of the cold water can be 1.2-1.5 m/s;
5) and (5) collecting the finished product condensed in the step (4), and cleaning the kaffir lily and the liquid in the reaction tank. Process and device for extracting effective components of kaffir lily by steam distillation method
Technical Field
The invention relates to the technical field of kaffir lily, in particular to a process and a device for extracting kaffir lily effective components by a steam distillation method.
Background
Kaffir lily, also called amaryllis and lycoris maxima, belongs to ornamental flowers, is originally produced in south Africa, has a flowering period as long as 30-50 days, mainly winter spring, blooms before and after spring festival, is not bright light, is a semi-negative plant, is pleased with cool and high temperature, is suitable for growing at the temperature of 15-25 ℃, stops growing when the temperature is lower than 5 ℃, is pleased with soil with good fatness and drainage and moist soil, is not suitable for dry environment, has high ornamental value, and is often potted in greenhouses for appreciation in China.
Experiments prove that the kaffir lily plant body contains lycorine and kaffir lily alkali and also contains trace element selenium, at present, pharmaceutical workers use the kaffir lily plant body containing the chemical components to carry out scientific research and treat cancer, hepatitis, cirrhosis ascites, poliovirus and the like, and in the process of extracting effective components by using a steam distillation method, the used device is too simple, the automation degree is not high, and the kaffir lily extraction efficiency is too low.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a process and a device for extracting effective components of kaffir lily by a steam distillation method, which have the advantage of high production efficiency and solve the problem that the extraction efficiency of kaffir lily is too slow due to too simple used devices and low automation degree in the process of extracting the effective components of kaffir lily by the steam distillation method in the prior art.
In order to achieve the purpose, the invention provides the following technical scheme: a device for extracting effective components of kaffir lily by a steam distillation method comprises a bottom plate, a reaction tank and a stirring structure, wherein the stirring structure is arranged at the top of the reaction tank, the inner side of the reaction tank is provided with a heat control structure, the left side of the reaction tank is provided with a cutting structure, the top of the bottom plate is provided with a liquid supply structure, and the top of the bottom plate is provided with a collection structure;
the stirring structure comprises a first rotating rod fixedly and rotatably connected inside the reaction tank, stirring rods distributed in an annular shape are fixedly connected to the outer side of the first rotating rod, a protection box is fixedly connected to the top of the reaction tank, and a first motor is fixedly connected to the inner top wall of the protection box;
the heat control structure comprises three temperature sensors fixedly arranged on the left side wall of the reaction tank, an annular groove is formed in the reaction tank, an electric heating plate is fixedly connected to the inner side of the annular groove, and a control panel is fixedly connected to the front side of the reaction tank;
the cutting structure includes the left cutting case of fixed mounting at the retort, the inboard rotation of cutting case is connected with the second dwang, the cutting knife that the outside fixedly connected with annular of second dwang distributes, the positive fixedly connected with headstock of cutting case.
Further, the liquid supply structure comprises a liquid supply box fixedly mounted at the top of the bottom plate, the top of the bottom plate is fixedly connected with a pump body, and the bottom of the reaction tank is communicated with a liquid return pipe.
Further, the bottom fixedly connected with waste liquid case of recovery tube, the inboard fixedly connected with filter screen of waste liquid case.
Further, the collection structure includes four pillars fixedly mounted at the top of the bottom plate, four fixedly connected with condensing boxes between the tops of the pillars, and cavities are formed in the condensing boxes.
Furthermore, the bottom of the condensing box is fixedly connected with a collecting pipe, and the bottom of the collecting pipe is fixedly connected with a collecting box.
Furthermore, the right side of the reaction tank is fixedly connected with a circulating pipe, the right end of the circulating pipe is communicated with the cavity inside the condensation box, and the top of the circulating pipe is fixedly connected with a third control valve.
The process for extracting effective components of kaffir lily by a steam distillation method comprises the following manufacturing process steps:
1) selecting 10kg of clivia miniata, soaking and cleaning for 5-10 minutes, after cleaning, washing the clivia miniata for 1-2 minutes, drying the cleaned clivia miniata for 3-5 minutes, and drying the surface of the clivia miniata;
2) placing the clivia miniata obtained in the step 1) into a cutting device for cutting, wherein the cutting length is 3-5cm, after the cutting is finished, placing the clivia miniata into a reaction tank, adding a mixed solution, submerging the clivia miniata by the added mixed solution, and heating at the same time; the heating temperature is 65-80 ℃, and the heating time is 15-20 minutes;
3) stirring the clivia miniata which is being heated in the step 2) for 1-2 minutes at a stirring interval of 10-15 minutes for 3-5 times;
4) condensing the hot steam generated in the step 3), wherein the temperature of cold water is 20-25 ℃, and the flow rate of the cold water can be 1.2-1.5 m/s;
5) and (4) collecting the finished product obtained by condensation in the step (4), and simultaneously cleaning the clivia and the liquid in the reaction tank.
Compared with the prior art, the technical scheme of the application has the following beneficial effects:
1. this technology and device that steam distillation method drawed kaffir lily active ingredient can cut kaffir lily through the inside cutting case of cutting structure, second dwang, cutting knife and headstock, let kaffir lily be heated sooner, active ingredient flows sooner, can stir the kaffir lily and the mixed liquid of retort inside through the inside first dwang of stirring structure, puddler, protective housing and first motor, it is more even to let kaffir lily be heated, improve the efficiency that kaffir lily active ingredient drawed.
2. This process and device for extracting kaffir lily active ingredient by steam distillation method can carry out annular heating to kaffir lily and mixed liquid inside the reaction tank through the inside temperature sensor, annular distribution, heating plate and the control panel of accuse heat structure, and it is more even to let it be heated to can conveniently monitor the inside different position temperatures of reaction tank through three temperature sensor, improve the accuracy that temperature detected.
3. This process and device for extracting kaffir lily active ingredient by steam distillation method can retrieve the waste material of processing completion through the inside waste liquid case, filter screen and the liquid return pipe of confession liquid structure to carry out the wet-dry separation, make things convenient for staff's recovery work.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a front view of the present invention;
FIG. 3 is a top cross-sectional view of a structural cutting box of the present invention.
In the figure: 1. a base plate; 2. a reaction tank; 200. a stirring structure; 201. a first rotating lever; 202. a stirring rod; 203. a protective box; 204. a first motor; 300. a heat control structure; 301. a temperature sensor; 302. an annular groove; 303. an electrical heating plate; 304. a control panel; 400. cutting the structure; 401. cutting the box; 402. a second rotating rod; 403. a cutting knife; 404. a power box; 500. a liquid supply structure; 501. a liquid supply tank; 502. a pump body; 503. a waste liquid tank; 504. Filtering with a screen; 505. a liquid return pipe; 600. a collection structure; 601. a pillar; 602. a condensing tank; 603. a cavity; 604. a collection tube; 605. and a collection box.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Referring to fig. 1 and 3, the apparatus for extracting kaffir lily effective components by steam distillation in this embodiment includes a bottom plate 1, a reaction tank 2 and a stirring structure 200, wherein the stirring structure 200 is disposed at the top of the reaction tank 2, a heat control structure 300 is disposed inside the reaction tank 2, and a cutting structure 400 is disposed on the left side of the reaction tank 2; the top of bottom plate 1 is provided with supplies liquid structure 500, and the top of bottom plate 1 is provided with collects structure 600, and wherein, stirring structure 200 makes 2 inside structures of stirring of retort, and cutting structure 400 is the structure to the cutting of kaffir lily, supplies liquid structure 500 to be the structure that provides mixed liquid and collect the waste liquid to 2 insides of retort, and it is the structure of carrying out the condensation to hot steam and collecting to collect structure 600, and accuse thermal structure 300 is the structure of heating 2 insides of retort.
As shown in fig. 1-3, the stirring structure 200 includes a first rotating rod 201 fixedly and rotatably connected inside the reaction tank 2, the outer side of the first rotating rod 201 is fixedly connected with stirring rods 202 distributed annularly, the top of the reaction tank 2 is fixedly connected with a protective box 203, the top end of the first rotating rod 201 sequentially penetrates through the reaction tank 2 and the protective box 203 and is fixedly connected with the output end of a first motor 204, and the inner top wall of the protective box 203 is fixedly connected with the first motor 204;
in addition, heat control structure 300 includes three temperature sensor 301 of fixed mounting at the retort 2 left side wall, and three temperature sensor 301 is located the top of reaction tube 2 left side wall respectively, and ring channel 302 has been seted up to the inside of retort 2, and the inboard fixedly connected with electric heating board 303 of ring channel 302, the positive fixedly connected with control panel 304 of retort 2.
The output end of the electric heating plate 303 is electrically connected with the input end of the control panel 304, and the output end of the temperature sensor 301 is electrically connected with the output end of the temperature sensor 301.
Meanwhile, the cutting structure 400 comprises a cutting box 401 fixedly mounted on the left side of the reaction tank 2, a front side wall fixedly connected with bearing of the cutting box 401, the inner side of the cutting box 401 is rotatably connected with a second rotating rod 402, the back side one end of the second rotating rod 402 is fixedly connected with the inner side of the bearing, a cutting knife 403 annularly distributed on the outer side of the second rotating rod 402 is fixedly connected with the cutting box 401, a front side wall fixedly connected with second motor of the cutting box 401 is fixedly connected with a power box 404, and the front side one end of the second rotating rod 402 sequentially penetrates through the cutting box 401 and the power box and is fixedly connected with the output end of the second motor.
The through-hole of mutual intercommunication is all seted up to cutting case 401's top fixedly connected with inlet pipe, cutting case 401's the right side and retort 2's left side.
As shown in fig. 1-2, the liquid supply structure 500 includes a liquid supply tank 501 fixedly mounted on the top of the bottom plate 1, a pump body 502 fixedly connected to the top of the bottom plate 1, a first connecting pipe fixedly connected to the left side of the pump body 502, a second connecting pipe fixedly connected to the right side of the pump body 502, the left side of the first connecting pipe is communicated with the liquid supply tank 501, one end of the second connecting pipe far away from the pump body 502 is communicated with the reaction tank 2, a liquid return pipe 505 is communicated with the bottom of the reaction tank 2, a waste liquid tank 503 is fixedly connected to the bottom of the recovery pipe 505, and a filter screen 504 is fixedly connected to the inner side of the waste liquid tank 503.
The right side of the second connecting pipe is fixedly connected with a first control valve, the waste liquid tank 503 is fixedly installed at the top of the bottom plate 1, the right side of the waste liquid tank 503 is fixedly connected with a liquid discharge pipe communicated with the outside, and the right side of the liquid return pipe 505 is fixedly connected with a second control valve.
As shown in fig. 1-2, the collecting structure 600 includes four pillars 601 fixedly mounted on the top of the bottom plate 1, the collecting box 605 is fixedly mounted on the top of the bottom plate 1, a condenser box 602 is fixedly connected between the tops of the four pillars 601, a water inlet pipe is fixedly connected to the top of the condenser box 602 and is communicated with the outside, two guide plates are fixedly connected to the inner bottom wall of the condenser box 602, a drain pipe is fixedly connected to the right side of the condenser box 602 and is communicated with the outside, a cavity 603 is formed in the condenser box 602, the left end of the drain pipe is communicated with the cavity 603, the bottom end of the water inlet pipe is communicated with the cavity 603, a collecting pipe 604 is fixedly connected to the bottom of the condenser box 602, and a collecting box 605 is fixedly connected to the bottom of the collecting pipe 604.
The right side of the reaction tank 2 is fixedly connected with a circulation pipe, the right end of the circulation pipe is communicated with a cavity 603 in the condensation box 602, and the top of the circulation pipe is fixedly connected with a third control valve.
The first embodiment is as follows: the process for extracting effective components of clivia miniata by a steam distillation method comprises the following manufacturing process steps:
1) selecting 10kg of clivia miniata, soaking and cleaning for 5 minutes, washing the clivia miniata after cleaning is finished, wherein the washing time is 1 minute, drying the cleaned clivia miniata for 3 minutes, and drying the surface of the clivia miniata;
2) placing the clivia miniata obtained in the step 1) into a cutting device for cutting, wherein the cutting length is 3cm, after the cutting is finished, placing the clivia miniata into a reaction tank, adding a mixed solution, submerging the clivia miniata by the added mixed solution, and heating the clivia miniata simultaneously; the heating temperature is 65 ℃, and the heating time is 15 minutes
3) Stirring the clivia miniata which is being heated in the step 2) for 1 minute, wherein the stirring interval is 10 minutes each time, and the stirring frequency is 3 times;
4) condensing the hot steam generated in the step 3), wherein the temperature of cold water is 20 ℃, and the flow velocity of the cold water can be 1.2 m/s;
5) and (4) collecting the finished product obtained by condensation in the step (4), and simultaneously cleaning the clivia and the liquid in the reaction tank.
The second embodiment: the process for extracting effective components of kaffir lily by a steam distillation method comprises the following manufacturing process steps:
1) selecting 10kg of clivia miniata, soaking and cleaning for 7 minutes, washing the clivia miniata after cleaning is finished, wherein the washing time is 1.5 minutes, drying the cleaned clivia miniata for 4 minutes, and drying the surface of the clivia miniata;
2) placing the clivia miniata obtained in the step 1) into a cutting device for cutting, wherein the cutting length is 4cm, after the cutting is finished, placing the clivia miniata into a reaction tank, adding a mixed solution, submerging the clivia miniata by the added mixed solution, and heating the clivia miniata simultaneously; the heating temperature is 75 ℃, and the heating time is 17 minutes;
3) stirring the heating clivia miniata in the step 2) for 1-2 minutes at a stirring interval of 12 minutes for 4 times;
4) condensing the hot steam generated in the step 3), wherein the temperature of cold water is 23 ℃, and the flow rate of the cold water can be 1.4/s;
5) and (5) collecting the finished product condensed in the step (4), and cleaning the kaffir lily and the liquid in the reaction tank.
Example three: the process for extracting effective components of kaffir lily by a steam distillation method comprises the following manufacturing process steps:
1) selecting 10kg of clivia miniata, soaking and cleaning for 10 minutes, washing the clivia miniata after cleaning is finished, wherein the washing time is 2 minutes, drying the cleaned clivia miniata for 5 minutes, and drying the surface of the clivia miniata;
2) placing the clivia miniata obtained in the step 1) into a cutting device for cutting, wherein the cutting length is 5cm, after the cutting is finished, placing the clivia miniata into a reaction tank, adding a mixed solution, submerging the clivia miniata by the added mixed solution, and heating the clivia miniata simultaneously; the heating temperature is 80 ℃, and the heating time is 20 minutes;
3) stirring the heating clivia miniata in the step 2) for 2 minutes at a stirring interval of 15 minutes for 5 times;
4) condensing the hot steam generated in the step 3), wherein the temperature of cold water is 20-25 ℃, and the flow velocity of the cold water can be 1.5 m/s;
5) and (5) collecting the finished product condensed in the step (4), and cleaning the kaffir lily and the liquid in the reaction tank.
Experiments prove that the extracting solution obtained by the third embodiment has higher efficiency, and the extracting solution amount obtained by kaffir lily with the same raw material is the largest.
The working principle of the above embodiment is as follows:
putting the kaffir lily into a cutting box 401, starting a second motor, driving a second rotating rod 402 to rotate by the second motor, driving a cutting knife 403 to cut the kaffir lily, enabling the kaffir lily cut into sections to enter a reaction tank 2, opening a first control valve, simultaneously starting a pump body 502 to send a mixed liquid into the reaction tank 2 through a first connecting pipe and a second connecting pipe, starting an electric heating plate 303 to heat the inside of the reaction tank 2, monitoring the inside temperature through a temperature sensor 301 and a control panel 304, controlling the inside temperature, then starting a first motor 204, driving the first rotating rod 201 to rotate by the first motor 204, further driving a stirring rod 202 to stir the mixed liquid and the kaffir lily, opening a third control valve, enabling hot steam generated by heating to enter a condensation box 602 through a circulation pipe, and enabling cooling water to flow in a cavity 603 through a water inlet pipe and a water outlet pipe, the water vapor is condensed, the finished product generated by condensation enters a collection tank 605 through a collection pipe 604, a second control valve is opened, the waste liquid in the reaction tank 2 enters a waste liquid tank 503 through a liquid return pipe 505, and dry-wet separation can be performed through a filter screen 504.
Compared with the prior art: through the inside cutting case 401 of cutting structure 400, the second dwang 402, cutting knife 403 and headstock 404 can cut kaffir lily, let kaffir lily be heated faster, the effective constituent flows out faster, through the inside first dwang 201 of stirring structure 200, puddler 202, guard box 203 and first motor 204 can stir kaffir lily and mixed liquid inside retort 2, let kaffir lily be heated more evenly, improve the efficiency that kaffir lily effective constituent drawed, through inside temperature sensor 301 of accuse heat structure 300, annular distribution 302, hot plate 303 and control panel 304 can carry out annular heating to kaffir lily and mixed liquid inside retort 2, let it be heated more evenly, and can conveniently monitor the inside different position temperatures of retort 2 through three temperature sensor 301, improve the accuracy that detects the temperature, through supplying the inside waste liquid case 503 of liquid structure 500, The filter screen 504 and the liquid return pipe can recycle the processed waste materials, and dry-wet separation is carried out, so that the recycling work of workers is facilitated.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in the process, method, article, or apparatus that comprises the element.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. Device of kaffir lily active ingredient is drawed to steam distillation method, its characterized in that: the reaction tank comprises a bottom plate (1), a reaction tank (2) and a stirring structure (200), wherein the stirring structure (200) is arranged at the top of the reaction tank (2), a heat control structure (300) is arranged on the inner side of the reaction tank (2), a cutting structure (400) is arranged on the left side of the reaction tank (2), a liquid supply structure (500) is arranged at the top of the bottom plate (1), and a collection structure (600) is arranged at the top of the bottom plate (1);
the stirring structure (200) comprises a first rotating rod (201) which is fixedly and rotatably connected inside the reaction tank (2), stirring rods (202) which are distributed annularly are fixedly connected to the outer side of the first rotating rod (201), a protection box (203) is fixedly connected to the top of the reaction tank (2), and a first motor (204) is fixedly connected to the inner top wall of the protection box (203);
the heat control structure (300) comprises three temperature sensors (301) fixedly mounted on the left side wall of the reaction tank (2), an annular groove (302) is formed in the reaction tank (2), an electric heating plate (303) is fixedly connected to the inner side of the annular groove (302), and a control panel (304) is fixedly connected to the front face of the reaction tank (2);
cutting structure (400) include fixed mounting at left cutting case (401) of retort (2), the inboard rotation of cutting case (401) is connected with second dwang (402), cutting knife (403) that the outside fixedly connected with annular of second dwang (402) distributes, the positive fixedly connected with headstock (404) of cutting case (401).
2. The device for extracting effective components of kaffir lily by using the steam distillation method as claimed in claim 1, is characterized in that: the liquid supply structure (500) comprises a liquid supply box (501) fixedly mounted at the top of the bottom plate (1), the top of the bottom plate (1) is fixedly connected with a pump body (502), and the bottom of the reaction tank (2) is communicated with a liquid return pipe (505).
3. The device for extracting effective components of kaffir lily by using the steam distillation method as claimed in claim 2, which is characterized in that: the bottom fixedly connected with waste liquid case (503) of recovery tube (505), the inboard fixedly connected with filter screen (504) of waste liquid case (503).
4. The device for extracting effective components of kaffir lily by the steam distillation method according to claim 1, which is characterized in that: collect structure (600) including four pillars (601) of fixed mounting at bottom plate (1) top, four fixedly connected with condensing box (602) between the top of pillar (601), cavity (603) have been seted up to condensing box (602) inside.
5. The device for extracting effective components of kaffir lily by the steam distillation method according to claim 4, which is characterized in that: the bottom of the condensing box (602) is fixedly connected with a collecting pipe (604), and the bottom of the collecting pipe (604) is fixedly connected with a collecting box (605).
6. The device for extracting effective components of kaffir lily by the steam distillation method according to claim 4, which is characterized in that: the right side of the reaction tank (2) is fixedly connected with a circulating pipe, the right end of the circulating pipe is communicated with a cavity (603) in the condensation box (602), and the top of the circulating pipe is fixedly connected with a third control valve.
7. The process for extracting effective components of kaffir lily by a steam distillation method according to claim 1, which is characterized by comprising the following steps:
1) selecting 10kg of clivia miniata, soaking and cleaning for 5-10 minutes, after cleaning, washing the clivia miniata for 1-2 minutes, drying the cleaned clivia miniata for 3-5 minutes, and drying the surface of the clivia miniata;
2) cutting the clivia miniata obtained in the step 1) in a cutting device, wherein the cutting length is 3-5cm, after the cutting is finished, putting the clivia miniata into a reaction tank, adding a mixed solution, submerging the clivia miniata in the added mixed solution, and heating the clivia miniata; the heating temperature is 65-80 ℃, and the heating time is 15-20 minutes;
3) stirring the clivia miniata which is being heated in the step 2) for 1-2 minutes at a stirring interval of 10-15 minutes for 3-5 times;
4) condensing the hot steam generated in the step 3), wherein the temperature of cold water is 20-25 ℃, and the flow speed of the cold water can be 1.2-1.5 m/s;
5) and (5) collecting the finished product condensed in the step (4), and cleaning the kaffir lily and the liquid in the reaction tank.
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