CN108740811A - 含松叶有效成分的营养黄花鱼干的制造方法及黄花鱼干 - Google Patents
含松叶有效成分的营养黄花鱼干的制造方法及黄花鱼干 Download PDFInfo
- Publication number
- CN108740811A CN108740811A CN201810355496.2A CN201810355496A CN108740811A CN 108740811 A CN108740811 A CN 108740811A CN 201810355496 A CN201810355496 A CN 201810355496A CN 108740811 A CN108740811 A CN 108740811A
- Authority
- CN
- China
- Prior art keywords
- yellow croaker
- pine needle
- brine
- dried yellow
- manufacturing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000008331 Pinus X rigitaeda Nutrition 0.000 title claims abstract description 81
- 235000011613 Pinus brutia Nutrition 0.000 title claims abstract description 81
- 241000018646 Pinus brutia Species 0.000 title claims abstract description 81
- 241001596950 Larimichthys crocea Species 0.000 title claims abstract description 70
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 45
- 239000004480 active ingredient Substances 0.000 title claims abstract description 21
- 235000016709 nutrition Nutrition 0.000 title abstract description 11
- 230000035764 nutrition Effects 0.000 title abstract description 10
- 241000356842 Larimichthys polyactis Species 0.000 claims abstract description 42
- 239000012267 brine Substances 0.000 claims abstract description 27
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 claims abstract description 27
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 23
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 22
- 229930003935 flavonoid Natural products 0.000 claims abstract description 20
- 150000002215 flavonoids Chemical class 0.000 claims abstract description 20
- 235000017173 flavonoids Nutrition 0.000 claims abstract description 20
- 239000000843 powder Substances 0.000 claims abstract description 19
- 239000004615 ingredient Substances 0.000 claims abstract description 18
- 238000005108 dry cleaning Methods 0.000 claims abstract description 4
- 230000003078 antioxidant effect Effects 0.000 claims description 5
- 229930003944 flavone Natural products 0.000 claims description 3
- 150000002213 flavones Chemical class 0.000 claims description 3
- 235000011949 flavones Nutrition 0.000 claims description 3
- 230000000050 nutritive effect Effects 0.000 abstract description 4
- 238000012360 testing method Methods 0.000 description 34
- 239000000523 sample Substances 0.000 description 31
- 239000007788 liquid Substances 0.000 description 28
- 239000000243 solution Substances 0.000 description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 17
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 16
- 238000002474 experimental method Methods 0.000 description 16
- 239000000126 substance Substances 0.000 description 14
- UEZVMMHDMIWARA-UHFFFAOYSA-N Metaphosphoric acid Chemical compound OP(=O)=O UEZVMMHDMIWARA-UHFFFAOYSA-N 0.000 description 13
- 238000002835 absorbance Methods 0.000 description 13
- 238000000034 method Methods 0.000 description 12
- 239000012153 distilled water Substances 0.000 description 10
- 239000012086 standard solution Substances 0.000 description 10
- 239000003153 chemical reaction reagent Substances 0.000 description 9
- 235000019441 ethanol Nutrition 0.000 description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 8
- 238000011088 calibration curve Methods 0.000 description 7
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 6
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000011550 stock solution Substances 0.000 description 6
- 239000012085 test solution Substances 0.000 description 6
- 239000000284 extract Substances 0.000 description 5
- 238000009616 inductively coupled plasma Methods 0.000 description 5
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical compound [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 description 5
- 229910021642 ultra pure water Inorganic materials 0.000 description 5
- 239000012498 ultrapure water Substances 0.000 description 5
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 description 4
- 240000004160 Capsicum annuum Species 0.000 description 4
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 4
- 229930003268 Vitamin C Natural products 0.000 description 4
- 229960005070 ascorbic acid Drugs 0.000 description 4
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 4
- 239000010931 gold Substances 0.000 description 4
- 229910052737 gold Inorganic materials 0.000 description 4
- 230000001678 irradiating effect Effects 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 235000015067 sauces Nutrition 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 description 4
- 238000001228 spectrum Methods 0.000 description 4
- 235000019154 vitamin C Nutrition 0.000 description 4
- 239000011718 vitamin C Substances 0.000 description 4
- GMGIWEZSKCNYSW-UHFFFAOYSA-N 2-(3,4-dihydroxyphenyl)-3,5,7-trihydroxychromen-4-one;dihydrate Chemical compound O.O.C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 GMGIWEZSKCNYSW-UHFFFAOYSA-N 0.000 description 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 206010028980 Neoplasm Diseases 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 229910052786 argon Inorganic materials 0.000 description 3
- 235000010323 ascorbic acid Nutrition 0.000 description 3
- 239000011668 ascorbic acid Substances 0.000 description 3
- 235000012000 cholesterol Nutrition 0.000 description 3
- 229940079593 drug Drugs 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 239000003925 fat Substances 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 210000004209 hair Anatomy 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 230000001766 physiological effect Effects 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000006228 supernatant Substances 0.000 description 3
- TUSDEZXZIZRFGC-UHFFFAOYSA-N 1-O-galloyl-3,6-(R)-HHDP-beta-D-glucose Natural products OC1C(O2)COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC1C(O)C2OC(=O)C1=CC(O)=C(O)C(O)=C1 TUSDEZXZIZRFGC-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 239000001263 FEMA 3042 Substances 0.000 description 2
- 102000003820 Lipoxygenases Human genes 0.000 description 2
- 108090000128 Lipoxygenases Proteins 0.000 description 2
- LRBQNJMCXXYXIU-PPKXGCFTSA-N Penta-digallate-beta-D-glucose Natural products OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-PPKXGCFTSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 102000004005 Prostaglandin-endoperoxide synthases Human genes 0.000 description 2
- 108090000459 Prostaglandin-endoperoxide synthases Proteins 0.000 description 2
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 2
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- JLDSOYXADOWAKB-UHFFFAOYSA-N aluminium nitrate Chemical compound [Al+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O JLDSOYXADOWAKB-UHFFFAOYSA-N 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 201000011510 cancer Diseases 0.000 description 2
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 235000011194 food seasoning agent Nutrition 0.000 description 2
- RWSXRVCMGQZWBV-WDSKDSINSA-N glutathione Chemical compound OC(=O)[C@@H](N)CCC(=O)N[C@@H](CS)C(=O)NCC(O)=O RWSXRVCMGQZWBV-WDSKDSINSA-N 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- DHRLEVQXOMLTIM-UHFFFAOYSA-N phosphoric acid;trioxomolybdenum Chemical compound O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.OP(O)(O)=O DHRLEVQXOMLTIM-UHFFFAOYSA-N 0.000 description 2
- IYDGMDWEHDFVQI-UHFFFAOYSA-N phosphoric acid;trioxotungsten Chemical compound O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.OP(O)(O)=O IYDGMDWEHDFVQI-UHFFFAOYSA-N 0.000 description 2
- 235000011056 potassium acetate Nutrition 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000003672 processing method Methods 0.000 description 2
- 235000005875 quercetin Nutrition 0.000 description 2
- 229960001285 quercetin Drugs 0.000 description 2
- LRBQNJMCXXYXIU-NRMVVENXSA-N tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 2
- 229940033123 tannic acid Drugs 0.000 description 2
- 235000015523 tannic acid Nutrition 0.000 description 2
- 229920002258 tannic acid Polymers 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- CWVRJTMFETXNAD-FWCWNIRPSA-N 3-O-Caffeoylquinic acid Natural products O[C@H]1[C@@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-FWCWNIRPSA-N 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 208000005623 Carcinogenesis Diseases 0.000 description 1
- 206010008190 Cerebrovascular accident Diseases 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 235000016623 Fragaria vesca Nutrition 0.000 description 1
- 240000009088 Fragaria x ananassa Species 0.000 description 1
- 235000011363 Fragaria x ananassa Nutrition 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 108010024636 Glutathione Proteins 0.000 description 1
- 102000005720 Glutathione transferase Human genes 0.000 description 1
- 108010070675 Glutathione transferase Proteins 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 208000031226 Hyperlipidaemia Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 206010021703 Indifference Diseases 0.000 description 1
- 239000002211 L-ascorbic acid Substances 0.000 description 1
- 235000000069 L-ascorbic acid Nutrition 0.000 description 1
- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 240000007263 Pinus koraiensis Species 0.000 description 1
- 235000011615 Pinus koraiensis Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241000241413 Propolis Species 0.000 description 1
- CVQUWLDCFXOXEN-UHFFFAOYSA-N Pyran-4-one Chemical group O=C1C=COC=C1 CVQUWLDCFXOXEN-UHFFFAOYSA-N 0.000 description 1
- 208000034189 Sclerosis Diseases 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 244000061458 Solanum melongena Species 0.000 description 1
- 235000002597 Solanum melongena Nutrition 0.000 description 1
- 208000006011 Stroke Diseases 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 244000299461 Theobroma cacao Species 0.000 description 1
- 235000009470 Theobroma cacao Nutrition 0.000 description 1
- 102000004357 Transferases Human genes 0.000 description 1
- 108090000992 Transferases Proteins 0.000 description 1
- 240000001417 Vigna umbellata Species 0.000 description 1
- 235000011453 Vigna umbellata Nutrition 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 208000007502 anemia Diseases 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 229930014669 anthocyanidin Natural products 0.000 description 1
- 150000001452 anthocyanidin derivatives Chemical class 0.000 description 1
- 235000008758 anthocyanidins Nutrition 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000003266 anti-allergic effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 210000001367 artery Anatomy 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 235000015179 biltong Nutrition 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 210000004958 brain cell Anatomy 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 125000001246 bromo group Chemical class Br* 0.000 description 1
- 239000007853 buffer solution Substances 0.000 description 1
- 230000036952 cancer formation Effects 0.000 description 1
- 231100000504 carcinogenesis Toxicity 0.000 description 1
- 230000003130 cardiopathic effect Effects 0.000 description 1
- 150000001765 catechin Chemical class 0.000 description 1
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 1
- 235000005487 catechin Nutrition 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 229940074393 chlorogenic acid Drugs 0.000 description 1
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 description 1
- FFQSDFBBSXGVKF-KHSQJDLVSA-N chlorogenic acid Natural products O[C@@H]1C[C@](O)(C[C@@H](CC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O FFQSDFBBSXGVKF-KHSQJDLVSA-N 0.000 description 1
- 235000001368 chlorogenic acid Nutrition 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- BMRSEYFENKXDIS-KLZCAUPSSA-N cis-3-O-p-coumaroylquinic acid Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)cc2)[C@@H]1O)C(=O)O BMRSEYFENKXDIS-KLZCAUPSSA-N 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000002532 enzyme inhibitor Substances 0.000 description 1
- 108010017796 epoxidase Proteins 0.000 description 1
- 238000012851 eutrophication Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- HVQAJTFOCKOKIN-UHFFFAOYSA-N flavonol Natural products O1C2=CC=CC=C2C(=O)C(O)=C1C1=CC=CC=C1 HVQAJTFOCKOKIN-UHFFFAOYSA-N 0.000 description 1
- 150000007946 flavonol Chemical class 0.000 description 1
- 235000011957 flavonols Nutrition 0.000 description 1
- 230000009246 food effect Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 239000011491 glass wool Substances 0.000 description 1
- 229960003180 glutathione Drugs 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 208000019622 heart disease Diseases 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 238000002354 inductively-coupled plasma atomic emission spectroscopy Methods 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000006193 liquid solution Substances 0.000 description 1
- INHCSSUBVCNVSK-UHFFFAOYSA-L lithium sulfate Inorganic materials [Li+].[Li+].[O-]S([O-])(=O)=O INHCSSUBVCNVSK-UHFFFAOYSA-L 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000011490 mineral wool Substances 0.000 description 1
- VLAPMBHFAWRUQP-UHFFFAOYSA-L molybdic acid Chemical compound O[Mo](O)(=O)=O VLAPMBHFAWRUQP-UHFFFAOYSA-L 0.000 description 1
- 229910000402 monopotassium phosphate Inorganic materials 0.000 description 1
- 235000019796 monopotassium phosphate Nutrition 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 230000008557 oxygen metabolism Effects 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 235000017807 phytochemicals Nutrition 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229930000223 plant secondary metabolite Natural products 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- -1 polyphenol compound Chemical class 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 229940069949 propolis Drugs 0.000 description 1
- 150000003180 prostaglandins Chemical class 0.000 description 1
- 235000020095 red wine Nutrition 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 230000036560 skin regeneration Effects 0.000 description 1
- XMVONEAAOPAGAO-UHFFFAOYSA-N sodium tungstate Chemical compound [Na+].[Na+].[O-][W]([O-])(=O)=O XMVONEAAOPAGAO-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000012128 staining reagent Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- RBTVSNLYYIMMKS-UHFFFAOYSA-N tert-butyl 3-aminoazetidine-1-carboxylate;hydrochloride Chemical compound Cl.CC(C)(C)OC(=O)N1CC(N)C1 RBTVSNLYYIMMKS-UHFFFAOYSA-N 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 239000002676 xenobiotic agent Substances 0.000 description 1
- 230000002034 xenobiotic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/428—Addition of flavours, spices, colours, amino acids or their salts, peptides, vitamins, yeast extract or autolysate, nucleic acid or derivatives, organic acidifying agents or their salts or acidogens, sweeteners, e.g. sugars or sugar alcohols; Addition of alcohol-containing products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
- A23L5/36—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using irradiation with frequencies of more than 10 MHz
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/50—Concentrating, enriching or enhancing in functional factors
Abstract
本发明提供一种含有松叶有效成分的营养黄花鱼干的制造方法及黄花鱼干，根据本发明的含松叶成分的黄花鱼干的制造方法包括如下步骤：准备小黄鱼、去除卤水2至5年而得到的日晒盐、生松叶及松叶粉；向所述小黄鱼添加所述日晒盐、生松叶及松叶粉；向添加了日晒盐、生松叶及松叶粉的所述小黄鱼的两面分别照射一次100至200分钟的具有2至20微米的波长的远红外线，从而使选自类黄酮或多酚的松叶的有效成分渗透至小黄鱼；使照射了远红外线的小黄鱼熟化；用盐水清洗熟化的小黄鱼；以及干燥清洗后的小黄鱼。根据所述制造方法，通过将类黄酮或多酚等松叶的有效成分充分包含，可以制造提高营养价值及功能性的黄花鱼干。
Description
技术领域
本发明涉及一种含松叶有效成分的含松叶成分的黄花鱼干的制造方法及据此制造的含松叶成分的黄花鱼干。
背景技术
通常，黄花鱼干是在节日中作为高档礼品而流通的高价水产，并且为了黄花鱼干的大众化及高营养化而探索了多种加工方法。具体地，例如，韩国授权专利第1996-16571号中公开了如下的制造辣椒酱黄花鱼干的方法：将小黄鱼干浸泡在辣椒酱而使辣椒酱通过渗透压作用而替代黄花鱼干体内的脂肪，并通过使辣椒酱渗透而表现出特有的味道。韩国授权专利第10-202300号中公开了即时烹饪式熏制黄花鱼干的烹饪方法。并且，韩国授权专利第10-265297号中公开了以如下工序执行的制造蒸黄花鱼干的方法：将干燥的黄花鱼干冷冻后解冻，并蒸制后立即急速冷却，然后分离黄花鱼干肉而选择性地进行调味处理，然后进行干燥而真空包装，并再次冷冻。韩国公开专利第2001-57544号中公开了保管容易且经过卫生的调味处理的新的调味黄花鱼干的制造方法。韩国公开专利第1998-43081号中公开了利用生物能量金字塔的生物黄花鱼干的制造方法。上述的黄花鱼干的制造方法分别具有不同的优点，但是为了黄花鱼干的大众化需要探索特性化的多样的加工方法，与此同时，对于如下技术的需求也在增加：使黄花鱼干包含食物等天然药材中所包含的有效成分，从而能够制造更具营养价值的黄花鱼干。
另外，由于长时间生吃松叶会不老且身体变轻、充满力量、白发变黑、耐寒和耐饿，因此从以前开始松叶称为神仙食品。在东医宝鉴中记载为，松叶被用作调理风湿疮(即由于湿气导致的关节麻或疼的疾病)、生发、舒缓五脏六腑，且作为谷物的替换物而使用。松叶含有大量的不饱和脂肪酸，因此阻挡胆固醇的堆积并防止动脉硬化。并且，扩张末梢血管而促进血液循环，从而提高脑细胞功能，除此之外，有助于高血压、糖尿病、心脏病、中风、贫血以及毒品、尼古丁解毒、去除有害的氧代谢物等。
因此，本发明的发明人在研究含松叶有效成分的黄花鱼干的制造方法的过程中，确认了在特定条件下制造黄花鱼干的情况下，不用单独提取松叶也可以使松叶的有效成分渗透至黄花鱼干，从而完成了本发明。
[现有技术文献]
[专利文献]
(专利文献1)韩国公开专利第10-2004-0036854号(2004.05.03)
发明内容
本发明的目的在于提供含松叶有效成分的营养黄花鱼干的制造方法。
本发明的另一目的在于提供含松叶有效成分的营养黄花鱼干。
为了实现上述目的，本发明提供如下的含松叶成分的黄花鱼干的制造方法，准备小黄鱼、去除卤水2至5年而得到的日晒盐、生松叶及松叶粉；向所述小黄鱼添加所述日晒盐、生松叶及松叶粉；向添加了日晒盐、生松叶及松叶粉的所述小黄鱼的两面分别照射一次100至200分钟的具有2至20微米的波长的远红外线，从而使选自类黄酮或多酚的松叶的有效成分渗透至小黄鱼；使照射了远红外线的小黄鱼熟化；用盐水清洗熟化的小黄鱼；以及干燥清洗后的小黄鱼。
为了实现上述目的，本发明提供通过上述制造方法制造的含松叶成分的黄花鱼干。
本发明涉及一种制造含松叶有效成分的营养黄花鱼干的方法，以往尝试了添加松叶粉或松叶液而使松叶的成分渗透至黄花鱼干内，但是上述成分不易渗透。但是，如本发明，通过在盐渍小黄鱼的步骤中照射远红外线，能够使松叶的有效成分容易渗透至黄花鱼干内，因此根据本发明的制造方法可以制造含有类黄酮及多酚而能够表现出抗氧化效果等多样的生理活性的高营养黄花鱼干。
附图说明
图1是示出根据本发明的含松叶成分的黄花鱼干的制造方法的流程图。
具体实施方式
以下，对本发明进行更详细的说明。
本发明提供一种含松叶成分的黄花鱼干的制造方法，其包括如下步骤：准备韩国产小黄鱼、2至5年内去除卤水而得到的日晒盐、生松叶及松叶粉；向所述小黄鱼添加所述日晒盐、生松叶及松叶粉；向添加了日晒盐、生松叶及松叶粉的所述小黄鱼照射远红外线而使松叶的有效成分渗透至小黄鱼；使照射了远红外线的小黄鱼熟化；用盐水清洗熟化的小黄鱼；以及干燥清洗后的小黄鱼。
优选地，所述日晒盐可以是去除卤水3年而得到的日晒盐，所述生松叶及松叶粉可以直接制作，也可以使用市销的产品。
所述生松叶及松叶粉可以相对于100重量份的小黄鱼而添加50重量份至100重量份，如果在上述含量范围内添加，则可以使松叶的有效成分充分渗透至黄花鱼干，因此优选。
并且，在照射所述远红外线的步骤中，可以将波长为2微米至20微米的远红外线向小黄鱼照射总共200至400分钟，更优选地，将波长为2微米至20微米的远红外线向小黄鱼照射2次，每次100至200分钟。
即，对小黄鱼的两面，每次分别照射波长为2微米至20微米的远红外线100至200分钟，从而向小黄鱼的两面总共照射200至400分钟的远红外线。如上所述，在将波长为2微米至20微米的远红外线照射所述时间范围的情况下，可以最大化渗透至黄花鱼干的松叶的有效成分，因此优选。
此时，所述松叶的有效成分可以是类黄酮或者多酚，根据本发明的一实施例，通过本发明的制造方法制造的黄花鱼干相比于普通的黄花鱼干含有2倍以上的类黄酮，并且含有未在普通黄花鱼干中包含的多酚。
因此，根据本发明的制造方法而制造的所述黄花鱼干可以表现出抗氧化效果，除此之外也可以表现出类黄酮或多酚所表现的多样的生理活性，因此，根据本发明可以制造提高营养性及功能性的营养黄花鱼干。
进而，本发明提供通过上述制造方法制造的含松叶成分的黄花鱼干。
如上所述，当制造所述黄花鱼干时，添加生松叶及松叶粉后将特定波长的远红外线照射特定时间，因此可以使生松叶及松叶粉中的松叶的有效成分充分地渗透至黄花鱼干，因此所述黄花鱼干含有大量的类黄酮或多酚而能够表现出多样的生理活性。
以下，为了有助于理解本发明而通过举出实施例进行详细说明。但是，下述的实施例为了向本领域中具有基本知识的人员更完整地说明本发明而提供，且仅举例示出本发明的内容，因此本发明的范围不限于以下实施例。
<实施例1>营养黄花鱼干的制造
本发明中公开的制造方法如图1所示。即，如图1所示，从韩国法圣浦水协购买了韩国产小黄鱼，并从韩国盐山日晒盐购买了去除卤水3年而得到的日晒盐，并在韩国松树造景农场采集了生松叶而准备，并购买了松叶粉(图1的S100)。此后，向所述小黄鱼添加所述日晒盐以及小黄鱼比重的50％(相对于小黄鱼100重量份的50重量份)的生松叶和松叶粉(图1的S110)，并向所述小黄鱼照射300分钟的2至20微米的远红外线(图1的S120)，从而使松叶的有效成分渗透至小黄鱼。即，向小黄鱼的每一面照射150分钟的远红外线而对两个面总共照射了300分钟的远红外线。
此后，使照射了远红外线的小黄鱼熟化30分钟(图1的S130)，并将熟化的小黄鱼用盐水清洗(图1的S140)以及干燥(图1的S150)而制作了含松叶成分的黄花鱼干。
<实验例1>营养黄花鱼干的营养成分分析
(1)试料的预处理
利用在所述实施例1中制造的黄花鱼干而准备了之后要使用的试料。具体地，先用肉眼确认试料的状态有无异常，然后仅将黄花鱼干的鱼肉分离，并利用粉碎用混合器(HMF3250S，韩日电器)及均质器(AESAP 1100，AES)而进行均质化。将如上所述地均质化的试料以1×2进行2等分，并分成小份而分别用于两次的实验(样品编号1)。此时，作为对照试料使用普通黄花鱼干(购自海上黄花鱼干)(样品编号2)，并以相同方法进行了两次的实验。
(2)确认维生素C的含量
为了确认所述实施例1中制造的本发明的含松叶成分黄花鱼干的成分差异，首先分析了维生素C的含量。首先，利用作为紫外检测器的Waters 996PDADetector执行了液相色谱，并作为试剂及试液而制造了10％偏磷酸溶液、5％偏磷酸溶液、标准溶液。偏磷酸具有100％地防止维生素C的氧化的效果，首先将纯度为35％的偏磷酸(制造公司：JUNSEI)28.57g(换算后为纯偏磷酸10g)溶于超纯水(电阻为18.2MΩ以上)而使体积达到100ml，并进行过滤而去除不溶物，从而制造了10％的偏磷酸溶液，将如上所述地制造的10％的偏磷酸溶液再次用超纯水稀释2倍而制造了5％偏磷酸溶液。并且，精确地测量10.0mg的抗坏血酸(制造公司：Sigma Aldrich)而溶于5％偏磷酸溶液而使体积达到100ml，然后用超声波均质化，然后为了防止抗坏血酸的氧化而放入棕色量瓶而用作标准原液(100ppm)。此时，标准原液的浓度根据13.8mg X 99.9％X 1,999μg/mg/100ml式而成为137.862μg/ml。此后，将5％偏磷酸溶液投入标准原液而稀释成所要浓度而得到了用于实验的标准溶液，此时，各标准溶液的浓度为2.7572μg/ml、6.8931μg/ml、13.7862μg/ml。
此后，将在所述实施例1中制造的黄花鱼干预定量(在维生素C含量为50mg/100g以上的情况下为2g左右，在维生素C含量为10～50mg/100g的情况下为5～10g左右)准确称重之后添加同量的10％的偏磷酸溶液而使其悬浊10分钟，然后投入适量的5％的偏磷酸而使其悬浊，且为了提取维生素C而利用超声波进行均质化30分钟。将如上所述地均质化的待检物移至100ml量瓶，并用少量的5％偏磷酸溶液清洗容器后合并到量瓶，使体积达到100ml。此后，在3,000rpm下利用离心分离器(韩日科学MF-300)进行10-15分钟的离心分离而提取上清液，并用5％的偏磷酸溶液适当地稀释而将其中的50ml用作试验溶液。
在进行液相色谱时，分别将试验溶液及标准溶液注入10μl，作为反相柱使用Jascopack Fine Sil-NH2(除此之外，可以使用Lichrosorb NH2，并改变条件而使用ZipaxSAX、Vydac SAX.Partisil-10SAX、μ-Bondapak C18、μ-Bondapak/CN、Pormaphase CPS等)，并作为移动相使用了0.05M KH2PO4/乙腈(60:40)，并作为缓冲溶液和离子配对试剂而使用磷酸二氢钾。流速为1.9ml/分，且在254nm波长下使用紫外(UV)检测器进行了测量。
求得如上所述地执行液相色谱后后得到的峰值的宽度或高度而制作校准曲线(Calibration Curve)，然后求得试验溶液的维生素C的浓度(μg/mL)，并如下<式1>地计算了待检物中的抗坏血酸的含量(mg/100g)。在换算为L-抗坏血酸钠的情况下，将L-抗坏血酸的量乘以系数1.125。
<式1>
(S：试验溶液中的抗坏血酸的浓度(μg/ml)，a：试验溶液的总量(ml)，b：试验溶液的稀释倍数)
其结果，可以得到如下<表1>所示的结果。
[表1]
具体地，将实验试料(样品编号1)作为对象的第一次实验(1-1)及第二次实验(1-2)中都表现出0mg/100g的含量，且将对照试料(样品编号2)作为对象的第一次实验(2-1)及第二次实验(2-2)中也都表现出0mg/100g的含量。即，实验试料与对照试料在维生素C的含量方面无差异。
(3)铁成分含量分析
将上文中准备的试料提取到200～300ml分解烧瓶之后，加入硝酸溶液(德山化学)5ml而缓慢地较弱地加热，并在最初的剧烈的反应结束之后再次升温而加热。即，加热至硝酸挥发而使内容物几乎干燥，此后添加10ml的硝酸溶液和70％的过盐酸(大井化金)10ml而调节加热，并加热至固形物完全溶解且溶液变成几乎无色，由此进行了分解。完成分解之后，进行冷却并用少量的水进行稀释，然后将溶液移至清洗后的直径为9cm的瓷蒸发皿而进行蒸发干燥而使过盐酸蒸发。将大约10ml的盐酸溶液加入残留物后用等量的水进行稀释，并在水浴上加热而完全融化，然后移至100ml的量瓶而加入水，并使总量为100ml而用作试验溶液。
此后，利用电感耦合等离子体法(inductively coupled plasma,ICP)将所述试验溶液定量。ICP是如下方法：利用电感耦合方法向氩气施加高频而放电，从而得到氩等离子体，将试验溶液注入所得到的氩等离子体而测量目标元素的原子线及离子线的发光光度或质量值而计算试验溶液中的目标元素的浓度。本实验中，使用了ICP-AES(EPCTRO BLUE,SPECTRO)，并将铁1ppm标准溶液(KANTO)、将其稀释而制作的铁1μg/ml溶液、所述试验溶液和空白试验溶液注入电感耦合等离子体而计算了试验溶液的浓度。
此时，标准溶液的校准曲线如下<表2>所示，并以如下<式2>中公开的内容计算了试验溶液的铁成分含量。
[表2]
| 浓度(ug/ml) | 吸光度 |
| 0.10 | 11162.000 |
| 0.50 | 44464.000 |
| 1.00 | 84676.000 |
<式2>
(S：试验溶液中的铁成分的浓度(μg/ml)，a：试验溶液的总量(ml)，b：试验溶液的稀释倍数)
其结果，如下<表3>所示，对实验试料的第一次实验(1-1)中，铁成分的测量值为6.52mg/100g，第二次实验(1-2)中，铁成分的测量值为6.36mg/100g，因此平均含有6.44mg/100g的铁成分。即，相比于对照试料而没有表现出有意义的区别。
[表3]
(4)总类黄酮含量分析
类黄酮为植物界中广泛分布的多酚化合物的一种，并且为天然色素，并具有γ-吡喃酮(γ-pyrone)结构[C6(benzene A ring)-C3-C6benzene B ring]，尤其在植物的叶子、开花组织及花粉等中存在较多。类黄酮具有抗炎症、抗过敏及抗氧化作用等多种生理学、药理学作用(Havesteen B.,Biochem.Pharmacol.,32:1141-1148,1983；Fukuzawa andTakaishi,J.Act.Oxy.Free Rad.,1:55-69,1990)，并且最近发现了可以通过摄取类黄酮含量较高的多种疏果类而降低慢性癌及心脏病的发病的事实(Yoshida M.et al.,FEBSLetter 260:10-13,1990；Hertog et al.,J.Agric Food Chem.,40:2379-2383,1992a；Verma A.K.et al.,Cancer Res.,48:5754-5758,1998)。并且，在报告中提到类黄酮是与肿瘤产生具有较大的关联的前列腺素合成酶(prostaglandin synthase)、脂肪氧合酶(lipoxygenase)及环氧酶(cyclooxygenas)等酶抑制剂(Bauman et al.,Prostaglandin20:627-639,1980；Yoshimoto et al.,Biochem.Biphys.Res.Commun.,116:612-618,1983；Moroney et al.,J.Pharmacol.Phamacodyn.,278:4-12,1988；Laughton et al.,Biochem.Pharmacol.,42:1673-1681,1991)，不仅如此，能够使抗老化物质的L-抗坏血酸(L-ascorbic acid)再生，或者诱导属于无毒化酶的谷胱甘肽s-转移酶(glutathione S-transferase)等酶(Smith and Yang,Effect of Food Phytochemicals on XenobioticMetabolism and Tumorigenesis,ACS,1994)。
这种类黄酮系物质在415nm具有最大吸收波长。因此，本发明中使作为代表性的类黄酮系物质(Flavonol)的槲皮素(quercetin)与铝结合而呈金色，从而测量吸光度并基于此进行了定量。更为具体地，作为标准物质使用了槲皮素二水合物(纯度97.02％，制造公司：HWI)，如果使槲皮素二水合物与铝进行反应，则与Al3+结合并呈金色。作为普通试剂使用了乙醇(德山化学)，作为普通试液使用了10％的硝酸铝溶液(Aluminium nitrate)及1M醋酸钾溶液(CH3COOK)。此时，准确地称重17.6g的硝酸铝9水合物(Al(NO3)39H2O；YAKURI)而用蒸馏水溶解而达到100ml，并准确地称重9.815g的醋酸钾(JUNSEI)而溶解于蒸馏水而达到100ml，从而作为各个普通试液使用。并且，使用了80％乙醇(20％的水使用超纯水)，90％乙醇(10％的水使用超纯水)。
此后，通过如下的方法调制了试验溶液。首先，称量上文中准备的黄花鱼干试料60～100mg，并用分液器滴加90％乙醇20ml而溶解。对于颗粒状及片状的产品，将试料充分破碎而使用，并对于包含明胶等的产品，将内容物取出而使用。此后，进行离心分离(3000rpm，10分钟)而提取上清液，并对残留物添加80％乙醇8ml而萃取3次。将所述上清液和萃取3次的萃取物集中在一处后使用80％乙醇而使体积达到50ml，从而制造了用作试验溶液的蜂胶萃取物。
标准溶液通过以下方法制造：将槲皮素二水合物以无水物混合而准确称重50mg而放入50ml体积的烧瓶，并将乙醇填充至标线而制造了标准原液。此后，添加乙醇而稀释100倍(0.01mg/ml)、20倍(0.05mg/ml)、10倍(0.1mg/ml)而制作了标准溶液，此时标准原液的浓度为0.8704mg/ml。
此后，分别将0.5ml的标准溶液及试验溶液用作对照液和试验液而取到两个试管，并在此添加乙醇1.5ml，10％硝酸铝溶液0.1ml，1M乙酸钾溶液0.1ml、蒸馏水2.8ml而充分搅拌。在按各浓度进行标准物质及试料的空白试验中，代替10％硝酸铝而添加0.1ml蒸馏水。将该试料在室温下停放40分钟后，对液层使用10mm单元(cell)并将水作为对照液而在415nm下测量了吸光度。
此时，按标准物质的浓度测量的吸光度与按浓度测量的空白试验的吸光度之差而如下<表4>所示地制造了标准物质的校准曲线。
[表4]
将试料的吸光度与试料的空白试验吸光度之差应用于校准曲线，然后用下述<式3>中示出的方法测量了类黄酮的总含量(mg/g)。
<式3>
类黄酮总含量(mg/g)＝C×a/S
(C：试验溶液中的类黄酮总含量(mg/ml或ug/ml)、S：试料提取量(g或ml)、a：试验溶液的总量(ml)＝30ml)
其结果，如下<表5>所示，在根据本发明的黄花鱼干试料的第一次实验(1-1)中，类黄酮的总含量为2.70mg/100g，第二次实验(1-2)中，类黄酮的总含量为2.71ml/100g。这种数值为将对照试料作为对象的两次实验(2-1,2-2)中分别测量的1.01mg/100g及1.00mg/100g的含量数值的大约2倍以上，因此可知，通过使根据本发明的黄花鱼干含有松叶有效成分，从而以高浓度包含能够以高浓度包含表现出抗氧化活性的物质。
[表5]
(5)多酚总含量分析
多酚表示苯环(C6H6)的氢中的一个被氢氧基(OH)取代的物质，具有上述结构的化合物在自然界中大量存在。被包含于绿茶的儿茶酚(catechins)、被包含于咖啡的绿原酸、诸如草莓或茄子、葡萄、黑豆、红豆等红色或紫色的花青素类色素等都是多酚类化合物。除此之外，多酚化合物被包含于蔬菜、水果、可可、红葡萄酒等多种。多酚类具有防止氧化的作用，即抗氧化功能。最近，多酚类受瞩目的原因为，该功能在生物体内也作为抗氧化剂而发挥作用，从而有望有助于维持健康、预防疾病等。并且，多酚类阻止胆固醇被消化管吸收，因此还起到降低血液中的胆固醇数值的作用。与此同时，被认为是去除皮肤老化的主要原因而使皮肤再生的最有效的成分。不仅如此，所述多酚能够改善女性的褐斑，并抑制中性脂肪，且已知在预防肥胖或高脂血症时具有卓越的效果。
本实验中，为了计算根据本发明的黄花鱼干的多酚总含量，将试料溶解于蒸馏水，并用超声波提取，然后与着色试剂进行反应而使用分光光度计进行定量。更为具体地，作为标准物质使用了单宁酸(Tannin acid；Sigma-Aldrich)，且作为普通试剂使用了佛林顿尼斯试剂(Folin-Denis reagent；Sigma-Aldrich)及蒸馏水(利用超纯水制造装置(NEXPOWER 2000；Human Corporation)制造)。所述Folin-Denis试剂通过如下方法制造：将钼酸钠25g、钨酸钠100g与85％磷酸50ml、浓盐酸100ml、水700ml一起加热10小时而进行回流，并继续添硫酸锂150g、水50ml、几滴溴后，加热15分钟而去除多余的溴，然后加水而稀释为1L。并且所述Folin-Denis以混合有磷钼酸(phosphomolybdic acid)和磷钨酸(phosphotungstic acid)的状态呈黄色。并且，作为试液使用35％碳酸钠溶液(Sodiumcarbonate)，此时，精确地称重35g的碳酸钠(大井化金)而投入蒸馏水100ml，并在70℃下溶解而放置在常温下，然后当在过饱和的溶液中生成Na2CO3·10H2O结晶时，用玻璃棉(glasswool)过滤。
精确地称量单宁酸10mg而放入100ml体积的烧瓶，并将蒸馏水填充至标线而制作了标准原液，利用蒸馏水稀释至适当浓度后用作标准溶液。此时，标准原液的浓度为103μg/ml。为了制造试验溶液，称量100mg的试料而装在100ml体积烧瓶，然后投入蒸馏水而达到标线，然后进行超声波处理而进行了溶解。
此后，将蒸馏水7.5ml投入到与要实验的试料的数量对应的数量的试管，然后分别将1ml的标准溶液及试验溶液投入所述试管，并依次添加Folin-Denis试剂0.5ml、碳酸钠1ml而进行了混合。将如上所述的混合有Folin-Denis试剂及碳酸钠的试管置于暗处1小时，然后在760nm下测量了吸光度。
此时，利用按标准物质的浓度测量的吸光度和各空白试验的吸光度之差制造了标准物质的校准曲线，且如下<表6>所示。
[表6]
| 浓度(ug/ml) | 吸光度 |
| 51.50 | 0.485 |
| 25.75 | 0.258 |
| 10.30 | 0.106 |
| 5.15 | 0.063 |
| 1.03 | 0.020 |
并且，将测量的试料的吸光度与试料的空白试验的吸光度之差应用于校准曲线，然后如下述<式4>所示地测量了多酚总含量(mg/g)。
<式4>
(A：试验溶液的总量(ml)、B：稀释倍数、C：试验溶液中的多酚总浓度(mg/ml)、D：试料提取量(g或ml))
其结果，如下述<表7>所示，可知不同于在两次实验中都完全没有测量出多酚的对照试料(2-1,2-2)，根据本发明的黄花鱼干试料的第一次实验(1-1)及第二次实验(1-2)中分别含有4.18mg/100g及4.21mg/100g的多酚。
[表7]
因此，考虑到所有上述实验结果，根据本发明的黄花鱼干通过照射远红外线而包含松叶中含有的类黄酮及多酚，如上所述，除了黄花鱼干本身的营养成分以外，还包括松叶的有效成分，因此可以作为提高了营养价值及功能性的黄花鱼干而使用。
以上详细记载了本发明的内容的特定部分，对于本领域中具有基本知识的人而言，上述的具体技术仅仅是优选的实施形态，需要明确的是，本发明不限于上述记载。即，本发明的实质范围根据权利要求及其等价物定义。
Claims (3)
1.一种含松叶成分的黄花鱼干的制造方法，包括如下步骤：
准备小黄鱼、去除卤水2至5年而得到的日晒盐、生松叶及松叶粉；
向所述小黄鱼添加所述日晒盐、生松叶及松叶粉；
向添加了日晒盐、生松叶及松叶粉的所述小黄鱼的两面分别照射一次100至200分钟的具有2至20微米的波长的远红外线，从而使选自类黄酮或多酚的松叶的有效成分渗透至小黄鱼；
使照射了远红外线的小黄鱼熟化；
用盐水清洗熟化的小黄鱼；以及
干燥清洗后的小黄鱼。
2.如权利要求1所述的含松叶成分的黄花鱼干的制造方法，其中，
所述黄花鱼干表现出抗氧化效果。
3.一种含松叶成分的黄花鱼干，通过权利要求1所述的制造方法而制造，且包括选自类黄酮或多酚的松叶的有效成分。
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR10-2017-0050184 | 2017-04-19 | ||
| KR1020170050184A KR101771435B1 (ko) | 2017-04-19 | 2017-04-19 | 솔잎의 유효성분을 함유하는 영양 굴비의 제조방법 및 이로 제조된 영양 굴비 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108740811A true CN108740811A (zh) | 2018-11-06 |
Family
ID=59759899
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810355496.2A Pending CN108740811A (zh) | 2017-04-19 | 2018-04-19 | 含松叶有效成分的营养黄花鱼干的制造方法及黄花鱼干 |
Country Status (2)
| Country | Link |
|---|---|
| KR (1) | KR101771435B1 (zh) |
| CN (1) | CN108740811A (zh) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102329328B1 (ko) | 2021-02-19 | 2021-11-19 | 이신성 | 인삼을 함유한 굴비 또는 보리굴비의 제조방법 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100454671B1 (ko) * | 2001-11-23 | 2004-11-03 | 최영주 | 천연재료를 함유한 굴비의 가공방법 |
| CN103082371A (zh) * | 2011-10-28 | 2013-05-08 | 周功堂 | 松针银杏系列保健饮料 |
| KR20150068155A (ko) * | 2013-12-11 | 2015-06-19 | 정훈 | 기능성 소금 및 그 제조방법 |
-
2017
- 2017-04-19 KR KR1020170050184A patent/KR101771435B1/ko active IP Right Grant
-
2018
- 2018-04-19 CN CN201810355496.2A patent/CN108740811A/zh active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100454671B1 (ko) * | 2001-11-23 | 2004-11-03 | 최영주 | 천연재료를 함유한 굴비의 가공방법 |
| CN103082371A (zh) * | 2011-10-28 | 2013-05-08 | 周功堂 | 松针银杏系列保健饮料 |
| KR20150068155A (ko) * | 2013-12-11 | 2015-06-19 | 정훈 | 기능성 소금 및 그 제조방법 |
Non-Patent Citations (1)
| Title |
|---|
| 徐敏: "《健康来自你1%的改变》", 30 November 2008, 内蒙古大学出版社 * |
Also Published As
| Publication number | Publication date |
|---|---|
| KR101771435B1 (ko) | 2017-08-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Barreca et al. | Evaluation of the antioxidant and cytoprotective properties of the exotic fruit Annona cherimola Mill.(Annonaceae) | |
| Siracusa et al. | Phenolic composition and antioxidant activity of aqueous infusions from Capparis spinosa L. and Crithmum maritimum L. before and after submission to a two-step in vitro digestion model | |
| Sbrana et al. | Beneficial mycorrhizal symbionts affecting the production of health‐promoting phytochemicals | |
| Kuźma et al. | Optimization of extraction conditions of some polyphenolic compounds from parsley leaves (Petroselinum crispum) | |
| Nath et al. | Phytochemical and proximate analysis of papaya (Carica papaya) leaves | |
| Guglani et al. | In-vitro antioxidant activity, total phenolic, flavonoid and tannin contents in the Ajuga bracteosa wall. ex benth, grown at middle hill climatic condition of western Himalayas | |
| Mohammedi et al. | The effect of solvents and extraction procedure on the recovery of phenolic compounds and the antioxidant capacity of Algerian Bassia muricata L. extracts | |
| CN108740811A (zh) | 含松叶有效成分的营养黄花鱼干的制造方法及黄花鱼干 | |
| Helvacıoğlu et al. | Comparatively investigation of grape molasses produced by conventional and industrial techniques | |
| Kozik et al. | Investigation of antioxidant activity of pomegranate juices by means of electron paramagnetic resonance and UV-Vis spectroscopy | |
| Haq et al. | Elemental analysis of Paeonia emodi and Punica granatum by atomic absorption spectroscopy | |
| Pathak¹ et al. | Pharmacognostical study of Anethum sowa (dill) seed | |
| Jung et al. | Thermal-assisted recovery of antioxidant compounds from Bauhinia forficata leaves: Effect of operational conditions | |
| Ananias | Antioxidant activities, phytochemical, and micro-nutrients analysis of African Moringa (Moringa Ovalifolla) | |
| Sukri | Effect of different types of solvent on extraction of phenolic compounds from Cosmos caudatus | |
| Kandemirli et al. | The investigation of the effect of freezing pretreatment on properties of black garlic produced from Kastamonu garlic | |
| Mirzaei et al. | Hepatoprotective effect and antioxidant activity of aqueous cherry extract on rats | |
| Krishnaveni et al. | Secondary metabolite, antioxidant, phyto nutrient assay of essential oil from dry Coriandrum sativum seed black variety | |
| KR20220077364A (ko) | 귀리로부터 대량의 페놀화합물과 플라보노이드의 추출방법 | |
| Panonnummal et al. | Non alcoholic palm nectar from Cocos nucifera as a promising nutraceutical preparation | |
| Memon et al. | Nutritional Profile and Medicinal Properties of Cucumis melo var Agrestis: A Non-Conventional Vegetable | |
| KR20110134541A (ko) | 원적외선 조사를 이용한 기능성 물질들의 함량이 증가된 산양산삼의 제조방법 | |
| Ma et al. | Quantification and purification of procyanidin B1 from food byproducts | |
| KR100830374B1 (ko) | 항산화 물질 추출방법 | |
| Bou Ajram | Effect of accelerated aging on total phenolic content, antioxidant and anti-diabetic activities of Lebanese homemade pomegranate molasses with and without addition of glutathione |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20181106 |