CN108713560A - A kind of glyphosate herbicidal and preparation method thereof suitable for vegetable field weeds - Google Patents

A kind of glyphosate herbicidal and preparation method thereof suitable for vegetable field weeds Download PDF

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Publication number
CN108713560A
CN108713560A CN201810629344.7A CN201810629344A CN108713560A CN 108713560 A CN108713560 A CN 108713560A CN 201810629344 A CN201810629344 A CN 201810629344A CN 108713560 A CN108713560 A CN 108713560A
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parts
extract
synergist
peet
rhizoma anemarrhenae
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徐益峰
方润
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ANHUI YINONG CHEMICAL Co Ltd
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ANHUI YINONG CHEMICAL Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/30Microbial fungi; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/10Apiaceae or Umbelliferae [Carrot family], e.g. parsley, caraway, dill, lovage, fennel or snakebed
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/22Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/26Meliaceae [Chinaberry or Mahogany family], e.g. mahogany, langsat or neem
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/42Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives

Abstract

The invention discloses a kind of glyphosate herbicidals suitable for vegetable field weeds, are made of the raw material of following parts by weight:35-40 parts of gyphosate solution, 3-5 parts of hyoscyamine, -4 parts of coumarin 1,2-4 parts of Sichuan chinaberry extract, 2-4 parts of bupleurum extract, 1-3 parts of RHIZOMA ANEMARRHENAE with peet extract, 5-10 parts of disk spore bacterium, 1-5 parts of synergist, 3-7 parts of gas-phase silica, 4-6 parts of rosemary oil, 3-5 parts of dispersant, 3-7 parts of diatomite, 2-8 parts of carboxymethyl cellulose, 40-55 parts of deionized water, the herbicide of the present invention, with apparent spread spectrum synergistic effect, there are good safety and activity of weeding, most of grassy weed and broad leaved weeds can be killed, herbicidal effect is enhanced.Herbicide is easy degradation in crop body, and safe, without side-effects, environmental pollution is smaller, and preparation method is reasonable, easy to operate, with short production cycle, and low energy consumption, and quality stability is good, application easy to spread.

Description

A kind of glyphosate herbicidal and preparation method thereof suitable for vegetable field weeds
Technical field
The present invention relates to agriculture field, specifically a kind of glyphosate herbicidal and its preparation side suitable for vegetable field weeds Method.
Background technology
Widely distributed weeds have 30000 kinds in the whole world, different degrees of harm are caused to crop for about 1800 kinds every year, often Crop production reduction is up to 9.7% year caused by Weed infestation.Herbicide refers to that weeds can be made thoroughly or selectively to occur is withered Dead medicament, also known as herbicide, to eliminate or inhibit a substance of plant growth.Common herbicide kind is to organise Object is closed, the ground such as prevention farmland, orchard, floral nursery, grassland and bare place, railway line, river, reservoir, warehouse are can be widely used for The noxious plants such as weeds, miscellaneous filling, miscellaneous tree.Many weeds have been efficiently controlled using herbicide in the last hundred years, but chemical agent It is a large amount of using also having caused a series of problem, the appearance, soil pollution of such as herbicide-resistant weeds plant, water quality are moved back Change and the harm etc. to non-weeds biology (especially people, animal).
The most of vegetable field weeds used at present are mostly type of killing either contact killing type herbicides with highy potent herbicide, Herbicidal effect is limited by the type and weeds type of crops, has greatly affected herbicidal effect.
Invention content
The purpose of the present invention is to provide a kind of glyphosate herbicidal and preparation method thereof suitable for vegetable field weeds, with Solve the problems mentioned above in the background art.
To achieve the above object, the present invention provides the following technical solutions:
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
35-40 parts of gyphosate solution, 3-5 parts of hyoscyamine, -4 parts of coumarin 1,2-4 parts of Sichuan chinaberry extract, radix bupleuri carry Take 2-4 parts of object, 1-3 parts of RHIZOMA ANEMARRHENAE with peet extract, 5-10 parts of disk spore bacterium, 1-5 parts of synergist, 3-7 parts of gas-phase silica, rosemary 4-6 parts oily, 3-5 parts of dispersant, 3-7 parts of diatomite, 2-8 parts of carboxymethyl cellulose, 40-55 parts of deionized water.
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
35 parts of gyphosate solution, 3 parts of hyoscyamine, coumarin 1 part, 2 parts of Sichuan chinaberry extract, bupleurum extract 2 part, mao 1 part of anemarrhena asphodefoides extract, 5 parts of disk spore bacterium, 1 part of synergist, 3 parts of gas-phase silica, 4 parts of rosemary oil, 3 parts of dispersant, diatomite 3 parts, 2 parts of carboxymethyl cellulose, 40 parts of deionized water.
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
40 parts of gyphosate solution, 5 parts of hyoscyamine, 4 parts of cumarin, 4 parts of Sichuan chinaberry extract, bupleurum extract 4 part, mao 3 parts of anemarrhena asphodefoides extract, 10 parts of disk spore bacterium, 5 parts of synergist, 7 parts of gas-phase silica, 6 parts of rosemary oil, 5 parts of dispersant, diatom 7 parts of soil, 8 parts of carboxymethyl cellulose, 55 parts of deionized water.
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
37 parts of gyphosate solution, 4 parts of hyoscyamine, 2.5 parts of cumarin, 3 parts of Sichuan chinaberry extract, 3 parts of bupleurum extract, 2 parts of RHIZOMA ANEMARRHENAE with peet extract, 8 parts of disk spore bacterium, 3 parts of synergist, 5 parts of gas-phase silica, 5 parts of rosemary oil, 4 parts of dispersant, diatom 5 parts of soil, 5 parts of carboxymethyl cellulose, 47 parts of deionized water.
The synergist is saturating agent T, one or more in beneficial agriculture bleeding agent A, B, C, azone.
A kind of preparation method of glyphosate herbicidal suitable for vegetable field weeds, includes the following steps:
(1) raw material in formula is weighed;
(2) preparation of Fructus meliae toosendan, radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract:It takes Fructus meliae toosendan crushed after being dried at coarse powder, Fructus meliae toosendan is added The ethyl alcohol of 6-10 times of coarse powder weight, refluxing extraction 30-50 minutes at 50-60 DEG C of temperature, filters, discards filter residue, what is obtained carries Liquid is taken to carry out flash concentration to the 5-10% of original volume using Reduced Pressure Concentration Device to get melia toosendan under the conditions of 60-70 DEG C Seed extract, same method prepare radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract;
(3) gyphosate solution, synergist, water are added in reaction kettle, are stirred evenly, sequentially add hyoscyamine, Cumarin, Sichuan chinaberry extract, bupleurum extract, RHIZOMA ANEMARRHENAE with peet extract, stir evenly;
(4) reaction kettle is warming up to 50-60 DEG C, sequentially adds disk spore bacterium, synergist, gas-phase silica, rosemary oil, divides Powder, diatomite, carboxymethyl cellulose, high-speed stirred 30 minutes, then stirring at low speed 30 minutes;
(5) it sterilizes, pack.
Compared with prior art, the beneficial effects of the invention are as follows:
Present invention is mainly applied to the rice seedling bed of vegetables, Honda and live streaming weedings, have apparent spread spectrum synergistic effect, have very Good safety and activity of weeding, can kill most of grassy weed and broad leaved weeds, enhance herbicidal effect.This hair Herbicide prepared by bright method is easy degradation in crop body, and safe, without side-effects, environmental pollution is smaller;To having gone out Soil, larger weeds can also be applicable in and have the effect of that applied once prevents and kill off a variety of single, double cotyledon weeds, play reduction and use Dose, times for spraying, the effect for improving environment and food security, meet China Agrochemicals direction.From alkaloids datura The hyoscyamine extracted in seed, if being a kind of castor alkane alkaloid compound, herbicide action period is long, has to grassy weed outstanding Go out except activity.Add Fructus meliae toosendan, radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract, it is significant effect, natural environmental-protective, without any side effects, have The effect of preventing vegetable field a variety of weeds.The preparation method of the present invention is reasonable, and easy to operate, with short production cycle, low energy consumption, is easy to Control, product qualification rate is high, and quality stability is good, application easy to spread.
Specific implementation mode
Embodiment 1
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
35 parts of gyphosate solution, 3 parts of hyoscyamine, coumarin 1 part, 2 parts of Sichuan chinaberry extract, bupleurum extract 2 part, mao 1 part of anemarrhena asphodefoides extract, 5 parts of disk spore bacterium, 1 part of synergist, 3 parts of gas-phase silica, 4 parts of rosemary oil, 3 parts of dispersant, diatomite 3 parts, 2 parts of carboxymethyl cellulose, 40 parts of deionized water.
The synergist is saturating agent T, one or more in beneficial agriculture bleeding agent A, B, C, azone.
A kind of preparation method of glyphosate herbicidal suitable for vegetable field weeds, includes the following steps:
(1) raw material in formula is weighed;
(2) preparation of Fructus meliae toosendan, radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract:It takes Fructus meliae toosendan crushed after being dried at coarse powder, Fructus meliae toosendan is added The ethyl alcohol of 6-10 times of coarse powder weight, refluxing extraction 30-50 minutes at 50-60 DEG C of temperature, filters, discards filter residue, what is obtained carries Liquid is taken to carry out flash concentration to the 5-10% of original volume using Reduced Pressure Concentration Device to get melia toosendan under the conditions of 60-70 DEG C Seed extract, same method prepare radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract;
(3) gyphosate solution, synergist, water are added in reaction kettle, are stirred evenly, sequentially add hyoscyamine, Cumarin, Sichuan chinaberry extract, bupleurum extract, RHIZOMA ANEMARRHENAE with peet extract, stir evenly;
(4) reaction kettle is warming up to 50-60 DEG C, sequentially adds disk spore bacterium, synergist, gas-phase silica, rosemary oil, divides Powder, diatomite, carboxymethyl cellulose, high-speed stirred 30 minutes, then stirring at low speed 30 minutes;
(5) it sterilizes, pack.
Embodiment 2
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
40 parts of gyphosate solution, 5 parts of hyoscyamine, 4 parts of cumarin, 4 parts of Sichuan chinaberry extract, bupleurum extract 4 part, mao 3 parts of anemarrhena asphodefoides extract, 10 parts of disk spore bacterium, 5 parts of synergist, 7 parts of gas-phase silica, 6 parts of rosemary oil, 5 parts of dispersant, diatom 7 parts of soil, 8 parts of carboxymethyl cellulose, 55 parts of deionized water.
The synergist is saturating agent T, one or more in beneficial agriculture bleeding agent A, B, C, azone.
A kind of preparation method of glyphosate herbicidal suitable for vegetable field weeds, includes the following steps:
(1) raw material in formula is weighed;
(2) preparation of Fructus meliae toosendan, radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract:It takes Fructus meliae toosendan crushed after being dried at coarse powder, Fructus meliae toosendan is added The ethyl alcohol of 6-10 times of coarse powder weight, refluxing extraction 30-50 minutes at 50-60 DEG C of temperature, filters, discards filter residue, what is obtained carries Liquid is taken to carry out flash concentration to the 5-10% of original volume using Reduced Pressure Concentration Device to get melia toosendan under the conditions of 60-70 DEG C Seed extract, same method prepare radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract;
(3) gyphosate solution, synergist, water are added in reaction kettle, are stirred evenly, sequentially add hyoscyamine, Cumarin, Sichuan chinaberry extract, bupleurum extract, RHIZOMA ANEMARRHENAE with peet extract, stir evenly;
(4) reaction kettle is warming up to 50-60 DEG C, sequentially adds disk spore bacterium, synergist, gas-phase silica, rosemary oil, divides Powder, diatomite, carboxymethyl cellulose, high-speed stirred 30 minutes, then stirring at low speed 30 minutes;
(5) it sterilizes, pack.
Embodiment 3
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
37 parts of gyphosate solution, 4 parts of hyoscyamine, 2.5 parts of cumarin, 3 parts of Sichuan chinaberry extract, 3 parts of bupleurum extract, 2 parts of RHIZOMA ANEMARRHENAE with peet extract, 8 parts of disk spore bacterium, 3 parts of synergist, 5 parts of gas-phase silica, 5 parts of rosemary oil, 4 parts of dispersant, diatom 5 parts of soil, 5 parts of carboxymethyl cellulose, 47 parts of deionized water.
The synergist is saturating agent T, one or more in beneficial agriculture bleeding agent A, B, C, azone.
A kind of preparation method of glyphosate herbicidal suitable for vegetable field weeds, includes the following steps:
(1) raw material in formula is weighed;
(2) preparation of Fructus meliae toosendan, radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract:It takes Fructus meliae toosendan crushed after being dried at coarse powder, Fructus meliae toosendan is added The ethyl alcohol of 6-10 times of coarse powder weight, refluxing extraction 30-50 minutes at 50-60 DEG C of temperature, filters, discards filter residue, what is obtained carries Liquid is taken to carry out flash concentration to the 5-10% of original volume using Reduced Pressure Concentration Device to get melia toosendan under the conditions of 60-70 DEG C Seed extract, same method prepare radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract;
(3) gyphosate solution, synergist, water are added in reaction kettle, are stirred evenly, sequentially add hyoscyamine, Cumarin, Sichuan chinaberry extract, bupleurum extract, RHIZOMA ANEMARRHENAE with peet extract, stir evenly;
(4) reaction kettle is warming up to 50-60 DEG C, sequentially adds disk spore bacterium, synergist, gas-phase silica, rosemary oil, divides Powder, diatomite, carboxymethyl cellulose, high-speed stirred 30 minutes, then stirring at low speed 30 minutes;
(5) it sterilizes, pack.
Embodiment 4
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
39 parts of gyphosate solution, 4.5 parts of hyoscyamine, 3.5 parts of cumarin, 3.5 parts of Sichuan chinaberry extract, radix bupleuri extraction 3.5 parts of object, 2.5 parts of RHIZOMA ANEMARRHENAE with peet extract, 9 parts of disk spore bacterium, 4 parts of synergist, 6 parts of gas-phase silica, rosemary oil 5.5 part, point 4.5 parts of powder, 6 parts of diatomite, 6 parts of carboxymethyl cellulose, 50 parts of deionized water.
The synergist is saturating agent T, one or more in beneficial agriculture bleeding agent A, B, C, azone.
A kind of preparation method of glyphosate herbicidal suitable for vegetable field weeds, includes the following steps:
(1) raw material in formula is weighed;
(2) preparation of Fructus meliae toosendan, radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract:It takes Fructus meliae toosendan crushed after being dried at coarse powder, Fructus meliae toosendan is added The ethyl alcohol that 9 times of coarse powder weight, the refluxing extraction 47 minutes at 58 DEG C of temperature, filters, discards filter residue, obtained extracting solution is at 68 DEG C Under the conditions of flash concentration carried out to original volume 9% to get Sichuan chinaberry extract, same method using Reduced Pressure Concentration Device Prepare radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract;
(3) gyphosate solution, synergist, water are added in reaction kettle, are stirred evenly, sequentially add hyoscyamine, Cumarin, Sichuan chinaberry extract, bupleurum extract, RHIZOMA ANEMARRHENAE with peet extract, stir evenly;
(4) reaction kettle is warming up to 58 DEG C, sequentially adds disk spore bacterium, synergist, gas-phase silica, rosemary oil, dispersion Agent, diatomite, carboxymethyl cellulose, high-speed stirred 30 minutes, then stirring at low speed 30 minutes;
(5) it sterilizes, pack.
Embodiment 5
A kind of glyphosate herbicidal suitable for vegetable field weeds is made of the raw material of following parts by weight:
36 parts of gyphosate solution, 3.5 parts of hyoscyamine, 2 parts of cumarin, 2.5 parts of Sichuan chinaberry extract, bupleurum extract 2.5 parts, 1.5 parts of RHIZOMA ANEMARRHENAE with peet extract, 6 parts of disk spore bacterium, 2 parts of synergist, 4 parts of gas-phase silica, 4.5 parts of rosemary oil, dispersion 3.5 parts of agent, 4 parts of diatomite, 3 parts of carboxymethyl cellulose, 43 parts of deionized water.
The synergist is saturating agent T, one or more in beneficial agriculture bleeding agent A, B, C, azone.
A kind of preparation method of glyphosate herbicidal suitable for vegetable field weeds, includes the following steps:
(1) raw material in formula is weighed;
(2) preparation of Fructus meliae toosendan, radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract:It takes Fructus meliae toosendan crushed after being dried at coarse powder, Fructus meliae toosendan is added The ethyl alcohol that 7 times of coarse powder weight, the refluxing extraction 35 minutes at 53 DEG C of temperature, filters, discards filter residue, obtained extracting solution is at 63 DEG C Under the conditions of flash concentration carried out to original volume 6% to get Sichuan chinaberry extract, same method using Reduced Pressure Concentration Device Prepare radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract;
(3) gyphosate solution, synergist, water are added in reaction kettle, are stirred evenly, sequentially add hyoscyamine, Cumarin, Sichuan chinaberry extract, bupleurum extract, RHIZOMA ANEMARRHENAE with peet extract, stir evenly;
(4) reaction kettle is warming up to 53 DEG C, sequentially adds disk spore bacterium, synergist, gas-phase silica, rosemary oil, dispersion Agent, diatomite, carboxymethyl cellulose, high-speed stirred 30 minutes, then stirring at low speed 30 minutes;
(5) it sterilizes, pack.

Claims (6)

1. a kind of glyphosate herbicidal suitable for vegetable field weeds, which is characterized in that be made of the raw material of following parts by weight:
35-40 parts of gyphosate solution, 3-5 parts of hyoscyamine, -4 parts of coumarin 1,2-4 parts of Sichuan chinaberry extract, bupleurum extract 2-4 parts, 1-3 parts of RHIZOMA ANEMARRHENAE with peet extract, 5-10 parts of disk spore bacterium, 1-5 parts of synergist, 3-7 parts of gas-phase silica, rosemary oil 4-6 Part, 3-5 parts of dispersant, 3-7 parts of diatomite, 2-8 parts of carboxymethyl cellulose, 40-55 parts of deionized water.
2. the glyphosate herbicidal according to claim 1 suitable for vegetable field weeds, which is characterized in that by following weight The raw material of part is made:
35 parts of gyphosate solution, 3 parts of hyoscyamine, coumarin 1 part, 2 parts of Sichuan chinaberry extract, 2 parts of bupleurum extract, RHIZOMA ANEMARRHENAE with peet 1 part of extract, 5 parts of disk spore bacterium, 1 part of synergist, 3 parts of gas-phase silica, 4 parts of rosemary oil, 3 parts of dispersant, 3 parts of diatomite, 2 parts of carboxymethyl cellulose, 40 parts of deionized water.
3. the glyphosate herbicidal according to claim 1 suitable for vegetable field weeds, which is characterized in that by following weight The raw material of part is made:
40 parts of gyphosate solution, 5 parts of hyoscyamine, 4 parts of cumarin, 4 parts of Sichuan chinaberry extract, 4 parts of bupleurum extract, RHIZOMA ANEMARRHENAE with peet 3 parts of extract, 10 parts of disk spore bacterium, 5 parts of synergist, 7 parts of gas-phase silica, 6 parts of rosemary oil, 5 parts of dispersant, 7 parts of diatomite, 8 parts of carboxymethyl cellulose, 55 parts of deionized water.
4. the glyphosate herbicidal according to claim 1 suitable for vegetable field weeds, which is characterized in that by following weight The raw material of part is made:
37 parts of gyphosate solution, 4 parts of hyoscyamine, 2.5 parts of cumarin, 3 parts of Sichuan chinaberry extract, 3 parts of bupleurum extract, Mao Zhi 2 parts of female extract, 8 parts of disk spore bacterium, 3 parts of synergist, 5 parts of gas-phase silica, 5 parts of rosemary oil, 4 parts of dispersant, diatomite 5 Part, 5 parts of carboxymethyl cellulose, 47 parts of deionized water.
5. the glyphosate herbicidal according to claim 1 suitable for vegetable field weeds, which is characterized in that the synergist It is one or more in saturating agent T, beneficial agriculture bleeding agent A, B, C, azone.
6. a kind of preparation method of glyphosate herbicidal suitable for vegetable field weeds, which is characterized in that include the following steps:
(1) raw material in formula is weighed;
(2) preparation of Fructus meliae toosendan, radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract:It takes Fructus meliae toosendan crushed after being dried at coarse powder, Fructus meliae toosendan coarse powder is added The ethyl alcohol of 6-10 times of weight, refluxing extraction 30-50 minutes at 50-60 DEG C of temperature, filters, discards filter residue, obtained extracting solution The 5-10% for being carried out flash concentration to original volume using Reduced Pressure Concentration Device under the conditions of 60-70 DEG C is carried to get Fructus meliae toosendan Object, same method is taken to prepare radix bupleuri, RHIZOMA ANEMARRHENAE with peet extract;
(3) gyphosate solution, synergist, water are added in reaction kettle, are stirred evenly, sequentially add hyoscyamine, tonka-bean Element, Sichuan chinaberry extract, bupleurum extract, RHIZOMA ANEMARRHENAE with peet extract, stir evenly;
(4) reaction kettle is warming up to 50-60 DEG C, sequentially adds disk spore bacterium, synergist, gas-phase silica, rosemary oil, dispersion Agent, diatomite, carboxymethyl cellulose, high-speed stirred 30 minutes, then stirring at low speed 30 minutes;
(5) it sterilizes, pack.
CN201810629344.7A 2018-06-19 2018-06-19 A kind of glyphosate herbicidal and preparation method thereof suitable for vegetable field weeds Withdrawn CN108713560A (en)

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