CN108709790A - A kind of exhaust apparatus of microwave dissolver - Google Patents

A kind of exhaust apparatus of microwave dissolver Download PDF

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Publication number
CN108709790A
CN108709790A CN201810407749.6A CN201810407749A CN108709790A CN 108709790 A CN108709790 A CN 108709790A CN 201810407749 A CN201810407749 A CN 201810407749A CN 108709790 A CN108709790 A CN 108709790A
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CN
China
Prior art keywords
exhaust
blast pipe
microwave dissolver
exhaust apparatus
mounting hole
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CN201810407749.6A
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CN108709790B (en
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区俊成
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Gaoming District Foshan City Poplar And Metal Material Professional Towns Innovation Centers
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Gaoming District Foshan City Poplar And Metal Material Professional Towns Innovation Centers
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Processing Of Solid Wastes (AREA)
  • Treating Waste Gases (AREA)

Abstract

The invention discloses a kind of exhaust apparatus of microwave dissolver, including:Shell, be arranged blast pipe inside the shell, exhaust duct, the cooling tube being connected between blast pipe and exhaust duct, be completely covered on blast pipe air inlet first exhaust fan and be completely covered on exhaust duct exhaust outlet second exhaust fan, be covered in the filter pad of first exhaust fan front end;The positive diagonal angle of the shell offers the first mounting hole and the second mounting hole respectively, one end of blast pipe is fixed on the first mounting hole, the other end is fixedly connected with cooling tube, one end of exhaust duct is fixed on the second mounting hole, the other end is fixedly connected with cooling tube, and first exhaust fan and second exhaust fan open and close simultaneously;The exhaust apparatus can rapidly cool after so that resolution instrument is worked, and improve work efficiency, and the pollutant purifications such as acid mist that can generate digestion process, prevent it from being polluted to atmospheric environment.

Description

A kind of exhaust apparatus of microwave dissolver
Technical field
The present invention relates to exhaust apparatus technical field, more particularly to a kind of microwave dissolver exhaust apparatus.
Background technology
Micro-wave digestion refers generally to using the digestion solution and sample in microwave heating closed container, in high temperature pressurised condition Under keep various samples rapidly-soluble wet digesting;Microwave dissolver be realize micro-wave digestion device, with its quickly, cleared up Entirely, it is each to be widely used in the departments such as industry, agricultural, environmental protection, sanitary inspection, metallurgy, geology, medicine, chemical industry for the white advantage in low latitude The resolution of kind sample, especially suitable for atom spectrum to micro, trace and ultratrace element the Accurate Determining in various samples; But high pressure is inevitably brought during micro-wave digestion, typically containing the more sample of organic matter its pressure can be bigger, In some temperature section heating rate than comparatively fast, there is the risk that counteracting tank bursts, general microwave dissolver is by digestion cavity Interior gas is directly extracted out by wind turbine, and atmospheric environment is discharged, and in the case of the air-tightness deficiency of counteracting tank or quick-fried tank, is disappeared Solve liquid(Usually nitric acid, sulfuric acid, lye, salt etc.)Gasify in high temperature and pressure, be discharged with gas, seriously affects air Environment.
As it can be seen that the prior art could be improved and improve.
Invention content
Place in view of above-mentioned deficiencies of the prior art, the purpose of the present invention is to provide a kind of exhaust of microwave dissolver dresses It sets, it is intended to the exhaust gas direct emission for solving microwave digestion in the prior art, the technical issues of being polluted to atmospheric environment.
In order to achieve the above object, this invention takes following technical schemes:
A kind of exhaust apparatus of microwave dissolver, including:Shell is arranged blast pipe inside the shell, exhaust duct, is connected to air inlet Manage exhaust duct between cooling tube, be completely covered on blast pipe air inlet first exhaust fan and be completely covered on exhaust duct Exhaust outlet second exhaust fan, be covered in the filter pad of first exhaust fan front end;The positive diagonal angle of the shell is distinguished The first mounting hole and the second mounting hole are offered, one end of blast pipe is fixed on the first mounting hole, and the other end is solid with cooling tube Fixed connection, one end of exhaust duct are fixed on the second mounting hole, and the other end is fixedly connected with cooling tube, first exhaust fan and second Exhaust fan opens and closes simultaneously.
In the exhaust apparatus of the microwave dissolver, the cooling tube includes outer tube and inner tube, and inner tube is fully wrapped around outside Inside pipe, the both ends of inner tube are closely connect with blast pipe and exhaust duct respectively, and the pipe of the junction blast pipe and exhaust duct Diameter is consistent with inner tube.
In the exhaust apparatus of the microwave dissolver, the both ends of the outer tube are tight with the outer wall of blast pipe and exhaust duct respectively Close connection.
In the exhaust apparatus of the microwave dissolver, water inlet and water outlet are respectively equipped on the side wall at the outer tube both ends Mouthful, the inlet and outlet are each passed through the side wall of the shell of the exhaust apparatus.
In the exhaust apparatus of the microwave dissolver, said inner tube is in the shape of a spiral.
In the exhaust apparatus of the microwave dissolver, the caliber of the air inlet of the blast pipe is bigger than the caliber of exhaust outlet, The caliber of the air outlet of the discharge pipe is bigger than the caliber of air inlet.
In the exhaust apparatus of the microwave dissolver, the filter pad includes strainer and adsorption layer, the adsorption layer package In strainer.
In the exhaust apparatus of the microwave dissolver, the sorbing material of the adsorption layer includes activated carbon and quick lime.
Advantageous effect:
The present invention provides a kind of exhaust apparatus of microwave dissolver, the first exhaust fan that is opened and closed simultaneously by setting with Second exhaust fan makes the gas in resolution instrument be recycled in exhaust apparatus and inner cavity, gas is made to pass through filtering in cyclic process Pad and cooling tube carry out purification and cooling, can rapidly cool, improve work efficiency after so that resolution instrument is worked, and The pollutant purifications such as the acid mist that can generate digestion process, prevent it from being polluted to atmospheric environment.
Description of the drawings
Fig. 1 is the structural schematic diagram of the exhaust apparatus of the microwave dissolver provided by the invention;
Wherein, direction shown in arrow is the direction of gas flowing.
Fig. 2 is the sectional view of the cooling tube;
Wherein, direction shown in arrow is the direction of flow of cooling water.
Fig. 3 is the sectional view of the filter pad.
Specific implementation mode
The present invention provides a kind of exhaust apparatus of microwave dissolver, to make the purpose of the present invention, technical solution and effect more Add clear, clear, the present invention is described in more detail for the embodiment that develops simultaneously referring to the drawings.It should be appreciated that described herein Specific examples are only used to explain the present invention, is not intended to limit the present invention.
It please referring to Fig.1 with 2, the present invention provides a kind of exhaust apparatus of microwave dissolver, including:Shell 1 is arranged in shell Blast pipe 2, exhaust duct 3 in 1, are completely covered on blast pipe 2 at the cooling tube 4 being connected between blast pipe 2 and exhaust duct 3 The first exhaust fan 5 of air inlet and be completely covered on exhaust duct 3 exhaust outlet second exhaust fan 6, be covered in first exhaust fan 5 The filter pad 7 of front end;The positive diagonal angle of the shell 1 offers the first mounting hole 11 and the second mounting hole 12 respectively, into One end of air hose 2 is fixed on the first mounting hole 11, and the other end is fixedly connected with cooling tube 4, and one end of exhaust duct 3 is fixed on On two mounting holes 12, the other end is fixedly connected with cooling tube 4, and first exhaust fan 5 and second exhaust fan 6 open and close simultaneously.
The exhaust apparatus is used for mounted on the back of microwave dissolver, and the gas of microwave dissolver inner cavity is by filtering Net, certain harmful components in gas are adsorbed, and are then entered in blast pipe 2 through first exhaust fan 5, are entered by blast pipe 2 It is cooled after cooling tube 4, is then vented back in the inner cavity of microwave dissolver through exhaust duct 3, so recycled, until micro-wave digestion The temperature of instrument inner cavity is down to safe range.First exhaust fan 5 and second exhaust fan 6 are driven by motor, are realized while being opened and closing It closes, ensures that gas circuit is unimpeded.The exhaust apparatus of microwave dissolver using the above structure can make the temperature of microwave dissolver inner cavity Rapid decrease reduces the required time that cools down, and improves the efficiency of work, and gas is wherein entrained in cyclic process Harmful components adsorbed by filter screen, avoid being expelled directly out atmospheric environment and causing damages to environment, also avoid experimenter Suck and endanger the health of experimenter.
Further, the cooling tube 4 includes outer tube 42 and inner tube 41, and inner tube 41 is completely encapsulated in inside outer tube 42, interior The both ends of pipe 41 are closely connect with blast pipe 2 and exhaust duct 3 respectively, and the caliber of the junction blast pipe 2 and exhaust duct 3 with Inner tube 41 is consistent.When air exhausting device work, gas is from the inner tube 41 that blast pipe 2 enters cooling tube 4, and cooling water is from outer tube It is flowed in 42, cools down the direction of flow with the direction of gas flowing on the contrary, enhancing the effect of heat exchange to a certain extent, accelerate The cooling rate of gas.
Further, the both ends of the outer tube 42 are closely connect with the outer wall of blast pipe 2 and exhaust duct 3 respectively.
Further, water inlet 421 and water outlet 422, the water inlet are respectively equipped on the side wall at 42 both ends of the outer tube Mouth 421 and water outlet 422 are each passed through the side wall of the shell 1 of the exhaust apparatus.The outer wall and outer tube of the inner tube 41 of cooling tube 4 The 422 closed space other than water inlet 421 and water outlet is formed between 42 inner wall, has been fully ensured that leakproofness, has been prevented from cooling down Water enters the inner cavity of microwave dissolver by pipeline, influences the normal work of instrument.
Preferably, said inner tube 41 is in the shape of a spiral;When spiral helicine inner tube 41 increases stop of the gas in cooling tube 4 Between, so that it is fully carried out heat exchange with cooling water, improves the utilization rate of cooling water.
Preferably, the caliber of the air inlet of the blast pipe 2 is bigger than the caliber of air outlet, the air outlet of the exhaust duct 3 Caliber it is bigger than the caliber of air inlet.After entering blast pipe 2, the air inlet bigger from caliber flows gas to cooling tube 4, Caliber narrows, and the flow velocity of gas is accelerated, and entering the inner tube 41 of cooling tube 4 for it provides power, makes gas not because spiral helicine cold But 4 inner tube 41 of pipe and flow over slow, cause the speed that gas is discharged more many than the speed of inflow and cause the difference of air pressure, to Cause inner tube 42 to be damaged, after the gas of outflow inner tube 42 enters exhaust duct 3, direction that the caliber of exhaust duct 3 is flowed with gas by Gradual change is big, and the flow velocity of gas is slack-off with the increase of caliber, and the air pressure in entire air duct is kept to be in a normal fluctuation model It encloses, also makes the flow velocity for the gas for entering microwave dissolver inner cavity from air outlet slack-off, it is excessive to micro-wave digestion to reduce airflow fluctuation The influence of instrument inner cavity environment.
Referring to Fig. 3, further, the filter pad 7 includes strainer 71 and adsorption layer 72, the adsorption layer 72 is wrapped in In strainer 71.
Preferably, the sorbing material of the adsorption layer 72 includes activated carbon and quick lime.The digestion solution of general micro-wave digestion For acid solutions such as nitric acid, sulfuric acid, the acid solution can be absorbed after activated carbon and quick lime, to make gas be purified, and And the cost of activated carbon and quick lime is low, so that timing is replaced filter pad and is unlikely to that cost is excessively high, the day of compound Routine Test Lab It is often used.
It, can according to the technique and scheme of the present invention and its hair it is understood that for those of ordinary skills Bright design is subject to equivalent substitution or change, and all these changes or replacement should all belong to the guarantor of appended claims of the invention Protect range.

Claims (8)

1. a kind of exhaust apparatus of microwave dissolver, which is characterized in that including:Blast pipe inside the shell, air draft is arranged in shell The cooling tube that manage, is connected between blast pipe and exhaust duct, the first exhaust fan of air inlet for being completely covered on blast pipe and complete All standing the exhaust outlet of exhaust duct second exhaust fan, be covered in the filter pad of first exhaust fan front end;The shell is just The diagonal angle in face offers the first mounting hole and the second mounting hole respectively, and one end of blast pipe is fixed on the first mounting hole, separately One end is fixedly connected with cooling tube, and one end of exhaust duct is fixed on the second mounting hole, and the other end is fixedly connected with cooling tube, the One exhaust fan and second exhaust fan open and close simultaneously.
2. the exhaust apparatus of microwave dissolver according to claim 1, which is characterized in that the cooling tube include outer tube and Inner tube, inner tube are completely encapsulated in outer tube, and the both ends of inner tube are closely connect with blast pipe and exhaust duct respectively, and the connection The caliber for locating blast pipe and exhaust duct is consistent with inner tube.
3. the exhaust apparatus of microwave dissolver according to claim 2, which is characterized in that the both ends of the outer tube respectively with The outer wall of blast pipe and exhaust duct closely connects.
4. the exhaust apparatus of microwave dissolver according to claim 2, which is characterized in that on the side wall at the outer tube both ends Inlet and outlet are respectively equipped with, the inlet and outlet are each passed through the side wall of the shell of the exhaust apparatus.
5. the exhaust apparatus of microwave dissolver according to claim 2, which is characterized in that said inner tube is in the shape of a spiral.
6. the exhaust apparatus of microwave dissolver according to claim 1, which is characterized in that the air inlet of the blast pipe Caliber is bigger than the caliber of air outlet, and the caliber of the exhaust outlet of the discharge pipe is bigger than the caliber of air inlet.
7. the exhaust apparatus of microwave dissolver according to claim 1, which is characterized in that the filter pad include strainer and Adsorption layer, the adsorption layer are wrapped in strainer.
8. the exhaust apparatus of microwave dissolver according to claim 7, which is characterized in that the sorbing material of the adsorption layer Including activated carbon and quick lime.
CN201810407749.6A 2018-05-02 2018-05-02 Exhaust device of microwave digestion instrument Active CN108709790B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810407749.6A CN108709790B (en) 2018-05-02 2018-05-02 Exhaust device of microwave digestion instrument

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Application Number Priority Date Filing Date Title
CN201810407749.6A CN108709790B (en) 2018-05-02 2018-05-02 Exhaust device of microwave digestion instrument

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CN108709790A true CN108709790A (en) 2018-10-26
CN108709790B CN108709790B (en) 2021-01-22

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Citations (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4613738A (en) * 1985-02-19 1986-09-23 Savillex Microwave heating digestion vessel
EP0522828B1 (en) * 1991-07-10 1997-09-24 CEM Corporation Microwave heated digesting system
US6054695A (en) * 1998-07-30 2000-04-25 Milestone S.R.L. Apparatus for condensing gases within a microwave radiation field
JP2000161868A (en) * 1998-12-01 2000-06-16 Hitachi Ltd Method for evaluating damage on refractory
CN1369324A (en) * 2001-02-16 2002-09-18 中华人民共和国吉林出入境检验检疫局 Acid discharger for specimen digestion system in chemical analysis
JP2006124442A (en) * 2004-10-27 2006-05-18 Hitachi Eng Co Ltd Method for feeding water to heat recovery system and exhaust heat recovery boiler
CN201389459Y (en) * 2008-08-05 2010-01-27 奥罗达(佛山)科技有限公司 Microwave digestion system
DE102008056739A1 (en) * 2008-11-11 2010-05-12 Christian Wenner Drying an air permeable substrate with warm-/hot air, useful for separating useable solid components of fermentation residues and/or sludge as fertilizer or fuel and for reducing amount of liquid fermentation residue and/or sludge
CN201964571U (en) * 2011-01-30 2011-09-07 周祚江 Indoor intake and exhaust device
CN202606176U (en) * 2012-03-29 2012-12-19 上海宝钢工业技术服务有限公司 Wind-power cooler for laboratory
CN103792130A (en) * 2014-01-14 2014-05-14 陕西师范大学 Efficient environment-friendly digestion device
CN104198746A (en) * 2014-09-15 2014-12-10 西安西北有色地质研究院有限公司 Automatic sample ashing pretreatment device
CN204142555U (en) * 2014-10-29 2015-02-04 武汉钢铁(集团)公司 With the microwave dissolver of ventilatory
DE102013007829B4 (en) * 2013-04-27 2015-04-16 Agri V Raiffeisen eG Process and device for the treatment of agricultural manure
CN204286913U (en) * 2014-10-19 2015-04-22 深圳市高迪科技有限公司 A kind of microwave dissolver
CN205786059U (en) * 2016-07-04 2016-12-07 中华人民共和国福清出入境检验检疫局 A kind of protein is cleared up and is used condensing unit
CN206191819U (en) * 2016-11-16 2017-05-24 杭州佰朗实验室设备科技有限公司 Energy -conserving ventilation system in laboratory
CN106769387A (en) * 2016-12-21 2017-05-31 安徽省建筑工程质量监督检测站 Pyrolysis analyzer air cooling equipment
CN206652372U (en) * 2017-03-28 2017-11-21 山东鲁友体育产业股份有限公司 A kind of exhaust apparatus for rubber production
CN107961633A (en) * 2017-11-30 2018-04-27 江苏飞视文化发展有限公司 A kind of printing machine waste gas recovery purification method

Patent Citations (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4613738A (en) * 1985-02-19 1986-09-23 Savillex Microwave heating digestion vessel
EP0522828B1 (en) * 1991-07-10 1997-09-24 CEM Corporation Microwave heated digesting system
US6054695A (en) * 1998-07-30 2000-04-25 Milestone S.R.L. Apparatus for condensing gases within a microwave radiation field
JP2000161868A (en) * 1998-12-01 2000-06-16 Hitachi Ltd Method for evaluating damage on refractory
CN1369324A (en) * 2001-02-16 2002-09-18 中华人民共和国吉林出入境检验检疫局 Acid discharger for specimen digestion system in chemical analysis
JP2006124442A (en) * 2004-10-27 2006-05-18 Hitachi Eng Co Ltd Method for feeding water to heat recovery system and exhaust heat recovery boiler
CN201389459Y (en) * 2008-08-05 2010-01-27 奥罗达(佛山)科技有限公司 Microwave digestion system
DE102008056739A1 (en) * 2008-11-11 2010-05-12 Christian Wenner Drying an air permeable substrate with warm-/hot air, useful for separating useable solid components of fermentation residues and/or sludge as fertilizer or fuel and for reducing amount of liquid fermentation residue and/or sludge
CN201964571U (en) * 2011-01-30 2011-09-07 周祚江 Indoor intake and exhaust device
CN202606176U (en) * 2012-03-29 2012-12-19 上海宝钢工业技术服务有限公司 Wind-power cooler for laboratory
DE102013007829B4 (en) * 2013-04-27 2015-04-16 Agri V Raiffeisen eG Process and device for the treatment of agricultural manure
CN103792130A (en) * 2014-01-14 2014-05-14 陕西师范大学 Efficient environment-friendly digestion device
CN104198746A (en) * 2014-09-15 2014-12-10 西安西北有色地质研究院有限公司 Automatic sample ashing pretreatment device
CN204286913U (en) * 2014-10-19 2015-04-22 深圳市高迪科技有限公司 A kind of microwave dissolver
CN204142555U (en) * 2014-10-29 2015-02-04 武汉钢铁(集团)公司 With the microwave dissolver of ventilatory
CN205786059U (en) * 2016-07-04 2016-12-07 中华人民共和国福清出入境检验检疫局 A kind of protein is cleared up and is used condensing unit
CN206191819U (en) * 2016-11-16 2017-05-24 杭州佰朗实验室设备科技有限公司 Energy -conserving ventilation system in laboratory
CN106769387A (en) * 2016-12-21 2017-05-31 安徽省建筑工程质量监督检测站 Pyrolysis analyzer air cooling equipment
CN206652372U (en) * 2017-03-28 2017-11-21 山东鲁友体育产业股份有限公司 A kind of exhaust apparatus for rubber production
CN107961633A (en) * 2017-11-30 2018-04-27 江苏飞视文化发展有限公司 A kind of printing machine waste gas recovery purification method

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