CN108690978A - A kind of metal surface conditioner and preparation method thereof - Google Patents
A kind of metal surface conditioner and preparation method thereof Download PDFInfo
- Publication number
- CN108690978A CN108690978A CN201710215938.9A CN201710215938A CN108690978A CN 108690978 A CN108690978 A CN 108690978A CN 201710215938 A CN201710215938 A CN 201710215938A CN 108690978 A CN108690978 A CN 108690978A
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- CN
- China
- Prior art keywords
- sodium
- parts
- metal surface
- phosphoric acid
- surface conditioner
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
- C23C22/23—Condensed phosphates
Abstract
A kind of metal surface conditioner of present invention offer and preparation method thereof, is related to a kind of metal surface pretreatment technology field.The invention is prepared by the raw material comprising following weight parts:Sodium hydroxide 8-15, sodium carbonate 20-30, sodium bicarbonate 4-6, phosphoric acid 20-30, sodium tripolyphosphate 20-30, titanyl sulfate 8-15.Present invention process is simple, excellent in stability, is suitble to produce in enormous quantities.
Description
Technical field
The present invention relates to a kind of metal surface pretreatment technology field, more particularly to a kind of metal surface conditioner and its
Preparation method.
Background technology
The dispersion stabilization of existing regulator is to be improved, is unable to long-term preservation.
Invention content
Shortcoming present in regarding to the issue above, a kind of metal surface conditioner of present invention offer and its preparation side
Method keeps its simple for process, excellent in stability, is suitble to produce in enormous quantities.
To solve the above-mentioned problems, the present invention provides a kind of metal surface conditioner, wherein by including following weight parts
Raw material is prepared:Sodium hydroxide 8-15, sodium carbonate 20-30, sodium bicarbonate 4-6, phosphoric acid 20-30, sodium tripolyphosphate 20-30,
Titanyl sulfate 8-15.
Preferably, it is prepared by the raw material comprising following weight parts:Sodium hydroxide 8, sodium carbonate 20, sodium bicarbonate 4, phosphorus
Acid 20, sodium tripolyphosphate 20, titanyl sulfate 8.
Preferably, it is prepared by the raw material comprising following weight parts:Sodium hydroxide 15, sodium carbonate 30, sodium bicarbonate 6,
Phosphoric acid 30, sodium tripolyphosphate 30, titanyl sulfate 15.
Preferably, it is prepared by the raw material comprising following weight parts:Sodium hydroxide 10, sodium carbonate 25, sodium bicarbonate 5,
Phosphoric acid 25, sodium tripolyphosphate 25, titanyl sulfate 10.
A kind of preparation method of metal surface conditioner, wherein include the following steps:
S10, it takes 10 parts of sodium hydroxides and 25 parts of sodium carbonate to be uniformly mixed, adds 5 parts of sodium bicarbonates and stir evenly;
S20,10 parts of water are added in said mixture, continue stirring until pulpous state;
S30, the above-mentioned solution of stirring, 20 parts of phosphoric acid is slowly added to while stirring, is stirred evenly, and is heated to 80 degree,
It is sufficiently stirred;
S40,25 parts of sodium tripolyphosphates are continuously added, it is lasting to stir, and it is 80 degree to keep temperature always, until having powdered
Crystal is precipitated;
S50, continue agitation crystal under conditions of temperature is 80 degree, while 10 parts of titanyl sulfates are added, be further continued for stirring
It is dry, until obtaining white powder.
Preferably, control time is 10 minutes in the S30.
Compared with prior art, the present invention has the following advantages:
Production method provided by the invention, it is simple for process, it is easy to accomplish, excellent in stability can long-term preservation.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, the present invention is made with reference to example
It is further described, but example is not as a limitation of the invention.
The technical solution that the present invention embodies is:
Embodiment 1
It is prepared by the raw material comprising following weight parts:Sodium hydroxide 8, sodium carbonate 20, sodium bicarbonate 4, phosphoric acid 20, three
Polyphosphate sodium 20, titanyl sulfate 8.
Embodiment 2
It is prepared by the raw material comprising following weight parts:Sodium hydroxide 15, sodium carbonate 30, sodium bicarbonate 6, phosphoric acid 30,
Sodium tripolyphosphate 30, titanyl sulfate 15.
Embodiment 3
Sodium hydroxide 10, sodium carbonate 25, sodium bicarbonate 5, phosphoric acid 25, sodium tripolyphosphate 25, titanyl sulfate 10.
According to the following steps:
It takes 10 parts of sodium hydroxides and 25 parts of sodium carbonate to be uniformly mixed, adds 5 parts of sodium bicarbonates and stir evenly;
10 parts of water are added in said mixture, continue stirring until pulpous state;
Above-mentioned solution is stirred, 20 parts of phosphoric acid is slowly added to while stirring, is stirred evenly, and is heated to 80 degree, fully
Stirring;
25 parts of sodium tripolyphosphates are continuously added, it is lasting to stir, and it is 80 degree to keep temperature always, until there is powdered crystal
It is precipitated;
Continue agitation crystal under conditions of temperature is 80 degree, while 10 parts of titanyl sulfates be added, is further continued for stirring drying,
Until obtaining white powder.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention.
Various modifications to these embodiments will be apparent to those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention
It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one
The widest range caused.
Claims (6)
1. a kind of metal surface conditioner, which is characterized in that be prepared by the raw material comprising following weight parts:Sodium hydroxide 8-
15, sodium carbonate 20-30, sodium bicarbonate 4-6, phosphoric acid 20-30, sodium tripolyphosphate 20-30, titanyl sulfate 8-15.
2. a kind of metal surface conditioner as described in claim 1, which is characterized in that by the raw material system for including following weight parts
It is standby to form:Sodium hydroxide 8, sodium carbonate 20, sodium bicarbonate 4, phosphoric acid 20, sodium tripolyphosphate 20, titanyl sulfate 8.
3. a kind of metal watch as claimed in claim 2 and regulator, which is characterized in that by the raw material system for including following weight parts
It is standby to form:Sodium hydroxide 15, sodium carbonate 30, sodium bicarbonate 6, phosphoric acid 30, sodium tripolyphosphate 30, titanyl sulfate 15.
4. a kind of metal surface conditioner as claimed in claim 3, which is characterized in that by the raw material system for including following weight parts
It is standby to form:Sodium hydroxide 10, sodium carbonate 25, sodium bicarbonate 5, phosphoric acid 25, sodium tripolyphosphate 25, titanyl sulfate 10.
5. a kind of preparation method of metal surface conditioner as described in claim 1, which is characterized in that include the following steps:
S10, it takes 10 parts of sodium hydroxides and 25 parts of sodium carbonate to be uniformly mixed, adds 5 parts of sodium bicarbonates and stir evenly;
S20,10 parts of water are added in said mixture, continue stirring until pulpous state;
S30, the above-mentioned solution of stirring, 20 parts of phosphoric acid is slowly added to while stirring, is stirred evenly, and is heated to 80 degree, fully
Stirring;
S40,25 parts of sodium tripolyphosphates are continuously added, it is lasting to stir, and it is 80 degree to keep temperature always, until there is powdered crystal
It is precipitated;
S50, continue agitation crystal under conditions of temperature is 80 degree, while 10 parts of titanyl sulfates be added, be further continued for stirring drying,
Until obtaining white powder.
6. a kind of preparation method of metal surface conditioner as claimed in claim 5, which is characterized in that controlled in the S30
Time is 10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710215938.9A CN108690978A (en) | 2017-04-05 | 2017-04-05 | A kind of metal surface conditioner and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710215938.9A CN108690978A (en) | 2017-04-05 | 2017-04-05 | A kind of metal surface conditioner and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN108690978A true CN108690978A (en) | 2018-10-23 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710215938.9A Pending CN108690978A (en) | 2017-04-05 | 2017-04-05 | A kind of metal surface conditioner and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114686867A (en) * | 2022-03-29 | 2022-07-01 | 东莞市精诚环保科技有限公司 | Novel efficient zinc series surface conditioner and preparation method and application thereof |
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| JP2001072767A (en) * | 1999-09-08 | 2001-03-21 | Kao Corp | Surface modifier |
| CN101974743A (en) * | 2010-10-27 | 2011-02-16 | 大连三达奥克化学股份有限公司 | Ti-Mg-B surface conditioner for zinc-phosphating and preparation method thereof |
| CN102251238A (en) * | 2010-05-20 | 2011-11-23 | 德清县康祺化学品有限公司 | Method for preparing metal surface conditioner |
| WO2012005722A1 (en) * | 2010-07-06 | 2012-01-12 | Zettacore, Inc. | Methods of treating metal surfaces and devices formed thereby |
| CN103602974A (en) * | 2013-11-22 | 2014-02-26 | 大连碧城环保科技有限公司 | Environment-friendly method for enhancing corrosion protection of inner wall of marine diesel engine pipeline |
| CN103741132A (en) * | 2014-01-10 | 2014-04-23 | 湖南金裕化工有限公司 | Colloid titanium surface conditioner and preparation method thereof |
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2017
- 2017-04-05 CN CN201710215938.9A patent/CN108690978A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001072767A (en) * | 1999-09-08 | 2001-03-21 | Kao Corp | Surface modifier |
| CN102251238A (en) * | 2010-05-20 | 2011-11-23 | 德清县康祺化学品有限公司 | Method for preparing metal surface conditioner |
| WO2012005722A1 (en) * | 2010-07-06 | 2012-01-12 | Zettacore, Inc. | Methods of treating metal surfaces and devices formed thereby |
| CN101974743A (en) * | 2010-10-27 | 2011-02-16 | 大连三达奥克化学股份有限公司 | Ti-Mg-B surface conditioner for zinc-phosphating and preparation method thereof |
| CN103602974A (en) * | 2013-11-22 | 2014-02-26 | 大连碧城环保科技有限公司 | Environment-friendly method for enhancing corrosion protection of inner wall of marine diesel engine pipeline |
| CN103741132A (en) * | 2014-01-10 | 2014-04-23 | 湖南金裕化工有限公司 | Colloid titanium surface conditioner and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114686867A (en) * | 2022-03-29 | 2022-07-01 | 东莞市精诚环保科技有限公司 | Novel efficient zinc series surface conditioner and preparation method and application thereof |
| CN114686867B (en) * | 2022-03-29 | 2023-10-24 | 东莞市精诚环保科技有限公司 | Novel efficient zinc series surface conditioner and preparation method and application thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181023 |
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| RJ01 | Rejection of invention patent application after publication |