CN108684914A - A kind of Europe mandarin orange fruits and vegetables pressed candy and preparation method thereof - Google Patents
A kind of Europe mandarin orange fruits and vegetables pressed candy and preparation method thereof Download PDFInfo
- Publication number
- CN108684914A CN108684914A CN201810418363.5A CN201810418363A CN108684914A CN 108684914 A CN108684914 A CN 108684914A CN 201810418363 A CN201810418363 A CN 201810418363A CN 108684914 A CN108684914 A CN 108684914A
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- China
- Prior art keywords
- mandarin orange
- powder
- europe
- parts
- pressed candy
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- 238000002360 preparation method Methods 0.000 title claims abstract description 52
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/362—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/364—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The present invention relates to a kind of Europe mandarin orange fruits and vegetables pressed candy and preparation method thereof, the Europe mandarin orange fruits and vegetables pressed candy includes following raw materials:Bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder, magnesium stearate.Europe mandarin orange fruits and vegetables pressed candy of the present invention, preparation method is simple, convenient, and nutriment is abundant, and mouthfeel is very good, has the function of invigorating the spleen, reducing blood lipid, removes interior free yl, improving eyesight and cancer-preventing health, also has effects that improve constipation, weight-reducing.
Description
Technical field
The present invention relates to a kind of pressed candies, specifically, being related to a kind of Europe mandarin orange fruits and vegetables pressed candy and preparation method thereof.
Background technology
Candy can be divided into hard candy, hard centre sweets, butterfat candy, gel candy, gel-based candy and pressed candy
Deng.Wherein pressed candy is also known as pulverized sugar or piece candy, is by the candy of granulation, bonding, compression moulding, manufacture mechanism is mainly borrowed
Pressing aid power is to be with refined Icing Sugar the process that particle or fine powder distance are contracted to generate enough cohesive force and combine closely
Main body, the adhesives such as filler materials and starch slurry, syrup, colloidal solution such as addition milk powder, fragrance, through the molding mixing of pelletizing press sheet
Object, without heating infusion, also referred to as cold machining process.Pressed candy can be divided into sugar-coat pressed candy, multilayer pressed candy, effervesce tabletting
Sugar and masticatory pattern pressed candy.
Further investigation reveals that the global year consumption per head of candy is 3 kilograms or so, and China only has 0.7 kilogram, therefore I
There is state's candy market huge development potentiality, the breakthrough of domestic enterprise also to focus in the update of product, continuous to release
New product and constantly abundant candy kind.At home when confectionery industry growth and expansion, health, low-sugar type, interest in the world
Various types of candies such as taste type and the ecotype more have the gesture for the high-end candy market in combined rush China of quickening one's step.
That can help digest it is understood that fruit contains the nutriments such as abundant vitamin, dietary fiber, succulence and
The main sense of taste is sweet taste and tart flavour and edible fruit.Fruit is very useful to our healths, each fruit pair
Human body nearly all has certain benefit, the high person of cholesterol that can eat a little apples, mango and tamarind in right amount more;Diabetic is suitble to
Eat pineapple, pears, shaddock, red bayberry;Patients with coronary heart disease is suitble to eat citrus, shaddock and strawberry;It is the most nicier pomegranate of enteron aisle patient, red
Fruit, lichee;It is beneficial that hemorrhoid patients eat a little figs, banana etc. more.
Europe mandarin orange in fruit is the famous local tradition citrus variety of important specialty and China in Wenzhou, Europe mandarin orange history
It is long, it is the tribute of ancient times imperial court, the civil good story for being known as " Dragon Boat Festival, Europe mandarin orange was like antelope " in Wenzhou.Europe mandarin orange fruit is golden yellow bright-coloured, clearly
Sweet tea succulence, slightly bitter taste, nutritive value is high, and containing multivitamin, and heat of dispelling is promoted the production of body fluid, preventing phlegm from forming and stopping coughing, the spies such as refreshing and detoxicating
Different medical efficiency, to treatment cough, measles, hepatitis, high fever, hypertension, diabetes, hyperthyroidism, neurasthenia enhances immunization machine
Can there be good effect.
The simple manufacture craft of the function nutrition characteristic and pressed candy of present invention combination Europe mandarin orange, gives full play to its edible health
Value, prepares a kind of Europe mandarin orange fruits and vegetables pressed candy, meets dual requirements of the people to emphasis health and fast pace life.
Invention content
The technical problem to be solved in the present invention is to provide a kind of Europe mandarin orange fruits and vegetables pressed candy and preparation method thereof, the Europe mandarin oranges
Fruits and vegetables pressed candy has the health-care efficacies such as treatment constipation and weight-reducing.
The present invention is achieved through the following technical solutions:
A kind of Europe mandarin orange fruits and vegetables pressed candy, including following raw materials:Bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, wheat
Piece, D-sorbite, sodium bicarbonate, vegetable fat powder, magnesium stearate.
A kind of Europe mandarin orange fruits and vegetables pressed candy, including the raw material of following weight parts are prepared:100-350 parts of bowl mandarin orange powder, salt
5-30 parts of algae powder, 5-30 parts of cherry powder, 50-100 parts of pectase powder, 200-400 parts of oatmeal, 60-200 parts of D-sorbite, carbon
5-30 parts of sour hydrogen sodium, 60-200 parts of vegetable fat powder, 0.5-1 parts of magnesium stearate.
The salt algae powder can be bought or be prepared.The preparation method of the salt algae powder is:By salt algae temperature be 45-
It is 4-8wt% to be dried at 65 DEG C to water content, is crushed to 80-140 mesh to obtain the final product.
The cherry powder can be bought or be prepared.The preparation method of the cherry powder is:By cherry temperature be 45-
It is that the cherry kernel removing after drying is crushed to 80-140 mesh to obtain the final product by 4-8wt% to be dried at 65 DEG C to water content.
The pectase powder is dried to obtain through everfermentation by fruits and vegetables.It, can be rapidly by human body after ferment powder enters human body
It absorbs and utilizes, do not increase stomach and intestine burden, also have anti-inflammatory effect to canker;And become cellular activity, especially brain cell
Movable necessity;Constitution can be increased, and various diseases can be prevented and occurred.
The vegetable fat powder can be bought or be prepared.The preparation method of the vegetable fat powder is:By vegetable oil, caseinic acid
Sodium, glucose, maltodextrin are 1 in mass ratio:(0.05-0.25):(0.1-0.2):(0.5-2) be uniformly mixed to get.It is described
Vegetable oil includes one or more in soybean oil, sesame oil, peanut oil, rapeseed oil.
The preparation method of the bowl mandarin orange powder is:Bowl mandarin orange is eluted with water, is drained;Bowl mandarin orange after draining is at -5~-20 DEG C
15-25h is freezed, the bowl mandarin orange after freezing is crushed to 10-30 in the environment of temperature is -5~-20 DEG C using freezing crusher
Bowl mandarin orange and water after crushing is 1 in mass ratio by mesh:(0.1-0.5) is added in beater and is beaten, and crosses 50-300 mesh sieve,
Obtain slurries;It is 1 in mass ratio by slurries, beta-cyclodextrin, stearoyl lactate, antioxidant:(0.02-0.06):(0.005-
0.02):(0.001-0.005) be uniformly mixed, spray drying to get.
The preparation method of the bowl mandarin orange powder is:Bowl mandarin orange is eluted with water, is drained;Bowl mandarin orange after draining is at -5~-20 DEG C
15-25h is freezed, the bowl mandarin orange after freezing is crushed to 10-30 in the environment of temperature is -5~-20 DEG C using freezing crusher
Bowl mandarin orange and water after crushing is 1 in mass ratio by mesh:(0.1-0.5) is added in beater and is beaten, and crosses 50-300 mesh sieve,
Obtain slurries;It is 1 in mass ratio by slurries, modified beta-cyclodextrin, stearoyl lactate, antioxidant:(0.02-0.06):
(0.005-0.02):(0.001-0.005) be uniformly mixed, spray drying to get.
The preparation method of the modified beta-cyclodextrin is:By citric acid, 2- octenyl succinic acid anhydrides, sodium hypophosphite, water
It is 1 in mass ratio:(0.03-0.09):(0.1-0.3):(0.8-1.1) is uniformly mixed, and adds the β-of 1-3 times of citric acid weight
Cyclodextrin, it is that 200-500r/min stirs 10-20min to be warming up to 75-85 DEG C with rotating speed, obtains mixed liquor;Mixed liquor is placed in
First it is 95-105 DEG C in temperature in blowing-type thermostatic drying chamber and dries 50-70min, then is 110-130 DEG C in temperature and dries 3-7h, reaction
After by the water dissolution of 1-3 times of reaction product weight of reaction product, then be added dropwise in absolute ethyl alcohol, precipitation be precipitated, will sink
Shallow lake is washed 2-6 times with absolute ethyl alcohol, then temperature be 50-60 DEG C it is dry to constant weight to get.
The antioxidant is D-araboascorbic acid laurate and/or ascorbyl palmitate.Preferably, described anti-
Oxygen agent is (2-3) in mass ratio by D-araboascorbic acid laurate, ascorbyl palmitate:1 composition.
The present invention also provides the preparation methods of above-mentioned Europe mandarin orange fruits and vegetables pressed candy, include the following steps:
(1) bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder are mixed
It closes uniformly, obtains mixture;
(2) it is 1 in mass ratio by starch and cold water:(0.5-1.5) after mixing, adds starch weight (5-10) times
Hot water in be uniformly mixed, obtain starch slurry;
(3) it is 1 in mass ratio by the starch slurry that the mixture that step (1) obtains is obtained with step (2):(0.01-0.05)
It is uniformly mixed, obtains wet feed;
(4) wet feed is pelletized with granulator, it is dry, obtain dry particl;
(5) dry particl is mixed with magnesium stearate, tabletting to get.
The temperature of the cold water is 1-40 DEG C, and the temperature of the hot water is 90-100 DEG C.
Compared with prior art, the present invention has the advantages that following prominent and effect:
Europe mandarin orange fruits and vegetables pressed candy of the present invention, preparation method is simple, convenient, and nutriment is abundant, and mouthfeel is very
It is good, have the function of invigorating the spleen, reducing blood lipid, remove interior free yl, improving eyesight and cancer-preventing health, also there is the work(for improving constipation, weight-reducing
Effect.
The present invention is added with the sodium bicarbonate (i.e. sodium bicarbonate) that can kill tumour cell, according to city bulletin (curing online in Zhejiang)
The report Zhe Yi Second Academys obtain important breakthrough on liver cancer treatment and kill tumour cell with sodium bicarbonate, this is also greatly reduced patient's
Financial burden.Advanced liver cancer patient makees targeted therapy with sodium bicarbonate (the sodium bicarbonate water being namely commonly called as), can effectively kill
Tumour cell.The therapy is applied to clinic 4 years, according to the preliminary statistics, in the advanced liver cancer patient for receiving the treatment at present
Position life cycle has been more than 3 years (originally at most only 9-10 months).International scientific journals"elife"Evaluation:This technology is swollen
It improves a lot on the Partial controll of tumor.
Specific implementation mode
The antioxidative measurement of bowl mandarin orange powder, using DPPH methods.DPPH accurately is weighed, is configured to the molten of 0.2mmol/LDPPH
Liquid is protected from light Cord blood in brown bottle.Bowl mandarin orange powder sample to be measured is diluted to 20mg/mL with deionized water, obtains sample liquid.It takes
2mL sample liquids are uniformly mixed in 2mL, 0.2mmol/LDPPH solution in test tube, is added, and are protected from light after standing 30min, use at room temperature
Ultraviolet specrophotometer UV-2000 (You Nike (Shanghai) limited instrument company) measures absorbance value at 517nm, is calculated as Ai, together
When measure 2mL, 1.0mg/mL sample liquid add 2mL absolute ethyl alcohols, be protected from light at room temperature stand 30min after, use ultraviolet specrophotometer
UV-2000 (You Nike (Shanghai) limited instrument company) measure at 517nm absorbance value, be calculated as Aj and 2mL,
0.2mmol/LDPPH solution adds 2ml distilled water to stand, with ultraviolet specrophotometer UV-2000 (You Nike (Shanghai) limited instruments
Company) absorbance value at 517nm is measured, it is calculated as Ac.The clearance rate of DPPH free radicals is calculated as follows in sample:DPPH is free
Base clearance rate=[1-(Ai-Aj)/Ac]× 100%.
Bowl mandarin orange powder is sealed with aluminum-plastic composite membrane bag and is wrapped using vitamin C as index ingredient by bowl mandarin orange powder stability test
Dress, places 3 months at a temperature of being placed in 38 DEG C, vitamin C when Vitamin C content when measuring March respectively and the sample 0 month contains
Amount, vitamin C when vitamin loss rate (%)=(Vitamin C content when Vitamin C content-March at 0 month)/0 month contain
Amount × 100.Using rp-hplc determination Vitamin C content, DiamonsilTM C18 chromatographic columns (4.6mm ×
250mm, 5 μm), mobile phase is -0.1% phosphoric acid (5 of methanol:95) it is mobile phase, flow velocity 1mLmin-1, 25 DEG C of column temperature, detection wave
A length of 242nm.
Beta-cyclodextrin is provided by one dream bio tech ltd of Zhejiang in embodiment, and rank is food-grade.
Oatmeal is the oatmeal that Hebei Kang Xi oat foods Co., Ltd provides in embodiment, and kind is naked oats.
D-sorbite in embodiment, No. CAS:50-70-4.
Sodium bicarbonate in embodiment, No. CAS:144-55-8.
Magnesium stearate in embodiment, No. CAS:557-04-0.
Salt algae in embodiment, English name:Dunaliella salina, also known as " Du Shi algaes ", Chlorophyceae, Yan Zao sections.
Cherry in embodiment, Classification system:Prunuspseudocerasus, it is acerola concentrate to use in the present embodiment.
Rapeseed oil is the refining level-one rapeseed oil of golden dragonfish board in embodiment.
Glucose in embodiment, No. CAS:492-62-6.
Maltodextrin is the food-grade maltodextrin that Shandong Xiwang Sugar Co., Ltd provides in embodiment.
Bowl mandarin orange in embodiment, Classification system:Citrus reticulata Blanco cv.Suavissima are that China writes
The local tradition citrus variety of name, is the important specialty in Wenzhou.
Stearoyl lactate in embodiment, No. CAS:18200-72-1.
Citric acid in embodiment, No. CAS:77-92-9.
2- octenyl succinic acid anhydrides in embodiment, No. CAS:26680-54-6.
Sodium hypophosphite in embodiment, No. CAS:7681-53-0.
Starch is the edible corn starch that Yu Feng Industry Group Co., Ltd provides in embodiment.
The paper that D-araboascorbic acid laurate is delivered according to Zhang little Lan, Zhu Xianhong, Zheng great Gui, remaining Si Lian in embodiment
"Lipase-catalyzed synthesis D-araboascorbic acid laurate"In 1.2 section shown in method synthesized.
Ascorbyl palmitate in embodiment, No. CAS:137-66-6.
Pectase powder is according to side shown in embodiment in the Chinese patent application No. is 201510554447.8 2 in embodiment
It is prepared by method.
Casein sodium in embodiment, No. CAS:9005-46-3.
Embodiment 1
Europe mandarin orange fruits and vegetables pressed candy, including the raw material of following weight parts are prepared:100 parts of bowl mandarin orange powder, 20 parts of salt algae powder,
20 parts of cherry powder, comprehensive 60 parts of pectase powder, 300 parts of oatmeal, 100 parts of D-sorbite, 15 parts of sodium bicarbonate, vegetable fat powder (by
It is commercially available to be commercially available) 100 parts, 0.8 part of magnesium stearate.
The preparation method of above-mentioned Europe mandarin orange fruits and vegetables pressed candy, includes the following steps:
(1) bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder are mixed
It closes uniformly, obtains mixture;
(2) it is 1 in mass ratio by starch and 20 DEG C of cold water:1 after mixing, adds 100 DEG C of 8 times of starch weight
It is uniformly mixed in hot water, obtains starch slurry;
(3) it is 1 in mass ratio by the starch slurry that the mixture that step (1) obtains is obtained with step (2):0.035 mixing is equal
It is even, obtain wet feed;
(4) by the YK-160 oscillating granulators of the wet feed Stainless Steel sieve for being equipped with 12-14 mesh (the color way machinery in Nanjing
Equipment Co., Ltd provides) granulation, scattered non-homogeneous shape wet granular is obtained, wet granular is laid on pallet, thickness control
For system at 4-5 centimetres, it is 4wt% to be dried to water content under 55 degrees Celsius, obtains dry particl;
(5) by dry particl and magnesium stearate with rotating speed for 500r/min mixing 10min, obtain the dry particl for waiting for tabletting;It will
Wait for that the dry particl of tabletting passes through mechanical pressurization with ZP-9B types rotary tablet machine (offer of Guangzhou Chen Diao mechanical equipments Co., Ltd)
Molding is to get Europe mandarin orange fruits and vegetables pressed candy.
Embodiment 2
Europe mandarin orange fruits and vegetables pressed candy, including the raw material of following weight parts are prepared:150 parts of bowl mandarin orange powder, 15 parts of salt algae powder,
It is 15 parts of cherry powder, 80 parts of pectase powder, 300 parts of oatmeal, 100 parts of D-sorbite, 15 parts of sodium bicarbonate, 100 parts of vegetable fat powder, hard
0.8 part of fatty acid magnesium.
The preparation method of the salt algae powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by salt algae, is crushed to
100 mesh to obtain the final product.
The preparation method of the cherry powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by cherry, will be dried
Cherry kernel removing afterwards is crushed to 100 mesh to obtain the final product.
The preparation method of the vegetable fat powder is:It is in mass ratio by rapeseed oil, casein sodium, glucose, maltodextrin
1:0.08:0.12:1 be uniformly mixed to get.
The preparation method of the bowl mandarin orange powder is:Bowl mandarin orange is eluted with water, is drained;Bowl mandarin orange after draining freezes at -10 DEG C
Bowl mandarin orange after freezing is crushed to 20 mesh, by the bowl after crushing by 20h in the environment of temperature is -10 DEG C using freezing crusher
Mandarin orange is 1 in mass ratio with water:It is beaten in 0.2 addition beater, crosses 200 mesh sieve, obtain slurries;By slurries, beta-cyclodextrin,
Stearoyl lactate, D-araboascorbic acid laurate are 1 in mass ratio:0.03:0.008:0.003 is uniformly mixed, and spraying is dry
Dry, the inlet air temperature of the spray drying is 180 DEG C, and leaving air temp is 75 DEG C, and hot wind wind speed is 4m3/ min, feeding speed are
40mL/min, atomizer rotating speed are 300 revs/min to get bowl mandarin orange powder.
The preparation method of above-mentioned Europe mandarin orange fruits and vegetables pressed candy, includes the following steps:
(1) bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder are mixed
It closes uniformly, obtains mixture;
(2) it is 1 in mass ratio by starch and 20 DEG C of cold water:1 after mixing, adds 100 DEG C of 8 times of starch weight
It is uniformly mixed in hot water, obtains starch slurry;
(3) it is 1 in mass ratio by the starch slurry that the mixture that step (1) obtains is obtained with step (2):0.035 mixing is equal
It is even, obtain wet feed;
(4) by the YK-160 oscillating granulators of the wet feed Stainless Steel sieve for being equipped with 12-14 mesh (the color way machinery in Nanjing
Equipment Co., Ltd provides) granulation, scattered non-homogeneous shape wet granular is obtained, wet granular is laid on pallet, thickness control
For system at 4-5 centimetres, it is 4wt% to be dried to water content under 55 degrees Celsius, obtains dry particl;
(5) by dry particl and magnesium stearate with rotating speed for 500r/min mixing 10min, obtain the dry particl for waiting for tabletting;It will
Wait for that the dry particl of tabletting passes through mechanical pressurization with ZP-9B types rotary tablet machine (offer of Guangzhou Chen Diao mechanical equipments Co., Ltd)
Molding is to get Europe mandarin orange fruits and vegetables pressed candy.
Embodiment 3
Europe mandarin orange fruits and vegetables pressed candy, including the raw material of following weight parts are prepared:150 parts of bowl mandarin orange powder, 15 parts of salt algae powder,
It is 15 parts of cherry powder, 80 parts of pectase powder, 300 parts of oatmeal, 100 parts of D-sorbite, 15 parts of sodium bicarbonate, 100 parts of vegetable fat powder, hard
0.8 part of fatty acid magnesium.
The preparation method of the salt algae powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by salt algae, is crushed to
100 mesh to obtain the final product.
The preparation method of the cherry powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by cherry, will be dried
Cherry kernel removing afterwards is crushed to 100 mesh to obtain the final product.
The preparation method of the vegetable fat powder is:It is in mass ratio by rapeseed oil, casein sodium, glucose, maltodextrin
1:0.08:0.12:1 be uniformly mixed to get.
The preparation method of the bowl mandarin orange powder is:Bowl mandarin orange is eluted with water, is drained;Bowl mandarin orange after draining freezes at -10 DEG C
Bowl mandarin orange after freezing is crushed to 20 mesh, by the bowl after crushing by 20h in the environment of temperature is -10 DEG C using freezing crusher
Mandarin orange is 1 in mass ratio with water:It is beaten in 0.2 addition beater, crosses 200 mesh sieve, obtain slurries;By slurries, modified β-ring
Dextrin, stearoyl lactate, D-araboascorbic acid laurate are 1 in mass ratio:0.03:0.008:0.003 is uniformly mixed, spray
Mist is dried, and the inlet air temperature of the spray drying is 180 DEG C, and leaving air temp is 75 DEG C, and hot wind wind speed is 4m3/ min, feed speed
Degree is 40mL/min, and atomizer rotating speed is 300 revs/min to get bowl mandarin orange powder.
The preparation method of the modified beta-cyclodextrin is:By citric acid, 2- octenyl succinic acid anhydrides, sodium hypophosphite, water
It is 1 in mass ratio:0.05:0.2:1 is uniformly mixed, and adds the beta-cyclodextrin of 2 times of citric acid weight, is warming up to 80 DEG C with rotating speed
15min is stirred for 300r/min, obtains mixed liquor;It is 100 DEG C in temperature that mixed liquor, which is placed in blowing-type thermostatic drying chamber first,
60min is dried, then in temperature is 120 DEG C of baking 5h, after reaction by the water dissolution of 1.5 times of reaction product weight of reaction product,
It is added dropwise in absolute ethyl alcohol again, precipitation is precipitated, precipitation is washed 5 times with absolute ethyl alcohol, then be 55 DEG C in temperature and dry to constant weight,
Up to modified beta-cyclodextrin.
The preparation method of above-mentioned Europe mandarin orange fruits and vegetables pressed candy, includes the following steps:
(1) bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder are mixed
It closes uniformly, obtains mixture;
(2) it is 1 in mass ratio by starch and 20 DEG C of cold water:1 after mixing, adds 100 DEG C of 8 times of starch weight
It is uniformly mixed in hot water, obtains starch slurry;
(3) it is 1 in mass ratio by the starch slurry that the mixture that step (1) obtains is obtained with step (2):0.035 mixing is equal
It is even, obtain wet feed;
(4) by the YK-160 oscillating granulators of the wet feed Stainless Steel sieve for being equipped with 12-14 mesh (the color way machinery in Nanjing
Equipment Co., Ltd provides) granulation, scattered non-homogeneous shape wet granular is obtained, wet granular is laid on pallet, thickness control
For system at 4-5 centimetres, it is 4wt% to be dried to water content under 55 degrees Celsius, obtains dry particl;
(5) by dry particl and magnesium stearate with rotating speed for 500r/min mixing 10min, obtain the dry particl for waiting for tabletting;It will
Wait for that the dry particl of tabletting passes through mechanical pressurization with ZP-9B types rotary tablet machine (offer of Guangzhou Chen Diao mechanical equipments Co., Ltd)
Molding is to get Europe mandarin orange fruits and vegetables pressed candy.
Embodiment 4
Europe mandarin orange fruits and vegetables pressed candy, including the raw material of following weight parts are prepared:150 parts of bowl mandarin orange powder, 15 parts of salt algae powder,
It is 15 parts of cherry powder, 80 parts of pectase powder, 300 parts of oatmeal, 100 parts of D-sorbite, 15 parts of sodium bicarbonate, 100 parts of vegetable fat powder, hard
0.8 part of fatty acid magnesium.
The preparation method of the salt algae powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by salt algae, is crushed to
100 mesh to obtain the final product.
The preparation method of the cherry powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by cherry, will be dried
Cherry kernel removing afterwards is crushed to 100 mesh to obtain the final product.
The preparation method of the vegetable fat powder is:It is in mass ratio by rapeseed oil, casein sodium, glucose, maltodextrin
1:0.08:0.12:1 be uniformly mixed to get.
The preparation method of the bowl mandarin orange powder is:Bowl mandarin orange is eluted with water, is drained;Bowl mandarin orange after draining freezes at -10 DEG C
Bowl mandarin orange after freezing is crushed to 20 mesh, by the bowl after crushing by 20h in the environment of temperature is -10 DEG C using freezing crusher
Mandarin orange is 1 in mass ratio with water:It is beaten in 0.2 addition beater, crosses 200 mesh sieve, obtain slurries;By slurries, modified β-ring
Dextrin, stearoyl lactate, D-araboascorbic acid laurate are 1 in mass ratio:0.03:0.008:0.003 is uniformly mixed, spray
Mist is dried, and the inlet air temperature of the spray drying is 180 DEG C, and leaving air temp is 75 DEG C, and hot wind wind speed is 4m3/ min, feed speed
Degree is 40mL/min, and atomizer rotating speed is 300 revs/min to get bowl mandarin orange powder.
The preparation method of the modified beta-cyclodextrin is:It is 1 in mass ratio by citric acid, sodium hypophosphite, water:0.2:1
It is uniformly mixed, adds the beta-cyclodextrin of 2 times of citric acid weight, it is that 300r/min stirs 15min to be warming up to 80 DEG C with rotating speed, is obtained
To mixed liquor;By mixed liquor be placed in blowing-type thermostatic drying chamber first temperature be 100 DEG C baking 60min, then temperature be 120 DEG C
5h is dried, after reaction by the water dissolution of 1.5 times of reaction product weight of reaction product, then is added dropwise in absolute ethyl alcohol, is precipitated
Precipitation, precipitation is washed 5 times with absolute ethyl alcohol, then is 55 DEG C in temperature and is dried to constant weight to get modified beta-cyclodextrin.
The preparation method of above-mentioned Europe mandarin orange fruits and vegetables pressed candy, includes the following steps:
(1) bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder are mixed
It closes uniformly, obtains mixture;
(2) it is 1 in mass ratio by starch and 20 DEG C of cold water:1 after mixing, adds 100 DEG C of 8 times of starch weight
It is uniformly mixed in hot water, obtains starch slurry;
(3) it is 1 in mass ratio by the starch slurry that the mixture that step (1) obtains is obtained with step (2):0.035 mixing is equal
It is even, obtain wet feed;
(4) by the YK-160 oscillating granulators of the wet feed Stainless Steel sieve for being equipped with 12-14 mesh (the color way machinery in Nanjing
Equipment Co., Ltd provides) granulation, scattered non-homogeneous shape wet granular is obtained, wet granular is laid on pallet, thickness control
For system at 4-5 centimetres, it is 4wt% to be dried to water content under 55 degrees Celsius, obtains dry particl;
(5) by dry particl and magnesium stearate with rotating speed for 500r/min mixing 10min, obtain the dry particl for waiting for tabletting;It will
Wait for that the dry particl of tabletting passes through mechanical pressurization with ZP-9B types rotary tablet machine (offer of Guangzhou Chen Diao mechanical equipments Co., Ltd)
Molding is to get Europe mandarin orange fruits and vegetables pressed candy.
Embodiment 5
Europe mandarin orange fruits and vegetables pressed candy, including the raw material of following weight parts are prepared:150 parts of bowl mandarin orange powder, 15 parts of salt algae powder,
It is 15 parts of cherry powder, 80 parts of pectase powder, 300 parts of oatmeal, 100 parts of D-sorbite, 15 parts of sodium bicarbonate, 100 parts of vegetable fat powder, hard
0.8 part of fatty acid magnesium.
The preparation method of the salt algae powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by salt algae, is crushed to
100 mesh to obtain the final product.
The preparation method of the cherry powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by cherry, will be dried
Cherry kernel removing afterwards is crushed to 100 mesh to obtain the final product.
The preparation method of the vegetable fat powder is:It is in mass ratio by rapeseed oil, casein sodium, glucose, maltodextrin
1:0.08:0.12:1 be uniformly mixed to get.
The preparation method of the bowl mandarin orange powder is:Bowl mandarin orange is eluted with water, is drained;Bowl mandarin orange after draining freezes at -10 DEG C
Bowl mandarin orange after freezing is crushed to 20 mesh, by the bowl after crushing by 20h in the environment of temperature is -10 DEG C using freezing crusher
Mandarin orange is 1 in mass ratio with water:It is beaten in 0.2 addition beater, crosses 200 mesh sieve, obtain slurries;By slurries, modified β-ring
Dextrin, stearoyl lactate, ascorbyl palmitate are 1 in mass ratio:0.03:0.008:0.003 is uniformly mixed, and spraying is dry
Dry, the inlet air temperature of the spray drying is 180 DEG C, and leaving air temp is 75 DEG C, and hot wind wind speed is 4m3/ min, feeding speed are
40mL/min, atomizer rotating speed are 300 revs/min to get bowl mandarin orange powder.
The preparation method of the modified beta-cyclodextrin is:By citric acid, 2- octenyl succinic acid anhydrides, sodium hypophosphite, water
It is 1 in mass ratio:0.05:0.2:1 is uniformly mixed, and adds the beta-cyclodextrin of 2 times of citric acid weight, is warming up to 80 DEG C with rotating speed
15min is stirred for 300r/min, obtains mixed liquor;It is 100 DEG C in temperature that mixed liquor, which is placed in blowing-type thermostatic drying chamber first,
60min is dried, then in temperature is 120 DEG C of baking 5h, after reaction by the water dissolution of 1.5 times of reaction product weight of reaction product,
It is added dropwise in absolute ethyl alcohol again, precipitation is precipitated, precipitation is washed 5 times with absolute ethyl alcohol, then be 55 DEG C in temperature and dry to constant weight,
Up to modified beta-cyclodextrin.
The present invention also provides the preparation methods of above-mentioned Europe mandarin orange fruits and vegetables pressed candy, include the following steps:
(1) bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder are mixed
It closes uniformly, obtains mixture;
(2) it is 1 in mass ratio by starch and 20 DEG C of cold water:1 after mixing, adds 100 DEG C of 8 times of starch weight
It is uniformly mixed in hot water, obtains starch slurry;
(3) it is 1 in mass ratio by the starch slurry that the mixture that step (1) obtains is obtained with step (2):0.035 mixing is equal
It is even, obtain wet feed;
(4) by the YK-160 oscillating granulators of the wet feed Stainless Steel sieve for being equipped with 12-14 mesh (the color way machinery in Nanjing
Equipment Co., Ltd provides) granulation, scattered non-homogeneous shape wet granular is obtained, wet granular is laid on pallet, thickness control
For system at 4-5 centimetres, it is 4wt% to be dried to water content under 55 degrees Celsius, obtains dry particl;
(5) by dry particl and magnesium stearate with rotating speed for 500r/min mixing 10min, obtain the dry particl for waiting for tabletting;It will
Wait for that the dry particl of tabletting passes through mechanical pressurization with ZP-9B types rotary tablet machine (offer of Guangzhou Chen Diao mechanical equipments Co., Ltd)
Molding is to get Europe mandarin orange fruits and vegetables pressed candy.
Embodiment 6
Europe mandarin orange fruits and vegetables pressed candy, including the raw material of following weight parts are prepared:150 parts of bowl mandarin orange powder, 15 parts of salt algae powder,
It is 15 parts of cherry powder, 80 parts of pectase powder, 300 parts of oatmeal, 100 parts of D-sorbite, 15 parts of sodium bicarbonate, 100 parts of vegetable fat powder, hard
0.8 part of fatty acid magnesium.
The preparation method of the salt algae powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by salt algae, is crushed to
100 mesh to obtain the final product.
The preparation method of the cherry powder is:It is 5wt% to be dried to water content at being 50 DEG C in temperature by cherry, will be dried
Cherry kernel removing afterwards is crushed to 100 mesh to obtain the final product.
The preparation method of the vegetable fat powder is:It is in mass ratio by rapeseed oil, casein sodium, glucose, maltodextrin
1:0.08:0.12:1 be uniformly mixed to get.
The preparation method of the bowl mandarin orange powder is:Bowl mandarin orange is eluted with water, is drained;Bowl mandarin orange after draining freezes at -10 DEG C
Bowl mandarin orange after freezing is crushed to 20 mesh, by the bowl after crushing by 20h in the environment of temperature is -10 DEG C using freezing crusher
Mandarin orange is 1 in mass ratio with water:It is beaten in 0.2 addition beater, crosses 200 mesh sieve, obtain slurries;By slurries, modified β-ring
Dextrin, stearoyl lactate, D-araboascorbic acid laurate, ascorbyl palmitate are 1 in mass ratio:0.03:
0.008:0.002:0.001 is uniformly mixed, spray drying, and the inlet air temperature of the spray drying is 180 DEG C, leaving air temp 75
DEG C, hot wind wind speed is 4m3/ min, feeding speed 40mL/min, atomizer rotating speed are 300 revs/min to get bowl mandarin orange powder.
The preparation method of the modified beta-cyclodextrin is:By citric acid, 2- octenyl succinic acid anhydrides, sodium hypophosphite, water
It is 1 in mass ratio:0.05:0.2:1 is uniformly mixed, and adds the beta-cyclodextrin of 2 times of citric acid weight, is warming up to 80 DEG C with rotating speed
15min is stirred for 300r/min, obtains mixed liquor;It is 100 DEG C in temperature that mixed liquor, which is placed in blowing-type thermostatic drying chamber first,
60min is dried, then in temperature is 120 DEG C of baking 5h, after reaction by the water dissolution of 1.5 times of reaction product weight of reaction product,
It is added dropwise in absolute ethyl alcohol again, precipitation is precipitated, precipitation is washed 5 times with absolute ethyl alcohol, then be 55 DEG C in temperature and dry to constant weight,
Up to modified beta-cyclodextrin.
The present invention also provides the preparation methods of above-mentioned Europe mandarin orange fruits and vegetables pressed candy, include the following steps:
(1) bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder are mixed
It closes uniformly, obtains mixture;
(2) it is 1 in mass ratio by starch and 20 DEG C of cold water:1 after mixing, adds 100 DEG C of 8 times of starch weight
It is uniformly mixed in hot water, obtains starch slurry;
(3) it is 1 in mass ratio by the starch slurry that the mixture that step (1) obtains is obtained with step (2):0.035 mixing is equal
It is even, obtain wet feed;
(4) by the YK-160 oscillating granulators of the wet feed Stainless Steel sieve for being equipped with 12-14 mesh (the color way machinery in Nanjing
Equipment Co., Ltd provides) granulation, scattered non-homogeneous shape wet granular is obtained, wet granular is laid on pallet, thickness control
For system at 4-5 centimetres, it is 4wt% to be dried to water content under 55 degrees Celsius, obtains dry particl;
(5) by dry particl and magnesium stearate with rotating speed for 500r/min mixing 10min, obtain the dry particl for waiting for tabletting;It will
Wait for that the dry particl of tabletting passes through mechanical pressurization with ZP-9B types rotary tablet machine (offer of Guangzhou Chen Diao mechanical equipments Co., Ltd)
Molding is to get Europe mandarin orange fruits and vegetables pressed candy.
Test case 1
The Europe mandarin orange fruits and vegetables pressed candy of embodiment 2-6 is subjected to treatment anti-constipation effect test.
1, patient data
150 constipation patients are selected, the course of disease was at 1 year to 2 years, age 35-45 Sui, average age 42 years old;By 150 patients
5 groups are randomly divided into, uses the Europe mandarin orange fruits and vegetables pressed candy of embodiment 2-6 respectively.
2, therapy
Treatment time is 6 weeks, takes the Europe 2g mandarin orange fruits and vegetables pressed candy oral daily.
3, treatment results:
Treat evaluation criteria judgement:
It cures:Constipation symptom disappears, daily defecation 2 times or more;
Effectively:Constipation symptom mitigates and alleviates, daily or every two days defecations 1 time;
In vain:Constipation symptom is without alleviation, and defecation is primary within every 3 days or more.
Specific treatment results are shown in Table 1.The relatively rear P< of each group therapeutic effect;0.05, difference has statistical significance.
Table 1:Therapeutic effect tables of data
| It cures | Effectively | In vain | |
| Embodiment 2 | 22 | 4 | 4 |
| Embodiment 3 | 25 | 4 | 1 |
| Embodiment 4 | 23 | 5 | 2 |
| Embodiment 5 | 24 | 4 | 2 |
| Embodiment 6 | 27 | 3 | 0 |
Test case 2
The Europe mandarin orange powder prepared in embodiment 2-6 is subjected to DPPH free radical scavenging abilities and stability test.Specific test
It the results are shown in Table 2.
Table 2:DPPH free radical scavenging activity tables of data
Europe mandarin orange fruits and vegetables pressed candy of the present invention, Europe mandarin orange fruits and vegetables pressed candy, preparation method is simple, convenient, nutrition
Material abundance, mouthfeel is very good, has the function of invigorating the spleen, reducing blood lipid, removes interior free yl, improving eyesight and cancer-preventing health, also has
The effect of improving constipation, weight-reducing.
Claims (10)
1. a kind of Europe mandarin orange fruits and vegetables pressed candy, which is characterized in that including following raw materials:Bowl mandarin orange powder, salt algae powder, cherry powder, fruits and vegetables
Ferment powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder, magnesium stearate.
2. a kind of Europe mandarin orange fruits and vegetables pressed candy, which is characterized in that the raw material including following weight parts is prepared:Bowl mandarin orange powder 100-
350 parts, 5-30 parts of salt algae powder, 5-30 parts of cherry powder, 50-100 parts of pectase powder, 200-400 parts of oatmeal, D-sorbite 60-
200 parts, 5-30 parts of sodium bicarbonate, 60-200 parts of vegetable fat powder, 0.5-1 parts of magnesium stearate.
3. Europe mandarin orange fruits and vegetables pressed candy as claimed in claim 2, which is characterized in that the preparation method of the salt algae powder is:It will
It is 4-8wt% that salt algae, which is dried at being 45-65 DEG C in temperature to water content, is crushed to 80-140 mesh to obtain the final product.
4. Europe mandarin orange fruits and vegetables pressed candy as claimed in claim 2, which is characterized in that the preparation method of the cherry powder is:It will
It is 4-8wt% that cherry, which is dried at being 45-65 DEG C in temperature to water content, by the cherry kernel removing after drying, is crushed to 80-140 mesh
To obtain the final product.
5. Europe mandarin orange fruits and vegetables pressed candy as claimed in claim 2, which is characterized in that the preparation method of the vegetable fat powder is:It will
Vegetable oil, casein sodium, glucose, maltodextrin are 1 in mass ratio:(0.05-0.25):(0.1-0.2):(0.5-2) is mixed
Close uniformly to get;The vegetable oil includes one or more in soybean oil, sesame oil, peanut oil, rapeseed oil.
6. Europe mandarin orange fruits and vegetables pressed candy as claimed in claim 2, which is characterized in that the preparation method of the bowl mandarin orange powder is:It will
Bowl mandarin orange is eluted with water, and drains;Bowl mandarin orange after draining freezes 15-25h at -5~-20 DEG C, by the bowl mandarin orange after freezing temperature be -
10-30 mesh is crushed to using freezing crusher in the environment of 5~-20 DEG C, is 1 in mass ratio by bowl mandarin orange and the water after crushing:
(0.1-0.5) is added in beater and is beaten, and crosses 50-300 mesh sieve, obtains slurries;By slurries, beta-cyclodextrin, stearoyl breast
Sour sodium, antioxidant are 1 in mass ratio:(0.02-0.06):(0.005-0.02):(0.001-0.005) is uniformly mixed, and spraying is dry
It is dry to get.
7. Europe mandarin orange fruits and vegetables pressed candy as claimed in claim 2, which is characterized in that the preparation method of the bowl mandarin orange powder is:It will
Bowl mandarin orange is eluted with water, and drains;Bowl mandarin orange after draining freezes 15-25h at -5~-20 DEG C, by the bowl mandarin orange after freezing temperature be -
10-30 mesh is crushed to using freezing crusher in the environment of 5~-20 DEG C, is 1 in mass ratio by bowl mandarin orange and the water after crushing:
(0.1-0.5) is added in beater and is beaten, and crosses 50-300 mesh sieve, obtains slurries;By slurries, modified beta-cyclodextrin, tristearin
Acyl lactylate, antioxidant are 1 in mass ratio:(0.02-0.06):(0.005-0.02):(0.001-0.005) is uniformly mixed, spray
Mist drying to get.
8. Europe mandarin orange fruits and vegetables pressed candy as claimed in claim 7, which is characterized in that the preparation method of the modified beta-cyclodextrin
For:It is 1 in mass ratio by citric acid, 2- octenyl succinic acid anhydrides, sodium hypophosphite, water:(0.03-0.09):(0.1-0.3):
(0.8-1.1) is uniformly mixed, and is added the beta-cyclodextrin of 1-3 times of citric acid weight, is warming up to 75-85 DEG C with rotating speed as 200-
500r/min stirs 10-20min, obtains mixed liquor;It is 95- in temperature that mixed liquor, which is placed in blowing-type thermostatic drying chamber first,
105 DEG C of baking 50-70min, then be 110-130 DEG C in temperature and dry 3-7h, after reaction by reaction product reaction product weight
1-3 times of water dissolution, then be added dropwise in absolute ethyl alcohol, precipitation is precipitated, precipitation is washed 2-6 times with absolute ethyl alcohol, then in temperature
For 50-60 DEG C it is dry to constant weight to get.
9. Europe mandarin orange fruits and vegetables pressed candy as claimed in claim 7, which is characterized in that the antioxidant is the D-araboascorbic acid moon
Cinnamic acid ester and/or ascorbyl palmitate.
10. the preparation method of Europe mandarin orange fruits and vegetables pressed candy, includes the following steps as described in any one of claim 1-9:
(1) bowl mandarin orange powder, salt algae powder, cherry powder, pectase powder, oatmeal, D-sorbite, sodium bicarbonate, vegetable fat powder are mixed equal
It is even, obtain mixture;
(2) it is 1 in mass ratio by starch and cold water:(0.5-1.5) after mixing, adds the heat of starch weight (5-10) times
It is uniformly mixed in water, obtains starch slurry;
(3) it is 1 in mass ratio by the starch slurry that the mixture that step (1) obtains is obtained with step (2):(0.01-0.05) is mixed
Uniformly, wet feed is obtained;
(4) wet feed is pelletized with granulator, it is dry, obtain dry particl;
(5) dry particl is mixed with magnesium stearate, tabletting to get.
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| CN110313536A (en) * | 2019-07-06 | 2019-10-11 | 孙杨 | A kind of seaweed ferment pressed candy formula and preparation method |
| CN113040253A (en) * | 2021-04-30 | 2021-06-29 | 和宜佳(广东)健康科技有限公司 | Tabletting candy for relaxing bowels and preparation method thereof |
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Application publication date: 20181023 |