CN108675578A - A kind of deodorant and preparation method thereof for livestock and poultry feces processing - Google Patents

A kind of deodorant and preparation method thereof for livestock and poultry feces processing Download PDF

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Publication number
CN108675578A
CN108675578A CN201810598909.XA CN201810598909A CN108675578A CN 108675578 A CN108675578 A CN 108675578A CN 201810598909 A CN201810598909 A CN 201810598909A CN 108675578 A CN108675578 A CN 108675578A
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parts
livestock
deionized water
weight
poultry feces
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王静
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Mengcheng County Jing Huizhou Agricultural Science And Technology Development Co Ltd
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Mengcheng County Jing Huizhou Agricultural Science And Technology Development Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/30Sulfur compounds
    • B01D2257/304Hydrogen sulfide
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/30Sulfur compounds
    • B01D2257/306Organic sulfur compounds, e.g. mercaptans
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/40Nitrogen compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/40Nitrogen compounds
    • B01D2257/406Ammonia
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/70Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00Specific treatment goals
    • C02F2303/02Odour removal or prevention of malodour

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  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Preparation Of Fruits And Vegetables (AREA)

Abstract

The invention discloses a kind of deodorant for livestock and poultry feces processing, including following raw material:Purple perilla, Chinese ilex, betel nut, Herba Andrographitis, spearmint, rhizoma imperatae, garlic, Lignum Aquilariae Resinatum extract, Lotus Leafextract, deionized water, lauryl sodium sulfate.The invention also discloses the preparation methods of the deodorant for livestock and poultry feces processing.Deodorant for livestock and poultry feces processing prepared by the present invention has good deodorizing effect, is cooperated by Lignum Aquilariae Resinatum extract and Lotus Leafextract, plays synergistic effect, can effectively improve deodorizing effect, especially notable to the removal effect of hydrogen sulfide;Simultaneously as active ingredient is all extracted from natural plants, health environment-friendly without any side effects to operating personnel;It is carried out in fermentation treatments moreover, can be used for livestock and poultry feces, avoids when use is applied fertilizer using livestock and poultry feces as the organic fertilizer that raw material produces and people and plant are damaged.

Description

A kind of deodorant and preparation method thereof for livestock and poultry feces processing
Technical field
The present invention relates to livestock and poultry feces process field, specifically a kind of deodorant and its preparation for livestock and poultry feces processing Method.
Background technology
With the continuous development of science and technology, animal husbandry is also increasingly towards intensive, large-scale development, still, livestock and poultry cultivation In livestock and poultry feces pollution problem increasingly become a great environmental problem, in order to reduce dirt of the livestock and poultry feces to environment Dye, the means that usually livestock and poultry feces are carried out with fermenting and producing organic fertilizer comprehensively utilize, still, during the fermentation, by It will produce strong stench in livestock and poultry feces, these stink odors include the nitrogen compounds such as ammonia, amine;Hydrogen sulfide, methyl sulphur The chalcogenide compounds such as alcohol;The aliphatic acid such as acetic acid, isovaleric acid, caproic acid;Aldehyde such as formaldehyde, acetaldehyde etc. can not only cause human body Harm, can also pollute atmospheric environment.Therefore, design it is a kind of for livestock and poultry feces processing deodorant, become there is an urgent need for solution Certainly the problem of.
Invention content
The purpose of the present invention is to provide a kind of deodorant and preparation method thereof for livestock and poultry feces processing, in solution State the problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions:
A kind of deodorant for livestock and poultry feces processing, including below according to the raw material of parts by weight:2-8 parts of purple perilla, Chinese ilex 10-20 parts, 5-12 parts of betel nut, 10-17 parts of Herba Andrographitis, 1-6 parts of spearmint, 2-9 parts of rhizoma imperatae, 2-9 parts of garlic, Lignum Aquilariae Resinatum extract 3-10 parts, 2-10 parts of Lotus Leafextract, 40-58 parts of deionized water, 0.2-2 parts of lauryl sodium sulfate.
As a further solution of the present invention:Including below according to the raw material of parts by weight:4-7 parts of purple perilla, Chinese ilex 12-18 Part, 7-10 parts of betel nut, 12-15 parts of Herba Andrographitis, 2-5 parts of spearmint, 4-7 parts of rhizoma imperatae, 4-7 parts of garlic, Lignum Aquilariae Resinatum extract 5-8 Part, 3-7 parts of Lotus Leafextract, 45-55 parts of deionized water, 0.5-1.5 parts of lauryl sodium sulfate.
As further scheme of the invention:Including below according to the raw material of parts by weight:6 parts of purple perilla, 15 parts of Chinese ilex, Bin Bulky 8 parts, 14 parts of Herba Andrographitis, 4 parts of spearmint, 6 parts of rhizoma imperatae, 6 parts of garlic, 7 parts of Lignum Aquilariae Resinatum extract, 4 parts of Lotus Leafextract, go from 50 parts of sub- water, 1 part of lauryl sodium sulfate.
As further scheme of the invention:The preparation method of the Lignum Aquilariae Resinatum extract is to clean agalloch eaglewood, is dried, powder It is put into percolator after being broken to 40-80 mesh, diacolation processing, the pure glutinous rice wine is carried out with the pure glutinous rice wine of 12-18 times of weight Alcoholic strength be 20-35 °, the percolate of acquisition is then recycled into pure glutinous rice wine therein by way of distillation, then through 600 mesh Filtering, obtains the Lignum Aquilariae Resinatum extract.
As further scheme of the invention:The preparation method of the Lotus Leafextract is that lotus leaf deionized water is clear It washes 4-6 times, dries, the deionized water of 16-24 times of weight is then added, carrying out high temperature and pressure using steam pressure cooker equipment carries It takes, extracting solution is concentrated under reduced pressure, then obtains the Lotus Leafextract after the filtering of 800 mesh.
The preparation method of the deodorant for livestock and poultry feces processing, steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 4-6 times with deionized water, must mixed after co-grinding Expect A;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly After stand 20-60min, be added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, it is broken using ultrasonic wave Wall technique is ultrasonically treated, then is filtered through 80 mesh screens, and liquor B and filter residue C are obtained;
3) deionized water of 16-24 times of weight will be added in the filter residue C obtained in step 2), using steam pressure cooker equipment High temperature and pressure extraction is carried out, extracting solution is uniformly mixed with the liquor B obtained in step 2), is recycled wherein by way of distillation Absolute ethyl alcohol, then through 400 mesh filter, obtain mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 4-6 times with deionized water, be then fed into juice extractor and squeeze the juice, then pass through The filtering of 40 mesh screens is crossed, filtrate E is obtained;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 4-6 times with deionized water, after co-grinding Obtain mixture F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), after stirring evenly Filtrate E, the mechanical agitation 20-60min obtained in step 4) is added, adds absolute ethyl alcohol, the absolute ethyl alcohol and mixture F Volume ratio be 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, then filtered through 80 mesh screens, obtains filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 16-24 times of weight, using steam pressure cooker equipment into Row high temperature and pressure is extracted, and the pressure of the high temperature and pressure extraction is 0.4-0.8MPa, time 20-30min, by extracting solution and step It is rapid 6) in obtained filtrate G be uniformly mixed, absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, obtained mixed Close liquid H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract And Lotus Leafextract, ultrasonic disperse 5-15min, it sequentially adds the mixed liquor D obtained in step 3) and is obtained in step 7) mixed Close liquid H, mechanical agitation 10-30min to get.
As further scheme of the invention:In step 2), the condition of the supersound process is ultrasonic power 80- 250W, ultrasonic time 10-50min.
As further scheme of the invention:In step 3), the pressure of the high temperature and pressure extraction is 0.4-0.8MPa, Time is 20-30min.
As further scheme of the invention:In step 6), the condition of the supersound process is ultrasonic power 100- 300W, ultrasonic time 15-45min.
The application for the deodorant of livestock and poultry feces processing in preparing deodorant.
Agalloch eaglewood, acrid flavour, hardship, slightly warm in nature, have the effect of reconcile strength, benefit mend internal organs, operation qi and blood, can antibacterial anti-inflammatory, Anti- inflammation, anti-spasm promote cell metabolism and cytothesis function, meanwhile, endocrine organ is adjusted, promotes hormone Brain fatigue is eliminated in secretion, help, is releived, is restored balance of body and spirit, gentle mood helps qi-blood circulating, help to be metabolized liver kidney poison Element enhances immunocompetence.
Lotus leaf, nature and flavor are bitter, put down, and Return liver, spleen, stomach, the heart channel of Hang-Shaoyin have clearing summer-heat and damp, sending up the lucid yang, cooling blood and hemostasis and other effects, But also there is antimitotic effect.
Compared with prior art, the beneficial effects of the invention are as follows:
Deodorant for livestock and poultry feces processing prepared by the present invention has good deodorizing effect, passes through Lignum Aquilariae Resinatum extract It cooperates with Lotus Leafextract, plays synergistic effect, deodorizing effect can be effectively improved, especially to hydrogen sulfide Removal effect is notable;Simultaneously as active ingredient is all extracted from natural plants, it is without any side effects to operating personnel, Health environment-friendly;Moreover, when carrying out fermentation process for livestock and poultry feces, will not as chemical deodorizing agent or microbial deodorant to Livestock and poultry feces be raw material production organic fertilizer generation pollute, avoid use produced using livestock and poultry feces as raw material it is organic People and plant are damaged when fertilizer is applied fertilizer, securely and reliably, have a vast market foreground.
Specific implementation mode
Technical scheme of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of deodorant for livestock and poultry feces processing, including below according to the raw material of parts by weight:2-8 parts of purple perilla, Chinese ilex 10-20 parts, 5-12 parts of betel nut, 10-17 parts of Herba Andrographitis, 1-6 parts of spearmint, 2-9 parts of rhizoma imperatae, 2-9 parts of garlic, Lignum Aquilariae Resinatum extract 3-10 parts, 2-10 parts of Lotus Leafextract, 40-58 parts of deionized water, 0.2-2 parts of lauryl sodium sulfate.Wherein, the agalloch eaglewood carries It is to clean agalloch eaglewood to take the preparation method of object, is dried, and is put into percolator after being crushed to 60 mesh, with the pure glutinous rice of 16 times of weight Wine carries out diacolation processing, and the alcoholic strength of the pure glutinous rice wine is 30 °, then recycles the percolate of acquisition by way of distillation Pure glutinous rice wine therein, then filtered through 600 mesh, obtain the Lignum Aquilariae Resinatum extract;The preparation method of the Lotus Leafextract is by lotus Leaf is cleaned 6 times with deionized water, then the deionized water of 20 times of weight is added in drying, is carried out using steam pressure cooker equipment high Warm high pressure extraction, extracting solution are concentrated under reduced pressure, then obtain the Lotus Leafextract after the filtering of 800 mesh.
In the present embodiment, the preparation method of the deodorant for livestock and poultry feces processing, steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 5 times with deionized water, mixture is obtained after co-grinding A;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly After stand 40min, be added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, using supersonic wave wall breaking skill Art is ultrasonically treated, and the condition of the supersound process is ultrasonic power 150W, ultrasonic time 30min, after the completion of ultrasound again It is filtered through 80 mesh screens, obtains liquor B and filter residue C;
3) will in the filter residue C that obtained in step 2) be added 20 times of weight deionized water, using steam pressure cooker equipment into Row high temperature and pressure is extracted, and the pressure of high temperature and pressure extraction is 0.6MPa, time 25min, will extracting solution in step 2) Obtained liquor B is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 5 times with deionized water, is then fed into juice extractor and squeezes the juice, using 40 mesh screens filter, and obtain filtrate E;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 5 times with deionized water, after co-grinding Mixture F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), after stirring evenly Filtrate E, the mechanical agitation 40min obtained in step 4) is added, adds absolute ethyl alcohol, the absolute ethyl alcohol is with mixture F's Volume ratio is 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 200W, ultrasonic time 30min, ultrasound are filtered through 80 mesh screens again after the completion, obtain filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 20 times of weight, is carried out using steam pressure cooker equipment High temperature and pressure is extracted, and the pressure of the high temperature and pressure extraction is 0.6MPa, time 25min, will be obtained in extracting solution and step 6) The filtrate G arrived is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract And Lotus Leafextract, ultrasonic disperse 8min, the mixed liquor for sequentially adding the mixed liquor D obtained in step 3) and being obtained in step 7) H, mechanical agitation 20min to get.
Embodiment 2
A kind of deodorant for livestock and poultry feces processing, including below according to the raw material of parts by weight:2-8 parts of purple perilla, Chinese ilex 10-20 parts, 5-12 parts of betel nut, 10-17 parts of Herba Andrographitis, 1-6 parts of spearmint, 2-9 parts of rhizoma imperatae, 2-9 parts of garlic, Lignum Aquilariae Resinatum extract 3-10 parts, 2-10 parts of Lotus Leafextract, 40-58 parts of deionized water, 0.2-2 parts of lauryl sodium sulfate.Wherein, the agalloch eaglewood carries It is to clean agalloch eaglewood to take the preparation method of object, is dried, and is put into percolator after being crushed to 60 mesh, with the pure glutinous rice of 16 times of weight Wine carries out diacolation processing, and the alcoholic strength of the pure glutinous rice wine is 30 °, then recycles the percolate of acquisition by way of distillation Pure glutinous rice wine therein, then filtered through 600 mesh, obtain the Lignum Aquilariae Resinatum extract;The preparation method of the Lotus Leafextract is by lotus Leaf is cleaned 6 times with deionized water, then the deionized water of 20 times of weight is added in drying, is carried out using steam pressure cooker equipment high Warm high pressure extraction, extracting solution are concentrated under reduced pressure, then obtain the Lotus Leafextract after the filtering of 800 mesh.
In the present embodiment, the preparation method of the deodorant for livestock and poultry feces processing, steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 5 times with deionized water, mixture is obtained after co-grinding A;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly After stand 40min, be added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, using supersonic wave wall breaking skill Art is ultrasonically treated, and the condition of the supersound process is ultrasonic power 150W, ultrasonic time 30min, after the completion of ultrasound again It is filtered through 80 mesh screens, obtains liquor B and filter residue C;
3) will in the filter residue C that obtained in step 2) be added 20 times of weight deionized water, using steam pressure cooker equipment into Row high temperature and pressure is extracted, and the pressure of high temperature and pressure extraction is 0.6MPa, time 25min, will extracting solution in step 2) Obtained liquor B is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 5 times with deionized water, is then fed into juice extractor and squeezes the juice, using 40 mesh screens filter, and obtain filtrate E;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 5 times with deionized water, after co-grinding Mixture F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), after stirring evenly Filtrate E, the mechanical agitation 40min obtained in step 4) is added, adds absolute ethyl alcohol, the absolute ethyl alcohol is with mixture F's Volume ratio is 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 200W, ultrasonic time 30min, ultrasound are filtered through 80 mesh screens again after the completion, obtain filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 20 times of weight, is carried out using steam pressure cooker equipment High temperature and pressure is extracted, and the pressure of the high temperature and pressure extraction is 0.6MPa, time 25min, will be obtained in extracting solution and step 6) The filtrate G arrived is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract And Lotus Leafextract, ultrasonic disperse 8min, the mixed liquor for sequentially adding the mixed liquor D obtained in step 3) and being obtained in step 7) H, mechanical agitation 20min to get.
Embodiment 3
A kind of deodorant for livestock and poultry feces processing, including below according to the raw material of parts by weight:2-8 parts of purple perilla, Chinese ilex 10-20 parts, 5-12 parts of betel nut, 10-17 parts of Herba Andrographitis, 1-6 parts of spearmint, 2-9 parts of rhizoma imperatae, 2-9 parts of garlic, Lignum Aquilariae Resinatum extract 3-10 parts, 2-10 parts of Lotus Leafextract, 40-58 parts of deionized water, 0.2-2 parts of lauryl sodium sulfate.Wherein, the agalloch eaglewood carries It is to clean agalloch eaglewood to take the preparation method of object, is dried, and is put into percolator after being crushed to 60 mesh, with the pure glutinous rice of 16 times of weight Wine carries out diacolation processing, and the alcoholic strength of the pure glutinous rice wine is 30 °, then recycles the percolate of acquisition by way of distillation Pure glutinous rice wine therein, then filtered through 600 mesh, obtain the Lignum Aquilariae Resinatum extract;The preparation method of the Lotus Leafextract is by lotus Leaf is cleaned 6 times with deionized water, then the deionized water of 20 times of weight is added in drying, is carried out using steam pressure cooker equipment high Warm high pressure extraction, extracting solution are concentrated under reduced pressure, then obtain the Lotus Leafextract after the filtering of 800 mesh.
In the present embodiment, the preparation method of the deodorant for livestock and poultry feces processing, steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 5 times with deionized water, mixture is obtained after co-grinding A;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly After stand 40min, be added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, using supersonic wave wall breaking skill Art is ultrasonically treated, and the condition of the supersound process is ultrasonic power 150W, ultrasonic time 30min, after the completion of ultrasound again It is filtered through 80 mesh screens, obtains liquor B and filter residue C;
3) will in the filter residue C that obtained in step 2) be added 20 times of weight deionized water, using steam pressure cooker equipment into Row high temperature and pressure is extracted, and the pressure of high temperature and pressure extraction is 0.6MPa, time 25min, will extracting solution in step 2) Obtained liquor B is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 5 times with deionized water, is then fed into juice extractor and squeezes the juice, using 40 mesh screens filter, and obtain filtrate E;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 5 times with deionized water, after co-grinding Mixture F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), after stirring evenly Filtrate E, the mechanical agitation 40min obtained in step 4) is added, adds absolute ethyl alcohol, the absolute ethyl alcohol is with mixture F's Volume ratio is 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 200W, ultrasonic time 30min, ultrasound are filtered through 80 mesh screens again after the completion, obtain filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 20 times of weight, is carried out using steam pressure cooker equipment High temperature and pressure is extracted, and the pressure of the high temperature and pressure extraction is 0.6MPa, time 25min, will be obtained in extracting solution and step 6) The filtrate G arrived is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract And Lotus Leafextract, ultrasonic disperse 8min, the mixed liquor for sequentially adding the mixed liquor D obtained in step 3) and being obtained in step 7) H, mechanical agitation 20min to get.
Embodiment 4
A kind of deodorant for livestock and poultry feces processing, including below according to the raw material of parts by weight:4-7 parts of purple perilla, Chinese ilex 12-18 parts, 7-10 parts of betel nut, 12-15 parts of Herba Andrographitis, 2-5 parts of spearmint, 4-7 parts of rhizoma imperatae, 4-7 parts of garlic, Lignum Aquilariae Resinatum extract 5-8 parts, 3-7 parts of Lotus Leafextract, 45-55 parts of deionized water, 0.5-1.5 parts of lauryl sodium sulfate.Wherein, the agalloch eaglewood carries It is to clean agalloch eaglewood to take the preparation method of object, is dried, and is put into percolator after being crushed to 60 mesh, with the pure glutinous rice of 16 times of weight Wine carries out diacolation processing, and the alcoholic strength of the pure glutinous rice wine is 30 °, then recycles the percolate of acquisition by way of distillation Pure glutinous rice wine therein, then filtered through 600 mesh, obtain the Lignum Aquilariae Resinatum extract;The preparation method of the Lotus Leafextract is by lotus Leaf is cleaned 6 times with deionized water, then the deionized water of 20 times of weight is added in drying, is carried out using steam pressure cooker equipment high Warm high pressure extraction, extracting solution are concentrated under reduced pressure, then obtain the Lotus Leafextract after the filtering of 800 mesh.
In the present embodiment, the preparation method of the deodorant for livestock and poultry feces processing, steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 5 times with deionized water, mixture is obtained after co-grinding A;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly After stand 40min, be added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, using supersonic wave wall breaking skill Art is ultrasonically treated, and the condition of the supersound process is ultrasonic power 150W, ultrasonic time 30min, after the completion of ultrasound again It is filtered through 80 mesh screens, obtains liquor B and filter residue C;
3) will in the filter residue C that obtained in step 2) be added 20 times of weight deionized water, using steam pressure cooker equipment into Row high temperature and pressure is extracted, and the pressure of high temperature and pressure extraction is 0.6MPa, time 25min, will extracting solution in step 2) Obtained liquor B is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 5 times with deionized water, is then fed into juice extractor and squeezes the juice, using 40 mesh screens filter, and obtain filtrate E;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 5 times with deionized water, after co-grinding Mixture F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), after stirring evenly Filtrate E, the mechanical agitation 40min obtained in step 4) is added, adds absolute ethyl alcohol, the absolute ethyl alcohol is with mixture F's Volume ratio is 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 200W, ultrasonic time 30min, ultrasound are filtered through 80 mesh screens again after the completion, obtain filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 20 times of weight, is carried out using steam pressure cooker equipment High temperature and pressure is extracted, and the pressure of the high temperature and pressure extraction is 0.6MPa, time 25min, will be obtained in extracting solution and step 6) The filtrate G arrived is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract And Lotus Leafextract, ultrasonic disperse 8min, the mixed liquor for sequentially adding the mixed liquor D obtained in step 3) and being obtained in step 7) H, mechanical agitation 20min to get.
Embodiment 5
A kind of deodorant for livestock and poultry feces processing, including below according to the raw material of parts by weight:4-7 parts of purple perilla, Chinese ilex 12-18 parts, 7-10 parts of betel nut, 12-15 parts of Herba Andrographitis, 2-5 parts of spearmint, 4-7 parts of rhizoma imperatae, 4-7 parts of garlic, Lignum Aquilariae Resinatum extract 5-8 parts, 3-7 parts of Lotus Leafextract, 45-55 parts of deionized water, 0.5-1.5 parts of lauryl sodium sulfate.Wherein, the agalloch eaglewood carries It is to clean agalloch eaglewood to take the preparation method of object, is dried, and is put into percolator after being crushed to 60 mesh, with the pure glutinous rice of 16 times of weight Wine carries out diacolation processing, and the alcoholic strength of the pure glutinous rice wine is 30 °, then recycles the percolate of acquisition by way of distillation Pure glutinous rice wine therein, then filtered through 600 mesh, obtain the Lignum Aquilariae Resinatum extract;The preparation method of the Lotus Leafextract is by lotus Leaf is cleaned 6 times with deionized water, then the deionized water of 20 times of weight is added in drying, is carried out using steam pressure cooker equipment high Warm high pressure extraction, extracting solution are concentrated under reduced pressure, then obtain the Lotus Leafextract after the filtering of 800 mesh.
In the present embodiment, the preparation method of the deodorant for livestock and poultry feces processing, steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 5 times with deionized water, mixture is obtained after co-grinding A;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly After stand 40min, be added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, using supersonic wave wall breaking skill Art is ultrasonically treated, and the condition of the supersound process is ultrasonic power 150W, ultrasonic time 30min, after the completion of ultrasound again It is filtered through 80 mesh screens, obtains liquor B and filter residue C;
3) will in the filter residue C that obtained in step 2) be added 20 times of weight deionized water, using steam pressure cooker equipment into Row high temperature and pressure is extracted, and the pressure of high temperature and pressure extraction is 0.6MPa, time 25min, will extracting solution in step 2) Obtained liquor B is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 5 times with deionized water, is then fed into juice extractor and squeezes the juice, using 40 mesh screens filter, and obtain filtrate E;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 5 times with deionized water, after co-grinding Mixture F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), after stirring evenly Filtrate E, the mechanical agitation 40min obtained in step 4) is added, adds absolute ethyl alcohol, the absolute ethyl alcohol is with mixture F's Volume ratio is 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 200W, ultrasonic time 30min, ultrasound are filtered through 80 mesh screens again after the completion, obtain filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 20 times of weight, is carried out using steam pressure cooker equipment High temperature and pressure is extracted, and the pressure of the high temperature and pressure extraction is 0.6MPa, time 25min, will be obtained in extracting solution and step 6) The filtrate G arrived is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract And Lotus Leafextract, ultrasonic disperse 8min, the mixed liquor for sequentially adding the mixed liquor D obtained in step 3) and being obtained in step 7) H, mechanical agitation 20min to get.
Embodiment 6
A kind of deodorant for livestock and poultry feces processing, including below according to the raw material of parts by weight:4-7 parts of purple perilla, Chinese ilex 12-18 parts, 7-10 parts of betel nut, 12-15 parts of Herba Andrographitis, 2-5 parts of spearmint, 4-7 parts of rhizoma imperatae, 4-7 parts of garlic, Lignum Aquilariae Resinatum extract 5-8 parts, 3-7 parts of Lotus Leafextract, 45-55 parts of deionized water, 0.5-1.5 parts of lauryl sodium sulfate.Wherein, the agalloch eaglewood carries It is to clean agalloch eaglewood to take the preparation method of object, is dried, and is put into percolator after being crushed to 60 mesh, with the pure glutinous rice of 16 times of weight Wine carries out diacolation processing, and the alcoholic strength of the pure glutinous rice wine is 30 °, then recycles the percolate of acquisition by way of distillation Pure glutinous rice wine therein, then filtered through 600 mesh, obtain the Lignum Aquilariae Resinatum extract;The preparation method of the Lotus Leafextract is by lotus Leaf is cleaned 6 times with deionized water, then the deionized water of 20 times of weight is added in drying, is carried out using steam pressure cooker equipment high Warm high pressure extraction, extracting solution are concentrated under reduced pressure, then obtain the Lotus Leafextract after the filtering of 800 mesh.
In the present embodiment, the preparation method of the deodorant for livestock and poultry feces processing, steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 5 times with deionized water, mixture is obtained after co-grinding A;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly After stand 40min, be added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, using supersonic wave wall breaking skill Art is ultrasonically treated, and the condition of the supersound process is ultrasonic power 150W, ultrasonic time 30min, after the completion of ultrasound again It is filtered through 80 mesh screens, obtains liquor B and filter residue C;
3) will in the filter residue C that obtained in step 2) be added 20 times of weight deionized water, using steam pressure cooker equipment into Row high temperature and pressure is extracted, and the pressure of high temperature and pressure extraction is 0.6MPa, time 25min, will extracting solution in step 2) Obtained liquor B is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 5 times with deionized water, is then fed into juice extractor and squeezes the juice, using 40 mesh screens filter, and obtain filtrate E;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 5 times with deionized water, after co-grinding Mixture F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), after stirring evenly Filtrate E, the mechanical agitation 40min obtained in step 4) is added, adds absolute ethyl alcohol, the absolute ethyl alcohol is with mixture F's Volume ratio is 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 200W, ultrasonic time 30min, ultrasound are filtered through 80 mesh screens again after the completion, obtain filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 20 times of weight, is carried out using steam pressure cooker equipment High temperature and pressure is extracted, and the pressure of the high temperature and pressure extraction is 0.6MPa, time 25min, will be obtained in extracting solution and step 6) The filtrate G arrived is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract And Lotus Leafextract, ultrasonic disperse 8min, the mixed liquor for sequentially adding the mixed liquor D obtained in step 3) and being obtained in step 7) H, mechanical agitation 20min to get.
Embodiment 7
A kind of deodorant for livestock and poultry feces processing, including below according to the raw material of parts by weight:6 parts of purple perilla, Chinese ilex 15 Part, 8 parts of betel nut, 14 parts of Herba Andrographitis, 4 parts of spearmint, 6 parts of rhizoma imperatae, 6 parts of garlic, 7 parts of Lignum Aquilariae Resinatum extract, Lotus Leafextract 4 Part, 50 parts of deionized water, 1 part of lauryl sodium sulfate.Wherein, the preparation method of the Lignum Aquilariae Resinatum extract is to clean agalloch eaglewood, Drying puts into percolator after being crushed to 60 mesh, diacolation processing, the pure glutinous rice wine is carried out with the pure glutinous rice wine of 16 times of weight Alcoholic strength be 30 °, the percolate of acquisition is then recycled into pure glutinous rice wine therein by way of distillation, then through 600 mesh mistakes Filter, obtains the Lignum Aquilariae Resinatum extract;The preparation method of the Lotus Leafextract is to clean lotus leaf 6 times with deionized water, is dried, so The deionized water of 20 times of weight is added afterwards, high temperature and pressure extraction is carried out using steam pressure cooker equipment, extracting solution depressurize dense Contracting, then obtain the Lotus Leafextract after the filtering of 800 mesh.
In the present embodiment, the preparation method of the deodorant for livestock and poultry feces processing, steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 5 times with deionized water, mixture is obtained after co-grinding A;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly After stand 40min, be added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, using supersonic wave wall breaking skill Art is ultrasonically treated, and the condition of the supersound process is ultrasonic power 150W, ultrasonic time 30min, after the completion of ultrasound again It is filtered through 80 mesh screens, obtains liquor B and filter residue C;
3) will in the filter residue C that obtained in step 2) be added 20 times of weight deionized water, using steam pressure cooker equipment into Row high temperature and pressure is extracted, and the pressure of high temperature and pressure extraction is 0.6MPa, time 25min, will extracting solution in step 2) Obtained liquor B is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 5 times with deionized water, is then fed into juice extractor and squeezes the juice, using 40 mesh screens filter, and obtain filtrate E;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 5 times with deionized water, after co-grinding Mixture F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), after stirring evenly Filtrate E, the mechanical agitation 40min obtained in step 4) is added, adds absolute ethyl alcohol, the absolute ethyl alcohol is with mixture F's Volume ratio is 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, the condition of the supersound process is ultrasonic power 200W, ultrasonic time 30min, ultrasound are filtered through 80 mesh screens again after the completion, obtain filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 20 times of weight, is carried out using steam pressure cooker equipment High temperature and pressure is extracted, and the pressure of the high temperature and pressure extraction is 0.6MPa, time 25min, will be obtained in extracting solution and step 6) The filtrate G arrived is uniformly mixed, and absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, is obtained mixed liquor H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract And Lotus Leafextract, ultrasonic disperse 8min, the mixed liquor for sequentially adding the mixed liquor D obtained in step 3) and being obtained in step 7) H, mechanical agitation 20min to get.
Comparative example 1
Compared with Example 7, Lignum Aquilariae Resinatum extract is free of, other are same as Example 7.
Comparative example 2
Compared with Example 7, Lotus Leafextract is free of, other are same as Example 7.
Comparative example 3
Compared with Example 7, Lignum Aquilariae Resinatum extract and Lotus Leafextract are free of, other are same as Example 7.
Performance test
Performance detection is carried out to the deodorant for livestock and poultry feces processing of the preparation of embodiment 7 and comparative example 1-3, specifically Method is that the deodorant for livestock and poultry feces processing of the preparation of embodiment 7 and comparative example 1-3 is diluted with water 300 times, with spray The surface that mist equipment is sprayed on the livestock and poultry feces pretreatment material for fermentation carries out deodorizing effect test, and the livestock and poultry feces are located in advance The preparation method of reason material be by livestock and poultry feces dry to water content be 35% after with the chopping bulk object by weight 100 such as straw:10 Ratio mixing, per double centner mixed fertilizer in 1 kilogram of powder that accelerates the ripening is added, abundant uniform mixing is located in advance to get the livestock and poultry feces Reason material, specific deodorizing effect test result are as shown in table 1.
It, can from can be seen that the present invention in the data comparison of embodiment 7 and comparative example 1 by adding Lignum Aquilariae Resinatum extract Deodorizing effect is effectively improved, it is especially notable to the removal effect of hydrogen sulfide;It can in data comparison from embodiment 7 with comparative example 2 To find out, the present invention adds Lotus Leafextract, can effectively improve deodorizing effect, especially notable to the removal effect of hydrogen sulfide; In addition, as can be seen that the present invention is extracted by Lignum Aquilariae Resinatum extract and lotus leaf from the data comparison of embodiment 7 and comparative example 1-3 Object cooperates, and plays synergistic effect, can further effectively improve deodorizing effect.
1 testing result table of table
Group Ammonia removal rate Hydrogen sulfide removal rate Odor concentration reduced rate
Embodiment 7 97% 90% 87%
Comparative example 1 80 68 65%
Comparative example 2 82 70 68%
Comparative example 3 70 53 50%
Agalloch eaglewood, acrid flavour, hardship, slightly warm in nature, have the effect of reconcile strength, benefit mend internal organs, operation qi and blood, can antibacterial anti-inflammatory, Anti- inflammation, anti-spasm promote cell metabolism and cytothesis function, meanwhile, endocrine organ is adjusted, promotes hormone Brain fatigue is eliminated in secretion, help, is releived, is restored balance of body and spirit, gentle mood helps qi-blood circulating, help to be metabolized liver kidney poison Element enhances immunocompetence.
Lotus leaf, nature and flavor are bitter, put down, and Return liver, spleen, stomach, the heart channel of Hang-Shaoyin have clearing summer-heat and damp, sending up the lucid yang, cooling blood and hemostasis and other effects, But also there is antimitotic effect.
As can be seen that the deodorant for livestock and poultry feces processing prepared by the present invention has good remove from result above Smelly effect is cooperated by Lignum Aquilariae Resinatum extract and Lotus Leafextract, is played synergistic effect, can be effectively improved and remove Smelly effect is especially notable to the removal effect of hydrogen sulfide;Simultaneously as active ingredient is all extracted from natural plants, to behaviour It is without any side effects to make personnel, health environment-friendly;Moreover, when carrying out fermentation process for livestock and poultry feces, will not be removed as chemistry Smelly dose or microbial deodorant pollute the organic fertilizer produced as raw material using livestock and poultry feces, avoid use with animal dung Dirt is that the organic fertilizer of raw material production damages people and plant when being applied fertilizer, securely and reliably, before having a vast market Scape.
The better embodiment of the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party Formula, one skilled in the relevant art within the scope of knowledge, can also be without departing from the purpose of the present invention Various changes can be made.There is no necessity and possibility to exhaust all the enbodiments.And it thus amplifies out apparent Variation or variation be still in the protection scope of this invention.

Claims (10)

1. a kind of deodorant for livestock and poultry feces processing, which is characterized in that including below according to the raw material of parts by weight:Purple perilla 2- 8 parts, it is 10-20 parts of Chinese ilex, 5-12 parts of betel nut, 10-17 parts of Herba Andrographitis, 1-6 parts of spearmint, 2-9 parts of rhizoma imperatae, 2-9 parts of garlic, heavy Fragrant extract 3-10 parts, 2-10 parts of Lotus Leafextract, 40-58 parts of deionized water, 0.2-2 parts of lauryl sodium sulfate.
2. the deodorant according to claim 1 for livestock and poultry feces processing, which is characterized in that including below according to weight The raw material of part:4-7 parts of purple perilla, 12-18 parts of Chinese ilex, 7-10 parts of betel nut, 12-15 parts of Herba Andrographitis, 2-5 parts of spearmint, rhizoma imperatae 4-7 Part, 4-7 parts of garlic, 5-8 parts of Lignum Aquilariae Resinatum extract, 3-7 parts of Lotus Leafextract, 45-55 parts of deionized water, lauryl sodium sulfate 0.5-1.5 parts.
3. the deodorant according to claim 2 for livestock and poultry feces processing, which is characterized in that including below according to weight The raw material of part:6 parts of purple perilla, 15 parts of Chinese ilex, 8 parts of betel nut, 14 parts of Herba Andrographitis, 4 parts of spearmint, 6 parts of rhizoma imperatae, 6 parts of garlic, agalloch eaglewood 7 parts of extract, 4 parts of Lotus Leafextract, 50 parts of deionized water, 1 part of lauryl sodium sulfate.
4. the deodorant according to claim 1 or 2 or 3 for livestock and poultry feces processing, which is characterized in that the agalloch eaglewood carries It is to clean agalloch eaglewood to take the preparation method of object, is dried, and is crushed to after 40-80 mesh in input to percolator, with 12-18 times of weight Pure glutinous rice wine carries out diacolation processing, and the alcoholic strength of the pure glutinous rice wine is 20-35 °, and the percolate of acquisition is then passed through distillation Mode recycle pure glutinous rice wine therein, then filtered through 600 mesh, obtain the Lignum Aquilariae Resinatum extract.
5. the deodorant according to claim 3 for livestock and poultry feces processing, which is characterized in that the Lotus Leafextract Preparation method is to clean lotus leaf 4-6 times with deionized water, is dried, and the deionized water of 16-24 times of weight is then added, using steaming Steam pressure pot equipment carries out high temperature and pressure extraction, and extracting solution is concentrated under reduced pressure, then the lotus leaf extraction is obtained after the filtering of 800 mesh Object.
6. a kind of preparation method of the deodorant according to any one of claims 1 to 5 for livestock and poultry feces processing, feature exist In steps are as follows:
1) purple perilla, Chinese ilex and betel nut are weighed according to parts by weight, is cleaned 4-6 times with deionized water, mixture A is obtained after co-grinding;
2) a concentration of 4% isometric sodium chloride solution will be added in the mixture A obtained in step 1), stirs evenly rear quiet It sets 20-60min, is added absolute ethyl alcohol, the volume ratio of the absolute ethyl alcohol and mixture A are 18:1, using supersonic wave wall breaking skill Art is ultrasonically treated, then is filtered through 80 mesh screens, and liquor B and filter residue C are obtained;
3) deionized water of 16-24 times of weight will be added in the filter residue C obtained in step 2), carried out using steam pressure cooker equipment High temperature and pressure is extracted, and extracting solution is uniformly mixed with the liquor B obtained in step 2), nothing therein is recycled by way of distillation Water-ethanol, then filtered through 400 mesh, obtain mixed liquor D;
4) garlic is weighed according to parts by weight, is cleaned 4-6 times with deionized water, be then fed into juice extractor and squeeze the juice, using 40 Mesh screen filters, and obtains filtrate E;
5) Herba Andrographitis, spearmint and rhizoma imperatae are weighed according to parts by weight, is cleaned 4-6 times with deionized water, must mixed after co-grinding Close material F;
6) a concentration of 4% isometric sodium chloride solution is added in the mixture F obtained in step 5), be stirring evenly and then adding into The filtrate E obtained in step 4), mechanical agitation 20-60min add absolute ethyl alcohol, the body of the absolute ethyl alcohol and mixture F Product is than being 18:1, it is ultrasonically treated using supersonic wave wall breaking technology, then filtered through 80 mesh screens, obtains filtrate G and filter residue H;
7) the filter residue H obtained in step 6) is added to the deionized water of 16-24 times of weight, is carried out using steam pressure cooker equipment high The pressure of warm high pressure extraction, the high temperature and pressure extraction is 0.4-0.8MPa, time 20-30min, by extracting solution and step 6) In obtained filtrate G be uniformly mixed, absolute ethyl alcohol therein is recycled by way of distillation, then filter through 400 mesh, obtains mixed liquor H;
8) deionized water is weighed according to parts by weight, lauryl sodium sulfate is added and is uniformly mixed, adds Lignum Aquilariae Resinatum extract and lotus Leaf extract, ultrasonic disperse 5-15min, the mixed liquor for sequentially adding the mixed liquor D obtained in step 3) and being obtained in step 7) H, mechanical agitation 10-30min to get.
7. the preparation method of the deodorant according to claim 6 for livestock and poultry feces processing, which is characterized in that step 2) In, the condition of the supersound process is ultrasonic power 80-250W, ultrasonic time 10-50min.
8. the preparation method of the deodorant according to claim 7 for livestock and poultry feces processing, which is characterized in that step 3) In, the pressure of the high temperature and pressure extraction is 0.4-0.8MPa, time 20-30min.
9. the preparation method of the deodorant according to claim 8 for livestock and poultry feces processing, which is characterized in that step 6) In, the condition of the supersound process is ultrasonic power 100-300W, ultrasonic time 15-45min.
10. a kind of deodorant answering in preparing deodorant according to any one of claims 1 to 5 for livestock and poultry feces processing With.
CN201810598909.XA 2018-06-12 2018-06-12 A kind of deodorant and preparation method thereof for livestock and poultry feces processing Pending CN108675578A (en)

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Application publication date: 20181019