CN108670890A - Organic sunscreen composition and its application - Google Patents
Organic sunscreen composition and its application Download PDFInfo
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- CN108670890A CN108670890A CN201810784709.3A CN201810784709A CN108670890A CN 108670890 A CN108670890 A CN 108670890A CN 201810784709 A CN201810784709 A CN 201810784709A CN 108670890 A CN108670890 A CN 108670890A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4966—Triazines or their condensed derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a kind of organic sunscreen composition and its applications, belong to cosmetics, technical field of skin care.The organic sunscreen composition is prepared from the following materials：Ethylhexyl methoxy cinnamate, 15 alcohol benzoic ethers of C12, Hamposyl L isopropyl ester, Octocrilene, double ethyl hexyl oxy phenol anisyl triazines, octyl polymethyl siloxane, Uvinul T 150, the own ester of diethylamino oxybenzene formylbenzoate, Dermol 105, butylmethoxydibenzoylmethane.Above-mentioned organic sunscreen composition includes different-waveband ultraviolet absorber, can play good sun-proof result, and has the characteristics that compatibility is good, it is high clearly to spend, including the sunscreen product of this composition can bring pleasant skin sense while protection skin comprehensively.The Orangic sunscreen composition can be applied in cosmetics or skin care item, such as the various dosage forms such as sun-proof gel, sunscreen spray, sun-proof creams, color make-up with sun-proof result prepared.
Description
Technical field
The present invention relates to cosmetics, technical field of skin care, more particularly to a kind of organic sunscreen composition and its application.
Background technology
With the improvement of people ' s living standards, the transformation of life style, people increasingly like out on tours, leisure is lived
Dynamic, the time of skin exposure under ultraviolet light is increasingly longer, and ultraviolet light has prodigious harm, over-exposure to exist human skin
It can lead to sunburn, tanned, skin aging, photo-induced disease etc. under ultraviolet light, cutaneum carcinoma may finally be caused.Therefore, at us
In daily life, the use of ultra-violet absorber is more and more common and important.
Existing sun-screening agent can be divided into Orangic sunscreen and physical sunscreen agent, be absorbed respectively by the principle for absorbing and scattering purple
Outside line reduces injury of the ultraviolet light to skin.The selection of the type of sun-screening agent and the collocation of grease are to sun-proof effect and finally
The skin sense of product has a serious impact, such as mismatch, lead to problems such as the precipitation of solid sun-screening agent, photochemical reaction, not only
The effect for not having protection skin comprehensively, can also bring a kind of not pleasant skin sense or injury to consumer.
Invention content
The purpose of the present invention exactly overcomes the deficiencies of the prior art and provide a kind of organic sunscreen composition and its application, should
Sunscreen composition has the advantages that compatibility is fabulous, salubrious degree is high, risk is precipitated in nodeless mesh.
In order to achieve the above object, it adopts the following technical scheme that：
A kind of organic sunscreen composition, is prepared from the following materials：Ethylhexyl methoxy cinnamate, C12-15 alcohol benzene
Formic acid esters, Hamposyl L isopropyl ester, Octocrilene, bis-ethylhexoxyphenol methoxyphenyl triazine, octyl methyl polysilicone
Alkane, Uvinul T 150, the own ester of diethylamino oxybenzene formylbenzoate, Dermol 105, butyl methoxy dibenzoyl
Methylmethane.
Above-mentioned organic sunscreen composition, including different-waveband ultraviolet absorber, can play good sun-proof result, pass through
Similar compatibility principle filters out optimal combination, has the characteristics that compatibility is good；The Orangic sunscreen composition is by using oil
The ability of liposoluble solution sun-screening agent is strong, skin sense is salubrious, spreadability is good, small and salubrious with interfacial tension is shown after sunscreen composition
High feature is spent, pleasant skin sense is brought while protection skin comprehensively, can be applicable to the various cosmetics agent such as sun-proof, color make-up
Type.
The mass percent of the raw material is in one of the embodiments,：
It is matched using above-mentioned raw materials, preferable compatibility and salubrious degree can be reached.
The mass percent of the raw material is in one of the embodiments,：
The mass percent of the raw material is in one of the embodiments,：
The invention also discloses a kind of sun care preparations or skin care item, including above-mentioned organic sunscreen composition.
Above-mentioned organic sunscreen composition can be applied in cosmetics or skin care item, for example, can be used for preparing sun-proof gel,
Various cosmetics or the skin care item dosage forms such as sunscreen spray, sun-proof creams, color make-up with sun-proof result.
In one of the embodiments, the sun care preparations or skin care item prepared by the raw material of following mass percent and
At：
The raw material of the organic sunscreen composition and the above-mentioned type is coordinated, preferable effect can be reached.
The oil phase base-material is selected from one of the embodiments,：Cetostearyl alcohol, titanium dioxide, salicylic acid ethyl hexyl
Ester, ring five dimethyl silicone polymer, silica, the poly- trimethicone of diphenyl silicon phenyl, vinyl poly- two
At least one of methylsiloxane/polymethyl siloxane silsesquioxane cross-linked polymer；
The emulsifier is selected from one of the embodiments,：Stearoyl-glutamic acid sodium, stearine, PEG-100
Stearate, cetyl PEG/PPG-10/1 dimethyl silicone polymers, polyglyceryl-3 diisostearate, stearoyl-glutamic acid
Sodium, PEG-10 Polydimethylsiloxane, C14-22 alcohol (and) at least one of C12-20 alkyl glucosides；
The polyalcohol is selected from：At least one of glycerine, butanediol.
The invention also discloses the preparation methods of above-mentioned sun care preparations or skin care item, include the following steps：
It is prepared by oil phase：The raw material of the oil phase component is uniformly mixed, oil phase substrate is obtained；
It is prepared by water phase：The raw material of the water phase components is uniformly mixed, aqueous phase substrate is obtained；
Emulsification：The aqueous phase substrate is mixed into the oil phase substrate, mixing；
Mixing：Remaining raw material is added after cooling, be uniformly mixed, filtering and discharging to get.
Above-mentioned preparation method has the characteristics that easy to operate, process stabilizing is controllable, is suitable for industrialized production.
In one of the embodiments, in the oil phase preparation process：It is stirred in 80-85 DEG C；The water phase system
In standby step：It is stirred at 80-85 DEG C；In the emulsifying step：At 80-85 DEG C, water phase pot, oil phase pot raw material are taken out
Enter to emulsify pot, with 3000r/min speed homogeneous 5 minutes, be stirred 15 minutes with 700r/min；In the mixing step：After cooling
Remaining raw material is added at a predetermined temperature, after mixing, 35 DEG C or less filtering and dischargings.
The cosmetics or skin care item are prepared with reference to above-mentioned technical parameter, there is preferable preparation effect.
Compared with prior art, the beneficial effects of the present invention are：
Orangic sunscreen composition includes different-waveband ultraviolet absorber, can play good sun-proof result, and have
Have the characteristics that compatibility is good；The Orangic sunscreen composition interfacial tension is very small, shows as clearly spending high feature, comprehensive
Pleasant skin sense is brought while protecting skin, can be applicable in the various cosmetics such as sun-proof, color make-up or skin care item dosage form.
Specific implementation mode
Below in conjunction with specific implementation method, the present invention will be described in detail, is used in the exemplary embodiment and description of the present invention
Explain the present invention, but not as a limitation of the invention.
Following embodiment is raw materials used, outer unless stated otherwise, is commercially available.
The clear thin sunscreen of embodiment 1
A kind of clear thin sunscreen has the characteristics that clearly degree is high, compatibility is fabulous, risk is precipitated in nodeless mesh, including following
The component of weight percent：
The preparation method of above-mentioned clear thin sunscreen is as follows：
One, prepared by oil phase：
Oil phase pot is added in the raw material of the oil phase component, is heated with stirring to 80-85 DEG C, keeps the temperature 20 minutes, it is ensured that completely
It is uniformly dispersed, obtains oil phase substrate；
Two, prepared by water phase：
Water phase pot is added in the raw material of the water phase components, is heated with stirring to 80-85 DEG C, keeps the temperature 20 minutes, it is ensured that completely
It is uniformly dispersed, obtains aqueous phase substrate；
Three, it emulsifies：
Water phase pot, oil phase pot raw material are pumped into emulsification pot, with 3000r/min speed homogeneous 5 minutes, stir (speed 700r/
Min it) stirs 15 minutes, cooling；
Four, it mixes：
It is cooled to 55-60 DEG C, pH adjusting agent is added, is stirred until homogeneous；
It is cooled to 40-45 DEG C, preservative, skin conditioning agent, antioxidant, ethyl alcohol, aromatic is added, is stirred until homogeneous；
After detection is qualified, 35 DEG C or less filtering and dischargings to get.
The salubrious suncream of 2 whitening of embodiment
A kind of salubrious suncream of whitening has the characteristics that clearly degree is high, compatibility is fabulous, risk is precipitated in nodeless mesh, including
Following components in percentage by weight：
The preparation method of the above-mentioned salubrious suncream of whitening is as follows：
One, prepared by oil phase：
Oil phase pot is added in the raw material of the oil phase component, is heated with stirring to 80-85 DEG C, keeps the temperature 20 minutes, it is ensured that completely
It is uniformly dispersed, obtains oil phase substrate；
Two, prepared by water phase：
Water phase pot is added in the raw material of the water phase components, is heated with stirring to 80-85 DEG C, keeps the temperature 20 minutes, it is ensured that completely
It is uniformly dispersed, obtains aqueous phase substrate；
Three, it emulsifies：
Oil phase pot raw material is pumped into emulsification pot, water phase pot raw material is slowly pumped into emulsification pot under stirring condition, is added after adding
Speed stirring, until material body is uniform and stable, cooling；
Four, it mixes：
It is cooled to 55-60 DEG C, it is 6.0-6.5 that pH adjusting agent, which is added, to pH, is stirred until homogeneous；
It is cooled to 40-45 DEG C, skin conditioning agent, antioxidant, aromatic is added, is stirred until homogeneous；
After detection is qualified, 35 DEG C or less filtering and dischargings to get.
3 sunlight lotion of embodiment
A kind of sunlight lotion has the characteristics that clearly degree is high, compatibility is fabulous, risk is precipitated in nodeless mesh, including following weight
The component of percentage：
The preparation method of above-mentioned sunlight lotion is as follows：
One, prepared by oil phase：
Oil phase pot is added in the raw material of the oil phase component, is heated with stirring to 80-85 DEG C, keeps the temperature 20 minutes, it is ensured that completely
It is uniformly dispersed, obtains oil phase substrate；
Two, prepared by water phase：
Water phase pot is added in the raw material of the water phase components, is heated with stirring to 80-85 DEG C, keeps the temperature 20 minutes, it is ensured that completely
It is uniformly dispersed, obtains aqueous phase substrate；
Three, it emulsifies：
Water phase pot, oil phase pot raw material are pumped into emulsification pot to stir with 700r/min with 3000r/min speed homogeneous 5 minutes
15 minutes, cooling；
Four, it mixes：
It is cooled to 55-60 DEG C, it is 6.0-6.5 that pH adjusting agent, which is added, to pH, is stirred until homogeneous；
It is cooled to 40-45 DEG C, skin conditioning agent, antioxidant, aromatic is added, is stirred until homogeneous；
After detection is qualified, 35 DEG C or less filtering and dischargings to get.
Embodiment 4
A kind of suncream, it is essentially identical with the salubrious suncream of whitening of embodiment 2, differ only in organic sunscreen composition
Raw material proportioning it is as follows：
Organic sunscreen composition：(totally 31.7%)
Comparative example 1
A kind of suncream, it is essentially identical with the component content of embodiment 1, it differs only in organic sunscreen composition and does not add
Add octyl polymethyl siloxane.
Comparative example 2
A kind of Whitening sunscreen cream, it is essentially identical with the component content of embodiment 2, it differs only in organic sunscreen composition
It is not added with Hamposyl L isopropyl ester.
Comparative example 3
A kind of sunlight lotion, it is essentially identical with the component content of embodiment 3, it differs only in new penta in organic sunscreen composition
Sour isodecyl ester and octyl polymethyl siloxane are replaced by glycerine three (thylhexoic acid) ester.
Experimental example
Cosmetics or skin care item that above-described embodiment and comparative example are prepared are tested for the property.
One, method.
The performances such as its compatibility, crystallization precipitation, stability are tested with reference to stability test method.
Test method：Heat-resisting (40 ± 1) DEG C are kept for 24 hours, and whether there is or not layerings and solid to be precipitated now for observation after recovery room temperature
As.
Cold-resistant (- 8 ± 2) DEG C are kept for 24 hours, and whether there is or not layering and solid precipitation phenomenons for observation after restoring room temperature.
Cold-resistant (4 ± 1) DEG C are kept for 24 hours, and whether there is or not layering and solid precipitation phenomenons for observation after restoring room temperature.
Two, result.
Test result is as follows shown in table.
1. cosmetics of table or skin care item the performance test results
Note：Salubrious degree, oil sense and residual sense are evaluated by experts' evaluation group.
Wherein：Salubrious degree refers to the water profit degree that skin can perceive, and scoring section is 0-15 points, score value 10-15/
Between, be judged to clearly spending it is high, score value 5-10/, be judged to clearly spending it is general, score value 0-5/, be determined as clear
Refreshing degree is low.
Oil sense refer to skin can perceive face attached thereto oil amount number, scoring section is 0-15 point, and score value exists
10-15/, be determined as strong oil feel, score value 5-10/, be determined as that oil sense is general, score value 0-5/, judgement
It is weak for oil sense.
The product surplus that can perceive of residual inductance value skin number, scoring section is 0-15 points, score value 10-15/
Between, be determined as that residual sense is strong, score value 5-10/, be determined as that residual sense is general, score value 0-5/, be determined as residual
Stay sense weak.
As can be seen that the product of embodiment 1-4, has selected the organic sunscreen composition of the present invention, tool in from the above
Have that preferable salubrious degree is high, compatibility, and nodeless mesh is precipitated, and the product of embodiment 1-3 has an optimum efficiency, and embodiment
4 product, due to the Hamposyl L isopropyl ester of selection, octyl polymethyl siloxane, Dermol 105 weight ratio not
Together, the tendency that slightly salubrious sense reduces is produced.
And the product of comparative example 1 is clearly felt bad due to lacking octyl polymethyl siloxane；The product of comparative example 2,
Due to lacking Hamposyl L isopropyl ester, compatibility is bad, and has crystallization that risk is precipitated；The product of comparative example 3, due to new
Valeric acid isodecyl ester and octyl polymethyl siloxane are replaced by glycerine three (thylhexoic acid) ester, clearly feel bad.
It is provided for the embodiments of the invention technical solution above to be described in detail, specific case used herein
The principle and embodiment of the embodiment of the present invention are expounded, the explanation of above example is only applicable to help to understand this
The principle of inventive embodiments；Meanwhile for those of ordinary skill in the art, embodiment according to the present invention, in specific embodiment party
There will be changes in formula and application range, in conclusion the content of the present specification should not be construed as limiting the invention.
Claims (10)
1. a kind of organic sunscreen composition, which is characterized in that be prepared from the following materials：Ethylhexyl methoxy cinnamate,
C12-15 alcohol benzoic ethers, Hamposyl L isopropyl ester, Octocrilene, bis-ethylhexoxyphenol methoxyphenyl triazine, octyl
Polymethyl siloxane, Uvinul T 150, the own ester of diethylamino oxybenzene formylbenzoate, Dermol 105, butyl methoxy
Base dibenzoyl methane.
2. organic sunscreen composition according to claim 1, it is characterised in that：The mass parts ratio of the raw material is：
3. organic sunscreen composition according to claim 2, it is characterised in that：The mass parts ratio of the raw material is：
4. organic sunscreen composition according to claim 3, it is characterised in that：The mass parts ratio of the raw material is：
5. a kind of sun care preparations or skin care item, it is characterised in that：Including claim 1-4 any one of them organic sunscreen groups
Close object.
6. sun care preparations according to claim 5 or skin care item, which is characterized in that by the raw material of following mass percent
It is prepared：
Oil phase component：
Organic sunscreen composition 10-50%
Oil phase base-material 0-33%
Emulsifier 0.3-8%
Water phase components：
7. sun care preparations according to claim 6 or skin care item, which is characterized in that the oil phase base-material is selected from：Spermaceti
Stearyl alcohol, titanium dioxide, ethylhexyl salicylate, ring five dimethyl silicone polymer, silica, diphenyl silicon oxygroup benzene
In the poly- trimethicone of base, vinyldimethicone/polymethyl siloxane silsesquioxane cross-linked polymer extremely
Few one kind.
8. sun care preparations according to claim 6 or skin care item, which is characterized in that the emulsifier is selected from：Stearoyl
It is sodium glutamate, stearine, PEG-100 stearates, cetyl PEG/PPG-10/1 dimethyl silicone polymers, poly- sweet
Oily -3 diisopstearates, stearoyl-glutamic acid sodium, PEG-10 Polydimethylsiloxane, C14-22 alcohol (and) C12-20 alkyl Portugal
At least one of glucosides；
The polyalcohol is selected from：At least one of glycerine, butanediol.
9. the preparation method of claim 6-8 any one of them sun care preparations or skin care item, which is characterized in that including following
Step：
It is prepared by oil phase：The raw material of the oil phase component is uniformly mixed, oil phase substrate is obtained；
It is prepared by water phase：The raw material of the water phase components is uniformly mixed, aqueous phase substrate is obtained；
Emulsification：The aqueous phase substrate is mixed into the oil phase substrate, mixing；
Mixing：Remaining raw material is added after cooling, be uniformly mixed, filtering and discharging to get.
10. the preparation method of the sun care preparations or skin care item described in claim 9, which is characterized in that
In the oil phase preparation process：It is stirred in 80-85 DEG C；
In the water phase preparation process：It is stirred at 80-85 DEG C；
In the emulsifying step：At 80-85 DEG C, water phase pot, oil phase pot raw material are pumped into emulsification pot, with 3000r/min speed
Homogeneous 5 minutes is stirred 15 minutes with 700r/min；
In the mixing step：Remaining raw material is added after cooling at a predetermined temperature, after mixing, 35 DEG C or less filter out
Material.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110538085A (en) * | 2019-10-12 | 2019-12-06 | 广州市百好博有限公司 | Sunscreen composition and preparation method thereof |
| CN111840151A (en) * | 2019-04-29 | 2020-10-30 | 西安博和医疗科技有限公司 | Sunscreen agent |
| CN113332213A (en) * | 2021-07-07 | 2021-09-03 | 广州天然国度生物科技有限公司 | All-band ultraviolet sunscreen lotion and preparation method thereof |
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| CN113332213A (en) * | 2021-07-07 | 2021-09-03 | 广州天然国度生物科技有限公司 | All-band ultraviolet sunscreen lotion and preparation method thereof |
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