CN108669542A - A kind of stem of noble dendrobium ferment microcapsules and preparation method thereof - Google Patents
A kind of stem of noble dendrobium ferment microcapsules and preparation method thereof Download PDFInfo
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- CN108669542A CN108669542A CN201810487167.3A CN201810487167A CN108669542A CN 108669542 A CN108669542 A CN 108669542A CN 201810487167 A CN201810487167 A CN 201810487167A CN 108669542 A CN108669542 A CN 108669542A
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- noble dendrobium
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- 240000004638 Dendrobium nobile Species 0.000 title claims abstract description 85
- 239000003094 microcapsule Substances 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000002131 composite material Substances 0.000 claims abstract description 30
- 239000000843 powder Substances 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 229920000858 Cyclodextrin Polymers 0.000 claims abstract description 17
- 239000001116 FEMA 4028 Substances 0.000 claims abstract description 17
- 229920000161 Locust bean gum Polymers 0.000 claims abstract description 17
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims abstract description 17
- 235000011175 beta-cyclodextrine Nutrition 0.000 claims abstract description 17
- 229960004853 betadex Drugs 0.000 claims abstract description 17
- 235000012907 honey Nutrition 0.000 claims abstract description 17
- 235000010420 locust bean gum Nutrition 0.000 claims abstract description 17
- 239000000711 locust bean gum Substances 0.000 claims abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 17
- 229920001661 Chitosan Polymers 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 238000009777 vacuum freeze-drying Methods 0.000 claims abstract description 6
- 238000000855 fermentation Methods 0.000 claims description 18
- 230000004151 fermentation Effects 0.000 claims description 18
- 241000193830 Bacillus <bacterium> Species 0.000 claims description 15
- 244000063299 Bacillus subtilis Species 0.000 claims description 14
- 235000014469 Bacillus subtilis Nutrition 0.000 claims description 14
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Chemical compound OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 14
- 239000008103 glucose Substances 0.000 claims description 13
- 240000005373 Panax quinquefolius Species 0.000 claims description 11
- 235000003140 Panax quinquefolius Nutrition 0.000 claims description 11
- 244000046146 Pueraria lobata Species 0.000 claims description 11
- 235000010575 Pueraria lobata Nutrition 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 239000012530 fluid Substances 0.000 claims description 10
- 244000080767 Areca catechu Species 0.000 claims description 8
- 235000006226 Areca catechu Nutrition 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 8
- 238000001291 vacuum drying Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 2
- 244000025254 Cannabis sativa Species 0.000 claims 1
- 241000726221 Gemma Species 0.000 claims 1
- 239000000470 constituent Substances 0.000 abstract description 6
- 238000004321 preservation Methods 0.000 abstract description 3
- 150000004676 glycans Chemical class 0.000 description 10
- 229920001282 polysaccharide Polymers 0.000 description 8
- 239000005017 polysaccharide Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 6
- 102000004190 Enzymes Human genes 0.000 description 4
- 108090000790 Enzymes Proteins 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 4
- 239000011162 core material Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- RYAHJFGVOCZDEI-UFFNCVEVSA-N Dendrobine Chemical compound C([C@H]1CC[C@@H]2[C@@]31C)N(C)[C@@H]3[C@H]1[C@@H](C(C)C)[C@@H]2C(=O)O1 RYAHJFGVOCZDEI-UFFNCVEVSA-N 0.000 description 2
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 2
- RYAHJFGVOCZDEI-CZKZLRAZSA-N dendrobine Natural products O=C1O[C@@H]2[C@H](C(C)C)[C@H]1[C@H]1[C@@]3(C)[C@@H]2N(C)C[C@H]3CC1 RYAHJFGVOCZDEI-CZKZLRAZSA-N 0.000 description 2
- 230000002496 gastric effect Effects 0.000 description 2
- 235000008434 ginseng Nutrition 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 1
- 235000017060 Arachis glabrata Nutrition 0.000 description 1
- 244000105624 Arachis hypogaea Species 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 235000018262 Arachis monticola Nutrition 0.000 description 1
- 206010011732 Cyst Diseases 0.000 description 1
- 241001523681 Dendrobium Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- RXUWDKBZZLIASQ-UHFFFAOYSA-N Puerarin Natural products OCC1OC(Oc2c(O)cc(O)c3C(=O)C(=COc23)c4ccc(O)cc4)C(O)C(O)C1O RXUWDKBZZLIASQ-UHFFFAOYSA-N 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 1
- 235000005487 catechin Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 description 1
- 229960001231 choline Drugs 0.000 description 1
- 229950001002 cianidanol Drugs 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 208000031513 cyst Diseases 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 238000010237 hybrid technique Methods 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 238000005360 mashing Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 235000020232 peanut Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- HKEAFJYKMMKDOR-VPRICQMDSA-N puerarin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1C1=C(O)C=CC(C2=O)=C1OC=C2C1=CC=C(O)C=C1 HKEAFJYKMMKDOR-VPRICQMDSA-N 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000002459 sustained effect Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
- A23L21/25—Honey; Honey substitutes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/065—Microorganisms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
- A23L29/35—Degradation products of starch, e.g. hydrolysates, dextrins; Enzymatically modified starches
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/40—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by drying or kilning; Subsequent reconstitution
- A23L3/44—Freeze-drying
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Nutrition Science (AREA)
- Molecular Biology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a kind of stem of noble dendrobium ferment microcapsules, raw material includes by weight：Stem of noble dendrobium composite ferment powder, locust bean gum, chitosan, beta cyclodextrin, honey, water.The present invention also proposes the preparation method of stem of noble dendrobium ferment microcapsules, includes the following steps：Locust bean gum, chitosan, beta cyclodextrin, honey are added to the water, after being heated to stirring and dissolving, cools down and prefabricated material is made；Stem of noble dendrobium composite ferment powder is added in prefabricated material, homogeneous, vacuum freeze drying, stem of noble dendrobium ferment microcapsules are made.The stem of noble dendrobium ferment microcapsules of the present invention have slow releasing function, and active constituent stability is high, are readily transported and preservation.
Description
Technical field
The present invention relates to microcapsules technology fields more particularly to a kind of stem of noble dendrobium ferment microcapsules and preparation method thereof.
Background technology
Microcapsules technology refers to by various natural or synthesis the high-molecular compounds of a certain purpose thing (core or interior phase)
Continuous film (wall or foreign minister) cladding completely is got up, and at all lossless to original chemical property of purpose thing, is then gradually led to
Crossing certain outside stimulus or slow releasing function makes the function of purpose thing be showed again in outside, or makees by the shielding of cyst wall
With play the role of protect core material.
Ferment refers to that plant carries out submerged fermentation, a kind of less salt liquid of matters of containing biological activities of extraction.Above-mentioned biology
Active constituent includes at least enzyme, fermentation participates in bacterium.Stem of noble dendrobium ferment is using composite vegetables such as the stems of noble dendrobium as raw material, after fermented bacterium fermentation
Fermented product is made using filter, concentration, hybrid technique, rich in a variety of work such as dendrobium polysaccharide, dendrobine, amino acid and biological enzyme
Property ingredient, but its active constituent is unstable to light, heat, oxygen, easily decomposes anyway, how to protect stem of noble dendrobium enzyme activity ingredient
It is the current technical issues that need to address.Currently, about the microencapsulation technology of stem of noble dendrobium ferment, there has been no report for work.
Invention content
Technical problems based on background technology, the present invention propose a kind of stem of noble dendrobium ferment microcapsules and its preparation side
Method has slow releasing function, and active constituent stability is high, is readily transported and preservation.
The present invention proposes that a kind of stem of noble dendrobium ferment microcapsules, raw material include by weight：Stem of noble dendrobium composite ferment powder 10-16
Part, 1.5-3 parts of locust bean gum, 0.6-1.2 parts of chitosan, 6-12 parts of beta-cyclodextrin, 2-4 parts of honey, 80-100 parts of water.
Preferably, stem of noble dendrobium composite ferment powder takes following technique to prepare：By the fresh stem of noble dendrobium, betel nut, American Ginseng, pueraria lobata difference
It is uniformly mixed obtained pre-feed after cleaning, mashing, adds water, glucose, bacillus subtilis and Bacillus acidi lactici and adjusts pH
Value, carries out the obtained zymotic fluid that ferments；After filtering fermentation liquor and vacuum drying, stem of noble dendrobium composite ferment powder is made.
Preferably, the fresh stem of noble dendrobium, betel nut, American Ginseng, pueraria lobata water weight ratio be 3-4：1-2：2-3：4-5.
Preferably, the weight ratio of pre-feed, water, glucose, bacillus subtilis and Bacillus acidi lactici is 100：100-150：
6-12：1-3：1-2.
Preferably, pH value 5-6.
Preferably, fermentation temperature is 25-35 DEG C, fermentation time 15-25d.
The present invention also proposes the preparation method of above-mentioned stem of noble dendrobium ferment microcapsules, includes the following steps：
S1, locust bean gum, chitosan, beta-cyclodextrin, honey are added to the water, after being heated to 60-70 DEG C of stirring and dissolving, cooling
Prefabricated material is made to 42-48 DEG C；
S2, stem of noble dendrobium composite ferment powder is added in prefabricated material, stem of noble dendrobium ferment microcapsules are made in homogeneous, vacuum freeze drying.
Preferably, homogeneous speed of agitator is 5000-6000r/min, mixing time 15-20min in S2.
The present invention using stem of noble dendrobium compound ferment powder as microcapsules core material, locust bean gum, chitosan, beta-cyclodextrin, honey it is mixed
Conjunction film forming matter is microcapsule wall material, and stem of noble dendrobium ferment microcapsules are made in coated and vacuum freeze drying.Wherein, the stem of noble dendrobium is rich in the stem of noble dendrobium
Polysaccharide, dendrobine, protein and amino acid, betel nut is rich in alkaloid, catechin, choline, and American Ginseng is rich in panaxoside and more
Kind of amino acid, pueraria lobata rich in Puerarin, daizeol glycosides, peanut element, amino acid, polysaccharide, the present invention with bacillus subtilis and
Bacillus acidi lactici is composite zymocyte, and stem of noble dendrobium compound ferment powder is made as microcapsules core material in fermented and vacuum freeze-drying technique,
Be conducive to nutriment conversion and the dissolution in the fresh stem of noble dendrobium, betel nut, American Ginseng and pueraria lobata, and also introduce a variety of new activity
Substance and biological enzyme can improve effect, increase flavor, mouthfeel, be easy to absorb；Chitosan is a kind of nontoxic, non-stimulated day
Right high molecular material has good biocompatibility and film forming, the viscosity high film build of locust bean gum, beta-cyclodextrin and honey
Good, the present invention is cooperated using chitosan, locust bean gum, beta-cyclodextrin and honey as microcapsule wall material, and package performance is strong, is sustained
Effect is good.The present invention using vacuum freeze-drying technique prepares stem of noble dendrobium ferment microcapsules active constituent stability high, slow release effect,
It is readily transported and preservation.
Specific implementation mode
In the following, technical scheme of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of stem of noble dendrobium ferment microcapsules, raw material include by weight：10 parts of stem of noble dendrobium composite ferment powder, 1.5 parts of locust bean gum,
0.6 part of chitosan, 6 parts of beta-cyclodextrin, 2 parts of honey, 80 parts of water.
Stem of noble dendrobium composite ferment powder takes following technique to prepare：It is 3 by weight ratio：1：2：The 4 fresh stem of noble dendrobium, betel nut, the West
Ginseng, pueraria lobata be respectively washed, be beaten after be uniformly mixed prepare pre-feed, by weight be 100：100：6：1：1 weighs preparation respectively
Material, water, glucose, bacillus subtilis and Bacillus acidi lactici, by being added, water, glucose, bacillus subtilis and Bacillus acidi lactici are pre-
In stock, and it is 5 to adjust pH value, and zymotic fluid is made in 25 DEG C of fermentation 15d of temperature；After filtering fermentation liquor and vacuum drying, system
Obtain stem of noble dendrobium composite ferment powder.
Embodiment 2
A kind of stem of noble dendrobium ferment microcapsules, raw material include by weight：16 parts of stem of noble dendrobium composite ferment powder, 3 parts of locust bean gum, shell
1.2 parts of glycan, 12 parts of beta-cyclodextrin, 4 parts of honey, 100 parts of water.
Stem of noble dendrobium composite ferment powder takes following technique to prepare：It is 4 by weight ratio：2：3：The 5 fresh stem of noble dendrobium, betel nut, the West
Ginseng, pueraria lobata be respectively washed, be beaten after be uniformly mixed prepare pre-feed, by weight be 100：150：12：3：2 weigh preparation respectively
Material, water, glucose, bacillus subtilis and Bacillus acidi lactici, by being added, water, glucose, bacillus subtilis and Bacillus acidi lactici are pre-
In stock, and it is 6 to adjust pH value, and zymotic fluid is made in 35 DEG C of fermentation 25d of temperature；After filtering fermentation liquor and vacuum drying, system
Obtain stem of noble dendrobium composite ferment powder.
Embodiment 3
A kind of stem of noble dendrobium ferment microcapsules, raw material include by weight：12 parts of stem of noble dendrobium composite ferment powder, 2 parts of locust bean gum, shell
0.8 part of glycan, 8 parts of beta-cyclodextrin, 2.5 parts of honey, 90 parts of water.
Stem of noble dendrobium composite ferment powder takes following technique to prepare：It is 3.4 by weight ratio：1.2：2.4：The 4.3 fresh stem of noble dendrobium, Bin
Bulky, American Ginseng, pueraria lobata be respectively washed, be beaten after be uniformly mixed and prepare pre-feed, by weight being 100：120：8：1.5：1.3 point
Also known as take pre-feed, water, glucose, bacillus subtilis and Bacillus acidi lactici, will be added water, glucose, bacillus subtilis and
In Bacillus acidi lactici pre-feed, and it is 5.4 to adjust pH value, and zymotic fluid is made in 30 DEG C of fermentation 20d of temperature；By filtering fermentation liquor and very
After sky is dry, stem of noble dendrobium composite ferment powder is made.
The preparation method of above-mentioned stem of noble dendrobium ferment microcapsules, includes the following steps：
S1, locust bean gum, chitosan, beta-cyclodextrin, honey are added to the water, after being heated to 60 DEG C of stirring and dissolvings, are cooled to
42 DEG C are made prefabricated material；
S2, stem of noble dendrobium composite ferment powder is added in prefabricated material, after stirring homogeneous 15min with 5000r/min speed, then through true
Stem of noble dendrobium ferment microcapsules are made in vacuum freecing-dry.
Embodiment 4
A kind of stem of noble dendrobium ferment microcapsules, raw material include by weight：14 parts of stem of noble dendrobium composite ferment powder, 2.5 parts of locust bean gum,
1.0 parts of chitosan, 10 parts of beta-cyclodextrin, 3.5 parts of honey, 95 parts of water.
Stem of noble dendrobium composite ferment powder takes following technique to prepare：It is 3.8 by weight ratio：1.6：2.6：The 4.8 fresh stem of noble dendrobium, Bin
Bulky, American Ginseng, pueraria lobata be respectively washed, be beaten after be uniformly mixed and prepare pre-feed, by weight being 100：140：10：2.5：1.6
Pre-feed, water, glucose, bacillus subtilis and Bacillus acidi lactici are weighed respectively, and water, glucose, bacillus subtilis will be added
And in Bacillus acidi lactici pre-feed, and it is 5.8 to adjust pH value, and zymotic fluid is made in 33 DEG C of fermentation 22d of temperature；By filtering fermentation liquor and
After vacuum drying, stem of noble dendrobium composite ferment powder is made.
The preparation method of above-mentioned stem of noble dendrobium ferment microcapsules, includes the following steps：
S1, locust bean gum, chitosan, beta-cyclodextrin, honey are added to the water, after being heated to 70 DEG C of stirring and dissolvings, are cooled to
48 DEG C are made prefabricated material；
S2, stem of noble dendrobium composite ferment powder is added in prefabricated material, after stirring homogeneous 20min with 6000r/min speed, then through true
Stem of noble dendrobium ferment microcapsules are made in vacuum freecing-dry.
Embodiment 5
A kind of stem of noble dendrobium ferment microcapsules, raw material include by weight：13 parts of stem of noble dendrobium composite ferment powder, 2.3 parts of locust bean gum,
0.9 part of chitosan, 9 parts of beta-cyclodextrin, 3 parts of honey, 90 parts of water.
Stem of noble dendrobium composite ferment powder takes following technique to prepare：It is 3.5 by weight ratio：1.5：2.5：The 4.5 fresh stem of noble dendrobium, Bin
Bulky, American Ginseng, pueraria lobata be respectively washed, be beaten after be uniformly mixed and prepare pre-feed, by weight being 100：125：9：2：1.5 respectively
Pre-feed, water, glucose, bacillus subtilis and Bacillus acidi lactici are weighed, water, glucose, bacillus subtilis and breast will be added
In acidfast bacilli pre-feed, and it is 5.2 to adjust pH value, and zymotic fluid is made in 30 DEG C of fermentation 18d of temperature；By filtering fermentation liquor and vacuum
After drying, stem of noble dendrobium composite ferment powder is made.
The preparation method of above-mentioned stem of noble dendrobium ferment microcapsules, includes the following steps：
S1, locust bean gum, chitosan, beta-cyclodextrin, honey are added to the water, after being heated to 65 DEG C of stirring and dissolvings, are cooled to
45 DEG C are made prefabricated material；
S2, stem of noble dendrobium composite ferment powder is added in prefabricated material, after stirring homogeneous 18min with 5500r/min speed, then through true
Stem of noble dendrobium ferment microcapsules are made in vacuum freecing-dry.
Stem of noble dendrobium ferment microcapsules are made in 1-5 of the embodiment of the present invention and press following condition test：1, it is separately added into simulated gastric fluid
After handling 3h in simulated intestinal fluid, undissolved stem of noble dendrobium ferment microcapsules are cleaned in filtering, test active polysaccharide；2, under the conditions of 20 DEG C
After storage 6 months, the activity of stem of noble dendrobium ferment microcapsules polysaccharide is tested；Examination is accounted for the active polysaccharide of stem of noble dendrobium ferment microcapsules after experiment
The percentage calculation of stem of noble dendrobium ferment microcapsules active polysaccharide, test data such as the following table 1 before testing.
Table 1
By the stem of noble dendrobium ferment microcapsules of the present invention known to upper table after storing 6 months and through simulated gastric fluid and artificial intestines
After handling 3h in liquid, active polysaccharide still keeps higher level, and active constituent stability is high, slow release effect.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (8)
1. a kind of stem of noble dendrobium ferment microcapsules, which is characterized in that its raw material includes by weight：10-16 parts of stem of noble dendrobium composite ferment powder,
1.5-3 parts of locust bean gum, 0.6-1.2 parts of chitosan, 6-12 parts of beta-cyclodextrin, 2-4 parts of honey, 80-100 parts of water.
2. stem of noble dendrobium ferment microcapsules according to claim 1, which is characterized in that stem of noble dendrobium composite ferment powder takes following technique system
It is standby：It is uniformly mixed obtained pre-feed after the fresh stem of noble dendrobium, betel nut, American Ginseng, pueraria lobata are respectively washed, are beaten, adds water, grape
Sugar, bacillus subtilis and Bacillus acidi lactici simultaneously adjust pH value, carry out the obtained zymotic fluid that ferments；By filtering fermentation liquor and vacuum drying
Afterwards, stem of noble dendrobium composite ferment powder is made.
3. stem of noble dendrobium ferment microcapsules according to claim 2, which is characterized in that the fresh stem of noble dendrobium, betel nut, American Ginseng, pueraria lobata water
Weight ratio be 3-4：1-2：2-3：4-5.
4. according to stem of noble dendrobium ferment microcapsules described in Claims 2 or 3, which is characterized in that pre-feed, water, glucose, withered grass gemma
The weight ratio of bacillus and Bacillus acidi lactici is 100：100-150：6-12：1-3：1-2.
5. according to any one of the claim 2-4 stem of noble dendrobium ferment microcapsules, which is characterized in that pH value 5-6.
6. according to any one of the claim 2-5 stem of noble dendrobium ferment microcapsules, which is characterized in that fermentation temperature is 25-35 DEG C, hair
The ferment time is 15-25d.
7. a kind of preparation method of the stem of noble dendrobium ferment microcapsules as described in claim any one of 1-6, which is characterized in that including as follows
Step：
S1, locust bean gum, chitosan, beta-cyclodextrin, honey are added to the water, after being heated to 60-70 DEG C of stirring and dissolving, are cooled to
42-48 DEG C is made prefabricated material；
S2, stem of noble dendrobium composite ferment powder is added in prefabricated material, stem of noble dendrobium ferment microcapsules are made in homogeneous, vacuum freeze drying.
8. the preparation method of stem of noble dendrobium ferment microcapsules according to claim 7, which is characterized in that homogeneous speed of agitator is in S2
5000-6000r/min, mixing time 15-20min.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111991368A (en) * | 2020-09-11 | 2020-11-27 | 中国药科大学 | Preparation method of tea polyphenol coated soybean isolated white-quaternary ammonium salt chitosan microcapsule |
| CN114287623A (en) * | 2021-12-31 | 2022-04-08 | 安徽阳光药业有限公司 | Dendrobium enzyme particle and preparation method thereof |
| CN114304616A (en) * | 2021-12-28 | 2022-04-12 | 广州市沐家健康产业有限公司 | Enzyme composition and preparation method thereof |
| CN116491649A (en) * | 2023-04-27 | 2023-07-28 | 哈尔滨工业大学 | Noni ferment slow-release microcapsule powder and preparation method thereof |
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2018
- 2018-05-21 CN CN201810487167.3A patent/CN108669542A/en not_active Withdrawn
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111991368A (en) * | 2020-09-11 | 2020-11-27 | 中国药科大学 | Preparation method of tea polyphenol coated soybean isolated white-quaternary ammonium salt chitosan microcapsule |
| CN111991368B (en) * | 2020-09-11 | 2021-11-12 | 中国药科大学 | Preparation method of tea polyphenol coated soy protein isolate-quaternary ammonium salt chitosan microcapsule |
| CN114304616A (en) * | 2021-12-28 | 2022-04-12 | 广州市沐家健康产业有限公司 | Enzyme composition and preparation method thereof |
| CN114287623A (en) * | 2021-12-31 | 2022-04-08 | 安徽阳光药业有限公司 | Dendrobium enzyme particle and preparation method thereof |
| CN116491649A (en) * | 2023-04-27 | 2023-07-28 | 哈尔滨工业大学 | Noni ferment slow-release microcapsule powder and preparation method thereof |
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