CN108660036A - A kind of processing method of deer's sinew liquor - Google Patents
A kind of processing method of deer's sinew liquor Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
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- A61K35/12—Materials from mammals; Compositions comprising non-specified tissues or cells; Compositions comprising non-embryonic stem cells; Genetically modified cells
- A61K35/32—Bones; Osteocytes; Osteoblasts; Tendons; Tenocytes; Teeth; Odontoblasts; Cartilage; Chondrocytes; Synovial membrane
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/72—Rhamnaceae (Buckthorn family), e.g. buckthorn, chewstick or umbrella-tree
- A61K36/725—Ziziphus, e.g. jujube
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
- A61K36/815—Lycium (desert-thorn)
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- A61K36/88—Liliopsida (monocotyledons)
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- A61P37/04—Immunostimulants
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- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H6/00—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
- C12H6/02—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by distillation
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Abstract
The present invention relates to belonging to deer's sinew processing technique field, more particularly to a kind of processing method of deer's sinew liquor, step includes:Metering, sterilizing, encapsulation, impregnates, distillation separation, secondary blends step at filtering;Wherein, filtering be by matrimony vine, jujube, ginseng, filter after the fermented processing of blackberry lily, take filter residue and filtrate;Sterilizing is will to filter gained filter residue through infrared sterilization;Encapsulation is to wrap up filter residue with NF membrane;Immersion is that encapsulation filter residue, deer's sinew are soaked in sauce incense liquor;Distillation separation is that first air-distillation to distillate alcoholic strength is 40 45 °, then distillation to distillate alcoholic strength is 35 38 ° in the case where vacuum degree is negative 50kPa, and then in the case where vacuum degree is negative 65kPa, distillation to distillate alcoholic strength is 28 32 °;Secondary blend is Ultrasonic Radiation after mixing distillate three times;Deer's sinew liquor of the present invention has played the effect of blood nourishing acupuncture-stimulating, beautifying face and moistering lotion, strengthen immunity, and health-care effect is good, and storage time is long.
Description
Technical field
The present invention relates to belonging to deer's sinew processing technique field, more particularly to a kind of processing method of deer's sinew liquor.
Background technology
Deer's sinew is the tendon of animal in deer family sika deer or red deer four limbs;Taste is salty, warm-natured, returns liver and kidney channel, have filling liver kidney,
The effect of strengthening the bones and muscles, wind-damp dispelling, is usually used in caused by liver and kidney deficiency, strain wound, arthralgia pain due to rheumatism, convulsion, rheumatic arthritis, Shou Zuwu absolutely
Power, systremma, man's essence decline, asthenia of essence and blood, all deficient, waist and leg aches, podomere are weak.
In deer's sinew containing a variety of amino acid such as sex hormone and proline, glycine such as stosterone, estradiol, sodium, iron,
A variety of inorganic elements such as manganese, zinc.Currently, people often impregnate deer's sinew and white spirit mixed, deer's sinew liquor is made.Utilize the row of white wine
Blood, diverging are easy the characteristics of absorption and growth encourage pharmacological property, and the nutritional ingredient in deer's sinew is made to be fully used;But shortage is rationally matched
5 and process so that medicinal material formula and wine product difference are big, especially so that nutritional ingredient in deer's sinew is using being not enough;And
And current deer's sinew liquor is that people buy deer's sinew from the market mostly, is then voluntarily steep in wine, therefore lack industrialized quality control
System, so that the deer's sinew liquor shelf-life is short, easily there are the bad phenomenons such as corruption in fishy smell weight.
Invention content
The present invention is in order to solve the above technical problems, the invention provides a kind of processing method of deer's sinew liquor.
It is realized particular by following technical scheme:
The present invention provides a kind of processing method of deer's sinew liquor, step includes:Metering, sterilizing, encapsulation, is impregnated, is steamed at filtering
Fraction from, secondary blend step;The metering is to weigh following major ingredient in parts by weight:6-10 parts of deer's sinew, matrimony vine 10-20
Part, 10-20 parts of jujube, 10-15 parts of ginseng, 5-10 parts of blackberry lily, 495-505 parts of sauce incense liquor;The filtering is by previous materials
In matrimony vine, jujube, ginseng, filter after the fermented processing of blackberry lily, take filter residue and filtrate;The sterilizing is will to filter gained filter residue
Through infrared sterilization;The encapsulation is to wrap up filter residue with NF membrane;The immersion is that encapsulation filter residue, deer's sinew are soaked in sauce
In flavor white spirit;It is 40-45 ° that the distillation separation, which is first air-distillation to distillate alcoholic strength, is then negative 50kPa in vacuum degree
Lower distillation to distillate alcoholic strength is 35-38 °, and then in the case where vacuum degree is negative 65kPa, distillation to distillate alcoholic strength is 28-
32°;Secondary blend is Ultrasonic Radiation 5-8min after mixing distillate three times.
Further, the filtering is that matrimony vine, jujube, ginseng, blackberry lily are placed in grinding machine for Chinese herb medicines, and gross mass is added
The degreased pupa powder of 0.01-0.02% was ground to 80 mesh sieve, and the composite zymocyte liquid that gross mass 70-80% is then added carries out
After cold fermentation 20-28h, after nanofiltration membrane, filter residue and filtrate are obtained.
The cold fermentation, temperature are 0-8 DEG C.
It according to mass ratio is 1 that the composite zymocyte liquid, which is by mushroom powder and yeast powder,:After (2-3) mixing, total matter is added
Measure the glucose of 2-5%, the protease of 0.07-0.12%, 0.02-0.05% cellulases, 0.01-0.04% pectases,
The calcium lactate of 0.2-0.6%, the sterile water of 80-95% configure.
The immersion is first to impregnate 1-2d under the conditions of thermostat temperature is 38-45 DEG C, and then cool down most subzero 5-0 DEG C of item
1-2d is impregnated under part.
The Ultrasonic Radiation, power 200-230W, frequency 7500-7800Hz.
The beneficial effects of the present invention are:
The method of the present invention confuses grinding by degreased pupa powder to matrimony vine, jujube, ginseng, blackberry lily, helps to improve aforementioned
The activity of medicinal material may also function as the effect to eliminate the unusual smell, and dried silkworm chrysalis meal combination process for sterilizing, and additionally aiding prevents wine from sinking
It forms sediment, the phenomenon of corruption;Combining with fermentation technique so that the substances decile such as cellulose, protein in matrimony vine, jujube, ginseng, blackberry lily
Solution, degradation, in favor of dissolutions such as polysaccharide material, trace element, collagens;In conjunction with soaking technology so that deer's sinew, matrimony vine, red
Active ingredient is fully dissolved out in jujube, ginseng, blackberry lily, improves the dissolution rate of collagen, peptide material, with prior art phase
Than collagen dissolution rate improves 17.3%, and peptide material dissolution rate improves 9.8%, impregnates, improves in conjunction with low temperature
The volatility of active ingredient has kept active constituent content to the greatest extent, and the immersion of this thermal type contributes to effectively
The relative motion of ingredient so that active ingredient cooperates, brings out the best in each other, and then is conducive to absorption of human body, utilizes decompression
It distills, alcohol compound, carbonyl complex, ester type compound and phenolic compound in the wine farthest retained, relatively
In the prior art, alcohol compound, carbonyl complex, ester type compound and phenolic compound be respectively increased 10.2%,
4.6%, 1.3%, 4.7%.
The effect of its blood nourishing acupuncture-stimulating, beautifying face and moistering lotion, strengthen immunity having been given full play in the deer's sinew liquor of the present invention, and its
Health-care effect is good, and storage time is up to 20 years.
Specific implementation mode
Specific embodiments of the present invention will be described in further detail below, but the invention is not limited in these realities
Mode is applied, it is claimed to still fall within the claims in the present invention for any improvement or replacement on the present embodiment essence spirit
Range.
Embodiment 1
A kind of processing method of deer's sinew liquor is present embodiments provided, step includes:
A is measured:Weigh following major ingredient:Deer's sinew 10g, matrimony vine 20g, jujube 20g, ginseng 15g, blackberry lily 10g, sauce incense liquor
505g
B is filtered:Matrimony vine, jujube, ginseng, blackberry lily are placed in grinding machine for Chinese herb medicines, the degreasing silkworm of gross mass 0.02% is added
Pupa powder was ground to 80 mesh sieve, cold fermentation 28h under the conditions of then the composite zymocyte liquid of addition gross mass 80% is carried out at 8 DEG C
Afterwards, with after nanofiltration membrane, filter residue and filtrate are obtained, wherein composite zymocyte liquid is by mushroom powder and yeast powder according to mass ratio
It is 1:3 mixing after, be added the glucose of gross mass 5%, 0.12% protease, 0.05% cellulase, 0.04% pectase,
0.6% calcium lactate, 95% sterile water configure;
C sterilizes:Gained filter residue and filtrate will be filtered through infrared sterilization;
D is encapsulated:Filter residue is wrapped up with NF membrane;
E impregnates:Encapsulation filter residue, deer's sinew are soaked in sauce incense liquor, first impregnate 2d under the conditions of thermostat temperature is 45 DEG C,
Then cool down and impregnate 2d under the conditions of most 0 DEG C;
F distillation separation:First air-distillation to distillate alcoholic strength is 40-45 °, is then steamed in the case where vacuum degree is negative 50kPa
It is 35-38 ° to evaporate to distillate alcoholic strength, and then in the case where vacuum degree is negative 65kPa, distillation to distillate alcoholic strength is 28-32 °;
G is blent for bis- times:After inciting somebody to action distillate mixing three times, it is 230W to be placed in power, and frequency is ultrasonic wave under the conditions of 7800Hz
Radiate 8min.
Embodiment 2
A kind of processing method of deer's sinew liquor is present embodiments provided, step includes:
A is measured:Weigh following major ingredient:Deer's sinew 6g, matrimony vine 10g, jujube 10g, ginseng 10g, blackberry lily 5g, sauce incense liquor 495g
B is filtered:Matrimony vine, jujube, ginseng, blackberry lily are placed in grinding machine for Chinese herb medicines, the degreasing silkworm of gross mass 0.01% is added
Pupa powder was ground to 80 mesh sieve, cold fermentation 20h under the conditions of then the composite zymocyte liquid of addition gross mass 70% is carried out at 0 DEG C
Afterwards, with after nanofiltration membrane, filter residue and filtrate are obtained, wherein composite zymocyte liquid is by mushroom powder and yeast powder according to mass ratio
It is 1:2 mixing after, be added the glucose of gross mass 2%, 0.07% protease, 0.02% cellulase, 0.01% pectase,
0.2% calcium lactate, 80% sterile water configure;
C sterilizes:Gained filter residue and filtrate will be filtered through infrared sterilization;
D is encapsulated:Filter residue is wrapped up with NF membrane;
E impregnates:Encapsulation filter residue, deer's sinew are soaked in sauce incense liquor, first impregnate 1d under the conditions of thermostat temperature is 38 DEG C,
Then cool down it is 5 DEG C most subzero under the conditions of impregnate 1d;
F distillation separation:First air-distillation to distillate alcoholic strength is 40-45 °, is then steamed in the case where vacuum degree is negative 50kPa
It is 35-38 ° to evaporate to distillate alcoholic strength, and then in the case where vacuum degree is negative 65kPa, distillation to distillate alcoholic strength is 28-32 °;
G is blent for bis- times:After inciting somebody to action distillate mixing three times, it is 200W to be placed in power, and frequency is ultrasonic wave under the conditions of 7500Hz
Radiate 5min.
Embodiment 3
A kind of processing method of deer's sinew liquor is present embodiments provided, step includes:
A is measured:Weigh following major ingredient:Deer's sinew 7g, matrimony vine 15g, jujube 15g, ginseng 13g, blackberry lily 8g, sauce incense liquor 500g
B is filtered:Matrimony vine, jujube, ginseng, blackberry lily are placed in grinding machine for Chinese herb medicines, the degreasing silkworm of gross mass 0.013% is added
Pupa powder be ground to 80 mesh sieve, then be added gross mass 75% composite zymocyte liquid be carried out at 4 DEG C under the conditions of cold fermentation for 24 hours
Afterwards, with after nanofiltration membrane, filter residue and filtrate are obtained, wherein composite zymocyte liquid is by mushroom powder and yeast powder according to mass ratio
It is 1:After 2.3 mixing, the glucose of gross mass 2.8%, 0.1% protease, 0.03% cellulase, 0.03% pectin is added
Enzyme, 0.4% calcium lactate, 85% sterile water configure;
C sterilizes:Gained filter residue and filtrate will be filtered through infrared sterilization;
D is encapsulated:Filter residue is wrapped up with NF membrane;
E impregnates:Encapsulation filter residue, deer's sinew are soaked in sauce incense liquor, first impregnate 1d under the conditions of thermostat temperature is 40 DEG C,
Then cool down it is 4 DEG C most subzero under the conditions of impregnate 2d;
F distillation separation:First air-distillation to distillate alcoholic strength is 40-45 °, is then steamed in the case where vacuum degree is negative 50kPa
It is 35-38 ° to evaporate to distillate alcoholic strength, and then in the case where vacuum degree is negative 65kPa, distillation to distillate alcoholic strength is 28-32 °;
G is blent for bis- times:After inciting somebody to action distillate mixing three times, it is 210W to be placed in power, and frequency is ultrasonic wave under the conditions of 7800Hz
Radiate 6min.
Embodiment 4
A kind of processing method of deer's sinew liquor is present embodiments provided, step includes:
A is measured:Weigh following major ingredient:Deer's sinew 8g, matrimony vine 18g, jujube 11g, ginseng 11g, blackberry lily 6g, sauce incense liquor 500g
B is filtered:Matrimony vine, jujube, ginseng, blackberry lily are placed in grinding machine for Chinese herb medicines, the degreasing silkworm of gross mass 0.015% is added
Pupa powder was ground to 80 mesh sieve, cold fermentation 27h under the conditions of then the composite zymocyte liquid of addition gross mass 72% is carried out at 2 DEG C
Afterwards, with after nanofiltration membrane, filter residue and filtrate are obtained, wherein composite zymocyte liquid is by mushroom powder and yeast powder according to mass ratio
It is 1:After 2.5 mixing, the glucose of gross mass 4%, 0.09% protease, 0.04% cellulase, 0.02% pectin is added
Enzyme, 0.3% calcium lactate, 90% sterile water configure;
C sterilizes:Gained filter residue and filtrate will be filtered through infrared sterilization;
D is encapsulated:Filter residue is wrapped up with NF membrane;
E impregnates:Encapsulation filter residue, deer's sinew are soaked in sauce incense liquor, first impregnate 2d under the conditions of thermostat temperature is 43 DEG C,
Then cool down it is 2 DEG C most subzero under the conditions of impregnate 2d;
F distillation separation:First air-distillation to distillate alcoholic strength is 40-45 °, is then steamed in the case where vacuum degree is negative 50kPa
It is 35-38 ° to evaporate to distillate alcoholic strength, and then in the case where vacuum degree is negative 65kPa, distillation to distillate alcoholic strength is 28-32 °;
G is blent for bis- times:After inciting somebody to action distillate mixing three times, it is 220W to be placed in power, and frequency is ultrasonic wave under the conditions of 7500Hz
Radiate 7min.
Embodiment 5
A kind of processing method of deer's sinew liquor is present embodiments provided, step includes:
A is measured:Weigh following major ingredient:Deer's sinew 9g, matrimony vine 13g, jujube 18g, ginseng 14g, blackberry lily 9g, sauce incense liquor 500g
B is filtered:Matrimony vine, jujube, ginseng, blackberry lily are placed in grinding machine for Chinese herb medicines, the degreasing silkworm of gross mass 0.017% is added
Pupa powder was ground to 80 mesh sieve, cold fermentation 25h under the conditions of then the composite zymocyte liquid of addition gross mass 78% is carried out at 6 DEG C
Afterwards, with after nanofiltration membrane, filter residue and filtrate are obtained, wherein composite zymocyte liquid is by mushroom powder and yeast powder according to mass ratio
It is 1:After 2.6 mixing, the glucose of gross mass 3.5%, 0.011% protease, 0.02% cellulase, 0.02% fruit is added
Glue enzyme, 0.5% calcium lactate, 87% sterile water configure;
C sterilizes:Gained filter residue and filtrate will be filtered through infrared sterilization;
D is encapsulated:Filter residue is wrapped up with NF membrane;
E impregnates:Encapsulation filter residue, deer's sinew are soaked in sauce incense liquor, first impregnate 1d under the conditions of thermostat temperature is 45 DEG C,
Then cool down it is 3 DEG C most subzero under the conditions of impregnate 1d;
F distillation separation:First air-distillation to distillate alcoholic strength is 40-45 °, is then steamed in the case where vacuum degree is negative 50kPa
It is 35-38 ° to evaporate to distillate alcoholic strength, and then in the case where vacuum degree is negative 65kPa, distillation to distillate alcoholic strength is 28-32 °;
G is blent for bis- times:After inciting somebody to action distillate mixing three times, it is 218W to be placed in power, and frequency is ultrasonic wave under the conditions of 7600Hz
Radiate 6min.
Test example 1
Immunity
Experimental method:70 healthy mices are selected, are divided into 7 groups at random, every group of mouse peritoneal injects cyclophosphamide
After under (40mg/kg, 2 times a week, totally 1 week) induced immunity, test group 1-5 is drunk with deer's sinew liquor daily, and control group 1 is every
Day is drunk with physiological saline, and control group 2 is brewed to be slurried with albumen powder and be drunk daily, drinks 2ml/ daily only, daily
It drinks once, after drinking 15 days, test mouse lymphocyte proliferative capacity (OD differences) and NK cell activity are as a result as follows:
Claims (6)
1. a kind of processing method of deer's sinew liquor, which is characterized in that step includes:Metering, sterilizing, encapsulation, is impregnated, distillation at filtering
Separation secondary blends step;The metering is to weigh following major ingredient in parts by weight:6-10 parts of deer's sinew, 10-20 parts of matrimony vine,
10-20 parts of jujube, 10-15 parts of ginseng, 5-10 parts of blackberry lily, 495-505 parts of sauce incense liquor;The filtering is will be in previous materials
It is filtered after the fermented processing of matrimony vine, jujube, ginseng, blackberry lily, takes filter residue and filtrate;The sterilizing is will to filter gained filter residue through red
Outside line is sterilized;The encapsulation is to wrap up filter residue with NF membrane;It is white that the immersion is encapsulation filter residue, deer's sinew is soaked in paste flavor
In wine;It is 40-45 ° that the distillation separation, which is first air-distillation to distillate alcoholic strength, is then steamed in the case where vacuum degree is negative 50kPa
It is 35-38 ° to evaporate to distillate alcoholic strength, and then in the case where vacuum degree is negative 65kPa, distillation to distillate alcoholic strength is 28-32 °;Institute
It is Ultrasonic Radiation 5-8min after mixing distillate three times to state secondary blend.
2. the processing method of deer's sinew liquor as described in claim 1, which is characterized in that the filtering is by matrimony vine, jujube, people
Ginseng, blackberry lily are placed in grinding machine for Chinese herb medicines, and the degreased pupa powder that gross mass 0.01-0.02% is added was ground to 80 mesh sieve, then
After the composite zymocyte liquid progress cold fermentation 20-28h of gross mass 70-80% is added, after nanofiltration membrane, filter residue and filter are obtained
Liquid.
3. the processing method of deer's sinew liquor as claimed in claim 2, which is characterized in that the cold fermentation, temperature 0-8
℃。
4. the processing method of deer's sinew liquor as claimed in claim 2, which is characterized in that the composite zymocyte liquid is by mushroom powder
With yeast powder according to mass ratio be 1:After (2-3) mixing, the glucose of gross mass 2-5%, the albumen of 0.07-0.12% is added
Enzyme, 0.02-0.05% cellulases, 0.01-0.04% pectases, the calcium lactate of 0.2-0.6%, 80-95% sterile water match
It sets.
5. the processing method of deer's sinew liquor as described in claim 1, which is characterized in that the immersion is to be first in thermostat temperature
1-2d is impregnated under the conditions of 38-45 DEG C, then cool down it is 5-0 DEG C most subzero under the conditions of impregnate 1-2d.
6. the processing method of deer's sinew liquor as described in claim 1, which is characterized in that the Ultrasonic Radiation, power are
200-230W, frequency 7500-7800Hz.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111548895A (en) * | 2020-04-28 | 2020-08-18 | 四川轻化工大学 | Experimental method for distillation process in liquor distillation |
CN113881539A (en) * | 2021-11-24 | 2022-01-04 | 宁夏红枸杞产业有限公司 | Medlar juice wine and preparation method thereof |
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CN113881539A (en) * | 2021-11-24 | 2022-01-04 | 宁夏红枸杞产业有限公司 | Medlar juice wine and preparation method thereof |
CN113881539B (en) * | 2021-11-24 | 2024-02-13 | 宁夏红枸杞产业有限公司 | Lycium barbarum juice wine and preparation method thereof |
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