CN108659944A - A kind of processing method of grinding fluid for the manufacture of paint spraying equipment part - Google Patents
A kind of processing method of grinding fluid for the manufacture of paint spraying equipment part Download PDFInfo
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- CN108659944A CN108659944A CN201810521312.5A CN201810521312A CN108659944A CN 108659944 A CN108659944 A CN 108659944A CN 201810521312 A CN201810521312 A CN 201810521312A CN 108659944 A CN108659944 A CN 108659944A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M173/00—Lubricating compositions containing more than 10% water
- C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M177/00—Special methods of preparation of lubricating compositions; Chemical modification by after-treatment of components or of the whole of a lubricating composition, not covered by other classes
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/085—Phosphorus oxides, acids or salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/087—Boron oxides, acids or salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/14—Inorganic compounds or elements as ingredients in lubricant compositions inorganic compounds surface treated with organic compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The invention discloses a kind of processing methods of the grinding fluid for the manufacture of paint spraying equipment part, include the following steps：（1）Material weigh it is spare,（2）Raw material mixing,（3）It is prepared by finished product.The method of the present invention integrated artistic is simple, application easy to spread, and grinding fluid cooling performance obtained, greasy property is more existing is obviously improved, integrated quality is effectively improved, and the efficiency and effect of grinding are improved well, the precision of part is improved, is had good value for applications.
Description
Technical field
The invention belongs to the working process technical fields of grinding fluid, and in particular to one kind being used for paint spraying equipment part system
The processing method for the grinding fluid made.
Background technology
Paint spraying equipment is the equipment for being sprayed on paint atomizing on workpiece, is common in modern people's life
, indispensable equipment, it is beautiful and bring facility using the improvement of quality for workpiece.Paint spraying equipment includes multiple sets
Standby, such as supercharging equipment, atomization spraying equipment, storage facilities, each equipment is formed by multiple part combinations, and such crowd
More parts in processing and manufacturing more need to carry out grinding processing, and in the presence that is ground the when of handling and can't do without grinding fluid, grinding
Liquid is the industrial type fluid for cooling down and lubricating grinding wheel and workpiece, and cutting fluid should have good cooling performance, lubricity
The characteristics of energy, rustless property, oil removing cleaning function, anti-corrosion function, easily dilutable.
For current metal working fluid mostly based on mineral oil, this needs a large amount of petroleum resources, the biology of mineral oil
Degradability is poor, containing harmful substances such as polycyclic aromatic hydrocarbons, is easy pollution environment.Therefore, many developed countries make laws in succession controls metal
The discharge of working fluid, it is desirable to which exploitation can biodegradable metal working fluid base oil substitute mineral oil.Though fully synthetic product using
Product based on industrial chemicals, but in low side grinding fluid even with the nitrite and organic phenol disabled be mainly at
Point, these additives have certain carcinogenesis, and the health of operator, contaminant water after discharge can be endangered during use
Body causes water resource pollution and environmental disruption.And that there are cleanings is poor, machining accuracy is inaccurate, is mostly served only for corase grinding processing, no
Suitable for fine grinding, greasy property is inadequate, and the skin and eyes to operating personnel have stimulation, and easily causes " nitrite " and bring
Health problem.Therefore, a kind of corrosion-free effect is researched and developed, it is comprehensive to use good quality, environment amenable nontoxic metal removal
Liquid is the art urgent problem to be solved.
Invention content
The purpose of the present invention is for existing problem, provide a kind of grinding for the manufacture of paint spraying equipment part
The processing method of liquid.
The present invention is achieved by the following technical solutions：
A kind of processing method of grinding fluid for the manufacture of paint spraying equipment part, includes the following steps：
（1）Material weighs spare：
It is spare that following materials are weighed by corresponding parts by weight：40 ~ 45 parts of antirust agent, 2 ~ 4 parts of antifoaming agent, 1 ~ 2 part of triethanolamine, 0.5 ~
1 part of calgon, 2 ~ 5 parts of neopelexes, 1 ~ 1.5 part of sodium tetraborate, 4 ~ 7 parts of modified inorganic fillers, 55 ~ 60 parts
Deionized water；
（2）Raw material mixes：
By step（1）The all materials weighed are put into agitator tank jointly, and it is 45 ~ 50 that heating, which is kept stirring the temperature in tank,
DEG C, it is spare to obtain premix after 30 ~ 35min of high-speed stirred processing；
（3）It is prepared by finished product：
By step（2）The premix of gained, which is put into ultrasonication instrument, carries out ultrasound wave irradiation 2 ~ 3h of processing, takes after the completion
Go out to get product grinding fluid.
Further, step（1）Described in antirust agent be water soluble anti-rust agent.
Further, step（1）Described in antifoaming agent be that polyoxyethylene polyoxypropylene pentaerythrite ether, polyoxyethylene are poly-
One kind in oxygen propyl alcohol amidogen ether.
Further, step（1）Described in the preparation method of modified inorganic filler be specifically：
A. 5 ~ 7min of immersion treatment in the hydrochloric acid solution that mass fraction is 8 ~ 10% first is put into montmorillonite, is put into again after taking-up
6 ~ 8min of immersion treatment in the sodium hydroxide solution for being 10 ~ 12% to mass fraction, finally taking-up are rinsed with deionized water to neutrality
It is spare afterwards；
B. will operation a treated that montmorillonite is put into calcining furnace carries out calcination processing, taken out after 1.5 ~ 2h spare；
C. first by dimethyldimethoxysil,ne and diethanol monoisopropanolamine according to weight ratio 1:2.5 ~ 2.7 are mixed, and are put
Enter into reaction kettle, it is 123 ~ 127 DEG C that then heating, which keeps the temperature in reaction kettle, after high-speed stirred handles 2.5 ~ 3h, then to
18 ~ 24% dibromopropane of dimethyldimethoxysil,ne gross mass, 2.5 ~ 3.5 times of absolute methanol are added in reaction kettle, then
Keep reaction kettle in temperature be 44 ~ 50 DEG C, high-speed stirred handle 2 ~ 2.5h after take out mixture A is spare；Utilize dimethyl
Dimethoxysilane reacts with diethanol monoisopropanolamine, and modified silane component is made, and then occurs with dibromopropane
Quaternization reaction forms compound quaternary ammonium salt component, can improve the surface-active of montmorillonite well, avoid mutual
Agglomeration is adsorbed, dispersion effect is improved；
D. by operate c obtained by mixture A and 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, odium stearate, titanium carbide, go from
Sub- water is according to weight ratio 6 ~ 8：0.3~0.5:1.6~2.2:2~3:90 ~ 95, which carry out mixing, puts into agitator tank, and high-speed stirred is equal
After even again will operation b treated that montmorillonite is put into agitator tank, ultrasonic vibration handles centrifugal filtration after 2.5 ~ 3h, then again
After vacuum dried processing.Under the action of the ingredients such as 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, titanium carbide is effective
Intercalation be fixed on the interlayer of montmorillonite, expand interlamellar spacing, enhance the slipping property of piece interlayer, while titanium carbide granule rises again
The effect for having arrived similar ball, improves the efficiency of lamella sliding, helps be ground the discharge of clast and the movement of heat, reduce
The damage of cutter, improves the precision of workpiece.
Further, it is 800 ~ 860 DEG C that heating, which keeps the temperature in calcining furnace, when operating the calcination processing described in b.
Further, speed of agitator when operating the high-speed stirred processing described in c is 2400 ~ 2600 revs/min.
Further, ultrasonic frequency when operating the ultrasonic vibration processing described in d is 200 ~ 240kHz.
Further, step（2）Described in high-speed stirred processing when speed of agitator be 1800 ~ 2000 revs/min.
Further, step（3）Described in ultrasound wave irradiation processing when ultrasonic frequency be 360 ~ 380kHz.
Present invention optimizes the processing methods of grinding fluid, be especially added to a kind of modified inorganic filler of formulated at
Point, different from common inorganic filler, this modified inorganic filler is uniformly dispersed, and is not easy to reunite, and can effectively promote the efficiency of grinding
And precision, prepared modified inorganic filler are that one kind substance based on montmorillonite is modified and handles, first to its into
It has gone soda acid immersion treatment, has effectively eliminated the impurity component on surface, then carried out calcination processing and improve its ratio well
Surface area enhances its adsorption reaction ability, lays a good foundation for subsequent processing, is finally carried out to montmorillonite with Multiple components
It is mixed and modified, its surface-active is improved, its dispersion effect is improved, avoid the generation of agglomeration, after final process
Montmorillonite good dispersion, lubricity is good, contribute to be ground clast timely discharge, reduce the probability of workpiece damage, improve
The precision and efficiency of grinding, it is final to coordinate being used in conjunction with for rest materials, it is effectively guaranteed the cooling of grinding fluid
Energy, greasy property, rustless property, oil removing cleaning function, anti-corrosion function etc..
The present invention has the following advantages compared with prior art：
The method of the present invention integrated artistic is simple, application easy to spread, and grinding fluid cooling performance obtained, greasy property are more existing
It is obviously improved, integrated quality is effectively improved, and improves the efficiency and effect of grinding well, improves the essence of part
Degree, has good value for applications.
Specific implementation mode
Embodiment 1
A kind of processing method of grinding fluid for the manufacture of paint spraying equipment part, includes the following steps：
（1）Material weighs spare：
It is spare that following materials are weighed by corresponding parts by weight：40 parts of antirust agent, 2 parts of antifoaming agent, 1 part of triethanolamine, 0.5 part of six inclined phosphorus
Sour sodium, 2 parts of neopelexes, 1 part of sodium tetraborate, 4 parts of modified inorganic fillers, 55 parts of deionized waters；
（2）Raw material mixes：
By step（1）The all materials weighed are put into agitator tank jointly, and it is 45 DEG C that heating, which is kept stirring the temperature in tank, high
It is spare that premix is obtained after fast stir process 30min；
（3）It is prepared by finished product：
By step（2）The premix of gained, which is put into ultrasonication instrument, carries out ultrasound wave irradiation processing 2h, takes out after the completion
Get product grinding fluid.
Further, step（1）Described in antirust agent be water soluble anti-rust agent.
Further, step（1）Described in antifoaming agent be polyoxyethylene polyoxypropylene pentaerythrite ether.
Further, step（1）Described in the preparation method of modified inorganic filler be specifically：
A. immersion treatment 5min in the hydrochloric acid solution that mass fraction is 8% first is put into montmorillonite, puts into quality after taking-up again
Immersion treatment 6min, spare after finally taking-up is rinsed with deionized water to neutrality in the sodium hydroxide solution that score is 10%；
B. will operation a treated that montmorillonite is put into calcining furnace carries out calcination processing, taken out after 1.5h spare；
C. first by dimethyldimethoxysil,ne and diethanol monoisopropanolamine according to weight ratio 1:2.5 are mixed, and are put into
In reaction kettle, it is 123 DEG C that then heating, which keeps the temperature in reaction kettle, after high-speed stirred handles 2.5h, then is added into reaction kettle
Enter dibromopropane, 2.5 times of the absolute methanol of dimethyldimethoxysil,ne gross mass 18%, then keeps the temperature in reaction kettle
Degree be 44 DEG C, high-speed stirred processing 2h after take out mixture A is spare；Utilize dimethyldimethoxysil,ne and diethanol Dan Yi
Propanolamine reacts, and modified silane component is made, and quaternization reaction then, which occurs, with dibromopropane forms compound quaternary ammonium
Salt component can improve the surface-active of montmorillonite well, avoid mutual absorption agglomeration, improve dispersion effect
Fruit；
D. by operate c obtained by mixture A and 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, odium stearate, titanium carbide, go from
Sub- water is according to weight ratio 6：0.3:1.6:2:90, which carry out mixing, puts into agitator tank, will be operated at b again after high-speed stirred is uniform
Montmorillonite after reason is put into agitator tank, and ultrasonic vibration handles centrifugal filtration after 2.5h, then again after vacuum dried processing
.Under the action of the ingredients such as 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, it is de- that the effective intercalation of titanium carbide is fixed on illiteracy
The interlayer of soil, expands interlamellar spacing, enhances the slipping property of piece interlayer, while titanium carbide granule plays the work of similar ball again
With, improve lamella sliding efficiency, help be ground clast discharge and heat movement, reduce the damage of cutter, carry
The high precision of workpiece.
Further, it is 800 DEG C that heating, which keeps the temperature in calcining furnace, when operating the calcination processing described in b.
Further, speed of agitator when operating the high-speed stirred processing described in c is 2400 revs/min.
Further, ultrasonic frequency when operating the ultrasonic vibration processing described in d is 200kHz.
Further, step（2）Described in high-speed stirred processing when speed of agitator be 1800 revs/min.
Further, step（3）Described in ultrasound wave irradiation processing when ultrasonic frequency be 360kHz.
Embodiment 2
A kind of processing method of grinding fluid for the manufacture of paint spraying equipment part, includes the following steps：
（1）Material weighs spare：
It is spare that following materials are weighed by corresponding parts by weight：43 parts of antirust agent, 3 parts of antifoaming agent, 1.5 parts of triethanolamines, 0.8 part six partially
Sodium phosphate, 4 parts of neopelexes, 1.2 parts of sodium tetraborates, 6 parts of modified inorganic fillers, 57 parts of deionized waters；
（2）Raw material mixes：
By step（1）The all materials weighed are put into agitator tank jointly, and it is 48 DEG C that heating, which is kept stirring the temperature in tank, high
It is spare that premix is obtained after fast stir process 33min；
（3）It is prepared by finished product：
By step（2）The premix of gained, which is put into ultrasonication instrument, carries out ultrasound wave irradiation processing 2.6h, takes after the completion
Go out to get product grinding fluid.
Further, step（1）Described in antirust agent be water soluble anti-rust agent.
Further, step（1）Described in antifoaming agent be polyoxyethylene polyoxypropylene pentaerythrite ether.
Further, step（1）Described in the preparation method of modified inorganic filler be specifically：
A. immersion treatment 6min in the hydrochloric acid solution that mass fraction is 9% first is put into montmorillonite, puts into quality after taking-up again
Immersion treatment 7min, spare after finally taking-up is rinsed with deionized water to neutrality in the sodium hydroxide solution that score is 11%；
B. will operation a treated that montmorillonite is put into calcining furnace carries out calcination processing, taken out after 1.8h spare；
C. first by dimethyldimethoxysil,ne and diethanol monoisopropanolamine according to weight ratio 1:2.6 are mixed, and are put into
In reaction kettle, it is 125 DEG C that then heating, which keeps the temperature in reaction kettle, after high-speed stirred handles 2.8h, then is added into reaction kettle
Enter dibromopropane, 3 times of the absolute methanol of dimethyldimethoxysil,ne gross mass 22%, then keeps the temperature in reaction kettle
Be 48 DEG C, high-speed stirred processing 2.2h after take out mixture A is spare；Utilize dimethyldimethoxysil,ne and diethanol Dan Yi
Propanolamine reacts, and modified silane component is made, and quaternization reaction then, which occurs, with dibromopropane forms compound quaternary ammonium
Salt component can improve the surface-active of montmorillonite well, avoid mutual absorption agglomeration, improve dispersion effect
Fruit；
D. by operate c obtained by mixture A and 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, odium stearate, titanium carbide, go from
Sub- water is according to weight ratio 7：0.4:1.8:2.5:93, which carry out mixing, puts into agitator tank, will operate b after high-speed stirred is uniform again
Treated, and montmorillonite is put into agitator tank, and ultrasonic vibration handles centrifugal filtration after 2.7h, then vacuum dried processing again
Afterwards.Under the action of the ingredients such as 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, the effective intercalation of titanium carbide is fixed on illiteracy
The interlayer for taking off soil, expands interlamellar spacing, enhances the slipping property of piece interlayer, while titanium carbide granule plays similar ball again
Effect improves the efficiency of lamella sliding, helps be ground the discharge of clast and the movement of heat, reduces the damage of cutter,
Improve the precision of workpiece.
Further, it is 830 DEG C that heating, which keeps the temperature in calcining furnace, when operating the calcination processing described in b.
Further, speed of agitator when operating the high-speed stirred processing described in c is 2500 revs/min.
Further, ultrasonic frequency when operating the ultrasonic vibration processing described in d is 220kHz.
Further, step（2）Described in high-speed stirred processing when speed of agitator be 1900 revs/min.
Further, step（3）Described in ultrasound wave irradiation processing when ultrasonic frequency be 370kHz.
Embodiment 3
A kind of processing method of grinding fluid for the manufacture of paint spraying equipment part, includes the following steps：
（1）Material weighs spare：
It is spare that following materials are weighed by corresponding parts by weight：45 parts of antirust agent, 4 parts of antifoaming agent, 2 parts of triethanolamines, 1 part of hexa metaphosphoric acid
Sodium, 5 parts of neopelexes, 1.5 parts of sodium tetraborates, 7 parts of modified inorganic fillers, 60 parts of deionized waters；
（2）Raw material mixes：
By step（1）The all materials weighed are put into agitator tank jointly, and it is 50 DEG C that heating, which is kept stirring the temperature in tank, high
It is spare that premix is obtained after fast stir process 35min；
（3）It is prepared by finished product：
By step（2）The premix of gained, which is put into ultrasonication instrument, carries out ultrasound wave irradiation processing 3h, takes out after the completion
Get product grinding fluid.
Further, step（1）Described in antirust agent be water soluble anti-rust agent.
Further, step（1）Described in antifoaming agent be polyoxyethylene polyoxy propyl alcohol amidogen ether.
Further, step（1）Described in the preparation method of modified inorganic filler be specifically：
A. immersion treatment 7min in the hydrochloric acid solution that mass fraction is 10% first is put into montmorillonite, puts into matter after taking-up again
Immersion treatment 8min in the sodium hydroxide solution that score is 12% is measured, it is spare after finally taking-up is rinsed with deionized water to neutrality；
B. will operation a treated that montmorillonite is put into calcining furnace carries out calcination processing, taken out after 2h spare；
C. first by dimethyldimethoxysil,ne and diethanol monoisopropanolamine according to weight ratio 1:2.7 are mixed, and are put into
In reaction kettle, it is 127 DEG C that then heating, which keeps the temperature in reaction kettle, after high-speed stirred handles 3h, then is added into reaction kettle
Then the dibromopropane of dimethyldimethoxysil,ne gross mass 24%, 3.5 times of absolute methanol keep the temperature in reaction kettle
Be 50 DEG C, high-speed stirred processing 2.5h after take out mixture A is spare；Utilize dimethyldimethoxysil,ne and diethanol Dan Yi
Propanolamine reacts, and modified silane component is made, and quaternization reaction then, which occurs, with dibromopropane forms compound quaternary ammonium
Salt component can improve the surface-active of montmorillonite well, avoid mutual absorption agglomeration, improve dispersion effect
Fruit；
D. by operate c obtained by mixture A and 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, odium stearate, titanium carbide, go from
Sub- water is according to weight ratio 8：0.5: 2.2:3:95, which carry out mixing, puts into agitator tank, will be operated at b again after high-speed stirred is uniform
Montmorillonite after reason is put into agitator tank, and ultrasonic vibration handles centrifugal filtration after 3h, is then after vacuum dried processing again
It can.Under the action of the ingredients such as 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, the effective intercalation of titanium carbide is fixed on montmorillonite
Interlayer, expand interlamellar spacing, enhance the slipping property of piece interlayer, while titanium carbide granule plays the work of similar ball again
With, improve lamella sliding efficiency, help be ground clast discharge and heat movement, reduce the damage of cutter, carry
The high precision of workpiece.
Further, it is 860 DEG C that heating, which keeps the temperature in calcining furnace, when operating the calcination processing described in b.
Further, speed of agitator when operating the high-speed stirred processing described in c is 2600 revs/min.
Further, ultrasonic frequency when operating the ultrasonic vibration processing described in d is 240kHz.
Further, step（2）Described in high-speed stirred processing when speed of agitator be 2000 revs/min.
Further, step（3）Described in ultrasound wave irradiation processing when ultrasonic frequency be 380kHz.
Claims (9)
1. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part, which is characterized in that include the following steps：
（1）Material weighs spare：
It is spare that following materials are weighed by corresponding parts by weight：40 ~ 45 parts of antirust agent, 2 ~ 4 parts of antifoaming agent, 1 ~ 2 part of triethanolamine, 0.5 ~
1 part of calgon, 2 ~ 5 parts of neopelexes, 1 ~ 1.5 part of sodium tetraborate, 4 ~ 7 parts of modified inorganic fillers, 55 ~ 60 parts
Deionized water；
（2）Raw material mixes：
By step（1）The all materials weighed are put into agitator tank jointly, and it is 45 ~ 50 that heating, which is kept stirring the temperature in tank,
DEG C, it is spare to obtain premix after 30 ~ 35min of high-speed stirred processing；
（3）It is prepared by finished product：
By step（2）The premix of gained, which is put into ultrasonication instrument, carries out ultrasound wave irradiation 2 ~ 3h of processing, takes after the completion
Go out to get product grinding fluid.
2. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part according to claim 1, special
Sign is, step（1）Described in antirust agent be water soluble anti-rust agent.
3. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part according to claim 1, special
Sign is, step（1）Described in antifoaming agent be polyoxyethylene polyoxypropylene pentaerythrite ether, polyoxyethylene polyoxy propyl alcohol amidogen ether
In one kind.
4. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part according to claim 1, special
Sign is, step（1）Described in the preparation method of modified inorganic filler be specifically：
A. 5 ~ 7min of immersion treatment in the hydrochloric acid solution that mass fraction is 8 ~ 10% first is put into montmorillonite, is put into again after taking-up
6 ~ 8min of immersion treatment in the sodium hydroxide solution for being 10 ~ 12% to mass fraction, finally taking-up are rinsed with deionized water to neutrality
It is spare afterwards；
B. will operation a treated that montmorillonite is put into calcining furnace carries out calcination processing, taken out after 1.5 ~ 2h spare；
C. first by dimethyldimethoxysil,ne and diethanol monoisopropanolamine according to weight ratio 1:2.5 ~ 2.7 are mixed, and are put
Enter into reaction kettle, it is 123 ~ 127 DEG C that then heating, which keeps the temperature in reaction kettle, after high-speed stirred handles 2.5 ~ 3h, then to
18 ~ 24% dibromopropane of dimethyldimethoxysil,ne gross mass, 2.5 ~ 3.5 times of absolute methanol are added in reaction kettle, then
Keep reaction kettle in temperature be 44 ~ 50 DEG C, high-speed stirred handle 2 ~ 2.5h after take out mixture A is spare；
D. by operate c obtained by mixture A and 4- (6- amidos hexyloxy) -4 '-cyanobiphenyl, odium stearate, titanium carbide, go from
Sub- water is according to weight ratio 6 ~ 8：0.3~0.5:1.6~2.2:2~3:90 ~ 95, which carry out mixing, puts into agitator tank, and high-speed stirred is equal
After even again will operation b treated that montmorillonite is put into agitator tank, ultrasonic vibration handles centrifugal filtration after 2.5 ~ 3h, then again
After vacuum dried processing.
5. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part according to claim 4, special
Sign is that it is 800 ~ 860 DEG C that heating, which keeps the temperature in calcining furnace, when operating the calcination processing described in b.
6. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part according to claim 4, special
Sign is that speed of agitator when operating the high-speed stirred processing described in c is 2400 ~ 2600 revs/min.
7. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part according to claim 4, special
Sign is that ultrasonic frequency when operating the ultrasonic vibration processing described in d is 200 ~ 240kHz.
8. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part according to claim 1, special
Sign is, step（2）Described in high-speed stirred processing when speed of agitator be 1800 ~ 2000 revs/min.
9. a kind of processing method of grinding fluid for the manufacture of paint spraying equipment part according to claim 1, special
Sign is, step（3）Described in ultrasound wave irradiation processing when ultrasonic frequency be 360 ~ 380kHz.
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| US20030100455A1 (en) * | 1999-05-18 | 2003-05-29 | Hiroshi Oishi | Aqueous grinding fluid for wire-sawing or band-sawing |
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| CN104017636A (en) * | 2014-06-06 | 2014-09-03 | 清华大学 | Water soluble full-alloy metal grinding fluid |
| CN106675749A (en) * | 2016-11-02 | 2017-05-17 | 清华大学天津高端装备研究院 | Fully-synthetic water-based glass grinding fluid and preparation method thereof |
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2018
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US20030100455A1 (en) * | 1999-05-18 | 2003-05-29 | Hiroshi Oishi | Aqueous grinding fluid for wire-sawing or band-sawing |
| JP2004315762A (en) * | 2003-04-21 | 2004-11-11 | Chiyoda Chemical Kk | Water dispersion type metal working agent composition and method for producing the same |
| CN1566295A (en) * | 2003-06-30 | 2005-01-19 | 中国石油化工股份有限公司 | Process for producing water based lubricating liquid |
| CN101405334A (en) * | 2006-01-20 | 2009-04-08 | 莫门蒂夫性能材料股份有限公司 | Inorganic-organic nanocomposite |
| CN103849450A (en) * | 2014-02-24 | 2014-06-11 | 昆明理工大学 | Water-based nanometer carbide fluid and preparation method thereof |
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