CN108653080A - One plant tea bran shampoo and preparation method thereof - Google Patents
One plant tea bran shampoo and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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Abstract
The present invention relates to plant tea bran shampoo and preparation method thereof, the raw material of the tea bran shampoo is tea bran, gleditsia sinensis, the tuber of multiflower knotweed, thickener, foaming agent, antipruritic, nutritional ingredient, moisturizer, preservative, pearling agent, citric acid, edible oil, flavouring agent, conditioner, pure water.Raw material of the present invention is compounded using hexamidine two (isethionate) and tea bran, can generate cleaning, fungistatic effect well.The preparation method of the preferred tea bran of preparation process, gleditsia sinensis fleece-flower root：It is combined with pulverizer and colloid mill, tea bran, gleditsia sinensis etc. can not only dissolved out to the greatest extent, but also can make what it stablized to be present in system, preferably play its effectiveness, while also more energy efficient；Preparation process is repeatedly combined with homogenizer, makes its system dispersion micronized, while keeping system more stable.Product cleaning effect of the present invention is good, and hair soft after hair washing is easy to comb, while can raise scalp, restore scalp ecological environment balance, inhibit head itch, dandruff the problems such as.
Description
Technical field
The invention belongs to hair shampoo article technical fields, are related to plant tea bran shampoo and preparation method thereof.
Background technology
Shampoo refers to a kind of hair products with functions such as anti-dandruff, treatment oil, contains Multiple components in shampoo, this
The comprehensive function of a little compositions can play the function of cleaning scalp and hair.Modern society's people's rhythm of life is getting faster, and is brought
The problems such as work and rest is irregular, stress is big, regular insomnia.Hair healthy problem, especially dandruff are more, scalp is sent out
It is one of insoluble problem of long-standing problem people to itch.Therefore, only there is traditional shampoo of clean hair function cannot expire
The demand of sufficient people.And contain vitamin B, vitamin E and tea polyphenols in tea bran, and tea polyphenols have the work(such as radioresistance anti-cancer
Can, while there is the shampoo of a variety of conditioning effects could be liked by consumer.Have in the prior art using tea bran as former
The shampoo of material, has the following problems：Tea bran cannot be uniform and stable be present in system, be easy sedimentation, in tea bran effectively at
The effect of divide to dissolve out to greatest extent, tea bran cannot be fully used, and cleaning fungistatic effect is undesirable.
The Chinese invention patent file of Publication No. CN106924116A discloses a plant tea bran shampoo, and the patent is by tea
Bran is ground into the micro mist of 2000 mesh or more, then impregnates 12-24h, so that the active ingredient in tea bran is dissolved out, adds oligomeric fruit
Sugar, hyaluronic acid, camellia oil.Do not illustrate how the micro mist that tea bran is ground into 2000 mesh or more in the patent clearly, it is practical to grasp
Those skilled in the art are difficult that tea bran is ground into 2000 mesh or more during work；If in addition, be only that tea bran is ground into micro mist, after
Preparation processes being present in system that continuous preparation process keeps tea bran micro mist uniform and stable without other, be prepared at
The effect of what product still had that tea bran cannot be uniform and stable is present in system, is easy sedimentation, tea bran cannot be fully used
The shortcomings that, tea bran is only added in the patent, is not added other and is cleaned antibacterial auxiliary element, cleaning, fungistatic effect are paid no attention to
Think, its moistening effect is also undesirable after cleaning.
Invention content
The technical problem to be solved by the present invention is to：There is provided a kind of cleaning of product, good antimicrobial effect tea bran shampoo and its
Preparation method can make tea bran, gleditsia sinensis, the tuber of multiflower knotweed thinner, and more stable is present in system, can preferably play its effect
Fruit solves tea bran during preparing shampoo and is not easy stable to be present in the problems in system.
Solving the technical solution of above-mentioned technical problem is：One plant tea bran shampoo, the shampoo is mainly by following weight parts
Several raw materials are prepared：The total number of each raw material be 100 parts, wherein tea bran 5-25 part, 0-5 parts of gleditsia sinensis, 0-5 parts of the tuber of multiflower knotweed, increasing
Thick dose 0.5-12 parts, 3-18 parts of foaming agent, 0.01-0.6 parts of antipruritic, 0.1-0.5 parts of nutritional ingredient, moisturizer 0.01-0.05
Part, 0.01-1.1 parts of preservative, 0.3-3 parts of pearling agent, 0.1-0.8 parts of citric acid, 0.01-0.5 parts of edible oil, flavouring agent
0.01-0.3 parts, 0.1-4 parts of conditioner, pure water surplus.
The antipruritic is hexamidine two (isethionate) and climbazole, to causing the fungi of dandruff to have good suppression
Effect processed.
The thickener is Cocoamidopropyl betaine (CAB-35), coconut oleoyl amine DEA, coconut oleoyl amine MEA and propylene
Acid（Ester）Analog copolymer.
The foaming agent is laureth sodium sulfovinate and laruyl alcohol sulfuric acid ester ammonium；With excellent decontamination, emulsification and
The effect of submissive conditioning hair.
The nutritional ingredient is oligofructose and D-pantothenyl aleohol；Oligofructose：It can inhibit the growth of skin surface harmful bacteria,
And it can effectively slow down pigementation, desalinate and eliminate color spot, have good effect to skin；D-pantothenyl aleohol：Lasting moisturizing work(
Can, hair jag is prevented, is damaged, the density of hair can be increased, improve the gloss of hair quality.
The moisturizer is sodium hyaluronate；It moisturizes the skin, hair, increases the gloss of hair.
The preservative is Phenoxyethanol and Kathon CG.
The pearling agent is two stearic acid sodium of ethylene glycol.
The edible oil is tea-seed oil.
The flavouring agent is essence.
The conditioner is polyquaternium and guar hydroxypropyltrimonium ammonium chloride.
The present invention further technical solution be：One plant tea bran shampoo, the shampoo is mainly by following portions by weight
Raw material is prepared：The total number of each raw material is 100 parts, wherein 10 parts of tea bran, 0.1 part of gleditsia sinensis, 0.1 part of the tuber of multiflower knotweed, coconut oleoyl amine
Propyl betaine（CAB-35）7 parts, 1 part of 1 part of coconut oleoyl amine DEA, coconut oleoyl amine MEA, acrylic acid（Ester）3 parts of analog copolymer,
9 parts of laureth sodium sulfovinate, 3 parts of bay alcohol sulfuric ester ammonium, hexamidine two（Isethionate）0.1 part, climbazole 0.5
Part, 0.2 part of oligofructose, 0.1 part of D-pantothenyl aleohol, 0.01 part of sodium hyaluronate, 1 part of Phenoxyethanol, 0.1 part of Kathon CG, ethylene glycol distearyl
0.8 part of acid esters, 0.4 part of citric acid, 0.1 part of tea-seed oil, 0.2 part of essence, 1.5 parts of polyquaternium -47, Polyquaternium-10 0.8
Part, 1 part of guar hydroxypropyltrimonium ammonium chloride, pure water surplus.
The present invention another technical solution be：A kind of preparation method of above-mentioned tea bran shampoo, includes the following steps：
(1) with pulverizer by the tea bran or tea bran and gleditsia sinensis or tea bran and the tuber of multiflower knotweed or tea bran and gleditsia sinensis, tuber of multiflower knotweed raw material powder after drying
It is broken, it is ground into 100-200 mesh powders；
(2) colloid mill is crossed after the raw material damping after (1) step being crushed, makes it at relatively stable colloidal state；
(3) 12-18 parts of pure water are added in emulsifying pot, adds (2) substance and tea-seed oil that step is made, is heated to 95~105
DEG C, 0.8~1.2h, 11~13h of cooling and standings are boiled at 95~105 DEG C；
(4) 78~83 DEG C are warmed to again, and acrylic acid is added in the first step（Ester）Analog copolymer, 15~20min of homogeneous, second step add
Enter the laureth sodium sulfovinate aqueous solution that homogeneous is crossed, 10~30min of homogeneous after addition；Bay alcohol sulfuric ester is added in third step
Aqueous ammonium and Cocoamidopropyl betaine (CAB-35)；Temperature maintains 78~83 DEG C when charging；
(5) temperature maintains 78~83 DEG C and coconut oleoyl amine DEA, coconut oleoyl amine MEA, climbazole, hexamidine two is added into emulsification pot
（Isethionate）And sodium hyaluronate；
(6) temperature maintains 78~83 DEG C then to -47 aqueous solution of addition polyquaternium, oligofructose aqueous solution, D- in emulsification pot
Then it is water-soluble Polyquaternium-10 to be added into emulsification pot in panthenol aqueous solution and guar hydroxypropyltrimonium aqueous ammonium chloride solution
Liquid；
(7) temperature maintains 78~83 DEG C and the good glycol distearate aqueous solution of homogeneous is added into emulsification pot, and stirring is equal
25~35min of matter；
(8) temperature maintains 78~83 DEG C and adds 2-3 parts of pure water into emulsification pot, can start to drop after 1.5~2.5h of stirring homogeneous
Temperature；
(9) it is cooled to 38~43 DEG C and aqueous citric acid solution, Phenoxyethanol, Kathon CG and essence is added into emulsification pot, finally supplement is surplus
1.5~2.5h of homogeneous is stirred after remaining moisture, obtains finished product.
The laureth sodium sulfovinate aqueous solution, bay alcohol sulfuric ester aqueous ammonium, -47 aqueous solution of polyquaternium,
The system of guar hydroxypropyltrimonium aqueous ammonium chloride solution, Polyquaternium-10 aqueous solution and glycol distearate aqueous solution
It is for process：It homogenizes after adding water that solute is made just to dissolve into solute；The oligofructose aqueous solution, D-pantothenyl aleohol aqueous solution
Preparation process with aqueous citric acid solution is：It is made after adding water that solute is made just to dissolve into solute.
Due to the adoption of the above technical scheme, beneficial effects of the present invention are：Tea bran, gleditsia sinensis, the tuber of multiflower knotweed can be made thinner, more surely
Fixed is present in system, can preferably play its effect.This product cleaning effect is good, and hair soft after hair washing is easy to
Comb, while scalp can be raised, restore scalp ecological environment balance, inhibit head to itch, dandruff the problems such as.Advantages of the present invention has
Body is described below：
1, raw material of the present invention is compounded using hexamidine two (isethionate) and tea bran, can be generated and be cleaned well, is antibacterial
Effect.
2, the preparation method of the present invention preferably tea bran, gleditsia sinensis fleece-flower root：It is combined with pulverizer and colloid mill, can not only be made
Tea bran, gleditsia sinensis etc. to the greatest extent dissolve out, and can make its stablize be present in system, preferably play its effectiveness, simultaneously
It is also more energy efficient.During preparing shampoo, repeatedly it is combined with homogenizer, makes its system dispersion micronized, while making system
It is more stable.
Specific implementation mode
Embodiment 1
One plant tea bran shampoo, each component parts by weight are（Totally 100 parts of pure water and material）：5 parts of tea bran, cocamidopropyl propyl amide
5 parts of glycine betaine (CAB-35), 0.5 part of 0.5 part of coconut oleoyl amine DEA, coconut oleoyl amine MEA, acrylic acid（Ester）Analog copolymer 1.5
Part, 5 parts of laureth sodium sulfovinate, 2 parts of bay alcohol sulfuric ester ammonium, hexamidine two（Isethionate）0.1 part, climbazole
0.5 part, 0.1 part of oligofructose, 0.1 part of D-pantothenyl aleohol, 0.01 part of sodium hyaluronate, 1 part of Phenoxyethanol, 0.1 part of Kathon CG, ethylene glycol two is firmly
0.4 part of resin acid ester, 0.2 part of citric acid, 0.1 part of tea-seed oil, 0.1 part of essence, 1 part of polyquaternium -47, Polyquaternium-10 0.5
Part, 0.5 part of guar hydroxypropyltrimonium ammonium chloride, pure water surplus（It is equivalent to 75.79 parts）.
Embodiment 2
One plant tea bran shampoo, each component parts by weight are（Totally 100 parts of pure water and material）：10 parts of tea bran, 0.1 part of gleditsia sinensis are first
0.1 part of crow, 7 parts of Cocoamidopropyl betaine (CAB-35), 1 part of 1 part of coconut oleoyl amine DEA, coconut oleoyl amine MEA, acrylic acid
（Ester）3 parts of analog copolymer, 9 parts of laureth sodium sulfovinate, 3 parts of bay alcohol sulfuric ester ammonium, hexamidine two（Isethionic acid
Salt）0.1 part, 0.5 part of climbazole, 0.2 part of oligofructose, 0.1 part of D-pantothenyl aleohol, 0.01 part of sodium hyaluronate, 1 part of Phenoxyethanol, Kathon CG
0.1 part, 0.8 part of glycol distearate, 0.4 part of citric acid, 0.1 part of tea-seed oil, 0.2 part of essence, polyquaternium -47 1.5
Part, 0.8 part of Polyquaternium-10,1 part of guar hydroxypropyltrimonium ammonium chloride, pure water surplus（It is equivalent to 58.99 parts）.
Embodiment 3
One plant tea bran shampoo, each component parts by weight are（Totally 100 parts of pure water and material）：25 parts of tea bran, 5 parts of gleditsia sinensis, the tuber of multiflower knotweed 5
Part, 7 parts of Cocoamidopropyl betaine (CAB-35), 1 part of 1 part of coconut oleoyl amine DEA, coconut oleoyl amine MEA, acrylic acid（Ester）Class
2 parts of copolymer, 12 parts of laureth sodium sulfovinate, 4 parts of bay alcohol sulfuric ester ammonium, hexamidine two（Isethionate）0.1
Part, 0.5 part of climbazole, 0.2 part of oligofructose, 0.1 part of D-pantothenyl aleohol, 0.01 part of sodium hyaluronate, 1 part of Phenoxyethanol, 0.1 part of Kathon CG,
0.8 part of glycol distearate, 0.4 part of citric acid, 0.2 part of tea-seed oil, 0.3 part of essence, 2 parts of polyquaternium -47, poly- season
1 part of ammonium salt -10,1 part of guar hydroxypropyltrimonium ammonium chloride, pure water surplus（It is equivalent to 30.29 parts）.
Embodiment 4
The preparation method of tea bran shampoo described in a kind of embodiment 1- embodiments 3 makes tea bran using pulverizer and colloid mill combination
Grouts, gleditsia sinensis, the tuber of multiflower knotweed form relatively stable colloidal state, so that it is not settled, what can be stablized is present in system, plays its effect
With, while mobile homogenizer is used for multiple times during preparing shampoo makes its system dispersion micronized.
Including step in detail below：
(1) tea bran, gleditsia sinensis, the tuber of multiflower knotweed raw material after drying are crushed with pulverizer, are ground into 150 mesh powders.
By after crushing tea bran, gleditsia sinensis, colloid mill is crossed after tuber of multiflower knotweed raw material damping（Colloid mill uses at normal temperatures and pressures）,
Make it at relatively stable colloidal state.
(3) 15 parts of pure water are added in emulsifying pot（Each step is added later for remaining）, added the tea of complete colloid mill
The substances such as bran, gleditsia sinensis, the tuber of multiflower knotweed and tea-seed oil are heated to 100 DEG C, turn off steam after boiling 1h at 100 DEG C, are stood in emulsifying pot
12h。
(4) heating makes temperature be 80 DEG C（To keep temperature basicly stable during charging）, first step addition acrylic acid
（Ester）Analog copolymer（SF-1, liquid）, 15~20min of homogeneous, the laureth sodium sulfovinate water that second step addition homogeneous is crossed
Solution（Laureth sodium sulfovinate is semisolid, is added after water makes it just dissolve homogeneous and emulsification pot is added）, after addition
Matter 30min；Bay alcohol sulfuric ester aqueous ammonium is added in third step（Bay alcohol sulfuric ester ammonium is semisolid, and water, which is added, makes it just
Emulsification pot is added after dissolving homogeneous）, Cocoamidopropyl betaine (CAB-35)（Liquid）.
(5) coconut oleoyl amine DEA and coconut oleoyl amine MEA is added（Liquid）, climbazole is added（Directly added with sieve）, own amidine
Fixed two（Isethionate）And sodium hyaluronate（Solid-state is directly added into）.
(6) -47 15~20min of homogeneous of polyquaternium is then added,（Polyquaternium -47 is liquid, and pure water, which is added, has made it just
Emulsification pot is added after good dissolving homogeneous）, oligofructose aqueous solution（Oligofructose is solid-state, that is, appropriate pure water, which is added, makes it just
Emulsification pot is added after dissolving）, D-pantothenyl aleohol aqueous solution（D-pantothenyl aleohol is liquid, can be added after appropriate pure water makes it just dissolve and be added
Emulsify pot）, guar hydroxypropyltrimonium aqueous ammonium chloride solution（Guar hydroxypropyltrimonium ammonium chloride is solid-state, that is, is added
Emulsification pot is added in pure water after so that it is just dissolved homogeneous）, Polyquaternium-10 aqueous solution is then added（Polyquaternium-10 is solid
Emulsification pot is added in state, addition after so that it is just dissolved homogeneous, which is easy swelling, so can be as possible in the case of permission
Add pure water）.
(7) the good glycol distearate aqueous solution of homogeneous is eventually adding（Pearlescent flake, glycol distearate are
Solid-state, pure water, which is first added, to be made it just dissolve homogeneous pearlescent flake to crush its particle）Stirring homogeneous 30min in emulsification pot is added.
(8) after 80 DEG C of all raw materials add, about 2-3 parts of pure water can be added at this temperature, after stirring homogeneous 2h
It can start to cool down（Probably 3 DEG C of decline per hour in its natural state, it is related with ambient temperature）.
(9) aqueous citric acid solution is added at 40 DEG C（Citric acid solid-state needs a small amount of water that it is made just to dissolve）, Phenoxyethanol
（Liquid）, Kathon CG（Liquid）, essence（Liquid）, raw material is all added, and stirs homogeneous 2h after supplementing remaining moisture, obtains into
Product.
The contrast test of excellent result of the present invention
1, power consumption compares.
The present invention is combined using pulverizer and colloid mill and uses ultramicro grinding, freezes superfine communication technique by crushing material
To identical fineness（800 mesh）, power consumption comparing result is shown in Table 1.
1 power consumption of table compares list
Note：Comparative example 1, using superfine communication technique；Comparative example 2, using freezing superfine communication technique.
As shown in Table 1, the present invention is more saved using pulverizer and colloid mill combination than using ultramicro grinding, freezing ultramicro grinding
Can, more conducively practical application is promoted.
2, shampoo cardability, flexibility, the performance comparison of moisture retention.
Comparative example：The tea bran shampoo of certain commercially available brand.
The shampoo of embodiment 1-3 obtained by method by the embodiment of the present invention 4 and comparative example product carry out performance detection,
Specific detection method is as follows：Volunteer is used, every group of 10 people.According to GB11432 to its cardability, softness
Property, moisture retention are tested, and it is specific as follows that properties are set as 6 grades：6：It is fabulous；5：It is good；4：Preferably；3：Generally；2：Compared with
Difference；1：Difference.Specific testing result is shown in Table 2.
The performance test results list of 2 shampoo cardability of table, flexibility, moisture retention
As shown in Table 2, the cardability, flexibility of shampoo of the present invention and moistening effect are all relatively good.
3, the material stability contrast of colloid mill is not used using colloid mill and.
Experimental group is by material（Tea bran, gleditsia sinensis, tuber of multiflower knotweed etc.）Pulverizer is first passed through after colloid mill, control group be using with
The identical material of the present invention does not use colloid mill only, but uses other means that crushing material is extremely identical with experimental group
Fineness, raw material stability experiment Comparative result are shown in Table 3.
3 material stability contrast list of table
As shown in Table 3, after excessively complete colloid mill, the stability of system significantly improves, and is conducive to being stabilized for system.
4, the shampoo stability contrast prepared using homogenizer.
Experimental group is according to the shampoo of embodiment 1-3 obtained by preparation method of the present invention, with Publication No.
Tea bran shampoo prepared by the Chinese invention patent of CN106924116A is compared as a comparison case, shampoo stability contrast
Experimental result is shown in Table 4.
4 shampoo stability result of table detects list
Note：It is record room temperature respectively in table 4（25℃）Under the conditions of place 1 week after detection obtain as a result, heat-resisting（48℃）Condition
Lower placement detects obtaining as a result, cold-resistant after 2 weeks（- 5~-18 DEG C）Under the conditions of place 3 weeks after the result that detects.Test-strips
Part " heat-resisting-cold-resistant cycle, room temperature ", 1 month time referred to is placed 10 days under heat conditions, placed 10 days under the conditions of resisting cold, often
The result detected after being placed 10 days under the conditions of temperature；2 months time referred to being placed 20 days under heat conditions, under the conditions of resisting cold
It places 20 days, the result detected after being placed 20 days under normal temperature condition；3 months time referred to being placed 30 days under heat conditions,
It is placed 30 days under the conditions of cold-resistant, the result detected after being placed 30 days under normal temperature condition.
As shown in Table 4, the present invention using move homogenizer after, acquired product it is more stable.
5, the physical and chemical index that shampoo of the present invention is tested according to GB/T29679-2013, the results are shown in Table 5.
5 shampoo index of table（GB/T19679-2013）List
6, shampoo fungistatic effect compares.
According to《Cosmetics microorganism examination criteria method total number of bacteria measures》Method, detection press the embodiment of the present invention 4
Method obtained by embodiment 1-3 shampoo product total plate count, what is obtained the results are shown in Table 6.
6 shampoo bacterium colony count results list of table
Note：1, it is to be not added with oneself to narrow the total plate count of fixed two (isethionates) to implement serial number 0.2、CFU：Bacterium colony forms list
Position.
As shown in Table 6, resulting product reaches state-set standard in embodiment 1,2,3（Total plate count≤
1000CFU/g）, the present invention adds after oneself narrows fixed two (isethionates), fungistatic effect highly significant.
Claims (5)
1. a plant tea bran shampoo, it is characterised in that：The shampoo is mainly prepared by the raw material of following portions by weight：Each original
The total number of material be 100 parts, wherein tea bran 5-25 parts, 0-5 parts of gleditsia sinensis, 0-5 parts of the tuber of multiflower knotweed, 0.5-12 parts of thickener, foaming agent 3-
18 parts, 0.01-0.6 parts of antipruritic, 0.1-0.5 parts of nutritional ingredient, 0.01-0.05 parts of moisturizer, 0.01-1.1 parts of preservative, pearl
0.3-3 parts of photo etching, 0.1-0.8 parts of citric acid, 0.01-0.5 parts of edible oil, 0.01-0.3 parts of flavouring agent, 0.1-4 parts of conditioner,
Pure water surplus；
The antipruritic is hexamidine two (isethionate) and climbazole.
2. plant tea bran shampoo according to claim 1, it is characterised in that：The thickener is cocamidopropyl propyl amide sweet tea
Dish alkali (CAB-35), coconut oleoyl amine DEA, coconut oleoyl amine MEA and acrylic acid（Ester）Analog copolymer；
The foaming agent is laureth sodium sulfovinate and laruyl alcohol sulfuric acid ester ammonium；
The nutritional ingredient is oligofructose and D-pantothenyl aleohol；
The moisturizer is sodium hyaluronate；
The preservative is Phenoxyethanol and Kathon CG；
The pearling agent is two stearic acid sodium of ethylene glycol；
The edible oil is tea-seed oil；
The flavouring agent is essence；
The conditioner is polyquaternium and guar hydroxypropyltrimonium ammonium chloride.
3. plant tea bran shampoo according to claim 2, it is characterised in that：The shampoo is mainly by following portions by weight
Raw material be prepared：The total number of each raw material is 100 parts, wherein 10 parts of tea bran, 0.1 part of gleditsia sinensis, 0.1 part of the tuber of multiflower knotweed, cocounut oil acyl
Amine propyl betaine（CAB-35）7 parts, 1 part of 1 part of coconut oleoyl amine DEA, coconut oleoyl amine MEA, acrylic acid（Ester）Analog copolymer 3
Part, 9 parts of laureth sodium sulfovinate, 3 parts of bay alcohol sulfuric ester ammonium, hexamidine two（Isethionate）0.1 part, climbazole
0.5 part, 0.2 part of oligofructose, 0.1 part of D-pantothenyl aleohol, 0.01 part of sodium hyaluronate, 1 part of Phenoxyethanol, 0.1 part of Kathon CG, ethylene glycol two is firmly
0.8 part of resin acid ester, 0.4 part of citric acid, 0.1 part of tea-seed oil, 0.2 part of essence, 1.5 parts of polyquaternium -47, Polyquaternium-10
0.8 part, 1 part of guar hydroxypropyltrimonium ammonium chloride, pure water surplus.
4. a kind of preparation method of the tea bran shampoo as described in Claims 2 or 3, it is characterised in that：Include the following steps：
(1) with pulverizer by the tea bran or tea bran and gleditsia sinensis or tea bran and the tuber of multiflower knotweed or tea bran and gleditsia sinensis, tuber of multiflower knotweed raw material powder after drying
It is broken, it is ground into 100~200 mesh powders；
(2) colloid mill is crossed after the raw material damping after (1) step being crushed, makes it at relatively stable colloidal state；
(3) 12~18 parts of pure water are added in emulsifying pot, adds (2) substance and tea-seed oil that step is made, is heated to 95~105
DEG C, 0.8~1.2h, 11~13h of cooling and standings are boiled at 95~105 DEG C；
(4) 78~83 DEG C are warmed to again, and acrylic acid is added in the first step（Ester）Analog copolymer, 15~20min of homogeneous, second step add
Enter the laureth sodium sulfovinate aqueous solution that homogeneous is crossed, 10~30min of homogeneous after addition；Bay alcohol sulfuric ester is added in third step
Aqueous ammonium and Cocoamidopropyl betaine (CAB-35)；Temperature maintains 78~83 DEG C when charging；
(5) temperature maintains 78~83 DEG C and coconut oleoyl amine DEA, coconut oleoyl amine MEA, climbazole, hexamidine two is added into emulsification pot
（Isethionate）And sodium hyaluronate；
(6) temperature maintains 78~83 DEG C then to -47 aqueous solution of addition polyquaternium, oligofructose aqueous solution, D- in emulsification pot
Then it is water-soluble Polyquaternium-10 to be added into emulsification pot in panthenol aqueous solution and guar hydroxypropyltrimonium aqueous ammonium chloride solution
Liquid；
(7) temperature maintains 78~83 DEG C and the good glycol distearate aqueous solution of homogeneous is added into emulsification pot, and stirring is equal
25~35min of matter；
(8) temperature maintains 78~83 DEG C and adds 2-3 parts of pure water into emulsification pot, can start to drop after 1.5~2.5h of stirring homogeneous
Temperature；
(9) it is cooled to 38~43 DEG C and aqueous citric acid solution, Phenoxyethanol, Kathon CG and essence is added into emulsification pot, finally supplement is surplus
1.5~2.5h of homogeneous is stirred after remaining moisture, obtains finished product.
5. the preparation method of tea bran shampoo as claimed in claim 4, it is characterised in that：The laureth sodium sulfovinate water
Solution, -47 aqueous solution of polyquaternium, guar hydroxypropyltrimonium aqueous ammonium chloride solution, gathers bay alcohol sulfuric ester aqueous ammonium
The preparation process of -10 aqueous solution of quaternary ammonium salt and glycol distearate aqueous solution is：Into solute plus water keeps solute just molten
It homogenizes after solution；The preparation process of the oligofructose aqueous solution, D-pantothenyl aleohol aqueous solution and aqueous citric acid solution is：To solute
In plus water so that solute just dissolve after it is obtained.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111388364A (en) * | 2020-03-02 | 2020-07-10 | 深圳苏露中医诊所 | Antibacterial shampoo |
| CN111419763A (en) * | 2020-06-02 | 2020-07-17 | 广州德谷个人护理用品有限公司 | Tea bran anti-dandruff itching-relieving shampoo and preparation method thereof |
| CN112089671A (en) * | 2020-10-19 | 2020-12-18 | 湖南金昌生物技术有限公司 | Camellia shampoo powder integrating washing and protecting functions and preparation method thereof |
| CN113730318A (en) * | 2021-09-17 | 2021-12-03 | 贵州中医药大学 | Shampoo containing dendrobium officinale-saponin enzyme liquid and preparation method thereof |
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| CN101690697A (en) * | 2009-09-29 | 2010-04-07 | 广东名臣有限公司 | Anti-dandruff shampoo composition |
| CN106265379A (en) * | 2016-10-12 | 2017-01-04 | 广州丹奇日用化工厂有限公司 | A kind of multiple-effect is repaired without silicone oil shampoo |
| CN106924116A (en) * | 2017-04-10 | 2017-07-07 | 广西象州县丹生物技术有限公司 | One plant tea bran shampoo and preparation method thereof |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101690697A (en) * | 2009-09-29 | 2010-04-07 | 广东名臣有限公司 | Anti-dandruff shampoo composition |
| CN106265379A (en) * | 2016-10-12 | 2017-01-04 | 广州丹奇日用化工厂有限公司 | A kind of multiple-effect is repaired without silicone oil shampoo |
| CN106924116A (en) * | 2017-04-10 | 2017-07-07 | 广西象州县丹生物技术有限公司 | One plant tea bran shampoo and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111388364A (en) * | 2020-03-02 | 2020-07-10 | 深圳苏露中医诊所 | Antibacterial shampoo |
| CN111419763A (en) * | 2020-06-02 | 2020-07-17 | 广州德谷个人护理用品有限公司 | Tea bran anti-dandruff itching-relieving shampoo and preparation method thereof |
| CN112089671A (en) * | 2020-10-19 | 2020-12-18 | 湖南金昌生物技术有限公司 | Camellia shampoo powder integrating washing and protecting functions and preparation method thereof |
| CN113730318A (en) * | 2021-09-17 | 2021-12-03 | 贵州中医药大学 | Shampoo containing dendrobium officinale-saponin enzyme liquid and preparation method thereof |
| CN113730318B (en) * | 2021-09-17 | 2024-01-26 | 贵州中医药大学 | Shampoo containing dendrobium candidum-gleditsia sinensis enzyme liquid and preparation method thereof |
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