CN108640717A - Nixing pottery inlays the manufacture craft of silverware ware - Google Patents
Nixing pottery inlays the manufacture craft of silverware ware Download PDFInfo
- Publication number
- CN108640717A CN108640717A CN201810525279.3A CN201810525279A CN108640717A CN 108640717 A CN108640717 A CN 108640717A CN 201810525279 A CN201810525279 A CN 201810525279A CN 108640717 A CN108640717 A CN 108640717A
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- CN
- China
- Prior art keywords
- nixing pottery
- silver powder
- cooling
- manufacture craft
- fired
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
- C04B41/90—Coating or impregnation for obtaining at least two superposed coatings having different compositions at least one coating being a metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B11/00—Apparatus or processes for treating or working the shaped or preshaped articles
- B28B11/001—Applying decorations on shaped articles, e.g. by painting
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Structural Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Powder Metallurgy (AREA)
Abstract
The present invention provides the manufacture crafts that Nixing pottery inlays silverware ware, include the following steps:1) Nixing pottery billet surface is carved out into pattern, then dried;2) last layer silver powder is uniformly spread in the pattern area of dry base substrate, 1~2h is fired at 900~950 DEG C, it is cooling;3) one layer of Nixing pottery blank is uniformly smeared on silver powder, and 1~3h is fired at 980~1000 DEG C, it is cooling;4) fill up pattern area with silver powder, fire 6~8h at 1150~1200 DEG C, it is cooling to get.The wellability of Nixing pottery and metallic silver can be greatly improved in the present invention, and good connecting effect is not easily to fall off.
Description
Technical field
The present invention relates to the manufacture crafts of Nixing pottery, and in particular to Nixing pottery inlays the manufacture craft of silverware ware.
Background technology
The technique of Nixing pottery includes mainly following steps:1) blank is prepared:Blank, which is selected, crosses admiring for Qiezhou urban district
The soil of Jiang Yidong, being commonly called as eastern mud, (for mild-clay, color is yellow-white, contains micro quartz sand, in the production technology of Nixing pottery
In serve adjustment plasticity with associativity), and by the emperor himself to the west of river region soil, be commonly called as western mud (containing a small amount of K2O、NaO、
CaO、MgO、Fe203、TiO2、MnO2, it is a kind of higher purple mudstone of iron-holder, color is aubergine, and superficial layer has a small amount of irony
Dip dyeing is hard paste, and plasticity and associativity are poor), the weight percent by eastern mud 40~60%, western mud 40~60% is mixed
It closes, blank is made in the series of process such as ground, dehydration;The moisture content of blank is 20~25%;2) blank forming:Using plastic
The green body of various types is made in blank by method or slip casting method;3) green body is modified:Green body is modified to reach design requirement;4) it does
It is dry:Green body is dried using aeration drying, green body moisture is made to exclude;5) drawing engraving:It picture and is carried out in green body writing of submitting a written statement to a higher authority
Engraving;6):Body drying;7) green body is fired:Dry green body loading of kiln to be fired, firing temperature is controlled at 1100~1200 DEG C,
Firing time is 10h, kiln discharge after cooling;8) polishing grinding:By green body polishing polish to get.Silver is inlayed on Nixing pottery green body,
Since silver is poor with the wellability of Nixing pottery, extremely it is easy to fall off.
Invention content
Technical problem to be solved by the invention is to provide the manufacture craft that Nixing pottery inlays silverware ware, which can greatly carry
The wellability of high Nixing pottery and silver powder, good connecting effect are not easily to fall off.
In order to solve the above technical problems, the technical solution adopted by the present invention is the manufacture craft of Nixing pottery edge silverware ware, packet
Include following steps:
1) Nixing pottery billet surface is carved out into pattern, then dried;
2) last layer silver powder is uniformly spread in the pattern area of dry base substrate, 1~2h is fired at 900~950 DEG C, it is cooling;
3) one layer of Nixing pottery blank is uniformly smeared on silver powder, and 1~3h is fired at 980~1000 DEG C, it is cooling;
4) fill up pattern area with silver powder, fire 6~8h at 1150~1200 DEG C, it is cooling to get.
In step 2), silver-colored melting temperature is 960 DEG C, melting temperature of the control firing temperature less than silver, it is ensured that few
The silver powder of amount will not form liquid phase, avoid silver powder diffusional resistance too small, lead to metal grain fast growth, it is ensured that silver powder crystal grain
Tinyization, and Nixing pottery green body is combined closely.The thickness of silver powder is 0.1~0.15mm.
In step 3), firing temperature is 980~1000 DEG C, is higher than the melting temperature of silver powder, but less than the burning of Nixing pottery
At temperature, the Al in Nixing pottery blank2O3、Fe2O3The spontaneous solid solution for being diffused into silver powder phase and carrying out certain depth with silver powder, simultaneously
Al2O3、Fe2O3It reacts with Ag and generates AgO and combined with silver powder surface, to realize the tight of Nixing pottery and silver powder two-phase interface
Close combination.The moisture content of Nixing pottery blank is 20~25%.The thickness of Nixing pottery blank is 0.1~0.15mm.
In step 4), since Nixing pottery green body outer layer has been sequentially filled silver powder layer, Nixing pottery blank material layer and silver powder layer, occupy
Silver powder particles growth can be limited in sintering procedure in intermediate Nixing pottery blank material layer so that silver powder crystal grain is tiny, more easily
Indenting shape is formed with Nixing pottery layer, to improve the bond strength of silver powder and Nixing pottery.
In step 4), the flyash of its weight 0.1~0.5% is mixed in silver powder.The addition of flyash is in cooled and solidified
In the process, silver powder crystal grain refinement, dendritic growth can be made to get muddled, preferably form dog with flyash and Nixing pottery
The staggered solid solution of tooth increases the bond strength of silver powder and Nixing pottery.The addition of flyash can also alleviate silver powder and be expanded with Nixing pottery
The difference of coefficient prevents falling off for silverware.
Compared with prior art, the wellability of Nixing pottery and metallic silver can be greatly improved in the present invention, and good connecting effect is not easy
It falls off.
Specific implementation mode
The essentiality content further illustrated the present invention below with embodiment, but the present invention is not limited with this.
Embodiment 1
1) 100 Nixing pottery green bodies are taken, its surface engraving is gone out into identical patterns, is then dried;
2) silver powder that a layer thickness is 0.1mm is uniformly sprinkled in the pattern area of dry base substrate, 1h is fired at 900 DEG C, it is cold
But;
3) the Nixing pottery blank that a layer thickness is 0.1mm is uniformly smeared on silver powder, and 1h is fired at 980 DEG C, it is cooling;Mud
The moisture content of emerging greenwave material is 20%;
4) fill up pattern area with silver powder, fire 6h at 1150 DEG C, it is cooling to get.
Through statistics, fall off 5, intact 95.
Embodiment 2
1) the Nixing pottery green body for taking 100 shape sizes same as Example 1 goes out its surface engraving and 1 phase of embodiment
Same pattern, is then dried;
2) silver powder that a layer thickness is 0.15mm is uniformly sprinkled in the pattern area of dry base substrate, 2h is fired at 950 DEG C, it is cold
But;
3) the Nixing pottery blank that a layer thickness is 0.15mm is uniformly smeared on silver powder, and 3h is fired at 1000 DEG C, it is cooling;
The moisture content of Nixing pottery blank is 25%;
4) flyash of its weight 0.5% is mixed in silver powder, mixing fills up pattern area, 8h is fired at 1200 DEG C, cold
But to get.
Through statistics, fall off 1, intact 99.
Embodiment 3
1) the Nixing pottery green body for taking 100 shape sizes same as Example 1 goes out its surface engraving and 1 phase of embodiment
Same pattern, is then dried;
2) silver powder that a layer thickness is 0.1mm is uniformly sprinkled in the pattern area of dry base substrate, 1.5h is fired at 920 DEG C,
It is cooling;
3) the Nixing pottery blank that a layer thickness is 0.1mm is uniformly smeared on silver powder, and 2h is fired at 990 DEG C, it is cooling;Mud
The moisture content of emerging greenwave material is 24%;
4) flyash of its weight 0.1% is mixed in silver powder, mixing fills up pattern area, 7h is fired at 1180 DEG C, cold
But to get.
Through statistics, fall off 1, intact 99.
Embodiment 4
1) the Nixing pottery green body for taking 100 shape sizes same as Example 1 goes out its surface engraving and 1 phase of embodiment
Same pattern, is then dried;
2) silver powder that a layer thickness is 0.1mm is uniformly sprinkled in the pattern area of dry base substrate, 1h is fired at 950 DEG C, it is cold
But;
3) the Nixing pottery blank that a layer thickness is 0.15mm is uniformly smeared on silver powder, and 3h is fired at 980 DEG C, it is cooling;
The moisture content of Nixing pottery blank is 20%;
4) flyash of its weight 0.5% is mixed in silver powder, mixing fills up pattern area, 8h is fired at 1150 DEG C, cold
But to get.
Through statistics, fall off 0, intact 100.
Claims (5)
1. Nixing pottery inlays the manufacture craft of silverware ware, it is characterised in that:Include the following steps:
1) Nixing pottery billet surface is carved out into pattern, then dried;
2) last layer silver powder is uniformly spread in the pattern area of dry base substrate, 1~2h is fired at 900~950 DEG C, it is cooling;
3) one layer of Nixing pottery blank is uniformly smeared on silver powder, and 1~3h is fired at 980~1000 DEG C, it is cooling;
4) fill up pattern area with silver powder, fire 6~8h at 1150~1200 DEG C, it is cooling to get.
2. the manufacture craft of Nixing pottery edge silverware ware according to claim 1, it is characterised in that:In step 3), Nixing pottery
The moisture content of blank is 20~25%.
3. the manufacture craft of Nixing pottery edge silverware ware according to claim 1, it is characterised in that:In step 2), silver powder
Thickness is 0.1~0.15mm.
4. the manufacture craft of Nixing pottery edge silverware ware according to claim 1, it is characterised in that:In step 3), Nixing pottery
The thickness of blank is 0.1~0.15mm.
5. the manufacture craft of Nixing pottery edge silverware ware according to claim 1, it is characterised in that:In step 4), in silver powder
The middle flyash for mixing its weight 0.1~0.5%.
Priority Applications (1)
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CN201810525279.3A CN108640717A (en) | 2018-05-28 | 2018-05-28 | Nixing pottery inlays the manufacture craft of silverware ware |
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CN201810525279.3A CN108640717A (en) | 2018-05-28 | 2018-05-28 | Nixing pottery inlays the manufacture craft of silverware ware |
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CN108640717A true CN108640717A (en) | 2018-10-12 |
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CN201810525279.3A Pending CN108640717A (en) | 2018-05-28 | 2018-05-28 | Nixing pottery inlays the manufacture craft of silverware ware |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2001309808A (en) * | 2000-04-28 | 2001-11-06 | Aida Kagaku Kogyo Kk | Decorating method of silver sintered body |
CN1338392A (en) * | 2000-08-16 | 2002-03-06 | 薛发伟 | Simple method for wrapping pottery artwork with copper layer |
CN1429714A (en) * | 2001-12-30 | 2003-07-16 | 毛志毅 | Metal pattern decorative ceramic product and its mannfacturing method |
CN104446592A (en) * | 2014-12-04 | 2015-03-25 | 河北工业大学 | Large-area connection method of ceramic and ceramic or ceramic and metal |
CN106431353A (en) * | 2016-09-23 | 2017-02-22 | 钦州学院 | Process for decorating nixing pottery with metal |
-
2018
- 2018-05-28 CN CN201810525279.3A patent/CN108640717A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2001309808A (en) * | 2000-04-28 | 2001-11-06 | Aida Kagaku Kogyo Kk | Decorating method of silver sintered body |
CN1338392A (en) * | 2000-08-16 | 2002-03-06 | 薛发伟 | Simple method for wrapping pottery artwork with copper layer |
CN1429714A (en) * | 2001-12-30 | 2003-07-16 | 毛志毅 | Metal pattern decorative ceramic product and its mannfacturing method |
CN104446592A (en) * | 2014-12-04 | 2015-03-25 | 河北工业大学 | Large-area connection method of ceramic and ceramic or ceramic and metal |
CN106431353A (en) * | 2016-09-23 | 2017-02-22 | 钦州学院 | Process for decorating nixing pottery with metal |
Non-Patent Citations (1)
Title |
---|
肖杰等: "陶瓷与金属的连接方法", 《硅酸盐通报》 * |
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Application publication date: 20181012 |