CN108640456A - A kind of black smelly modifying agent of aquaculture substrate - Google Patents

A kind of black smelly modifying agent of aquaculture substrate Download PDF

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Publication number
CN108640456A
CN108640456A CN201810593207.2A CN201810593207A CN108640456A CN 108640456 A CN108640456 A CN 108640456A CN 201810593207 A CN201810593207 A CN 201810593207A CN 108640456 A CN108640456 A CN 108640456A
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China
Prior art keywords
sodium
black smelly
modifying agent
aquaculture
mentioned
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CN201810593207.2A
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Inventor
刘军
梁金培
王小花
丁河峰
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Rizhao Ao Sheng Biological Technology Co Ltd
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Rizhao Ao Sheng Biological Technology Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/02Biological treatment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/20Nature of the water, waste water, sewage or sludge to be treated from animal husbandry
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00Specific treatment goals
    • C02F2303/02Odour removal or prevention of malodour

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Fodder In General (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of black smelly modifying agents of aquaculture substrate, including below according to the raw material of weight percent:Including below according to the raw material of weight percent:Sodium chlorite 8% 10%, anhydrous magnesium sulfate 5% 7%, anhydrous sodium sulphate 40% 45%, lime stone 10% 12%, sodium humate 8% 9%, kaolin 5% 7%, modified zeolite 6% 7%, microorganism formulation 3% 18%.The present invention is using anhydrous sodium sulphate as carrier, it is mixed with sodium chlorite and anhydrous magnesium sulfate, the black smelly phenomenon on aquaculture ground can be effectively improved, microorganism formulation is added in modifying agent simultaneously, further to aquaculture improve, the using effect for improving aquaculture ground, has a vast market foreground.

Description

A kind of black smelly modifying agent of aquaculture substrate
Technical field
The present invention relates to modifying agent technical field, specifically a kind of black smelly modifying agent of aquaculture substrate.
Background technology
Aquaculture is the production activity of the lower breeding of artificial control, cultivation and harvest aquatic animals and plants.It is commonly included in people The overall process of aquatic products is formed under work feeding management from seed.It broadly may also comprise Enhancement of fishery resources.Aquaculture has slightly The modes such as foster, intensive culture and high density culture.Extensive cultivation is that seed is launched in medium and small natural water area, is supported completely by natural bait It breeds fish at aquatic products, such as lake and reservoir and supports shellfish with shallow sea.Intensive culture is to form aquatic products with bait throwing in, fertilizing method in compared with small size pond Product, such as aqiuculrue, fish culture in net pen and enclosure culture, net enclosure culture.High density culture is using flowing water, temperature control, oxygenation and feeds high-quality bait The methods of, high-density breeding is carried out in small size pond, to obtain high yield, such as Running Water Intensive Fish Farming, shrimp.
Invention content
The purpose of the present invention is to provide a kind of black smelly modifying agents of aquaculture substrate, to solve to carry in above-mentioned background technology The problem of going out.
To achieve the above object, the present invention provides the following technical solutions:
A kind of black smelly modifying agent of aquaculture substrate, including below according to the raw material of weight percent:Sodium chlorite 8%-10%, nothing Water magnesium sulfate 5%-7%, anhydrous sodium sulphate 40%-45%, lime stone 10%-12%, sodium humate 8%-9%, kaolin 5%-7%, modified zeolite 6%-7%, microorganism formulation 3%-18%.
As a further solution of the present invention:Including below according to the raw material of weight percent:Sodium chlorite 8%-9%, nothing Water magnesium sulfate 5%-6%, anhydrous sodium sulphate 40%-43%, lime stone 10%-11%, sodium humate 8%-9%, kaolin 5%-6%, modified zeolite 6%-7%, microorganism formulation 9%-18%.
As further scheme of the invention:Including below according to the raw material of weight percent:It is sodium chlorite 9%, anhydrous Magnesium sulfate 6%, anhydrous sodium sulphate 42%, lime stone 11%, sodium humate 8%, kaolin 6%, modified zeolite 6%, microorganism formulation 12%.
As further scheme of the invention:The microorganism formulation is bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria Mixed bacteria.
As further scheme of the invention:The weight percent score of the bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria It is not:25%, 45% and 30%.
The preparation method of the black smelly modifying agent of aquaculture substrate, steps are as follows:
1)Each raw material is weighed by weight percentage;
2)Lime stone, sodium humate and kaolin are poured into blender and are stirred 5 minutes, then direct packaging or uses roller The granulate mixture A of 3-5mm is made in compacting grain machine;
3)To sodium chlorite, anhydrous magnesium sulfate, anhydrous sodium sulphate carry out first time crushing, to be chosen at it is above-mentioned through first time crush Particle of the diameter within the scope of 25~30mm in particulate matter, and drying for the first time is carried out to the particle of above-mentioned selection, it later, will be upper It states and is cooled down with the temperature within the scope of 10~15 DEG C in cooling tower through first time dry particle, next, using 60~ Gas within the scope of 80 DEG C carries out second of drying to remove the moisture of above-mentioned inside particles, and powder to above-mentioned through cooling particle The broken above-mentioned granulate mixture B that 2-4mm is made through second of dry particle;
4)It takes natural zeolite to be placed in sodium hydroxide solution, then in 75-82 DEG C of heating water bath 2.0-2.5 hours, repeatedly stirs After extract filtrate, be washed to neutrality with distillation, in 30-35 DEG C, 200-250r/min constant temperature oscillations 60-80 minutes, discard supernatant Liquid and with distilled water flushing 3-5 times, obtains solid powder C in dry 1.5-2 hour at 100-105 DEG C;
5)Microorganism formulation is added after above-mentioned granulate mixture A, granulate mixture B and solid powder C are mixed evenly, i.e., Obtain the black smelly modifying agent of aquaculture substrate.
As further scheme of the invention:Step 4)In, the concentration of sodium hydroxide solution is 0.8-1.0mol/L.
Compared with prior art, the beneficial effects of the invention are as follows:The present invention using anhydrous sodium sulphate as carrier, be mixed with sodium chlorite and Anhydrous magnesium sulfate, can effectively improve the black smelly phenomenon on aquaculture ground, while microorganism formulation being added in modifying agent, into One step to aquaculture improves, and improves the using effect on aquaculture ground, has a vast market foreground.
Specific implementation mode
Technical scheme of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of black smelly modifying agent of aquaculture substrate, including below according to the raw material of weight percent:Sodium chlorite 8%, anhydrous sulphur Sour magnesium 5%, anhydrous sodium sulphate 40%, lime stone 10%, sodium humate 8%, kaolin 5%, modified zeolite 6%, microorganism formulation 18%.
The microorganism formulation be bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria mixed bacteria.
The bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria weight percent be respectively:25%, 45% and 30%.
The preparation method of the black smelly modifying agent of aquaculture substrate, steps are as follows:
1)Each raw material is weighed by weight percentage;
2)Lime stone, sodium humate and kaolin are poured into blender and are stirred 5 minutes, then direct packaging or uses roller The granulate mixture A of 3mm is made in compacting grain machine;
3)To sodium chlorite, anhydrous magnesium sulfate, anhydrous sodium sulphate carry out first time crushing, to be chosen at it is above-mentioned through first time crush Particle of the diameter within the scope of 25mm in particulate matter, and drying for the first time is carried out to the particle of above-mentioned selection, later, by above-mentioned warp Dry particle is cooled down in cooling tower with the temperature within the scope of 10 DEG C for the first time, next, utilizing 60~80 DEG C of ranges Interior gas carries out second of drying to remove the moisture of above-mentioned inside particles to above-mentioned through cooling particle, and crushes above-mentioned warp The granulate mixture B of 2mm is made in second of dry particle;
4)It takes natural zeolite to be placed in sodium hydroxide solution, then in 75 DEG C of heating water baths 2.0 hours, repeatedly extracts filter after stirring Liquid is washed to neutrality with distillation, in 30 DEG C, 200r/min constant temperature oscillations 60 minutes, discards supernatant liquid and with distilled water flushing 3 It is secondary, obtain solid powder C within dry 1.5 hours at 100 DEG C;
5)Microorganism formulation is added after above-mentioned granulate mixture A, granulate mixture B and solid powder C are mixed evenly, i.e., Obtain the black smelly modifying agent of aquaculture substrate.
Step 4)In, the concentration of sodium hydroxide solution is 0.8mol/L.
Embodiment 2
A kind of black smelly modifying agent of aquaculture substrate, including below according to the raw material of weight percent:Sodium chlorite 9%, anhydrous sulphur Sour magnesium 6%, anhydrous sodium sulphate 41%, lime stone 11%, sodium humate 8%, kaolin 6%, modified zeolite 7%, microorganism formulation 12%.
The microorganism formulation be bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria mixed bacteria.
The bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria weight percent be respectively:25%, 45% and 30%.
The preparation method of the black smelly modifying agent of aquaculture substrate, steps are as follows:
1)Each raw material is weighed by weight percentage;
2)Lime stone, sodium humate and kaolin are poured into blender and are stirred 5 minutes, then direct packaging or uses roller The granulate mixture A of 4mm is made in compacting grain machine;
3)To sodium chlorite, anhydrous magnesium sulfate, anhydrous sodium sulphate carry out first time crushing, to be chosen at it is above-mentioned through first time crush Particle of the diameter within the scope of 27mm in particulate matter, and drying for the first time is carried out to the particle of above-mentioned selection, later, by above-mentioned warp Dry particle is cooled down in cooling tower with the temperature within the scope of 12 DEG C for the first time, next, using within the scope of 70 DEG C Gas carries out second of drying to remove the moisture of above-mentioned inside particles to above-mentioned through cooling particle, and crushes above-mentioned through second The granulate mixture B of 2-4mm is made in the particle of secondary drying;
4)It takes natural zeolite to be placed in sodium hydroxide solution, then in 76 DEG C of heating water baths 2.0-2.5 hours, is repeatedly taken out after stirring Filtrate is taken, neutrality is washed to distillation, in 33 DEG C, 220r/min constant temperature oscillations 65 minutes, liquid is discarded supernatant and is rushed with distilled water It washes 4 times, obtains solid powder C within dry 1.6 hours at 102 DEG C;
5)Microorganism formulation is added after above-mentioned granulate mixture A, granulate mixture B and solid powder C are mixed evenly, i.e., Obtain the black smelly modifying agent of aquaculture substrate.
Step 4)In, the concentration of sodium hydroxide solution is 0.9mol/L.
Embodiment 3
A kind of black smelly modifying agent of aquaculture substrate, including below according to the raw material of weight percent:Sodium chlorite 9%, anhydrous sulphur Sour magnesium 6%, anhydrous sodium sulphate 42%, lime stone 11%, sodium humate 8%, kaolin 6%, modified zeolite 6%, microorganism formulation 12%.
The microorganism formulation be bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria mixed bacteria.
The bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria weight percent be respectively:25%, 45% and 30%.
The preparation method of the black smelly modifying agent of aquaculture substrate, steps are as follows:
1)Each raw material is weighed by weight percentage;
2)Lime stone, sodium humate and kaolin are poured into blender and are stirred 5 minutes, then direct packaging or uses roller Suppress the granulate mixture A of grain mechanism 4mm;
3)To sodium chlorite, anhydrous magnesium sulfate, anhydrous sodium sulphate carry out first time crushing, to be chosen at it is above-mentioned through first time crush Particle of the diameter within the scope of 28mm in particulate matter, and drying for the first time is carried out to the particle of above-mentioned selection, later, by above-mentioned warp Dry particle is cooled down in cooling tower with the temperature within the scope of 14 DEG C for the first time, next, using within the scope of 70 DEG C Gas carries out second of drying to remove the moisture of above-mentioned inside particles to above-mentioned through cooling particle, and crushes above-mentioned through second The granulate mixture B of 3mm is made in the particle of secondary drying;
4)It takes natural zeolite to be placed in sodium hydroxide solution, then in 78 DEG C of heating water baths 2.5 hours, repeatedly extracts filter after stirring Liquid is washed to neutrality with distillation, in 34 DEG C, 240r/min constant temperature oscillations 75 minutes, discards supernatant liquid and with distilled water flushing 4 It is secondary, obtain solid powder C within dry 2 hours at 102 DEG C;
5)Microorganism formulation is added after above-mentioned granulate mixture A, granulate mixture B and solid powder C are mixed evenly, i.e., Obtain the black smelly modifying agent of aquaculture substrate.
Step 4)In, the concentration of sodium hydroxide solution is 1.0mol/L.
Embodiment 4
A kind of black smelly modifying agent of aquaculture substrate, including below according to the raw material of weight percent:It is sodium chlorite 10%, anhydrous Magnesium sulfate 7%, anhydrous sodium sulphate 45%, lime stone 12%, sodium humate 9%, kaolin 7%, modified zeolite 7%, microorganism formulation 3%.
The microorganism formulation be bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria mixed bacteria.
The bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria weight percent be respectively:25%, 45% and 30%.
The preparation method of the black smelly modifying agent of aquaculture substrate, steps are as follows:
1)Each raw material is weighed by weight percentage;
2)Lime stone, sodium humate and kaolin are poured into blender and are stirred 5 minutes, then direct packaging or uses roller The granulate mixture A of 5mm is made in compacting grain machine;
3)To sodium chlorite, anhydrous magnesium sulfate, anhydrous sodium sulphate carry out first time crushing, to be chosen at it is above-mentioned through first time crush Particle of the diameter within the scope of 30mm in particulate matter, and drying for the first time is carried out to the particle of above-mentioned selection, later, by above-mentioned warp Dry particle is cooled down in cooling tower with the temperature within the scope of 15 DEG C for the first time, next, using within the scope of 80 DEG C Gas carries out second of drying to remove the moisture of above-mentioned inside particles to above-mentioned through cooling particle, and crushes above-mentioned through second The granulate mixture B of 4mm is made in the particle of secondary drying;
4)It takes natural zeolite to be placed in sodium hydroxide solution, then in 82 DEG C of heating water baths 2.5 hours, repeatedly extracts filter after stirring Liquid is washed to neutrality with distillation, in 35 DEG C, 250r/min constant temperature oscillations 80 minutes, discards supernatant liquid and with distilled water flushing 5 It is secondary, obtain solid powder C within dry 2 hours at 105 DEG C;
5)Microorganism formulation is added after above-mentioned granulate mixture A, granulate mixture B and solid powder C are mixed evenly, i.e., Obtain the black smelly modifying agent of aquaculture substrate.
Step 4)In, the concentration of sodium hydroxide solution is 1.0mol/L.
The present invention is mixed with sodium chlorite and anhydrous magnesium sulfate using anhydrous sodium sulphate as carrier, can effectively improve aquaculture The black smelly phenomenon on ground, while microorganism formulation being added in modifying agent, further to aquaculture improve, improves aquatic products The using effect for cultivating ground, has a vast market foreground.
The better embodiment of the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party Formula, one skilled in the relevant art within the scope of knowledge, can also be without departing from the purpose of the present invention Various changes can be made.

Claims (7)

1. a kind of black smelly modifying agent of aquaculture substrate, which is characterized in that including below according to the raw material of weight percent:Sub- chlorine Sour sodium 8%-10%, anhydrous magnesium sulfate 5%-7%, anhydrous sodium sulphate 40%-45%, lime stone 10%-12%, sodium humate 8%-9%, kaolin 5%-7%, modified zeolite 6%-7%, microorganism formulation 3%-18%.
2. the black smelly modifying agent of aquaculture substrate according to claim 1, which is characterized in that including below according to weight hundred Divide the raw material of ratio:Sodium chlorite 8%-9%, anhydrous magnesium sulfate 5%-6%, anhydrous sodium sulphate 40%-43%, lime stone 10%-11%, humic acid Sodium 8%-9%, kaolin 5%-6%, modified zeolite 6%-7%, microorganism formulation 9%-18%.
3. the black smelly modifying agent of aquaculture substrate according to claim 1, which is characterized in that including below according to weight hundred Divide the raw material of ratio:Sodium chlorite 9%, anhydrous magnesium sulfate 6%, anhydrous sodium sulphate 42%, lime stone 11%, sodium humate 8%, kaolin 6%, Modified zeolite 6%, microorganism formulation 12%.
4. according to any black smelly modifying agents of aquaculture substrate of claim 1-3, which is characterized in that the microorganism Preparation be bacillus subtilis, nitrogen-fixing bacteria, acetic acid bacteria mixed bacteria.
5. the black smelly modifying agent of aquaculture substrate according to claim 4, which is characterized in that the bacillus subtilis, Nitrogen-fixing bacteria, acetic acid bacteria weight percent be respectively:25%, 45% and 30%.
6. a kind of preparation method of the black smelly modifying agent of aquaculture substrate as described in any one of claims 1-3, which is characterized in that Steps are as follows:
1)Each raw material is weighed by weight percentage;
2)Lime stone, sodium humate and kaolin are poured into blender and are stirred 5 minutes, then direct packaging or uses roller The granulate mixture A of 3-5mm is made in compacting grain machine;
3)To sodium chlorite, anhydrous magnesium sulfate, anhydrous sodium sulphate carry out first time crushing, to be chosen at it is above-mentioned through first time crush Particle of the diameter within the scope of 25~30mm in particulate matter, and drying for the first time is carried out to the particle of above-mentioned selection, it later, will be upper It states and is cooled down with the temperature within the scope of 10~15 DEG C in cooling tower through first time dry particle, next, using 60~ Gas within the scope of 80 DEG C carries out second of drying to remove the moisture of above-mentioned inside particles, and powder to above-mentioned through cooling particle The broken above-mentioned granulate mixture B that 2-4mm is made through second of dry particle;
4)It takes natural zeolite to be placed in sodium hydroxide solution, then in 75-82 DEG C of heating water bath 2.0-2.5 hours, repeatedly stirs After extract filtrate, be washed to neutrality with distillation, in 30-35 DEG C, 200-250r/min constant temperature oscillations 60-80 minutes, discard supernatant Liquid and with distilled water flushing 3-5 times, obtains solid powder C in dry 1.5-2 hour at 100-105 DEG C;
5)Microorganism formulation is added after above-mentioned granulate mixture A, granulate mixture B and solid powder C are mixed evenly, i.e., Obtain the black smelly modifying agent of aquaculture substrate.
7. the black smelly modifying agent of aquaculture substrate according to claim 6, which is characterized in that step 4)In, the hydrogen-oxygen Change a concentration of 0.8-1.0mol/L of sodium solution.
CN201810593207.2A 2018-06-11 2018-06-11 A kind of black smelly modifying agent of aquaculture substrate Pending CN108640456A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111434623A (en) * 2019-01-12 2020-07-21 广州金水动物保健品有限公司 Tablet for improving culture environment of culture pond and preparation method and application thereof

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Application publication date: 20181012