CN108635901A - Spray cooling type crystallization kettle - Google Patents
Spray cooling type crystallization kettle Download PDFInfo
- Publication number
- CN108635901A CN108635901A CN201810529552.XA CN201810529552A CN108635901A CN 108635901 A CN108635901 A CN 108635901A CN 201810529552 A CN201810529552 A CN 201810529552A CN 108635901 A CN108635901 A CN 108635901A
- Authority
- CN
- China
- Prior art keywords
- autoclave body
- cooling
- outside sandwich
- spray
- spray tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D2009/0086—Processes or apparatus therefor
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- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
Abstract
The invention discloses a kind of spray cooling type crystallization kettles, it has autoclave body, outside sandwich, blender, spray tube, flow control valve, temperature of charge sensor, cooling-water temperature sensor and controller, feed inlet is arranged at the top of the autoclave body, there are blender and temperature of charge sensor in autoclave body, blender is connected with rotating mechanism, discharge port is arranged at autoclave body lower part, the outside sandwich is outside autoclave body, there is a spray tube around autoclave body at the top of outside sandwich, there are spray apertures on spray tube, spray tube is communicated with the cooling water inlet of outside sandwich, there is flow control valve in cooling water inlet pipeline, there is cooling-water temperature sensor in outside sandwich, cooling water outlet is arranged at the bottom of outside sandwich.Compared with the prior art, the advantages of the present invention are as follows simple in structure, production efficiency height, easy to operate, using water wisely.
Description
Technical field
The present invention relates to a kind of chemical production equipment, especially a kind of spray cooling type crystallization kettle.
Background technology
The cooling of current crystallization kettle is all ceaselessly to flow through the outside sandwich of autoclave body using cooling water, in this way it is easy to produce
Raw crystal wall built-up phenomenon greatly reduces the yield of crystallization kettle, and cooling water consumption is also very big, increases energy consumption and life
Produce cost.
Invention content
For overcome the deficiencies in the prior art, the present invention provides a kind of sprays simple in structure, yield is high, water consumption is small
Cooled crystallization kettle.
The present invention adopts the following technical scheme that.
A kind of spray cooling type crystallization kettle, there is autoclave body, outside sandwich, blender, spray tube, flow control valve, temperature of charge
Feed inlet is arranged at the top of sensor, cooling-water temperature sensor and controller, the autoclave body, there is blender and material temperature in autoclave body
Sensor is spent, blender is connected with rotating mechanism, and discharge port is arranged at autoclave body lower part, and the outside sandwich is outside autoclave body, outside sandwich
Top have a spray tube around autoclave body, there are spray apertures, spray tube to be communicated with the cooling water inlet of outside sandwich on spray tube,
There is flow control valve in cooling water inlet pipeline, there is cooling-water temperature sensor, the bottom of outside sandwich to have cooling water in outside sandwich
Outlet.
The flow control valve is hand flow regulating valve or electric flow control valve.
Compared with the prior art, the advantages of the present invention are as follows simple in structure, production efficiency height, easy to operate, using water wisely.
Description of the drawings
Fig. 1 is the structural schematic diagram of the embodiment of the present invention.
Specific implementation mode
Below in conjunction with drawings and examples, present invention is further described in detail.
Embodiment 1, as shown in Fig. 1, a kind of spray cooling type crystallization kettle has autoclave body 4, outside sandwich 8, blender 9, spray
Pipe 2, flow control valve 10, temperature of charge sensor 12, cooling-water temperature sensor 7 and controller, the top of the autoclave body 4
There is feed inlet 13, there is blender 9 and temperature of charge sensor 12, the output shaft of blender 9 and the retarder 1 of translator in autoclave body
It is connected, autoclave body lower part has discharge port 5, the outside sandwich 8 to be mounted in the outside of autoclave body 4, and the top of outside sandwich 8 has one to surround autoclave body
Spray tube 2, there are spray apertures 3, spray tube 2 to be communicated with the cooling water inlet 11 of outside sandwich 8 on spray tube 2, cooling water inlet pipe
There is hand flow regulating valve 10 in road, there is cooling-water temperature sensor 7, the bottom of outside sandwich to have cooling water outlet 6 in outside sandwich.
Operator is shown by observation temperature of charge and cooling water temperature is shown, controls hand flow regulating valve 10, makes two
Person's temperature difference is not more than 10 DEG C.The wall built-up phenomenon for both having prevented crystal in this way, substantially increases the yield of crystallization kettle, and reduces cold
But the dosage of water.
Hand flow regulating valve is replaced with electric flow control valve, temperature of charge is passed by embodiment 2 in embodiment 1
The signal wire of sensor and cooling-water temperature sensor is connected with the input terminal of the PLC of controller, the control of electric flow control valve
Line processed is connected with the output end of the PLC of controller.
Claims (2)
1. a kind of spray cooling type crystallization kettle, it is characterised in that have autoclave body, outside sandwich, blender, spray tube, flow control valve,
Feed inlet is arranged at the top of temperature of charge sensor, cooling-water temperature sensor and controller, the autoclave body, has blender in autoclave body
With temperature of charge sensor, blender is connected with rotating mechanism, and discharge port is arranged at autoclave body lower part, and the outside sandwich is outside autoclave body
There is a spray tube around autoclave body in portion at the top of outside sandwich, there is spray apertures, the cooling water of spray tube and outside sandwich on spray tube
Import communicates, and has flow control valve in cooling water inlet pipeline, there is cooling-water temperature sensor, the bottom of outside sandwich in outside sandwich
There is cooling water outlet.
2. spray cooling type crystallization kettle according to claim 1, it is characterised in that the flow control valve is manual flow
Regulating valve or electric flow control valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810529552.XA CN108635901A (en) | 2018-05-29 | 2018-05-29 | Spray cooling type crystallization kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810529552.XA CN108635901A (en) | 2018-05-29 | 2018-05-29 | Spray cooling type crystallization kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108635901A true CN108635901A (en) | 2018-10-12 |
Family
ID=63758429
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810529552.XA Pending CN108635901A (en) | 2018-05-29 | 2018-05-29 | Spray cooling type crystallization kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108635901A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112205565A (en) * | 2020-11-09 | 2021-01-12 | 湖南金健乳业股份有限公司 | Oat preprocessing device |
Citations (15)
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|---|---|---|---|---|
| CN2124093U (en) * | 1992-05-25 | 1992-12-09 | 冶金工业部北京冶金设备研究所 | Spray cooling tube type continuous casting crystallizer |
| JPH07314096A (en) * | 1994-05-27 | 1995-12-05 | Nippon Steel Corp | Spray cooling type mold in continuous caster |
| CN2235336Y (en) * | 1995-10-30 | 1996-09-18 | 冶金工业部北京冶金设备研究院 | Mixing cooling tubular continuous casting mould |
| JPH10244102A (en) * | 1997-03-07 | 1998-09-14 | Konica Corp | Crystallizer and method thereof |
| JPH10263307A (en) * | 1997-03-28 | 1998-10-06 | Konica Corp | Crystallizer |
| CN203954727U (en) * | 2014-07-07 | 2014-11-26 | 山东祥瑞药业有限公司 | A kind of glucose equipment of crystallisation by cooling |
| CN203990582U (en) * | 2014-01-02 | 2014-12-10 | 北京宝沃石油技术有限责任公司 | A kind of controllable temperature heating reactor |
| CN104815451A (en) * | 2015-04-17 | 2015-08-05 | 池州龙华医药化工有限公司 | Water cooling crystallization kettle |
| CN104815450A (en) * | 2015-04-17 | 2015-08-05 | 安徽扬子化工有限公司 | Pyrazole ketone synthesis crystal kettle |
| CN204656528U (en) * | 2015-04-10 | 2015-09-23 | 天津旺久科技发展有限公司 | A kind of naphthalene water reducer neutralizing tank |
| CN204910854U (en) * | 2015-09-18 | 2015-12-30 | 山东创利添加剂研发科技有限公司 | Glucose cooling crystallization device |
| CN106730979A (en) * | 2016-12-09 | 2017-05-31 | 李伟科 | A kind of observable multi-functional chemical engineering crystallization kettle |
| CN206793090U (en) * | 2017-05-03 | 2017-12-26 | 江西宇能制药有限公司 | A kind of crystallization kettle of controllable temperature |
| CN206995915U (en) * | 2017-07-21 | 2018-02-13 | 滨海金海立医药化工有限公司 | A kind of Omeprazole chloride crystallization groove |
| CN208389439U (en) * | 2018-05-29 | 2019-01-18 | 长沙鑫本药业有限公司 | Spray cooling type crystallization kettle |
-
2018
- 2018-05-29 CN CN201810529552.XA patent/CN108635901A/en active Pending
Patent Citations (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2124093U (en) * | 1992-05-25 | 1992-12-09 | 冶金工业部北京冶金设备研究所 | Spray cooling tube type continuous casting crystallizer |
| JPH07314096A (en) * | 1994-05-27 | 1995-12-05 | Nippon Steel Corp | Spray cooling type mold in continuous caster |
| CN2235336Y (en) * | 1995-10-30 | 1996-09-18 | 冶金工业部北京冶金设备研究院 | Mixing cooling tubular continuous casting mould |
| JPH10244102A (en) * | 1997-03-07 | 1998-09-14 | Konica Corp | Crystallizer and method thereof |
| JPH10263307A (en) * | 1997-03-28 | 1998-10-06 | Konica Corp | Crystallizer |
| CN203990582U (en) * | 2014-01-02 | 2014-12-10 | 北京宝沃石油技术有限责任公司 | A kind of controllable temperature heating reactor |
| CN203954727U (en) * | 2014-07-07 | 2014-11-26 | 山东祥瑞药业有限公司 | A kind of glucose equipment of crystallisation by cooling |
| CN204656528U (en) * | 2015-04-10 | 2015-09-23 | 天津旺久科技发展有限公司 | A kind of naphthalene water reducer neutralizing tank |
| CN104815451A (en) * | 2015-04-17 | 2015-08-05 | 池州龙华医药化工有限公司 | Water cooling crystallization kettle |
| CN104815450A (en) * | 2015-04-17 | 2015-08-05 | 安徽扬子化工有限公司 | Pyrazole ketone synthesis crystal kettle |
| CN204910854U (en) * | 2015-09-18 | 2015-12-30 | 山东创利添加剂研发科技有限公司 | Glucose cooling crystallization device |
| CN106730979A (en) * | 2016-12-09 | 2017-05-31 | 李伟科 | A kind of observable multi-functional chemical engineering crystallization kettle |
| CN206793090U (en) * | 2017-05-03 | 2017-12-26 | 江西宇能制药有限公司 | A kind of crystallization kettle of controllable temperature |
| CN206995915U (en) * | 2017-07-21 | 2018-02-13 | 滨海金海立医药化工有限公司 | A kind of Omeprazole chloride crystallization groove |
| CN208389439U (en) * | 2018-05-29 | 2019-01-18 | 长沙鑫本药业有限公司 | Spray cooling type crystallization kettle |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112205565A (en) * | 2020-11-09 | 2021-01-12 | 湖南金健乳业股份有限公司 | Oat preprocessing device |
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