CN203620635U - Neutral reaction kettle capable of separating liquid easily - Google Patents
Neutral reaction kettle capable of separating liquid easily Download PDFInfo
- Publication number
- CN203620635U CN203620635U CN201320862783.5U CN201320862783U CN203620635U CN 203620635 U CN203620635 U CN 203620635U CN 201320862783 U CN201320862783 U CN 201320862783U CN 203620635 U CN203620635 U CN 203620635U
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- CN
- China
- Prior art keywords
- coil pipe
- reactor body
- end socket
- valve
- reaction kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000006243 chemical reaction Methods 0.000 title abstract description 10
- 239000007788 liquid Substances 0.000 title abstract 5
- 230000007935 neutral effect Effects 0.000 title abstract 3
- 238000003756 stirring Methods 0.000 claims abstract description 10
- 238000006386 neutralization reaction Methods 0.000 claims description 13
- 239000000463 material Substances 0.000 abstract description 8
- 238000010438 heat treatment Methods 0.000 abstract description 6
- 238000000926 separation method Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 239000002699 waste material Substances 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 239000011521 glass Substances 0.000 abstract 2
- 239000002355 dual-layer Substances 0.000 abstract 1
- 239000010410 layer Substances 0.000 abstract 1
- 238000007599 discharging Methods 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Images
Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model relates to a neutral reaction kettle capable of separating a liquid easily. The reaction kettle comprises a reaction kettle body, an upper end seal head, a lower end seal head, first coil pipes, second coil pipes, a steam exhaust pipe, a motor, a stirring shaft, stirring blades, a first material inlet, a second material inlet, a discharge pipe, a first valve, a second valve and a sight glass. According to the utility model, dual layers of coil pipes are adopted for enlarging the heating area, and the heating efficiency is improved; the conical lower end seal head is adopted so as to enable liquid separation to be controlled easily; a stirring type of three layers of stirring paddles enables stirring to be more uniform, and the reaction efficiency is higher; two valves are arranged at the material discharge pipe, so that material discharge and liquid separation can be controlled much easily; the discharge pipe is provided with the sight glass, so that the liquid separation and discharge can be observed easily. The neutral reaction kettle is simple in structure, is good in water separation effect, and cannot waste materials.
Description
Technical field
The utility model relates to a kind of neutralization reaction still that is easy to separatory, belongs to technical field of chemical.
Background technology
As rubber antiager RD (2,2,4-trimethyl-1,2-dihyaroquinoline condensate) etc. chemical products in process of production, polymerisation under the effect of acidic materials (example hydrochloric acid), after reaction finishes, the pH value of reacted material need to be adjusted to alkalescence in order to carry out product separation, then carry out separatory.Neutralization reaction still is the key equipment of neutralization reaction, and still, current neutralization reaction still separatory effect is poor, operation too complex.
Summary of the invention
For the deficiencies in the prior art, the utility model provides a kind of neutralization reaction still that is easy to separatory.
The technical solution of the utility model is as follows:
A kind of neutralization reaction still that is easy to separatory, comprise reactor body, the upper end of described reactor body is fixedly connected with upper end end socket, the lower end of described reactor body is fixedly connected with lower end end socket, described upper end end socket is provided with the first charging aperture and the second charging aperture, and described lower end end socket is conical head;
Described reactor body is provided with agitating device, described agitating device comprises motor, shaft and stirrer paddle, described motor is fixedly installed on the upper end of upper end end socket, and shaft connects motor and is arranged on the inside of reactor body, and stirring blade is fixedly installed on shaft;
The spiral inner wall of described reactor body is provided with the first coil pipe and the second coil pipe, and the first described coil pipe and the second coil pipe concentric spiral arrange, and the diameter of the first coil pipe is greater than the diameter of the second coil pipe; The top of described reactor body is provided with steam inlet pipe and is connected with the upper end of the first coil pipe and the upper end of the second coil pipe respectively, and the bottom of described reactor body is provided with steam outlet pipe and is connected with the lower end of the first coil pipe and the lower end of the second coil pipe respectively;
Described lower end end socket is provided with discharge nozzle, and described discharge nozzle is provided with the first valve and the second valve, between the first valve and the second valve, is provided with visor.
According to the utility model, preferred, described upper end end socket is arc end socket.
According to the utility model, preferred, described lower end end socket is 90 ° of conical heads.
According to the utility model, preferred, described stirrer paddle is three layers, and three layers of stirrer paddle are separately positioned on the upper, middle and lower of shaft.
The utility model entirety can adopt enamel material, service life that can extension device.
The beneficial effects of the utility model are:
1, the utility model adopts duplex coil that heating surface (area) (HS is increased, and the efficiency of heating surface improves.
2, the utility model adopts the lower end end socket of taper to make separatory easier and be easy to control.
3, the utility model adopts the whipped form of three layers of stirrer paddle to make stirring more even, and reaction efficiency is higher.
4, the utility model discharge nozzle be provided with two valves make discharging and separatory be more prone to control, on discharge nozzle, be provided with visor separatory and discharging easily observed.
5, the utility model is simple in structure, and point water is effective, is not easy to cause the waste of material.
Accompanying drawing explanation
Fig. 1 is the agent structure schematic diagram that the utility model embodiment 1 is easy to the neutralization reaction still of separatory.
Wherein, 1, reactor body, 2, upper end end socket, 3, lower end end socket, 4, the first coil pipe, 5, the second coil pipe, 6, steam inlet pipe, 7, steam outlet pipe, 8, motor, 9, shaft, 10, stirrer paddle, 11, the first charging aperture, 12, the second charging aperture, 13, discharge nozzle, 14, the first valve, 15, the second valve, 16, visor.
The specific embodiment
Below by specific embodiment, the utility model is described further, but is not limited to this.
Embodiment 1
A kind of neutralization reaction still that is easy to separatory, comprise reactor body 1, the upper end of described reactor body 1 is fixedly connected with upper end end socket 2, the lower end of described reactor body 1 is fixedly connected with lower end end socket 3, described upper end end socket 2 is provided with the first charging aperture 11 and the second charging aperture 12, and described lower end end socket 3 is conical head;
Described reactor body 1 is provided with agitating device, described agitating device comprises motor 8, shaft 9 and stirrer paddle 10, described motor 8 is fixedly installed on the upper end of upper end end socket 2, shaft 9 connects motor 8 and is arranged on the inside of reactor body 1, and stirring blade 10 is fixedly installed on shaft 9;
The spiral inner wall of described reactor body 1 is provided with the first coil pipe 4 and the second coil pipe 5, and the first described coil pipe 4 and the second coil pipe 5 concentric spirals arrange, and the diameter of the first coil pipe 4 is greater than the diameter of the second coil pipe 5; The top of described reactor body 1 is provided with steam inlet pipe 6 and is connected with the upper end of the first coil pipe 4 and the upper end of the second coil pipe 5 respectively, and the bottom of described reactor body 1 is provided with steam outlet pipe 7 and is connected with the lower end of the first coil pipe 4 and the lower end of the second coil pipe 5 respectively;
Described lower end end socket 3 is provided with discharge nozzle 13, and described discharge nozzle 13 is provided with between the first valve 14 and the second valve 15, the first valves 14 and the second valve 15 and is provided with visor 16.
In the present embodiment, described lower end end socket 3 is 90 ° of conical heads, and described upper end end socket 2 is arc end socket, and described stirrer paddle 10 is three layers, and three layers of stirrer paddle 10 are separately positioned on the upper, middle and lower of shaft 9.
The first charging aperture 11 and the second charging aperture 12 be respectively used to add reaction raw materials and in and alkali lye, adopt duplex coil make heating surface (area) (HS increase, the efficiency of heating surface improve; Adopt the lower end end socket 3 of taper to make separatory easier and be easy to control; Adopt the whipped form of three layers of stirrer paddle 10 to make stirring more even, reaction efficiency is higher.Be provided with two valves at discharge nozzle 13 and make discharging and separatory be more prone to control, on discharge nozzle 13, be provided with visor 16 separatory and discharging are easily observed.
Claims (4)
1. one kind is easy to the neutralization reaction still of separatory, this reactor comprises reactor body, the upper end that it is characterized in that described reactor body is fixedly connected with upper end end socket, the lower end of described reactor body is fixedly connected with lower end end socket, described upper end end socket is provided with the first charging aperture and the second charging aperture, and described lower end end socket is conical head;
Described reactor body is provided with agitating device, described agitating device comprises motor, shaft and stirrer paddle, described motor is fixedly installed on the upper end of upper end end socket, and shaft connects motor and is arranged on the inside of reactor body, and stirring blade is fixedly installed on shaft;
The spiral inner wall of described reactor body is provided with the first coil pipe and the second coil pipe, and the first described coil pipe and the second coil pipe concentric spiral arrange, and the diameter of the first coil pipe is greater than the diameter of the second coil pipe; The top of described reactor body is provided with steam inlet pipe and is connected with the upper end of the first coil pipe and the upper end of the second coil pipe respectively, and the bottom of described reactor body is provided with steam outlet pipe and is connected with the lower end of the first coil pipe and the lower end of the second coil pipe respectively;
Described lower end end socket is provided with discharge nozzle, and described discharge nozzle is provided with the first valve and the second valve, between the first valve and the second valve, is provided with visor.
2. the neutralization reaction still that is easy to separatory according to claim 1, is characterized in that described upper end end socket is arc end socket.
3. the neutralization reaction still that is easy to separatory according to claim 1, is characterized in that described lower end end socket is 90 ° of conical heads.
4. the neutralization reaction still that is easy to separatory according to claim 1, is characterized in that described stirrer paddle is three layers, and three layers of stirrer paddle are separately positioned on the upper, middle and lower of shaft.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201320862783.5U CN203620635U (en) | 2013-12-25 | 2013-12-25 | Neutral reaction kettle capable of separating liquid easily |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201320862783.5U CN203620635U (en) | 2013-12-25 | 2013-12-25 | Neutral reaction kettle capable of separating liquid easily |
Publications (1)
Publication Number | Publication Date |
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CN203620635U true CN203620635U (en) | 2014-06-04 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201320862783.5U Expired - Lifetime CN203620635U (en) | 2013-12-25 | 2013-12-25 | Neutral reaction kettle capable of separating liquid easily |
Country Status (1)
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CN (1) | CN203620635U (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115350671A (en) * | 2022-08-18 | 2022-11-18 | 长春生物制品研究所有限责任公司 | A novel aging system for preparing aluminium hydroxide adjuvant |
-
2013
- 2013-12-25 CN CN201320862783.5U patent/CN203620635U/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115350671A (en) * | 2022-08-18 | 2022-11-18 | 长春生物制品研究所有限责任公司 | A novel aging system for preparing aluminium hydroxide adjuvant |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CX01 | Expiry of patent term |
Granted publication date: 20140604 |
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CX01 | Expiry of patent term |