CN108635254A - A kind of reparation water and preparation method thereof significantly improving hand hangnail - Google Patents

A kind of reparation water and preparation method thereof significantly improving hand hangnail Download PDF

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CN108635254A
CN108635254A CN201810276458.8A CN201810276458A CN108635254A CN 108635254 A CN108635254 A CN 108635254A CN 201810276458 A CN201810276458 A CN 201810276458A CN 108635254 A CN108635254 A CN 108635254A
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water
hangnail
hand
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不公告发明人
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/591—Mixtures of compounds not provided for by any of the codes A61K2800/592 - A61K2800/596

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  • Life Sciences & Earth Sciences (AREA)
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Abstract

The invention discloses a kind of reparation water and preparation method thereof significantly improving hand hangnail, this method is to provide a kind of reparation water, the reparation water of the invention, including following component by weight：150 190 parts of the petal of sweet blueness Microula sikkimensis, 40 60 parts of the blade of chaff Qiong Nan, 220 240 parts of the petal of lanceolata Camellia fraternal, 700 parts of water.The reparation water of the present invention combines multiple element, effective to improve hand hangnail, and significantly alleviates hand hangnail reproduction condition, to make up deficiency of the prior art for improvement hand hangnail.

Description

A kind of reparation water and preparation method thereof significantly improving hand hangnail
Technical field
The present invention relates to a kind of reparation water, especially a kind of effective improvement hand hangnail simultaneously significantly alleviates hand hangnail regeneration shape The reparation water of condition.
Background technology
Hand hangnail is skin too dry, and caused by cuticula has crackle, hangnail is generally grown beside nail, there is hangnail on hand When, always anxious it is not pulled out, because hangnail connects together with muscle, when tearing hangnail with hand or other tools, Not only pain, can also allow the skin damage of surrounding, or even can cause and bleed, and lead to hand infection.
The prior art does not have significant effect to improving hand hangnail, due to the petal of sweet green Microula sikkimensis, the leaf of chaff Qiong Nan The petal of piece, lanceolata Camellia fraternal contains many chemical compositions, accordingly, it is determined that the mixed proportion of three kinds of plant tissues, to Reaching not only improves hand hangnail, but also can reach and prevent its regenerated effect, is of great significance.
Invention content
It is an object of the invention to overcome the shortage of prior art, a kind of reparation water is provided, especially can effectively improve hand falls Thorn, and hand hangnail reproduction condition is significantly improved, the purpose of the present invention is realized by following technical proposals：It is added and plants in the present invention The ingredient and weight proportion of object tissue be：
150-190 parts of the petal of sweet blueness Microula sikkimensis, preferred weight part are 165-175 parts.Sweet blueness Microula sikkimensis (Classification system： Microula pseudotrichocarpa W.T.Wang) it is Boraginaceae Microula plant, inflorescence axillary or basidixed, it is just close Collection, subsphaeroidal, fruiting period often extends, and is up to 1.5 centimetres, and corolla blue is hairless, the petal for the sweet green Microula sikkimensis used in the present invention Pick up from Gansu Xiahe.
40-60 parts of the blade of chaff Qiong Nan, preferred weight part are 42-48 parts.Chaff Qiong Nan (Classification systems： Beilschmiedia furfuracea Chun ex H.T.Chang) be Lauraceae fine jade Phoebe arbor, it is 8-15 meters high, leaf to raw or Closely to life, thin keratin, oblong or long round shape ellipse, 7-14 centimetres long, 3-6 centimetres wide, apex is sharp sharp or slightly blunt, base portion wedge The blade of shape or subcircular, the chaff Qiong Nan used in of the invention picks up from the mountain valley shaw of Period In Maoming.
220-240 parts of the petal of lanceolata Camellia fraternal, preferred weight part are 222-230 parts.Lanceolata Camellia fraternal (Latin Name：Camellia lancilimba H.T.Chang) it is Theaceae Camellia shrub, 3 meters high, petal 5, white, wealthy ovum Shape, base portion omit phase adhesion, and outside two panels keratin has microtriche, remaining petal obovate has microtriche, and stamen is shorter than petal, foreign steamer flower At short tube, the first half is free, hairless for silk lower half joint, and the petal for the lanceolata Camellia fraternal used in the present invention picks up from Guangdong breast Source and even the mountainous region evergreen forest in Nan County.
700 parts of water.
Production method of the present invention is as follows：
(1) petal of the petal of fresh sweet green Microula sikkimensis, chaff fine jade nanmu petal, lanceolata Camellia fraternal is taken to be rinsed with clear water After twice, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtains pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
The water-bath brand used in the present invention is to win fast, model HH.S11-6, and the biological instrument of fast medical treatment is won purchased from Shanghai Device limited liability company；The ultrasonic extraction instrument brand used is opened up for sea, model HI-T00, and the mechanical limited public affairs of science and technology are opened up purchased from sea Department；The centrifuge brand used is Hunan instrument, and model H2100R is purchased from Xiang Yi centrifuges Instrument Ltd.；The high pressure used Steam sterilization pan brand is four directions, and model MJQ50-1 is purchased from Xuzhou four directions Medical Devices Co., Ltd.；The shaking table product used Board is permanent promise, model HWS-250B, is made the science and technology prosperous Co., Ltd purchased from Beijing's perseverance promise profit.
It is as follows that the present invention repairs aqueous energy evaluation test：
One, skin irritation test：
2.5~3kg healthy rabbits 60 are selected, every rabbit back is symmetrical to select shaving 2.5cm at 202, right with itself According to test method(s) carry out, every time apply 0.5g products of the present invention, twice daily, left or right side is smeared at random, observe and record for 24 hours, The reacting phenomenon of skin after 72h.
The result shows that：It applies product of the present invention and has no that the local stimulations such as rubefaction, dermexanthesis, water lump are reacted for 24 hours, after 72h, say It is to be perfectly safe that the bright present invention, which repairs water, without any adverse reactions.
Two, efficacy validation
260 hand hangnail radicals and the similar 25-45 Sui volunteer of distribution, wherein 25-35 Sui volunteer are selected to have 130 Name, each 65 people of men and women, 36-45 Sui volunteer have 130, and each 65 people of men and women, test site is Nanchang City, Jiangxi Province, the above will Hope person is checked by the hospital dermatology department expert of Nanchang City, Jiangxi Province ten to be complied with standard and selects, and is divided into 13 groups, and 11 groups are experiment Group, 2 groups are control group, and every group of 20 people, wherein 25-35 Sui volunteer have 10 people, each 5 people of men and women, 36-45 Sui volunteer to have 10 people, each 5 people of men and women, the common hand lotion of one group of control group, one group of control group do not smear any product, the test group present invention Product, August takes pictures to every human hand on 31st within 2015, and records the radical of everyone hand hangnail, tests in September 1 in 2015 Day starts, and product is smeared at hand hangnail, once in the morning and once at night, is used continuously three months (i.e.：September, October, November).Three months Afterwards (i.e. December 1), (i.e. on March 1st, 2016) after six months, (i.e. 2016 on September 1) records each human hand respectively after 1 year The radical of hangnail.Note：Daily life of subject etc. is usually accustomed to according to subject during experiment.
Specific implementation mode
Embodiment 1-11 is test group, and embodiment 12 and 13 is control group, experiment 20 people of number per embodiment, 2015 8 It month takes pictures to every human hand within 31st, and records the radical of everyone hand hangnail, experiment was in September in 2015 1 day, by product It smears at hand hangnail, once in the morning and once at night, is used continuously three months (i.e.：September, October, November).(i.e. December 1) after three months, (i.e. on March 1st, 2016) after six months, (i.e. 2016 on September 1) records the radical of each human hand hangnail respectively after 1 year.Note： Daily life of subject etc. is usually accustomed to according to subject during experiment.
The embodiment of the present invention and its result are further elaborated below.
Embodiment 1
A kind of preparation method for repairing water, includes the following steps：
(1) 170 parts by weight of petal, 45 parts by weight of chaff fine jade nanmu petal, lanceolata of fresh sweet green Microula sikkimensis is taken to connect stamen After 225 parts by weight of petal of tea are rinsed twice with clear water, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtain Pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 26.5 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 28.2；25-35 Sui average every volunteer's hand hangnail is 4.3 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 5.1；25-35 Sui average every volunteer's hand hangnail is 4.0 after 6 months, 36-45 Average every volunteer's hand hangnail in year is 4.9；25-35 Sui average every volunteer's hand hangnail is 3.8 after 1 year, 36-45 Sui average every volunteer's hand hangnail is 4.2.
Embodiment 2
A kind of preparation method for repairing water, includes the following steps：
(1) 160 parts by weight of petal, 50 parts by weight of chaff fine jade nanmu petal, lanceolata of fresh sweet green Microula sikkimensis is taken to connect stamen After 240 parts by weight of petal of tea are rinsed twice with clear water, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtain Pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 25.7 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 26.8；25-35 Sui average every volunteer's hand hangnail is 4.4 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 5.0；25-35 Sui average every volunteer's hand hangnail is 4.2 after 6 months, 36-45 Average every volunteer's hand hangnail in year is 4.7；25-35 Sui average every volunteer's hand hangnail is 3.9 after 1 year, 36-45 Sui average every volunteer's hand hangnail is 4.1.
Embodiment 3
A kind of preparation method for repairing water, includes the following steps：
(1) 190 parts by weight of petal, 40 parts by weight of chaff fine jade nanmu petal, lanceolata of fresh sweet green Microula sikkimensis is taken to connect stamen After 220 parts by weight of petal of tea are rinsed twice with clear water, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtain Pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 27.2 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 28.5；25-35 Sui average every volunteer's hand hangnail is 4.6 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 5.4；25-35 Sui average every volunteer's hand hangnail is 4.3 after 6 months, 36-45 Average every volunteer's hand hangnail in year is 5.2；25-35 Sui average every volunteer's hand hangnail is 4.0 after 1 year, 36-45 Sui average every volunteer's hand hangnail is 4.9.
Embodiment 4
A kind of preparation method for repairing water, includes the following steps：
(1) 180 parts by weight of petal, 55 parts by weight of chaff fine jade nanmu petal, lanceolata of fresh sweet green Microula sikkimensis is taken to connect stamen After 230 parts by weight of petal of tea are rinsed twice with clear water, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtain Pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 26.9 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 27.1；25-35 Sui average every volunteer's hand hangnail is 4.2 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 4.8；25-35 Sui average every volunteer's hand hangnail is 3.9 after 6 months, 36-45 Average every volunteer's hand hangnail in year is 4.5；25-35 Sui average every volunteer's hand hangnail is 3.6 after 1 year, 36-45 Sui average every volunteer's hand hangnail is 4.0.
Embodiment 5
A kind of preparation method for repairing water, includes the following steps：
(1) 150 parts by weight of petal, 60 parts by weight of chaff fine jade nanmu petal, lanceolata of fresh sweet green Microula sikkimensis is taken to connect stamen After 235 parts by weight of petal of tea are rinsed twice with clear water, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtain Pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 27.0 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 27.8；25-35 Sui average every volunteer's hand hangnail is 4.5 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 5.2；25-35 Sui average every volunteer's hand hangnail is 4.3 after 6 months, 36-45 Average every volunteer's hand hangnail in year is 4.8；25-35 Sui average every volunteer's hand hangnail is 4.0 after 1 year, 36-45 Sui average every volunteer's hand hangnail is 4.4.
Embodiment 6
A kind of preparation method for repairing water, includes the following steps：
(1) after taking the 170 parts by weight clear water of petal of fresh sweet green Microula sikkimensis to rinse twice, with filter paper by its surface Water blots, and is put into mortar and grinds, and obtains purees, spare；
(2) purees that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, taken after 6 hours Go out, the purees in beaker is filtered, collects filtrate respectively and residue bottling is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 26.9 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 27.4；25-35 Sui average every volunteer's hand hangnail is 16.3 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 16.7；25-35 Sui average every volunteer's hand hangnail is 16.0 after 6 months, 36- 45 years old average every volunteer's hand hangnails are 16.5；25-35 Sui average every volunteer's hand hangnail is 15.8 after 1 year Root, 36-45 Sui average every volunteer's hand hangnail is 15.9.
Embodiment 7
A kind of preparation method for repairing water, includes the following steps：
(1) after taking fresh 45 parts by weight clear water of chaff fine jade nanmu petal to rinse twice, the water on its surface is inhaled with filter paper It is dry, it is put into mortar and grinds, obtain purees, it is spare；
(2) purees that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, taken after 6 hours Go out, the purees in beaker is filtered, collects filtrate respectively and residue bottling is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 27.4 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 28.1；25-35 Sui average every volunteer's hand hangnail is 16.5 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 17.0；25-35 Sui average every volunteer's hand hangnail is 16.2 after 6 months, 36- 45 years old average every volunteer's hand hangnails are 16.7；25-35 Sui average every volunteer's hand hangnail is 15.9 after 1 year Root, 36-45 Sui average every volunteer's hand hangnail is 16.3.
Embodiment 8
A kind of preparation method for repairing water, includes the following steps：
(1) after taking the 225 parts by weight clear water of petal of fresh lanceolata Camellia fraternal to rinse twice, with filter paper by its surface Water blot, be put into mortar and grind, obtain purees, it is spare；
(2) purees that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, taken after 6 hours Go out, the purees in beaker is filtered, collects filtrate respectively and residue bottling is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 27.2 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 27.8；25-35 Sui average every volunteer's hand hangnail is 16.8 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 17.7；25-35 Sui average every volunteer's hand hangnail is 16.4 after 6 months, 36- 45 years old average every volunteer's hand hangnails are 17.2；25-35 Sui average every volunteer's hand hangnail is 16.0 after 1 year Root, 36-45 Sui average every volunteer's hand hangnail is 17.1.
Embodiment 9
A kind of preparation method for repairing water, includes the following steps：
(1) 170 parts by weight of petal of fresh sweet green Microula sikkimensis, 45 parts by weight clear water of chaff fine jade nanmu petal is taken to rinse two After, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtains pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 26.3 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 27.2；25-35 Sui average every volunteer's hand hangnail is 11.2 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 12.3；25-35 Sui average every volunteer's hand hangnail is 11.0 after 6 months, 36- 45 years old average every volunteer's hand hangnails are 12.1；25-35 Sui average every volunteer's hand hangnail is 10.8 after 1 year Root, 36-45 Sui average every volunteer's hand hangnail is 11.9.
Embodiment 10
A kind of preparation method for repairing water, includes the following steps：
(1) 170 parts by weight of petal, 225 parts by weight of petal of lanceolata Camellia fraternal of fresh sweet green Microula sikkimensis are taken to use clear After water rinses twice, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtains pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 26.5 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 27.6；25-35 Sui average every volunteer's hand hangnail is 11.4 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 12.5；25-35 Sui average every volunteer's hand hangnail is 11.1 after 6 months, 36- 45 years old average every volunteer's hand hangnails are 12.3；25-35 Sui average every volunteer's hand hangnail is 10.9 after 1 year Root, 36-45 Sui average every volunteer's hand hangnail is 12.0.
Embodiment 11
A kind of preparation method for repairing water, includes the following steps：
(1) fresh 45 parts by weight of chaff fine jade nanmu petal, 225 parts by weight of petal of lanceolata Camellia fraternal is taken to be rinsed with clear water After twice, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtains pureed mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, 6 hours After take out, by beaker pureed mixture filter, respectively collect filtrate and residue bottling it is spare；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put Enter in 45 DEG C of water-baths, filtering is taken out after 8 hours, discard residue, collects filtrate and mixed with the filtrate that step (2) obtains, it is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 revs/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature 120 DEG C, pressure 100kpa are set as, 650 parts by weight water are added after taking-up, are placed on shaking table, temperature setting is 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
Test result：25-35 Sui average every volunteer's hand hangnail is 26.9 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 27.8；25-35 Sui average every volunteer's hand hangnail is 12.0 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 12.7；25-35 Sui average every volunteer's hand hangnail is 11.8 after 6 months, 36- 45 years old average every volunteer's hand hangnails are 12.6；25-35 Sui average every volunteer's hand hangnail is 11.4 after 1 year Root, 36-45 Sui average every volunteer's hand hangnail is 12.1.
Embodiment 12
The present embodiment is check experiment, and common hand lotion is smeared at volunteer's hand hangnail.
Test result：25-35 Sui average every volunteer's hand hangnail is 27.1 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 27.5；25-35 Sui average every volunteer's hand hangnail is 20.3 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 21.0；25-35 Sui average every volunteer's hand hangnail is 26.8 after 6 months, 36- 45 years old average every volunteer's hand hangnails are 26.9；25-35 Sui average every volunteer's hand hangnail is 27.4 after 1 year Root, 36-45 Sui average every volunteer's hand hangnail is 27.3.
Embodiment 13
The present embodiment is check experiment, without any processing at volunteer's hand hangnail.
Test result：25-35 Sui average every volunteer's hand hangnail is 26.1 before experiment, 36-45 Sui averagely often Name volunteer's hand hangnail is 28.4；25-35 Sui average every volunteer's hand hangnail is 26.3 after 3 months, 36-45 Sui Average every volunteer's hand hangnail is 29.2；25-35 Sui average every volunteer's hand hangnail is 25.6 after 6 months, 36- 45 years old average every volunteer's hand hangnails are 27.4；25-35 Sui average every volunteer's hand hangnail is 26.8 after 1 year Root, 36-45 Sui average every volunteer's hand hangnail is 28.9.

Claims (2)

1. a kind of reparation water significantly improving hand hangnail, it is characterized in that being prepared by following methods：
(1) 190 parts by weight of petal of fresh sweet green Microula sikkimensis, 40 parts by weight of chaff fine jade nanmu petal, lanceolata Camellia fraternal are taken After 220 parts by weight of petal are rinsed twice with clear water, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtain pureed Mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, taken after 6 hours Go out, the pureed mixture in beaker is filtered, the pureed mixture in beaker is filtered, collects filtrate respectively and residue bottling is standby With；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put into 45 In DEG C water-bath, filtering is taken out after 8 hours, discards residue, discard residue, collect filtrate and mixed with the filtrate that step (2) obtains, It is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 Rev/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature setting It is 120 DEG C, pressure 100kpa, 650 parts by weight water is added after taking-up, are placed on shaking table, temperature setting is about 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
2. a kind of preparation method for the reparation water significantly improving hand hangnail, it is characterized in that including the following steps：
(1) 190 parts by weight of petal of fresh sweet green Microula sikkimensis, 40 parts by weight of chaff fine jade nanmu petal, lanceolata Camellia fraternal are taken After 220 parts by weight of petal are rinsed twice with clear water, the water on its surface is blotted with filter paper, is put into mortar and grinds, obtain pureed Mixture, it is spare；
(2) the pureed mixture that step (1) obtains is transferred in beaker and is sealed, be put into 45 DEG C of water-baths, taken after 6 hours Go out, the pureed mixture in beaker is filtered, the pureed mixture in beaker is filtered, collects filtrate respectively and residue bottling is standby With；
(3) it will be added in residue that step (2) obtains after 50 parts by weight water after 60 DEG C of ultrasonic extractions 25 minutes, sealing is put into 45 In DEG C water-bath, filtering is taken out after 8 hours, discards residue, discard residue, collect filtrate and mixed with the filtrate that step (2) obtains, It is spare；
(4) filtrate that step (3) obtains is put into centrifuge and is centrifuged 30 minutes, temperature setting is 4 DEG C, and rotating speed is set as 5000 Rev/min, sediment is discarded after taking-up, stays supernatant, it is spare；
(5) it is put into high-pressure steam sterilizing pan and sterilizes 30 minutes after sealing the supernatant bottling that step (4) obtains, temperature setting It is 120 DEG C, pressure 100kpa, 650 parts by weight water is added after taking-up, are placed on shaking table, temperature setting is about 30 DEG C, is turned Speed for after 80 revs/min, 15 days up to the reparation water.
CN201810276458.8A 2018-03-30 2018-03-30 A kind of reparation water and preparation method thereof significantly improving hand hangnail Withdrawn CN108635254A (en)

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