CN108610497A - A kind of nanometer anti-fog glass-film - Google Patents

A kind of nanometer anti-fog glass-film Download PDF

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Publication number
CN108610497A
CN108610497A CN201810292080.0A CN201810292080A CN108610497A CN 108610497 A CN108610497 A CN 108610497A CN 201810292080 A CN201810292080 A CN 201810292080A CN 108610497 A CN108610497 A CN 108610497A
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accounts
glass
film
sorbierite
makrolon
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Pending
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CN201810292080.0A
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Chinese (zh)
Inventor
刘涛
陈倩
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Shangluo University
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Shangluo University
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Priority to CN201810292080.0A priority Critical patent/CN108610497A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J7/00—Adhesives in the form of films or foils
    • C09J7/20—Adhesives in the form of films or foils characterised by their carriers
    • C09J7/22—Plastics; Metallised plastics
    • C09J7/24—Plastics; Metallised plastics based on macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
    • C08J7/04—Coating
    • C08J7/042—Coating with two or more layers, where at least one layer of a composition contains a polymer binder
    • C08J7/0423—Coating with two or more layers, where at least one layer of a composition contains a polymer binder with at least one layer of inorganic material and at least one layer of a composition containing a polymer binder
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J7/00—Adhesives in the form of films or foils
    • C09J7/30—Adhesives in the form of films or foils characterised by the adhesive composition
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
    • C08J2423/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
    • C08J2423/04—Homopolymers or copolymers of ethene
    • C08J2423/06—Polyethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2469/00—Characterised by the use of polycarbonates; Derivatives of polycarbonates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
    • C08K13/04—Ingredients characterised by their shape and organic or inorganic ingredients
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00—Use of ingredients characterised by shape
    • C08K7/02—Fibres or whiskers
    • C08K7/04—Fibres or whiskers inorganic
    • C08K7/14—Glass
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2301/00—Additional features of adhesives in the form of films or foils
    • C09J2301/10—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
    • C09J2301/12—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers
    • C09J2301/122—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present only on one side of the carrier, e.g. single-sided adhesive tape
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2433/00—Presence of (meth)acrylic polymer
    • C09J2433/006—Presence of (meth)acrylic polymer in the substrate

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a kind of nanometer anti-fog glass-films, are made of low density polyethylene (LDPE), glass fibre, makrolon, mica powder, polyethylene wax, n-butanol, glycerine fatty acid methyl esters, the double stearates of sorbierite, acrylic resin, dimethyl methyl acid amide, methyl acrylate, polyacrylamide, shrink Span, polyoxyethylene nonyl phenyl vinethene, nanometer titanium dioxide coating and layer of silica gel；Compared with prior art, the film that the present invention makes, toughness is high, improves the explosion-proof performance of glass, in addition, when water mist condenses in film surface, droplet will not be caused, shrink Span can be such that the droplet of condensation spreads, and to prevent glass fogging, have the value of popularization and application.

Description

A kind of nanometer anti-fog glass-film
Technical field
The present invention relates to field of material technology more particularly to a kind of nanometer anti-fog glass-films.
Background technology
Glass is amorphous inorganic non-metallic material, and usually with a variety of inorganic minerals, (such as quartz sand, borax, boric acid, weight are brilliant Stone, barium carbonate, lime stone, feldspar, soda ash etc.) it is primary raw material, it additionally incorporates made of a small amount of auxiliary material.The prior art In, glass conduct makes various windows, and glass understands surface fogging, especially automotive window because of the temperature difference, and fogging can influence to drive Sight, accordingly, there exist rooms for improvement.
Invention content
The purpose of the present invention is that solve the above-mentioned problems and provides a kind of nanometer anti-fog glass-film.
The present invention is achieved through the following technical solutions above-mentioned purpose：
The present invention is by low density polyethylene (LDPE), glass fibre, makrolon, mica powder, polyethylene wax, n-butanol, glyceride Fatty acid methyl esters, sorbierite double stearate, acrylic resin, dimethyl methyl acid amide, methyl acrylate, polyacrylamide, shrinks Span, polyoxyethylene nonyl phenyl vinethene, nanometer titanium dioxide coating and layer of silica gel composition；
Preparation method includes the following steps：
(1) by low density polyethylene (LDPE), glass fibre, makrolon, mica powder, polyethylene wax, n-butanol, glycerine fatty acid Stirring is added in the double stearates of methyl esters, sorbierite, acrylic resin, dimethyl methyl acid amide, methyl acrylate and polyacrylamide Device is uniformly mixed, and film-making machine is placed in after being heated to 180-210 DEG C, coating layer is made；
(2) step (1) is coated on after shrink Span and polyoxyethylene nonyl phenyl vinethene being heated to 120 DEG C The wherein one side of the coating layer of preparation；
(3) nanometer titanium dioxide coating is coated on to the surface of step (2) coat using electrostatic spray；
(4) another side that silica gel heating is coated on step (1) coating layer to 230-260 DEG C, cooling are got product.
Further, the surface of the layer of silica gel covers peeling layer.
Preferably, by weight, the material proportion of coating layer is in the step (1)：The low density polyethylene (LDPE) accounts for 3-5%, the glass fibre account for 4-8%, the makrolon accounts for 10-25%, the mica powder accounts for 3-5%, the polyethylene Wax accounts for 5-8%, the n-butanol accounts for 5-8%, the glycerine fatty acid methyl esters accounts for the double stearates of 10-15%, the sorbierite Account for 3-5%, the acrylic resin accounts for 30-40%, the dimethyl methyl acid amide accounts for 1-2%, the methyl acrylate accounts for 1- 2%, the polyacrylamide accounts for 2-3%.
Specifically, the low density polyethylene (LDPE), which accounts for the 5%, glass fibre and accounts for the 5%, makrolon, accounts for 15%, institute It states mica powder and accounts for the 5%, polyethylene wax and account for the 5%, n-butanol and account for 5%, the glycerine fatty acid methyl esters and account for 15%, is described The double stearates of sorbierite, which account for the 5%, acrylic resin and account for 35%, the dimethyl methyl acid amide, accounts for 2%, the acrylic acid first Ester accounts for the 1%, polyacrylamide and accounts for 2%.
The beneficial effects of the present invention are：
The present invention is a kind of nanometer anti-fog glass-film, and compared with prior art, the film that the present invention makes, toughness is high, improves The explosion-proof performance of glass will not cause droplet, shrink Span that can make to coagulate in addition, when water mist condenses in film surface The droplet of knot is spread, and to prevent glass fogging, is had the value of popularization and application.
Specific implementation mode
The invention will be further described below：
The present invention is by low density polyethylene (LDPE), glass fibre, makrolon, mica powder, polyethylene wax, n-butanol, glyceride Fatty acid methyl esters, sorbierite double stearate, acrylic resin, dimethyl methyl acid amide, methyl acrylate, polyacrylamide, shrinks Span, polyoxyethylene nonyl phenyl vinethene, nanometer titanium dioxide coating and layer of silica gel composition；
Preparation method includes the following steps：
(1) by low density polyethylene (LDPE), glass fibre, makrolon, mica powder, polyethylene wax, n-butanol, glycerine fatty acid Stirring is added in the double stearates of methyl esters, sorbierite, acrylic resin, dimethyl methyl acid amide, methyl acrylate and polyacrylamide Device is uniformly mixed, and film-making machine is placed in after being heated to 180-210 DEG C, coating layer is made；
(2) step (1) is coated on after shrink Span and polyoxyethylene nonyl phenyl vinethene being heated to 120 DEG C The wherein one side of the coating layer of preparation；
(3) nanometer titanium dioxide coating is coated on to the surface of step (2) coat using electrostatic spray；
(4) another side that silica gel heating is coated on step (1) coating layer to 230-260 DEG C, cooling are got product.
Further, the surface of the layer of silica gel covers peeling layer.
Preferably, by weight, the material proportion of coating layer is in the step (1)：The low density polyethylene (LDPE) accounts for 3-5%, the glass fibre account for 4-8%, the makrolon accounts for 10-25%, the mica powder accounts for 3-5%, the polyethylene Wax accounts for 5-8%, the n-butanol accounts for 5-8%, the glycerine fatty acid methyl esters accounts for the double stearates of 10-15%, the sorbierite Account for 3-5%, the acrylic resin accounts for 30-40%, the dimethyl methyl acid amide accounts for 1-2%, the methyl acrylate accounts for 1- 2%, the polyacrylamide accounts for 2-3%.
Specifically, the low density polyethylene (LDPE), which accounts for the 5%, glass fibre and accounts for the 5%, makrolon, accounts for 15%, institute It states mica powder and accounts for the 5%, polyethylene wax and account for the 5%, n-butanol and account for 5%, the glycerine fatty acid methyl esters and account for 15%, is described The double stearates of sorbierite, which account for the 5%, acrylic resin and account for 35%, the dimethyl methyl acid amide, accounts for 2%, the acrylic acid first Ester accounts for the 1%, polyacrylamide and accounts for 2%.
The basic principles and main features and advantages of the present invention of the present invention have been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (4)

1. a kind of nanometer anti-fog glass-film, it is characterised in that：By low density polyethylene (LDPE), glass fibre, makrolon, mica powder, Polyethylene wax, n-butanol, glycerine fatty acid methyl esters, sorbierite double stearate, acrylic resin, dimethyl methyl acid amide, propylene Sour methyl esters, polyacrylamide, shrink Span, polyoxyethylene nonyl phenyl vinethene, nanometer titanium dioxide coating and silicon Glue-line forms；
Preparation method includes the following steps：
(1) by low density polyethylene (LDPE), glass fibre, makrolon, mica powder, polyethylene wax, n-butanol, glycerine fatty acid first Blender is added in the double stearates of ester, sorbierite, acrylic resin, dimethyl methyl acid amide, methyl acrylate and polyacrylamide It is uniformly mixed, film-making machine is placed in after being heated to 180-210 DEG C, coating layer is made；
(2) step (1) is coated on after shrink Span and polyoxyethylene nonyl phenyl vinethene being heated to 120 DEG C to prepare Coating layer wherein one side；
(3) nanometer titanium dioxide coating is coated on to the surface of step (2) coat using electrostatic spray；
(4) another side that silica gel heating is coated on step (1) coating layer to 230-260 DEG C, cooling are got product.
2. nanometer anti-fog glass-film according to claim 1, it is characterised in that：The surface covering stripping of the layer of silica gel Layer.
3. nanometer anti-fog glass-film according to claim 1, it is characterised in that：By weight, overlay film in the step (1) Layer material proportion be：The low density polyethylene (LDPE) accounts for 3-5%, the glass fibre accounts for 4-8%, the makrolon accounts for 10- 25%, the mica powder accounts for 3-5%, the polyethylene wax accounts for 5-8%, the n-butanol accounts for 5-8%, the glycerine fatty acid first Ester accounts for 10-15%, the sorbierite, and double stearate accounts for 3-5%, the acrylic resin accounts for 30-40%, the dimethyl methyl Acid amide accounts for 1-2%, the methyl acrylate accounts for 1-2%, the polyacrylamide accounts for 2-3%.
4. nanometer anti-fog glass-film according to claim 3, it is characterised in that：The low density polyethylene (LDPE) accounts for 5%, is described Glass fibre, which accounts for the 5%, makrolon and accounts for the 15%, mica powder and account for the 5%, polyethylene wax, accounts for the 5%, n-butanol It accounts for 5%, the glycerine fatty acid methyl esters and accounts for the double stearates of the 15%, sorbierite and account for the 5%, acrylic resin and account for 35%, the dimethyl methyl acid amide, which accounts for the 2%, methyl acrylate and accounts for the 1%, polyacrylamide, accounts for 2%.
CN201810292080.0A 2018-04-03 2018-04-03 A kind of nanometer anti-fog glass-film Pending CN108610497A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109849464A (en) * 2018-12-06 2019-06-07 吉林工程技术师范学院 A kind of computer display film

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102794965A (en) * 2012-08-06 2012-11-28 宁波长阳科技有限公司 Anti-fog polyester film and preparation method thereof
CN103772795A (en) * 2014-01-24 2014-05-07 南通红石科技发展有限公司 Anti-fog material and preparation method thereof
CN106398576A (en) * 2016-09-29 2017-02-15 四川天视车镜有限责任公司 High-definition and anti-fogging film for car rearview mirrors and production method of high-definition and anti-fogging film
CN106519551A (en) * 2016-11-18 2017-03-22 陕西理工学院 Heat insulating window film formula and preparing method
CN107081946A (en) * 2017-05-12 2017-08-22 商洛学院 A kind of screen sticking film based on nano material

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102794965A (en) * 2012-08-06 2012-11-28 宁波长阳科技有限公司 Anti-fog polyester film and preparation method thereof
CN103772795A (en) * 2014-01-24 2014-05-07 南通红石科技发展有限公司 Anti-fog material and preparation method thereof
CN106398576A (en) * 2016-09-29 2017-02-15 四川天视车镜有限责任公司 High-definition and anti-fogging film for car rearview mirrors and production method of high-definition and anti-fogging film
CN106519551A (en) * 2016-11-18 2017-03-22 陕西理工学院 Heat insulating window film formula and preparing method
CN107081946A (en) * 2017-05-12 2017-08-22 商洛学院 A kind of screen sticking film based on nano material

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109849464A (en) * 2018-12-06 2019-06-07 吉林工程技术师范学院 A kind of computer display film

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Application publication date: 20181002