CN108587792A - A kind of chemical experiment vapor water proof distillation essential oil extraction equipment - Google Patents

A kind of chemical experiment vapor water proof distillation essential oil extraction equipment Download PDF

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Publication number
CN108587792A
CN108587792A CN201810650320.XA CN201810650320A CN108587792A CN 108587792 A CN108587792 A CN 108587792A CN 201810650320 A CN201810650320 A CN 201810650320A CN 108587792 A CN108587792 A CN 108587792A
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CN
China
Prior art keywords
essential oil
storage bottle
extraction equipment
outlet
mouthfuls
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Pending
Application number
CN201810650320.XA
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Chinese (zh)
Inventor
何华英
沈小玲
林楚迎
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Individual
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Individual
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Priority to CN201810650320.XA priority Critical patent/CN108587792A/en
Publication of CN108587792A publication Critical patent/CN108587792A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38Steam distillation

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a kind of chemical experiment vapor water proofs to distill essential oil extraction equipment, it includes two mouthfuls of eggplant type flasks, storage bottle, connecting tube, condensation and essential oil hydrosol separator, bottleneck is equipped at the top of the storage bottle, the storage bottle bottom is equipped with flask connector, the spherical porous filter chamber being recessed to storage bottle inner space is equipped at the flask connector, two mouthfuls of eggplant type flasks are equipped with the fluid infusion positioned at the gas outlet at top and positioned at side.The present invention is by setting the sieve plate being used as between two mouthfuls of eggplant type flasks of steam generator and the storage bottle for housing fragrant plant to the spherical porous filter chamber being recessed to storage bottle inner space, enable and heats fragrant plant to vapor divergence expression in operating process, make the vapor generated in two mouthfuls of eggplant type flasks can equably, 360 ° omni-directional without dead angle heat fragrant plant, to substantially increase the essential oil distilling effect of fragrant plant, shorten the rectifying time.

Description

A kind of chemical experiment vapor water proof distillation essential oil extraction equipment
Technical field
The present invention relates to experimental instrument field, more particularly to a kind of extraction equipment.
Background technology
Essential oil distillation extraction refers to that distillation extraction goes out essential oil from fragrant plant by vapor, this is that extraction essential oil is most normal With most clean method.Vapor water proof distillation essential oil be the saturated vapor that is generated by steam generator by sieve plate to it is lower by Upper heating fragrant plant, the volatile ingredient in fragrant plant are taken out of with steam distillation, since fragrance and water constitute essential oil With the immiscible system of water, when heating, with increasing for temperature, essential oil and water are intended to accelerate evaporation, generate mixture steam, Its steam imports in condenser and obtains the liquid mixture of water and essential oil, and essential oil product is can be obtained after water-oil separating, existing In stage chemistry curricula, teacher shows distillation process using chemical experiment essential oil distilling and extracting device to student.Currently, compared with Chemical experiment vapor water proof distillation essential oil extraction equipment used in more teaching is relatively simple, in steam generator and fragrance Sieve plate between plant accumulator, some school instructions replace sieve plate with clean gauze, but gauze gets wet or oil is easy to slide, Also the school instruction having use parallel more air filter plates, but the vapor of parallel more air filter plates be vertically to it is lower and on, two cannot be made The fragrant plant of side is completely heated up, causes aromatic essential oil to distill ineffective, experimental period is long, does not only take up students Quality time, and affect the authenticity of experimental analysis.
Invention content
The technical problem to be solved by the present invention is to:In view of the above shortcomings of the prior art, a kind of chemical laboratory water is provided Steam water proof distills essential oil extraction equipment.
The solution that the present invention solves its technical problem is:A kind of chemical experiment vapor water proof distillation essential oil extraction dress It sets comprising two mouthfuls of eggplant type flasks, storage bottle, connecting tube, condensation and essential oil hydrosol separator, the storage bottle top are set There are bottleneck, the storage bottle bottom to be equipped with flask connector, be equipped with to storage bottle inner space and be recessed at the flask connector Spherical porous filter chamber, two mouthfuls of eggplant type flasks are equipped with the gas outlet positioned at top and fluid infusion positioned at side, the company The one end taken over is connected to the bottleneck of storage bottle, and the other end of connecting tube is connected to one end of condensation, the condensation The other end be connected to the essential oil hydrosol separator.
As a further improvement of the above technical scheme, the spherical porous filter chamber is integrally formed with storage bottle.
As a further improvement of the above technical scheme, the condensation includes serpentine condenser, condenser pipe water inlet It is connected to connecting tube with the upper end of condenser pipe water outlet, the serpentine condenser, the lower end of the serpentine condenser and separator Connection, the condenser pipe water inlet are located at the lower half of serpentine condenser, and the water outlet of the condenser pipe is located at serpentine condenser The first half.
As a further improvement of the above technical scheme, the essential oil hydrosol separator includes that separator body, essential oil go out Mouth, exhaust pipe and hydrosol outlet, the separator body are connected to the lower end of the condenser pipe, and separator body is equipped with bottom Discharge port and side discharge port, the bottom discharge mouth and essential oil outlet, the side discharge port and exhaust pipe and hydrosol Outlet, the exhaust pipe opening upwards, the hydrosol exit opening are downward.
As a further improvement of the above technical scheme, the essential oil exit is equipped with valve.
As a further improvement of the above technical scheme, flask connector, the Liang Kou of the bottleneck of the storage bottle, storage bottle The bore inner wall of the gas outlet of eggplant type flask is equipped with frosting.
As a further improvement of the above technical scheme, the connecting tube is double right-angle elbow pipes.
The beneficial effects of the invention are as follows:
The present invention by will be used as two mouthfuls of eggplant type flasks of steam generator with for house fragrant plant storage bottle it Between sieve plate be set as the spherical porous filter chamber being recessed to storage bottle inner space so that vapor not only can be in operating process The fragrant plant in storage bottle is vertically heated from bottom to top, and can heat fragrant plant to divergence expression, makes two mouthfuls of eggplant type flasks The vapor of middle generation can equably, 360 ° omni-directional without dead angle heat fragrant plant, to substantially increase fragrant plant Essential oil distilling effect, shorten the rectifying time.
The essential oil extraction equipment of the present invention is simple in structure, and operation is simple, safe and efficient, especially suitable for chemical experiment.
Description of the drawings
To describe the technical solutions in the embodiments of the present invention more clearly, make required in being described below to embodiment Attached drawing is briefly described.Obviously, described attached drawing is a part of the embodiment of the present invention, rather than is all implemented Example, those skilled in the art without creative efforts, can also be obtained according to these attached drawings other designs Scheme and attached drawing.
Fig. 1 is the positive structure diagram of the present invention.
Specific implementation mode
The technique effect of the design of the present invention, concrete structure and generation is carried out below with reference to embodiment and attached drawing clear Chu, complete description, to be completely understood by the purpose of the present invention, feature and effect.Obviously, described embodiment is this hair Bright a part of the embodiment, rather than whole embodiments, based on the embodiment of the present invention, those skilled in the art are not being paid The other embodiment obtained under the premise of creative work, belongs to the scope of protection of the invention.In addition, be previously mentioned in text All connection/connection relations not singly refer to component and directly connect, and refer to that can be added deduct according to specific implementation situation by adding Few couple auxiliary, to form more preferably coupling structure.Each technical characteristic in the invention, in not conflicting conflict Under the premise of can be with combination of interactions.
Referring to Fig.1, a kind of chemical experiment vapor water proof distills essential oil extraction equipment comprising two mouthfuls of eggplant type flasks 1, storage Expect that bottle 2, connecting tube 3, condensation and essential oil hydrosol separator 5,2 top of the storage bottle are equipped with bottleneck 21, the storage bottle 2 Bottom is equipped with flask connector, and the spherical porous filter chamber 22 being recessed to storage bottle inner space is equipped at the flask connector, Two mouthfuls of eggplant type flasks 1 are equipped with the fluid infusion 12 positioned at the gas outlet 11 at top and positioned at side, one end of the connecting tube 3 Be connected to the bottleneck 21 of storage bottle 2, the other end of connecting tube 3 is connected to one end of condensation, the condensation it is another End is connected to the essential oil hydrosol separator 5.
Specifically, two mouthfuls of eggplant type flasks 1 in extraction equipment of the invention are used as steam generator, and storage bottle 2 is as virtue The container of fragrant plant, vapor by the spherical porous filter chamber 22 of storage bottle 2 to fragrant plant carry out uniformly, 360 ° omni-directional without Dead angle is heated, to greatly improve the effect of extracting of fragrant plant.The wherein described spherical porous filter chamber 22 compares traditional plane Sieve plate or gauze have the material contact area of bigger, while its setting being recessed to 2 inner space of storage bottle makes storage bottle 2 It is internal it is heated evenly, it is more efficient.
It is further used as preferred embodiment, the spherical porous filter chamber 22 is integrally formed with storage bottle 2.Specifically, It is integrally formed the vapor that setting can be such that two mouthfuls of 1 inside of eggplant type flask generate to be all introduced into storage bottle 2, effectively improves water steaming Gas utilization rate.
It is further used as preferred embodiment, the condensation includes serpentine condenser 41, condenser pipe water inlet 42 Be connected to connecting tube 3 with the upper end of condenser pipe water outlet 43, the serpentine condenser 41, the lower end of the serpentine condenser 41 with Essential oil hydrosol separator 5 is connected to, and the condenser pipe water inlet 42 is located at the lower half of serpentine condenser 41, the condenser pipe water outlet Mouth 43 is located at the first half of serpentine condenser 41.Specifically, condensed water continues from condenser pipe water inlet 42 in actual mechanical process It flows into and then the high-temperature vapor containing essential oil is cooled down from the outflow realization of condenser pipe water outlet 43.
It is further used as preferred embodiment, the essential oil hydrosol separator 5 includes separator body 51, essential oil outlet 52, exhaust pipe 53 and hydrosol outlet 54, the separator body 51 is connected to the lower end of the serpentine condenser 41, separator sheet Body 51 is equipped with bottom discharge mouth and side discharge port, and the bottom discharge mouth is connected to essential oil outlet 52, the side discharging Mouth is connected to exhaust pipe 53 and hydrosol outlet 54,53 opening upwards of the exhaust pipe, and Open Side Down for the hydrosol outlet 54.It is practical In operating process, the condensed component vapor after cooling containing essential oil flows into the essential oil hydrosol separator 5, flows through separation Water layer and oil reservoir are respectively formed after device ontology 51, wherein water layer is hydrosol, and oil reservoir is essential oil, and essential oil is gone out by essential oil after the completion of separation Mouth 52 flows out, and hydrosol is by 54 outflow of hydrosol outlet.
It is further used as preferred embodiment, valve is equipped at the essential oil outlet 52.
It is further used as preferred embodiment, the bottleneck 21 of the storage bottle, the flask connector of storage bottle, two mouthfuls of eggplants The bore inner wall of the gas outlet 11 of type flask is equipped with frosting.The frosting is conducive to improve the sealing performance of connection.
It is further used as preferred embodiment, the connecting tube 3 is double right-angle elbow pipes.
The better embodiment of the present invention is illustrated above, but the invention is not limited to the implementation Example, those skilled in the art can also make various equivalent modifications or be replaced under the premise of without prejudice to spirit of that invention It changes, these equivalent modifications or replacement are all contained in the application claim limited range.

Claims (7)

1. a kind of chemical experiment vapor water proof distills essential oil extraction equipment, it is characterised in that:Including two mouthfuls of eggplant type flasks, storings Bottle, connecting tube, condensation and essential oil hydrosol separator, the storage bottle top are equipped with bottleneck, and the storage bottle bottom is equipped with Flask connector is equipped with the spherical porous filter chamber being recessed to storage bottle inner space, two mouthfuls of eggplants at the flask connector Type flask is equipped with the fluid infusion positioned at the gas outlet at top and positioned at side, and one end of the connecting tube and the bottleneck of storage bottle connect Logical, the other end of connecting tube is connected to one end of condensation, and the other end of the condensation is detached with the essential oil hydrosol Device is connected to.
2. a kind of chemical experiment vapor water proof according to claim 1 distills essential oil extraction equipment, it is characterised in that:Institute Spherical porous filter chamber is stated to be integrally formed with storage bottle.
3. a kind of chemical experiment vapor water proof according to claim 1 distills essential oil extraction equipment, it is characterised in that:Institute It includes serpentine condenser, condenser pipe water inlet and condenser pipe water outlet to state condensation, the upper end of the serpentine condenser and company Connection is taken over, the lower end of the serpentine condenser is connected to separator, and the condenser pipe water inlet is located under serpentine condenser The water outlet of half portion, the condenser pipe is located at the first half of serpentine condenser.
4. a kind of chemical experiment vapor water proof according to claim 1 distills essential oil extraction equipment, it is characterised in that:Institute State essential oil hydrosol separator include separator body, essential oil outlet, exhaust pipe and hydrosol outlet, the separator body with it is described The lower end of condenser pipe is connected to, and separator body is equipped with bottom discharge mouth and side discharge port, the bottom discharge mouth and essential oil Outlet, the side discharge port and exhaust pipe and hydrosol outlet, the exhaust pipe opening upwards, the hydrosol outlet Open Side Down.
5. a kind of chemical laboratory vapor water proof according to claim 4 distills essential oil extraction equipment, it is characterised in that: The essential oil exit is equipped with valve.
6. a kind of chemical laboratory vapor water proof according to claim 1 distills essential oil extraction equipment, it is characterised in that: The bore inner wall of the gas outlet of the bottleneck of the storage bottle, the flask connector of storage bottle, two mouthfuls of eggplant type flasks is equipped with frosted Face.
7. a kind of chemical laboratory vapor water proof according to claim 1 distills essential oil extraction equipment, it is characterised in that: The connecting tube is double right-angle elbow pipes.
CN201810650320.XA 2018-06-21 2018-06-21 A kind of chemical experiment vapor water proof distillation essential oil extraction equipment Pending CN108587792A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI693027B (en) * 2019-10-28 2020-05-11 嘉藥學校財團法人嘉南藥理大學 Smell preservation device
CN114854492A (en) * 2022-05-19 2022-08-05 河北中烟工业有限责任公司 Device for extracting fragrant component from perfume

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202161826U (en) * 2011-06-30 2012-03-14 何节玉 Novel steam distillation experimental facility
CN202284201U (en) * 2011-09-22 2012-06-27 陇东学院 Rapid extraction instrument of trace volatile oil of ground openings
WO2014116143A1 (en) * 2013-01-25 2014-07-31 Novikov Oleg Nikolaevich Apparatus for processing essential oil raw material
CN204689970U (en) * 2015-05-29 2015-10-07 张杨 The parallel extraction element of distillation plants essential oil and hydrosol
CN105273845A (en) * 2014-07-16 2016-01-27 上海禾汽玻璃仪器有限公司 Rose oil distillation purification unit
CN205223176U (en) * 2015-11-26 2016-05-11 四川省宜宾市天坛酒业有限责任公司 Novel wine brewing and distilling device
CN105713726A (en) * 2016-03-31 2016-06-29 李颖 Method and device for rapidly extracting natural plant essential oil and hydrolat without solvents
CN205501258U (en) * 2016-03-31 2016-08-24 李颖 Preparation facilities of microwave gravity extraction natural fibre essential oil and pure dew
CN106281701A (en) * 2016-08-17 2017-01-04 上海清轩生物科技有限公司 Essential oil extraction device and plants essential oil extracting method
CN107930173A (en) * 2017-11-27 2018-04-20 成都市阿李科技有限公司 A kind of alembic
CN207276584U (en) * 2017-09-27 2018-04-27 昆明市农业机械化技术学校 A kind of fragrant plant hydrosol extraction of essential oil system

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202161826U (en) * 2011-06-30 2012-03-14 何节玉 Novel steam distillation experimental facility
CN202284201U (en) * 2011-09-22 2012-06-27 陇东学院 Rapid extraction instrument of trace volatile oil of ground openings
WO2014116143A1 (en) * 2013-01-25 2014-07-31 Novikov Oleg Nikolaevich Apparatus for processing essential oil raw material
CN105273845A (en) * 2014-07-16 2016-01-27 上海禾汽玻璃仪器有限公司 Rose oil distillation purification unit
CN204689970U (en) * 2015-05-29 2015-10-07 张杨 The parallel extraction element of distillation plants essential oil and hydrosol
CN205223176U (en) * 2015-11-26 2016-05-11 四川省宜宾市天坛酒业有限责任公司 Novel wine brewing and distilling device
CN105713726A (en) * 2016-03-31 2016-06-29 李颖 Method and device for rapidly extracting natural plant essential oil and hydrolat without solvents
CN205501258U (en) * 2016-03-31 2016-08-24 李颖 Preparation facilities of microwave gravity extraction natural fibre essential oil and pure dew
CN106281701A (en) * 2016-08-17 2017-01-04 上海清轩生物科技有限公司 Essential oil extraction device and plants essential oil extracting method
CN207276584U (en) * 2017-09-27 2018-04-27 昆明市农业机械化技术学校 A kind of fragrant plant hydrosol extraction of essential oil system
CN107930173A (en) * 2017-11-27 2018-04-20 成都市阿李科技有限公司 A kind of alembic

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI693027B (en) * 2019-10-28 2020-05-11 嘉藥學校財團法人嘉南藥理大學 Smell preservation device
CN114854492A (en) * 2022-05-19 2022-08-05 河北中烟工业有限责任公司 Device for extracting fragrant component from perfume

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Application publication date: 20180928

RJ01 Rejection of invention patent application after publication