CN108559655A - 一种超浓缩洗衣液及其制备方法 - Google Patents

一种超浓缩洗衣液及其制备方法 Download PDF

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CN108559655A
CN108559655A CN201810585252.3A CN201810585252A CN108559655A CN 108559655 A CN108559655 A CN 108559655A CN 201810585252 A CN201810585252 A CN 201810585252A CN 108559655 A CN108559655 A CN 108559655A
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陈圆圆
毛建林
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Compaq Technology (suzhou) Co Ltd
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    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
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    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
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    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
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    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38618—Protease or amylase in liquid compositions only
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
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    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
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    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
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    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
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Abstract

本发明公开了一种超浓缩洗衣液及其制备方法，所述超浓缩洗衣液的各原料及其重量份数配比为：水20‑40份、椰油酸钾10‑20份、非离子表面活性剂40‑70份、椰油酰胺DEA 1‑5份、丙二醇1‑5份、蛋白酶0.1‑1份、纤维素酶0.1‑1份、EDTA 0.1‑1份、柠檬酸0.1‑1份、防腐剂0.1‑1份、香精0.1‑1份；该超浓缩洗衣液制备方法首先按配比量称量各原料，再将称量的原料水、椰油酸钾、非离子表面活性剂、椰油酰胺DEA和丙二醇加入乳化锅内混合，搅拌并升温至80‑85℃，保温搅拌至完全溶解；再降温；待混合液降温至45℃以下后依次加入称量的原料蛋白酶、纤维素酶、EDTA、柠檬酸、防腐剂和香精，搅拌均匀；最后检验混合液是否符合要求，符合后过滤、出料，完成超浓缩洗衣液的制备。

Description

一种超浓缩洗衣液及其制备方法
技术领域
本发明属于日用化工产品技术领域，尤其涉及一种超浓缩洗衣液及其制备方法。
背景技术
洗衣液作为洗涤用品，比洗衣粉等传统洗涤用品使用方便，节能、生物降解性好，洗涤残留少，且不伤手，具有洗护合一的多重功能，为越来越多的家庭认可并接受。虽然洗衣液洗涤效果好、优点多，但市售的普通洗衣液仅15％-17％有效物含量，单次洗涤普通洗衣液的耗量相对较多，这导致目前市场洗衣液都采用大瓶包装，占空间，运输成本高，不利于家庭存放，大瓶洗衣液同时也导致了市场弊端的日趋凸显，浓缩洗衣液和超浓缩洗衣液的出现是洗涤剂市场发展的大趋势。
发明内容
本发明所要解决的技术问题是：提供一种超浓缩洗衣液及其制备方法，缓解了瓶洗衣液带来的市场弊端，清洗相同量衣服使用量少，低泡易过水，节水更环保；
为了达到上述技术效果，本发明采用的技术方案是：
一种超浓缩洗衣液，所述洗衣液的各原料及其重量份数配比如下：
进一步地，所述洗衣液的各原料及其重量份数如下：
进一步地，所述非离子表面活性剂为异构脂肪醇聚醚。
一种超浓缩洗衣液的制备方法，该制备方法包括如下的工艺步骤：
S1.按照配方量称量各原料；
S2.将称量的原料水、椰油酸钾、非离子表面活性剂、椰油酰胺DEA和丙二醇加入乳化锅内混合，搅拌并升温至80-85℃，保温搅拌至完全溶解；
S3.将完全溶解后的混合液降温；
S4.待混合液降温至45℃以下后依次加入称量的原料蛋白酶、纤维素酶、EDTA、柠檬酸、防腐剂和香精，搅拌均匀；
S5.检验经过步骤S4搅拌均匀后的混合液是否符合要求，符合要求后过滤、出料，完成超浓缩洗衣液的制备。
进一步地，所述步骤S2中的搅拌速度为15r/min。
与现有技术相比，本发明的有益效果是：
1)传统浓缩洗衣液有效物含量为25-30％；本发明的超浓缩洗衣液有效物含量达到60％以上，极低用量即可达到理想去污效果，节能、环保。
2)配方通过合理的原料比例搭配，在低温5℃时仍有较好流动性；有效解决了50％有效物含量以上洗衣液低温果冻现象，使用更方便。
具体实施方式
下面结合实施例对本发明做进一步详细说明：
一种超浓缩洗衣液，其各原料及其重量份数配比为：水20-40份、椰油酸钾10-20份、异构脂肪醇聚醚40-70份、椰油酰胺DEA 1-5份、丙二醇1-5份、蛋白酶0.1-1份、纤维素酶0.1-1份、EDTA 0.1-1份、柠檬酸0.1-1份、防腐剂0.1-1份、香精0.1-1份。作为优选，水30份、椰油酸钾15份、异构脂肪醇聚醚60份、椰油酰胺DEA4份、丙二醇3份、蛋白酶0.6份、纤维素酶0.6份、EDTA 0.6份、柠檬酸0.4份、防腐剂0.5份、香精0.5份。该超浓缩洗衣液制备方法是首先按配比量称量各原料，再将称量的原料水、椰油酸钾、非离子表面活性剂、椰油酰胺DEA和丙二醇加入乳化锅内混合，以15r/min的搅拌速度搅拌并升温至80-85℃，保温搅拌至完全溶解；再将完全溶解的混合液降温；待混合液降温至45℃以下后依次加入称量的原料蛋白酶、纤维素酶、EDTA、柠檬酸、防腐剂和香精，搅拌均匀；最后检验混合液是否符合要求，符合后过滤、出料，即完成超浓缩洗衣液的制备。
本发明制备的超浓缩洗衣液的超浓缩有效物含量达到60％以上；极低用量即可达到理想去污效果，低泡且易过水，节水更环保；配方通过合理的原料比例搭配，在低温5℃时仍有较好流动性；而非离子表面活性剂异构脂肪醇聚醚作为主要成分，更能有效解决了50％有效物含量以上洗衣液低温果冻现象，使用更方便。
本发明不局限于上述具体的实施方式，对于本领域的普通技术人员来说从上述构思出发，不经过创造性的劳动，所作出的种种变换，均落在本发明的保护范围之内。

Claims (5)

1.一种超浓缩洗衣液，其特征在于，所述洗衣液的各原料及其重量份数配比如下：
2.如权利要求1所述的超浓缩洗衣液，其特征在于，所述洗衣液的各原料及其重量份数如下：
3.如权利要求1或2所述的一种超浓缩洗衣液，其特征在于，所述非离子表面活性剂为异构脂肪醇聚醚。
4.一种如权利要求1或2所述的超浓缩洗衣液的制备方法，其特征在于，该制备方法包括如下的工艺步骤：
S1.按照配方量称量各原料；
S2.将称量的原料水、椰油酸钾、非离子表面活性剂、椰油酰胺DEA和丙二醇加入乳化锅内混合，搅拌并升温至80-85℃，保温搅拌至完全溶解；
S3.将完全溶解后的混合液降温；
S4.待混合液降温至45℃以下后依次加入称量的原料蛋白酶、纤维素酶、EDTA、
柠檬酸、防腐剂和香精，搅拌均匀；
S5.检验经过步骤S4搅拌均匀后的混合液是否符合要求，符合要求后过滤、出料，完成超浓缩洗衣液的制备。
5.如权利要求4所述的超浓缩洗衣液的制备方法，其特征在于，所述步骤S2中的搅拌速度为15r/min。
CN201810585252.3A 2018-06-08 2018-06-08 一种超浓缩洗衣液及其制备方法 Pending CN108559655A (zh)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109504572A (zh) * 2019-01-07 2019-03-22 江南大学 一种超高浓缩型洗衣液制作配方及工艺
CN110982645A (zh) * 2019-12-18 2020-04-10 苏州东方之宝生物药业有限公司 一种洗衣皂液的配方及其生产工艺

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102242022A (zh) * 2011-06-15 2011-11-16 于文 环保型超浓缩生物酶洗衣液及其制备方法
CN102918142A (zh) * 2010-06-03 2013-02-06 荷兰联合利华有限公司 洗衣洗涤剂组合物
CN103275829A (zh) * 2013-06-17 2013-09-04 纳爱斯集团有限公司 一种不含溶剂的超浓缩洗衣液及其制备方法
CN104673521A (zh) * 2013-11-27 2015-06-03 常州校果信息服务有限公司 一种超浓缩洗衣液
CN105062703A (zh) * 2015-07-27 2015-11-18 东莞市香与化工有限公司 一种蛋白酶超浓缩洗衣液及其制备方法
CN106318678A (zh) * 2016-07-25 2017-01-11 广州普爱生物科技有限公司 无水无防腐剂无酒精的蛋白酶超浓缩洗衣液

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102918142A (zh) * 2010-06-03 2013-02-06 荷兰联合利华有限公司 洗衣洗涤剂组合物
CN102242022A (zh) * 2011-06-15 2011-11-16 于文 环保型超浓缩生物酶洗衣液及其制备方法
CN103275829A (zh) * 2013-06-17 2013-09-04 纳爱斯集团有限公司 一种不含溶剂的超浓缩洗衣液及其制备方法
CN104673521A (zh) * 2013-11-27 2015-06-03 常州校果信息服务有限公司 一种超浓缩洗衣液
CN105062703A (zh) * 2015-07-27 2015-11-18 东莞市香与化工有限公司 一种蛋白酶超浓缩洗衣液及其制备方法
CN106318678A (zh) * 2016-07-25 2017-01-11 广州普爱生物科技有限公司 无水无防腐剂无酒精的蛋白酶超浓缩洗衣液

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109504572A (zh) * 2019-01-07 2019-03-22 江南大学 一种超高浓缩型洗衣液制作配方及工艺
CN109504572B (zh) * 2019-01-07 2021-02-26 江南大学 一种超高浓缩型洗衣液制作配方及工艺
CN110982645A (zh) * 2019-12-18 2020-04-10 苏州东方之宝生物药业有限公司 一种洗衣皂液的配方及其生产工艺

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