CN108542938A - Antiseptic - Google Patents
Antiseptic Download PDFInfo
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- CN108542938A CN108542938A CN201810475053.7A CN201810475053A CN108542938A CN 108542938 A CN108542938 A CN 108542938A CN 201810475053 A CN201810475053 A CN 201810475053A CN 108542938 A CN108542938 A CN 108542938A
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- 230000002421 anti-septic effect Effects 0.000 title claims abstract description 45
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000008213 purified water Substances 0.000 claims abstract description 26
- JBIROUFYLSSYDX-UHFFFAOYSA-M benzododecinium chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 JBIROUFYLSSYDX-UHFFFAOYSA-M 0.000 claims abstract description 21
- 235000009024 Ceanothus sanguineus Nutrition 0.000 claims abstract description 20
- 235000004204 Foeniculum vulgare Nutrition 0.000 claims abstract description 20
- QQILFGKZUJYXGS-UHFFFAOYSA-N Indigo dye Chemical compound C1=CC=C2C(=O)C(C3=C(C4=CC=CC=C4N3)O)=NC2=C1 QQILFGKZUJYXGS-UHFFFAOYSA-N 0.000 claims abstract description 20
- 240000003553 Leptospermum scoparium Species 0.000 claims abstract description 20
- 235000015459 Lycium barbarum Nutrition 0.000 claims abstract description 20
- 240000002853 Nelumbo nucifera Species 0.000 claims abstract description 20
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims abstract description 20
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims abstract description 20
- 241000951473 Schizonepeta Species 0.000 claims abstract description 20
- 235000011187 glycerol Nutrition 0.000 claims abstract description 20
- 240000007673 Origanum vulgare Species 0.000 claims abstract description 19
- 235000004383 Origanum vulgare subsp. vulgare Nutrition 0.000 claims abstract description 19
- 239000000341 volatile oil Substances 0.000 claims abstract description 19
- 244000178231 Rosmarinus officinalis Species 0.000 claims abstract description 14
- 240000006927 Foeniculum vulgare Species 0.000 claims abstract 4
- 239000003814 drug Substances 0.000 claims description 44
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 36
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 18
- 239000001569 carbon dioxide Substances 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 17
- 229920002690 Polyoxyl 40 HydrogenatedCastorOil Polymers 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 238000000605 extraction Methods 0.000 claims description 5
- 235000004443 Ricinus communis Nutrition 0.000 claims description 2
- 238000001704 evaporation Methods 0.000 claims description 2
- 230000008020 evaporation Effects 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims description 2
- 239000003921 oil Substances 0.000 claims description 2
- 239000006228 supernatant Substances 0.000 claims description 2
- 240000008821 Menyanthes trifoliata Species 0.000 claims 1
- 229940079593 drug Drugs 0.000 claims 1
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 15
- 230000001954 sterilising effect Effects 0.000 abstract description 9
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 6
- 230000003385 bacteriostatic effect Effects 0.000 abstract description 5
- 208000003251 Pruritus Diseases 0.000 abstract description 3
- 230000002159 abnormal effect Effects 0.000 abstract description 3
- 230000003110 anti-inflammatory effect Effects 0.000 abstract description 3
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- 230000007803 itching Effects 0.000 abstract description 2
- 241000212314 Foeniculum Species 0.000 description 16
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 8
- 239000002994 raw material Substances 0.000 description 8
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- 241000588724 Escherichia coli Species 0.000 description 6
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- 229940095731 candida albicans Drugs 0.000 description 6
- 238000005119 centrifugation Methods 0.000 description 6
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- 235000013599 spices Nutrition 0.000 description 6
- 230000003020 moisturizing effect Effects 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 230000001139 anti-pruritic effect Effects 0.000 description 4
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- 206010035664 Pneumonia Diseases 0.000 description 2
- 239000004359 castor oil Substances 0.000 description 2
- 235000019438 castor oil Nutrition 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- -1 ethyl vanillin aldehydes Chemical class 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000001408 fungistatic effect Effects 0.000 description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
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- 238000012986 modification Methods 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 229920002101 Chitin Polymers 0.000 description 1
- 241000305071 Enterobacterales Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 206010067268 Post procedural infection Diseases 0.000 description 1
- 241000235342 Saccharomycetes Species 0.000 description 1
- 241000607764 Shigella dysenteriae Species 0.000 description 1
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical class [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 241000191940 Staphylococcus Species 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 206010048038 Wound infection Diseases 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 229940064004 antiseptic throat preparations Drugs 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 239000000022 bacteriostatic agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
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- 238000001816 cooling Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 229940073505 ethyl vanillin Drugs 0.000 description 1
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Natural products CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 229930003658 monoterpene Natural products 0.000 description 1
- 150000002773 monoterpene derivatives Chemical class 0.000 description 1
- 235000002577 monoterpenes Nutrition 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000002980 postoperative effect Effects 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 239000010668 rosemary oil Substances 0.000 description 1
- 229940058206 rosemary oil Drugs 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 229940007046 shigella dysenteriae Drugs 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 238000010200 validation analysis Methods 0.000 description 1
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 1
Classifications
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- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/704—Polygonum, e.g. knotweed
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- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
- A61K31/047—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates having two or more hydroxy groups, e.g. sorbitol
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- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
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- A61K2236/30—Extraction of the material
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Abstract
The invention discloses antibacterial anti-inflammatory technical fields, specific field is antiseptic, the antiseptic is grouped as by the group of following parts by weight, 30~40 parts of granatum, 22~32 parts of kuh-seng, 20~30 parts of lotus leaf, 17~27 parts of elscholtiza, 15~25 parts of schizonepeta, 15~25 parts of wild marjoram, 13~23 parts of mountain fennel, 10~20 parts of indigo naturalis, 10~20 parts of rosemary, 20~30 parts of glycerine, 15~25 parts of 40 rilanit specials of PEG, 2~5 parts of dodecyl benzyl dimethyl ammonium chloride, 0.5~2 part of tea tree ethereal oil, 55~65 parts of purified water, it can be with quick sterilization by using antiseptic, long-acting bacteriostatic, it is clearing heat and detoxicating, dispelling wind and arresting itching, dispelling abnormal flavor and moisten it is non-stimulated.
Description
Technical field
The present invention relates to antibacterial anti-inflammatory technical field, specific field is antiseptic.
Background technology
Antiseptic is to refer within a certain period of time, make certain micro-organisms (fungi, bacterium, saccharomycete, algae and virus
Deng) growth or breeding be maintained at necessary chemical substance below horizontal, there is antibacterial and bactericidal property substance or product,
Antiseptic is generally divided into inorganic antiseptic, organic antibacterial agent and natural antibacterial agent, and inorganic antiseptic is mainly silver ion class antibacterial
Agent, advantage is safe, but manufacturing process of high cost is complicated；Organic antibacterial agent is generally vanillic aldehyde or ethyl vanillin aldehydes
Close object, advantage is that sterilization is rapid, and sterilizing ability is strong, but the short easy decomposition of the term of validity and safety it is not completely clear；Natural antibacterial
Agent is mainly chitin, castor oil etc., and advantage uses simplicity, safe, but antibacterial action is limited, and sterilizing rate is low.Existing day
The fungistatic effect of right antiseptic is limited, and the organic antibacterial agent term of validity is short and safety is unable to get guarantee, for this purpose, the present invention carries
Go out a kind of antiseptic, safe low concentration chemistry antibacterial substance is combined with traditional Chinese medicine extraction so that bacteriostatic agent is quickly antibacterial, long-acting suppression
Bacterium.
Invention content
The purpose of the present invention is to provide antiseptics, to solve the problems mentioned in the above background technology.
To achieve the above object, the present invention provides the following technical solutions：Antiseptic, it is characterised in that：The antiseptic by
Following components forms：
Granatum, kuh-seng, lotus leaf, elscholtiza, schizonepeta, wild marjoram, mountain fennel, indigo naturalis, rosemary, glycerine, PEG-40 hydrogenate castor
Sesame oil, dodecyl benzyl dimethyl ammonium chloride, tea tree ethereal oil, purified water.
Preferably, the antiseptic is made of following parts by weight：
30~40 parts of granatum, 22~32 parts of kuh-seng, 20~30 parts of lotus leaf, 17~27 parts of elscholtiza, 15~25 parts of schizonepeta, ox
It is hydrogenated to 15~25 parts, 13~23 parts of mountain fennel, 10~20 parts of indigo naturalis, 10~20 parts of rosemary, 20~30 parts of glycerine, PEG-40
15~25 parts of castor oil, 2~5 parts of dodecyl benzyl dimethyl ammonium chloride, 0.5~2 part of tea tree ethereal oil, purified water 55~65
Part.
Preferably, the preparation method of the antiseptic includes the following steps：
1) it uses medicinal herb grinder to crush kuh-seng, elscholtiza, mountain fennel, rosemary, crosses 40 mesh sieve, obtain herb powder A,
Herb powder A is positioned in supercritical carbon dioxide extracting kettle, it is extracted by carbon dioxide, carbon dioxide is passed through
Flow velocity is 18~25 ls/h, and extracting pressure is 15~30 megapascal, and extraction temperature is 35~50 degrees Celsius, and extraction makes after 1 hour
It is centrifuged with centrifuge, takes supernatant, obtain Chinese medicine stoste A, it is spare；
2) it uses medicinal herb grinder to crush granatum, lotus leaf, schizonepeta, wild marjoram, indigo naturalis, crosses 40 mesh sieve, obtain traditional Chinese medicine powder
The purified water of 10 times of volumes is added into herb powder B by last B, after impregnating 1 hour, is decocted 2 hours, is decocted using micro-pressure medicine decocting machine
It is 3 times to boil number, filters merging filtrate, is concentrated by evaporation, and Chinese medicine stoste B is obtained, spare；
3) glycerine water-bath is heated to 45~65 degrees Celsius, Chinese medicine stoste A, Chinese medicine stoste B and tea tree essence is added thereto
Oil is sufficiently mixed, and cools the temperature to 35~45 degrees Celsius, and dodecyl benzyl dimethyl ammonium chloride is added into mixture, is used
Blender is constantly stirred, it is made to be sufficiently mixed, and Cremophor RH40 is added and at the uniform velocity stirs, obtains mixed liquor, is added
Purified water stirs evenly, and obtains antiseptic.
Compared with prior art, the beneficial effects of the invention are as follows：Antiseptic, the present invention will have suppression using Chinese medicine as raw material
The Chinese medical extract of bacterium antibacterial and the chemical antibacterial substance of safe low concentration are compounded, and there is raw material to be easy to get, be formulated rationally, soon
Speed sterilization, long-acting bacteriostatic and mild non-stimulated advantage, granatum have preferable restraining and sterilizing bacteria effect to Pseudomonas aeruginosa, can be pre-
Prevent postoperative and wound infection；Mountain fennel has monoterpene and terpene alcohol compound and volatile alkaloid isoreactivity ingredient, to golden yellow
Staphylococcus, Diplococcus pneumopniae, Escherichia coli, shigella dysenteriae, Pseudomonas aeruginosa have to be acted on compared with high inhibition；Wild marjoram is natural antibiosis
Element, can flu-prevention, bactericidal；In addition elscholtiza and kuh-seng also have preferable anti-inflammatory fungistatic effect；Dodecyl dimethyl
Benzyl ammonium chloride is cationic surfactant, and dodecyl benzyl dimethyl ammonium chloride is non oxidizing bactericide, is had
The ability of broad-spectrum high efficacy sterilization algae removal, lotus leaf, schizonepeta and indigo naturalis have the effect of clearing heat and detoxicating, wind-dispelling blood-cooling itch-relieving；Rosemary is
Excellent anti-oxidation characteristics oxidant, Rosemary Oil has effects that tranquilizing and allaying excitement, refreshes the mind and disinfection；Tea tree ethereal oil can
Dispelling abnormal flavor；Glycerine has preferable moisturizing effect.By using antiseptic can with quick sterilization, long-acting bacteriostatic, it is clearing heat and detoxicating,
Dispelling wind and arresting itching, dispelling abnormal flavor and moisten it is non-stimulated.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme of the present invention is clearly and completely described, it is clear that institute
The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention,
Every other embodiment obtained by those of ordinary skill in the art without making creative efforts, belongs to this hair
The range of bright protection.
Embodiment 1：
Antiseptic is made of the raw material of following weight grams：30 grams of granatum, 22 grams of kuh-seng, 20 grams of lotus leaf, 17 grams of elscholtiza,
15 grams of schizonepeta, 15 grams of wild marjoram, 13 grams of mountain fennel, 10 grams of indigo naturalis, 10 grams of rosemary, 20 grams of glycerine, Cremophor RH40 15
Gram, 2 grams of dodecyl benzyl dimethyl ammonium chloride, 0.5 gram of tea tree ethereal oil, 55 grams of purified water.
The preparation process of antiseptic：Use the kuh-seng of 40 mesh of supercritical carbon dioxide extracting kettle pair, elscholtiza, mountain fennel, fan
Repeatedly perfume (or spice) is extracted, 18 ls/h of carbon dioxide flow rate, 15 megapascal of extracting pressure, is extracted 1 hour under 35 degrees Celsius, and centrifugation obtains
Obtain Chinese medicine stoste A；
The granatum of 40 mesh, lotus leaf, schizonepeta, wild marjoram, indigo naturalis powder are immersed in the purified water of 10 times of volumes 1 hour,
It is decocted 2 hours using micro-pressure medicine decocting machine, decocts number 3 times, filtered, concentration obtains Chinese medicine stoste B；
Glycerine water-bath is heated to 45 degrees Celsius, it is abundant that Chinese medicine stoste A, Chinese medicine stoste B and tea tree ethereal oil are added thereto
Mixing, cools the temperature to 35 degrees Celsius, dodecyl benzyl dimethyl ammonium chloride is added into mixture, continuous using blender
It is stirred, it is made to be sufficiently mixed, Cremophor RH40 is added and at the uniform velocity stirs, obtains mixed liquor, purified water stirring is added
Uniformly, antiseptic is obtained.
Embodiment 2：
Antiseptic is made of the raw material of following weight grams：32 grams of granatum, 24 grams of kuh-seng, 22 grams of lotus leaf, 19 grams of elscholtiza,
17 grams of schizonepeta, 17 grams of wild marjoram, 15 grams of mountain fennel, 12 grams of indigo naturalis, 12 grams of rosemary, 22 grams of glycerine, Cremophor RH40 17
Gram, 3 grams of dodecyl benzyl dimethyl ammonium chloride, 0.8 gram of tea tree ethereal oil, 57 grams of purified water.
The preparation process of antiseptic：Use the kuh-seng of 40 mesh of supercritical carbon dioxide extracting kettle pair, elscholtiza, mountain fennel, fan
Repeatedly perfume (or spice) is extracted, 20 ls/h of carbon dioxide flow rate, 18 megapascal of extracting pressure, is extracted 1 hour under 38 degrees Celsius, and centrifugation obtains
Obtain Chinese medicine stoste A；
The granatum of 40 mesh, lotus leaf, schizonepeta, wild marjoram, indigo naturalis powder are immersed in the purified water of 10 times of volumes 1 hour,
It is decocted 2 hours using micro-pressure medicine decocting machine, decocts number 3 times, filtered, concentration obtains Chinese medicine stoste B；
Glycerine water-bath is heated to 49 degrees Celsius, it is abundant that Chinese medicine stoste A, Chinese medicine stoste B and tea tree ethereal oil are added thereto
Mixing, cools the temperature to 37 degrees Celsius, dodecyl benzyl dimethyl ammonium chloride is added into mixture, continuous using blender
It is stirred, it is made to be sufficiently mixed, Cremophor RH40 is added and at the uniform velocity stirs, obtains mixed liquor, purified water stirring is added
Uniformly, antiseptic is obtained.
Embodiment 3：
Antiseptic is made of the raw material of following weight grams：34 grams of granatum, 26 grams of kuh-seng, 24 grams of lotus leaf, 21 grams of elscholtiza,
19 grams of schizonepeta, 19 grams of wild marjoram, 17 grams of mountain fennel, 14 grams of indigo naturalis, 14 grams of rosemary, 24 grams of glycerine, Cremophor RH40 19
Gram, 3.5 grams of dodecyl benzyl dimethyl ammonium chloride, 1.1 grams of tea tree ethereal oil, 59 grams of purified water.
The preparation process of antiseptic：Use the kuh-seng of 40 mesh of supercritical carbon dioxide extracting kettle pair, elscholtiza, mountain fennel, fan
Repeatedly perfume (or spice) is extracted, 22 ls/h of carbon dioxide flow rate, 23 megapascal of extracting pressure, is extracted 1 hour under 42 degrees Celsius, and centrifugation obtains
Obtain Chinese medicine stoste A；
The granatum of 40 mesh, lotus leaf, schizonepeta, wild marjoram, indigo naturalis powder are immersed in the purified water of 10 times of volumes 1 hour,
It is decocted 2 hours using micro-pressure medicine decocting machine, decocts number 3 times, filtered, concentration obtains Chinese medicine stoste B；
Glycerine water-bath is heated to 53 degrees Celsius, it is abundant that Chinese medicine stoste A, Chinese medicine stoste B and tea tree ethereal oil are added thereto
Mixing, cools the temperature to 39 degrees Celsius, dodecyl benzyl dimethyl ammonium chloride is added into mixture, continuous using blender
It is stirred, it is made to be sufficiently mixed, Cremophor RH40 is added and at the uniform velocity stirs, obtains mixed liquor, purified water stirring is added
Uniformly, antiseptic is obtained.
Embodiment 4：
Antiseptic is made of the raw material of following weight grams：36 grams of granatum, 28 grams of kuh-seng, 26 grams of lotus leaf, 23 grams of elscholtiza,
21 grams of schizonepeta, 21 grams of wild marjoram, 19 grams of mountain fennel, 16 grams of indigo naturalis, 16 grams of rosemary, 26 grams of glycerine, Cremophor RH40 21
Gram, 3.9 grams of dodecyl benzyl dimethyl ammonium chloride, 1.4 grams of tea tree ethereal oil, 61 grams of purified water.
The preparation process of antiseptic：Use the kuh-seng of 40 mesh of supercritical carbon dioxide extracting kettle pair, elscholtiza, mountain fennel, fan
Repeatedly perfume (or spice) is extracted, 23 ls/h of carbon dioxide flow rate, 26 megapascal of extracting pressure, is extracted 1 hour under 45 degrees Celsius, and centrifugation obtains
Obtain Chinese medicine stoste A；
The granatum of 40 mesh, lotus leaf, schizonepeta, wild marjoram, indigo naturalis powder are immersed in the purified water of 10 times of volumes 1 hour,
It is decocted 2 hours using micro-pressure medicine decocting machine, decocts number 3 times, filtered, concentration obtains Chinese medicine stoste B；
Glycerine water-bath is heated to 58 degrees Celsius, it is abundant that Chinese medicine stoste A, Chinese medicine stoste B and tea tree ethereal oil are added thereto
Mixing, cools the temperature to 41 degrees Celsius, dodecyl benzyl dimethyl ammonium chloride is added into mixture, continuous using blender
It is stirred, it is made to be sufficiently mixed, Cremophor RH40 is added and at the uniform velocity stirs, obtains mixed liquor, purified water stirring is added
Uniformly, antiseptic is obtained.
Embodiment 5：
Antiseptic is made of the raw material of following weight grams：38 grams of granatum, 30 grams of kuh-seng, 28 grams of lotus leaf, 25 grams of elscholtiza,
23 grams of schizonepeta, 23 grams of wild marjoram, 21 grams of mountain fennel, 18 grams of indigo naturalis, 18 grams of rosemary, 28 grams of glycerine, Cremophor RH40 23
Gram, 4.5 grams of dodecyl benzyl dimethyl ammonium chloride, 1.7 grams of tea tree ethereal oil, 63 grams of purified water.
The preparation process of antiseptic：Use the kuh-seng of 40 mesh of supercritical carbon dioxide extracting kettle pair, elscholtiza, mountain fennel, fan
Repeatedly perfume (or spice) is extracted, 24 ls/h of carbon dioxide flow rate, 28 megapascal of extracting pressure, is extracted 1 hour under 47 degrees Celsius, and centrifugation obtains
Obtain Chinese medicine stoste A；
The granatum of 40 mesh, lotus leaf, schizonepeta, wild marjoram, indigo naturalis powder are immersed in the purified water of 10 times of volumes 1 hour,
It is decocted 2 hours using micro-pressure medicine decocting machine, decocts number 3 times, filtered, concentration obtains Chinese medicine stoste B；
Glycerine water-bath is heated to 62 degrees Celsius, it is abundant that Chinese medicine stoste A, Chinese medicine stoste B and tea tree ethereal oil are added thereto
Mixing, cools the temperature to 43 degrees Celsius, dodecyl benzyl dimethyl ammonium chloride is added into mixture, continuous using blender
It is stirred, it is made to be sufficiently mixed, Cremophor RH40 is added and at the uniform velocity stirs, obtains mixed liquor, purified water stirring is added
Uniformly, antiseptic is obtained.
Embodiment 6：
Antiseptic is made of the raw material of following weight grams：40 grams of granatum, 32 grams of kuh-seng, 30 grams of lotus leaf, 27 grams of elscholtiza,
25 grams of schizonepeta, 25 grams of wild marjoram, 23 grams of mountain fennel, 20 grams of indigo naturalis, 20 grams of rosemary, 30 grams of glycerine, Cremophor RH40 25
Gram, 5 grams of dodecyl benzyl dimethyl ammonium chloride, 2 grams of tea tree ethereal oil, 65 grams of purified water.
The preparation process of antiseptic：Use the kuh-seng of 40 mesh of supercritical carbon dioxide extracting kettle pair, elscholtiza, mountain fennel, fan
Repeatedly perfume (or spice) is extracted, 24 ls/h of carbon dioxide flow rate, 30 megapascal of extracting pressure, is extracted 1 hour under 50 degrees Celsius, and centrifugation obtains
Obtain Chinese medicine stoste A；
The granatum of 40 mesh, lotus leaf, schizonepeta, wild marjoram, indigo naturalis powder are immersed in the purified water of 10 times of volumes 1 hour,
It is decocted 2 hours using micro-pressure medicine decocting machine, decocts number 3 times, filtered, concentration obtains Chinese medicine stoste B；
Glycerine water-bath is heated to 65 degrees Celsius, it is abundant that Chinese medicine stoste A, Chinese medicine stoste B and tea tree ethereal oil are added thereto
Mixing, cools the temperature to 45 degrees Celsius, dodecyl benzyl dimethyl ammonium chloride is added into mixture, continuous using blender
It is stirred, it is made to be sufficiently mixed, Cremophor RH40 is added and at the uniform velocity stirs, obtains mixed liquor, purified water stirring is added
Uniformly, antiseptic is obtained.
Efficacy validation：Detection result on probation is carried out to product prepared by Examples 1 to 6；
Test event 1：The present invention is to the double balls of Pseudomonas aeruginosa, Staphylococcus aureus, Escherichia coli, Candida albicans and pneumonia
Bacterium carries out bactericidal effect detection in 30,50 and 60 seconds, test result is as follows table 1：
The result shows that the embodiment of the present invention 1~6 can quickly kill Pseudomonas aeruginosa, Staphylococcus aureus, big in 30 seconds
Enterobacteria, Candida albicans and Diplococcus pneumopniae, bactericidal effect are substantially better than blank group, the wherein bactericidal effect of embodiment 5 most
It is good, the sterilizing rate of Pseudomonas aeruginosa, Staphylococcus aureus, Escherichia coli, Candida albicans and Diplococcus pneumopniae is reached in 30 seconds
To 99.8%.
Test event 2：The present invention is to the double balls of Pseudomonas aeruginosa, Staphylococcus aureus, Escherichia coli, Candida albicans and pneumonia
Bacterium carries out long-acting bacteriostatic experiment in 0,2,4 hour, test result is as follows table 2：
The result shows that 1~6 pair of Pseudomonas aeruginosa, Staphylococcus aureus, Escherichia coli, Candida albicans of the embodiment of the present invention
With Diplococcus pneumopniae there is long-acting bacteriostatic effect, four hours bacteriostasis rates to reach 95%, wherein the bactericidal effect of embodiment 5 is most
It is good, the bacteriostasis rate of Pseudomonas aeruginosa, Staphylococcus aureus, Escherichia coli, Candida albicans and Diplococcus pneumopniae is reached in 4 hours
98.1%.
Test event 3：The antipruritic effect of the embodiment of the present invention 1~6, peculiar smell effect of dispelling, moisturizing effect and to skin whether there is or not
Irritation carries out test experiments, and Examples 1 to 6 chooses 50 triers and try out respectively, test result is as follows table 3：
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | |
| The apparent number of antipruritic effect | 42 | 45 | 46 | 47 | 49 | 48 |
| Peculiar smell of dispelling number with obvious effects | 47 | 48 | 48 | 49 | 50 | 49 |
| The apparent number of moisturizing effect | 41 | 43 | 45 | 47 | 49 | 49 |
| Irritation | Nothing | Nothing | Nothing | Nothing | Nothing | Nothing |
The result shows that the embodiment of the present invention 1~6 has preferable antipruritic effect, dispel peculiar smell effect, moisturizing effect, and it is right
No skin irritation.The wherein best results of embodiment 5,49 people feel that antipruritic effect is apparent, and 50 peculiar smell of feeling to dispel are with obvious effects,
49 people feel there is apparent moisturizing effect after.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (3)
1. antiseptic, it is characterised in that：The antiseptic is composed of the following components：
Granatum, kuh-seng, lotus leaf, elscholtiza, schizonepeta, wild marjoram, mountain fennel, indigo naturalis, rosemary, glycerine, Cremophor RH40,
Dodecyl benzyl dimethyl ammonium chloride, tea tree ethereal oil, purified water.
2. antiseptic according to claim 1, which is characterized in that the antiseptic is made of following parts by weight：
30~40 parts of granatum, 22~32 parts of kuh-seng, 20~30 parts of lotus leaf, 17~27 parts of elscholtiza, 15~25 parts of schizonepeta, wild marjoram 15
~25 parts, 13~23 parts of mountain fennel, 10~20 parts of indigo naturalis, 10~20 parts of rosemary, 20~30 parts of glycerine, PEG-40 hydrogenated castors
15~25 parts of oil, 2~5 parts of dodecyl benzyl dimethyl ammonium chloride, 0.5~2 part of tea tree ethereal oil, 55~65 parts of purified water.
3. antiseptic according to claim 1, which is characterized in that the preparation method of the antiseptic includes the following steps：
1) use medicinal herb grinder by kuh-seng, elscholtiza, mountain fennel, rosemary crush, cross 40 mesh sieve, obtain herb powder A, will in
Medicine powders A is positioned in supercritical carbon dioxide extracting kettle, is extracted to it by carbon dioxide, carbon dioxide is passed through flow velocity
Be 18~25 ls/h, extracting pressure be 15~30 megapascal, extraction temperature be 35~50 degrees Celsius, extraction 1 hour after use from
Scheming is centrifuged, and takes supernatant, obtains Chinese medicine stoste A, spare；
2) it uses medicinal herb grinder to crush granatum, lotus leaf, schizonepeta, wild marjoram, indigo naturalis, crosses 40 mesh sieve, obtain herb powder B,
The purified water of 10 times of volumes is added into herb powder B, after impregnating 1 hour, is decocted 2 hours using micro-pressure medicine decocting machine, decocts secondary
Number is 3 times, filters merging filtrate, is concentrated by evaporation, and Chinese medicine stoste B is obtained, spare；
3) glycerine water-bath is heated to 45~65 degrees Celsius, Chinese medicine stoste A, Chinese medicine stoste B and tea tree ethereal oil is added thereto and fills
Divide mixing, cools the temperature to 35~45 degrees Celsius, dodecyl benzyl dimethyl ammonium chloride is added into mixture, use stirring
Machine is constantly stirred, it is made to be sufficiently mixed, and Cremophor RH40 is added and at the uniform velocity stirs, obtains mixed liquor, purifying is added
Water stirs evenly, and obtains antiseptic.
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