CN108535067A - A kind of electricity toilet seat test standard analog excreta - Google Patents

A kind of electricity toilet seat test standard analog excreta Download PDF

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Publication number
CN108535067A
CN108535067A CN201810301467.8A CN201810301467A CN108535067A CN 108535067 A CN108535067 A CN 108535067A CN 201810301467 A CN201810301467 A CN 201810301467A CN 108535067 A CN108535067 A CN 108535067A
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CN
China
Prior art keywords
excreta
toilet seat
standard analog
electricity
calcium carbonate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201810301467.8A
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Chinese (zh)
Inventor
马德军
鲁建国
陈松涛
刘民
李珊珊
霍雨佳
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CHINA DOMESTIC ELECTRICAL EQUIPMENT INST
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CHINA DOMESTIC ELECTRICAL EQUIPMENT INST
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Priority to CN201810301467.8A priority Critical patent/CN108535067A/en
Publication of CN108535067A publication Critical patent/CN108535067A/en
Withdrawn legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/38Diluting, dispersing or mixing samples
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N2001/2893Preparing calibration standards
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/38Diluting, dispersing or mixing samples
    • G01N2001/386Other diluting or mixing processes

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a kind of electric toilet seat test standard analog excretas.Selection including the reference substance raw material and preparation process.Calcium carbonate and sodium alginate are the important raw material of two of which.By the selection and the preparation process that strictly control raw material, so that the stability of characteristics such as viscosity, uniformity, density, moisture content of standard analog excreta for preparing, uniform, consistency is good, the repeatability and stability that ensure that test result, so as to the clean-up performance of the electric toilet seat of evaluation of more objective.

Description

A kind of electricity toilet seat test standard analog excreta
Technical field
Present invention design is related to a kind of selection of raw material of electric toilet seat test standard analog excreta and prepares work Skill.
Background technology
Electric toilet seat refers to cleaning human body residual draining object by water by electric drive, can carry blowing, seat ring heating etc. Single or multiple functions utensils (hereinafter referred to as " utensil ").Clean rate is an important finger of the electric toilet seat clean-up performance of evaluation Mark indicates cleaning capacity with the percentage of removal slop.Existing national standard GB/T 23131《Electric toilet seat》Middle use Weight method measures clean rate:Standard analog faecal samples are applied on load substrate first, weigh the gross mass W of substrate1, After running cleaning procedure 1min, with blotting paper adsorption surface moisture, substrate is weighed again and remains the gross mass W of loaded article2, clearly Clean rate calculation formula is as follows:
In formula:
C-clean rate, is expressed as a percentage;
Wo- transparent substrate quality, unit are gram (g);
W1The gross mass of substrate and dirt load criteria sample before-flushing, unit are gram (g);
W2The gross mass of-flushing metacoxal plate and remaining dirt load criteria sample, unit are gram (g).
Wherein, the preparation process of simulation faecal samples used is as follows:
A) the 100g calcium carbonate and 1g sodium alginates weighed pours into the same beaker, is stirred at same direction with glass bar 10min;
B) 0.2g methyl blues are weighed, are put into beaker, the distilled water of 76mL are injected thereto, with glass bar stir about 5min;
C) calcium carbonate stirred evenly and sodium alginate mixed-powder are put into a glass container, methyl blue solution is slow Slowly it uniformly pours into glass container, is stirred with glass bar when pouring into, after liquid is poured into completely, at least with glass bar stirring 30min, until simulation slop color is uniform, surface is smooth.
Producing for standard analog excreta need to strictly control raw material and preparation process, to ensure to test in different laboratory As a result consistency and repeatability reduce the uncertainty of test, to which science objectively reacts the spatter property of electric toilet seat The quality of energy.
Calcium carbonate is commonly called as lime stone, marble, calcite, is a kind of inorganic compound, chemical formula CaCO3, there is heavy carbon The variety classes such as sour calcium, precipitated calcium carbonate, powdered whiting density ratio precipitated calcium carbonate density weight, are prepared using physical method, Whiteness is relatively low;Precipitated calcium carbonate is prepared using chemical method, and density is light, and whiteness is high, and grain size can be accomplished very thin.According to heavy Calcium carbonate produces electric toilet seat and surveys tentative standard excreta, it may appear that is difficult to shape, the poor problem of viscosity.
Sodium alginate is the mixture of polyuronide, can be used as additive and is used for increasing vicidity, is widely used in food, spins The making of fabric, cosmetics etc., sodium alginate are two kinds by two kinds of monomer compositions of mannuronic acid (M) and glucuronic acid (G) The ratio of monomer is different, and performance is also different.High G/M than sodium alginate combined with calcium carbonate after the gelatinous mass hardness that is formed It is big and more crisp, cause the standard analog excreta viscosity produced inadequate.
The committed step for preparing the standard analog excreta is that methyl blue solution is poured slowly into calcium carbonate and sodium alginate Mixture after, be kept stirring at least 30 minutes.If stir speed (S.S.) is unstable during being somebody's turn to do, the standard analog prepared row can be caused The viscosity for letting out object is inconsistent, to meet the requirement of experiment repeatability and consistency.
Invention content
The purpose of the present invention is to provide a kind of electric toilet seat test standard analog excretas, solve standard analog row The bad problem of the stickiness of object, uniformity, consistency is let out, ensure that the repeatability and stability of test result, so as to The clean-up performance of the electric toilet seat of evaluation of more objective.
In order to achieve the above objectives, the technical scheme is that:A kind of electricity toilet seat test standard analog excreta, It is characterized in that, includes selection and preparation process two parts of raw material.
Further, a kind of electric toilet seat, which is tested, uses standard analog excreta, and the calcium carbonate in raw material selects 200 purposes light Matter calcium carbonate.
Further, a kind of electric toilet seat, which is tested, uses standard analog excreta, and the sodium alginate in raw material selects low G/M ratios Sodium alginate.
Further, a kind of electric toilet seat, which is tested, uses standard analog excreta, the control of the mixing speed in preparation process: After methyl blue solution slowly pours into the mixture of calcium carbonate and sodium alginate, the stir speed (S.S.) for being kept stirring stick is certain, be 55~ 60 revs/min.
Due to the adoption of the above technical scheme, the beneficial effects of the invention are as follows:
The present invention is using the precipitated calcium carbonate of 200 mesh as the one kind for making electric toilet seat test standard analog excreta Raw material, overcomes that powdered whiting density is larger to cause obtained standard analog excreta stickiness inadequate, shapeless, character With really differ larger problem.Meanwhile calcium carbonate selects 200 mesh, can make its conjugation higher with other raw materials, more accord with Close truth.
The present invention using low G/M than sodium alginate, the stickiness of standard analog excreta that can be obtained meets the requirements.
After methyl blue solution slowly pours into the mixture of calcium carbonate and sodium alginate, stir speed (S.S.) keeps certain, can make every The characteristic of secondary standard analog excreta obtained is consistent, and meets the requirement of repeatability, stability.
Description of the drawings
Fig. 1 is a kind of Comparability test data profile of embodiment of the present invention.
Specific implementation mode
Experimental method used in following embodiments is conventional method unless otherwise specified.
The materials, reagents and the like used in the following examples is commercially available unless otherwise specified.
Embodiment 1
A kind of electricity toilet seat test standard analog excreta, selected dispensing are as follows:The precipitated calcium carbonate powder of 200 mesh (divides Analyse pure) 100g, low G/M than sodium alginate (analysis pure) 1g, methyl blue (analysis is pure) 0.2g, distilled water 76ml.
It configures according to the following steps:
1. the 100g calcium carbonate weighed and 1g sodium alginates are poured into the same beaker, stirred at same direction with glass bar Mix 10min;
2. weighing 0.2g methyl blues, it is put into beaker, the distilled water of 76mL is injected thereto, with glass bar stir about 5min;
3. the calcium carbonate stirred evenly and sodium alginate mixed-powder are put into a glass container, methyl blue solution is slow Slowly it uniformly pours into glass container, is stirred when pouring into, then all mixed raw materials are poured into a mixing speed together can In the blender of control, it is 56 beats/min to be kept stirring rate, is stirred at least 30min, until simulation slop color is equal Even, surface is smooth.
After the standard analog excreta of preparation is compared experiment in the laboratories Duo Jia, experimental data is distributed as shown in Figure 1. Show that the standard analog excreta stickiness, uniformity, consistency are good, ensure that the repeatability and stabilization of test result Property.

Claims (4)

1. a kind of electricity toilet seat test standard analog excreta, which is characterized in that the selection including raw material and preparation process Two parts.
2. electricity toilet seat test standard analog excreta as described in claim 1, which is characterized in that the calcium carbonate in raw material Select the precipitated calcium carbonate of 200 mesh.
3. electricity toilet seat test standard analog excreta as described in claim 1, which is characterized in that the alginic acid in raw material Sodium select low G/M than sodium alginate.
4. electricity toilet seat test standard analog excreta as described in claim 1, which is characterized in that stirring in preparation process Mix the control of speed:After methyl blue solution slowly pours into calcium carbonate and sodium alginate mixture, it is kept stirring the stir speed (S.S.) of stick Centainly, 55 ~ 60 revs/min are taken.
CN201810301467.8A 2018-04-05 2018-04-05 A kind of electricity toilet seat test standard analog excreta Withdrawn CN108535067A (en)

Priority Applications (1)

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CN201810301467.8A CN108535067A (en) 2018-04-05 2018-04-05 A kind of electricity toilet seat test standard analog excreta

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CN201810301467.8A CN108535067A (en) 2018-04-05 2018-04-05 A kind of electricity toilet seat test standard analog excreta

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110426229A (en) * 2019-09-06 2019-11-08 中国家用电器研究院 It is a kind of electricity Seat of the toilet clean rate test use tooling
CN113109066A (en) * 2021-04-14 2021-07-13 中国家用电器研究院 Simulated kitchen residue for testing performance of dish-washing machine and preparation device thereof
CN113838352A (en) * 2021-08-26 2021-12-24 新疆医科大学第六附属医院 Demonstration model for gastroenterology department

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0427352A (en) * 1990-05-22 1992-01-30 Fuji Capsule Kk Enteric soft capsule for health food
CN106344496A (en) * 2016-09-05 2017-01-25 四川大学 Preparation method of macromolecular laminar drug-loaded hydrogel with controllable drug distribution

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0427352A (en) * 1990-05-22 1992-01-30 Fuji Capsule Kk Enteric soft capsule for health food
CN106344496A (en) * 2016-09-05 2017-01-25 四川大学 Preparation method of macromolecular laminar drug-loaded hydrogel with controllable drug distribution

Non-Patent Citations (4)

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Title
FILMSGUO LILING ET AL.: "Effects of ionic crosslinking on physical and mechanical propertiesof alginate mulching films", 《CARBOHYDRATE POLYMERS》 *
吴国华等: "海藻酸钠/CaCO3医用封闭剂凝胶化时间的调控", 《东华大学学报(自然科学版)》 *
杨琴等: "海藻酸钠的复合特性及其在肉制品中的应用研究进展", 《中国食品添加剂》 *
陈松涛等: "电子坐便器清洁率测试方法的研究", 《标准》 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110426229A (en) * 2019-09-06 2019-11-08 中国家用电器研究院 It is a kind of electricity Seat of the toilet clean rate test use tooling
CN110426229B (en) * 2019-09-06 2024-05-10 中国家用电器研究院 Tool for testing cleaning rate of electric toilet seat
CN113109066A (en) * 2021-04-14 2021-07-13 中国家用电器研究院 Simulated kitchen residue for testing performance of dish-washing machine and preparation device thereof
CN113109066B (en) * 2021-04-14 2022-10-14 中国家用电器研究院 Simulated kitchen residue for testing performance of dish-washing machine and preparation device thereof
CN113838352A (en) * 2021-08-26 2021-12-24 新疆医科大学第六附属医院 Demonstration model for gastroenterology department

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Application publication date: 20180914