CN108531307A - A kind of method for washing improving natural feather fluffy degree - Google Patents
A kind of method for washing improving natural feather fluffy degree Download PDFInfo
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- CN108531307A CN108531307A CN201810178080.8A CN201810178080A CN108531307A CN 108531307 A CN108531307 A CN 108531307A CN 201810178080 A CN201810178080 A CN 201810178080A CN 108531307 A CN108531307 A CN 108531307A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/001—Softening compositions
- C11D3/0015—Softening compositions liquid
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0026—Low foaming or foam regulating compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/32—Amides; Substituted amides
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3719—Polyamides or polyimides
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38618—Protease or amylase in liquid compositions only
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38627—Preparations containing enzymes, e.g. protease or amylase containing lipase
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38636—Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/12—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/74—Carboxylates or sulfonates esters of polyoxyalkylene glycols
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Abstract
The invention discloses a kind of method for washing improving natural feather fluffy degree, it is related to Eider down processing technical field, first natural feather is sent into rotary drum washer, and cleaning solution is injected into rotary drum washer, cleaning solution adds water to be formulated by cleaning agent, cleaning solution temperature maintains 45 50 DEG C, cleaning solution is drained after cleaning 10 15min, the injected clear water into rotary drum washer again, rinsing liquid is drained after rinsing 10 15min, then natural feather is sent into roller dryer, and in 70 75 DEG C of drying, closing temperature switchs after drying, lower suede after 10 15min of opening machine mouth blowing.Cleaning agent of the present invention can ensure the fluffy degree of natural feather after washing while high-efficiency washing natural feather improves natural feather whiteness, keep the natural feather after washing slim and graceful, soft, flexible, to improve the processing quality of natural feather.
Description
Technical field：
The present invention relates to Eider down processing technical fields, and in particular to a kind of method for washing improving natural feather fluffy degree.
Background technology：
Natural feather is the abdomen grown in geese and ducks, lupine-like villus, and slabbing is feather.Since natural feather is a kind of
Animal protein fiber, the tiny stomata for ten million triangle that gathers on natural feather nodular fibrous, can shrink with temperature change
Expansion, generates temperature adjustment function, and absorbable human body distributes the hot gas of flowing, completely cuts off the invasion of cool ambient air.From the inspection of fluffy degree
It is analyzed in survey, natural feather will a high grade than silk, the heat insulating materials such as cotton.Natural feather is purely by way of a heat insulating material,
Its economic value is significantly larger than other heat insulating materials.
The natural feather come from raiser's purchase is generally all without any processing, in addition to being stained with wax, grease etc. above natural feather
Outside oil-soluble dirt, the dirts such as soil, sand, dust, excrement, blood are also stained with, these will cause natural feather to generate stench taste,
Grow a large amount of bacteriums and germ simultaneously.Therefore, it needs to carry out strictly natural feather before down products is made in Eider down processing
Washing, to ensure the processing quality and safety in utilization of natural feather.
Currently, conventional natural feather cleaning way uses WATER-WASHING METHOD, used by the auxiliary of cleaning agent improve cleaning efficiency with
Ensure cleaning performance.But general cleaning agent is usually made of a variety of surfactants, will produce while cleaning dirt a large amount of
Foam subsequently needs to carry out rinsing to natural feather in this way and rinsing water amount is big.
Invention content：
Technical problem to be solved by the present invention lies in one kind is provided, operation is simple, cleaning efficiency is high and is steeped when cleaning
The few method for washing for improving natural feather fluffy degree of foam yield.
The technical problems to be solved by the invention are realized using technical solution below：
Natural feather, is first sent into rotary drum washer, and clear to drum-type by a kind of method for washing improving natural feather fluffy degree
Cleaning solution is injected in washing machine, cleaning solution adds water to be formulated by cleaning agent, and cleaning solution temperature maintains 45-50 DEG C, cleans 10-
Cleaning solution, then the injected clear water into rotary drum washer are drained after 15min, rinsing liquid is drained after rinsing 10-15min, then will
Natural feather is sent into roller dryer, and in 70-75 DEG C of drying, closing temperature switchs after drying, opens machine mouth blowing 10-
Lower suede after 15min.
The cleaning agent is made of the raw material of following weight percent：
Ethoxylated fatty-acid methyl ester 20-40%, sodium cocoyl methyl sodium taurocholate 10-30%, food-grade polyglutamic acid
10-30%, ethoxylated lanolin 5-10%, sterilization Chinese medical extract 1-2%, sodium cocoyl glycinate 1-2%, compound bio
Enzyme 1-2%；
The compound biological enzyme is made of the raw material of following weight percent：
Neutral proteinase 20-40%, lipase 10-30%, amylase 5-20%, cellulase 5-20%, lysozyme 1-
10%.
The sterilization Chinese medical extract is carried by the Chinese medicine fruit of summer cypress, frutus cnidii, the root of Dahurain angelica, castor bean, smilax, stone-like omphalia, crotons
Take obtained, preparation method is：It is added in 70% ethyl alcohol of 5 times of gross weights after powder is made in above-mentioned Chinese medicine, impregnates 10-15min
Power 1.5kW paste mill grinding 15-30min are utilized afterwards, and are heated to reflux state insulated and stirred 1-3h, are filtered, and are filtered to gained
Decolorising agent is added in liquid, 15-30min is stood after being sufficiently stirred, is filtered to remove decolorising agent again, it is fine that carboxymethyl is added into filtrate
The plain sodium of dimension, is sent into after stirring evenly in spray dryer, and micro mist is made to get in sterilization through micronizer in dry gained particle
Medicament extract.
The mass ratio of the fruit of summer cypress, frutus cnidii, the root of Dahurain angelica, castor bean, smilax, stone-like omphalia, crotons, sodium carboxymethylcellulose
It is 5:3:2:1:1:1:0.5:0.5-1.
Sterilize Chinese medical extract prepare when, using sodium carboxymethylcellulose as excipient, by the use of decolorising agent come
Remove pigment impurity contained by Chinese medical extract.
The decolorising agent selects active powdered carbon.
The decolorising agent is made of aluminium-magnesium silicate, guaiacol glycerol ether and magnesium dimethacrylate, and preparation method is：
Guaiacol glycerol ether and magnesium dimethacrylate are added into n-butanol, and is heated to reflux state insulated and stirred 10-
15min adds aluminium-magnesium silicate, continues the insulated and stirred 0.5-2h that flows back, gained mixture recycles n-butanol through being concentrated under reduced pressure, dense
Contracting residue is dried in 120-125 DEG C of baking oven to constant weight, and micro mist is made through micronizer in obtained solid, most afterwards through granulator
Particle is made to get decolorising agent.
The n-butanol, guaiacol glycerol ether, magnesium dimethacrylate, aluminium-magnesium silicate mass ratio be 50-100:1-
5:5-10:20-30。
The food-grade polyglutamic acid is substituted by equivalent polyethylene glycol glutamic acid-cetanol carboxylate.
Polyethylene glycol glutamic acid-cetanol the carboxylate is by polyethylene glycol 400, food-grade polyglutamic acid and spermaceti
Alcohol is made through esterification, and preparation method is：It is dripped into the mixture of polyethylene glycol 400 and food-grade polyglutamic acid under stirring
Add deionized water until being completely dissolved, and the concentrated sulfuric acid is added dropwise and adjusts solution ph to 4-5, is again heated to reflux state insulated and stirred
Reaction, waits for that cetanol is added after polyethylene glycol 400 esterification, continues the insulated and stirred reaction that flows back, and esterification is complete
After lotion is made in the reduced pressure of gained mixture, lotion is sent into after cooled to room temperature in freeze drier, dry
Micro mist is made to get polyethylene glycol glutamic acid-cetanol carboxylate through micronizer in dry obtained solid.
The polyethylene glycol 400, food-grade polyglutamic acid, cetanol mass ratio be 5-10:15-25:1-5.
By with polyethylene glycol glutamic acid-cetanol carboxylate substitute food product grade polyglutamic acid, further enhancing cleaning
Effect.
The beneficial effects of the invention are as follows：
(1) Chinese medicine preparation used in present invention sterilization Chinese medical extract follows stringent monarch compatibility relationship, wherein
Skin, frutus cnidii are as monarch drug in a prescription, and the root of Dahurain angelica, castor bean are as ministerial drug, smilax, stone-like omphalia as adjutant, and crotons are as making medicine, in this
Medicine composition is attached on natural feather to coordinate sodium lauroyl glutamate and lysozyme effectively to kill using bacterium, germ as controlling object
The bacterium and germ；
(2) the made decolorising agent of the present invention has the decolorizing effect comparable with identical mesh number activity powdered carbon, and in decoloration
The loss amount for reducing active ingredient in antibacterial Chinese medicine extract simultaneously avoids extracting using antibacterial Chinese medicine existing for activated carbon decolorizing
In object the problem of active ingredient excessive loss；
(3) present invention is subtracted by the use of food-grade polyglutamic acid or polyethylene glycol glutamic acid-cetanol carboxylate
The dosage of conventional surfactants in few cleaning agent, foam yield in cleaning solution when to reduce natural feather cleaning, and then reduce
Residual rate of the natural feather rinsing water amount with reduction cleaning agent on natural feather surface；
(4) natural feather is fluffy after cleaning agent of the present invention can ensure to wash while high-efficiency washing natural feather raising natural feather whiteness
Looseness keeps the natural feather after washing slim and graceful, soft, flexible, to improve the processing quality of natural feather.
Specific implementation mode：
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1
First natural feather is sent into rotary drum washer, and injects cleaning solution into rotary drum washer, cleaning solution is by cleaning
Agent adds water to be formulated, and cleaning solution temperature maintains 45-50 DEG C, cleans after 15min and drains cleaning solution, then to rotary drum washer
Middle injected clear water drains rinsing liquid after rinsing 10min, and then natural feather is sent into roller dryer, and in 70-75 DEG C of baking
Dry, closing temperature switchs after drying, opens lower suede after machine mouth blowing 15min.
Cleaning agent is made of the raw material of following weight percent：Ethoxylated fatty-acid methyl ester 35%, sodium cocoyl methyl
Sodium taurocholate 26%, food-grade polyglutamic acid 25%, ethoxylated lanolin 8%, sterilization Chinese medical extract 2%, cocounut oil acyl are sweet
Propylhomoserin sodium 2%, compound biological enzyme 2%.
Wherein, compound biological enzyme is made of the raw material of following weight percent：Neutral proteinase 35%, lipase 30%,
Amylase 15%, cellulase 15%, lysozyme 5%.
Sterilize the preparation of Chinese medical extract：By the 5g fruit of summer cypress, 3g frutus cnidiis, the 2g roots of Dahurain angelica, 1g castor beans, 1g smilaxs, 1g
Stone-like omphalia, 0.5g crotons Chinese medicines are added after powder is made in 70% ethyl alcohol of 5 times of gross weights, are ground using power 1.5kW after impregnating 10min
Pulp grinder defibrination 15min, and it is heated to reflux state insulated and stirred 3h, it filters, decolorising agent is added into gained filtrate, is sufficiently stirred
After stand 30min, be filtered to remove decolorising agent again, into filtrate be added 1g sodium carboxymethylcelluloses, after stirring evenly be sent into spray
In mist drying machine, micro mist is made to get sterilization Chinese medical extract through micronizer in dry gained particle.Wherein, decolorising agent selects
With the active powdered carbon of 200 mesh.
Embodiment 2
First natural feather is sent into rotary drum washer, and injects cleaning solution into rotary drum washer, cleaning solution is by cleaning
Agent adds water to be formulated, and cleaning solution temperature maintains 45-50 DEG C, cleans after 15min and drains cleaning solution, then to rotary drum washer
Middle injected clear water drains rinsing liquid after rinsing 10min, and then natural feather is sent into roller dryer, and in 70-75 DEG C of baking
Dry, closing temperature switchs after drying, opens lower suede after machine mouth blowing 15min.
Cleaning agent is made of the raw material of following weight percent：Ethoxylated fatty-acid methyl ester 35%, sodium cocoyl methyl
Sodium taurocholate 26%, food-grade polyglutamic acid 25%, ethoxylated lanolin 8%, sterilization Chinese medical extract 2%, cocounut oil acyl are sweet
Propylhomoserin sodium 2%, compound biological enzyme 2%.
Wherein, compound biological enzyme is made of the raw material of following weight percent：Neutral proteinase 35%, lipase 30%,
Amylase 15%, cellulase 15%, lysozyme 5%.
Sterilize the preparation of Chinese medical extract：By the 5g fruit of summer cypress, 3g frutus cnidiis, the 2g roots of Dahurain angelica, 1g castor beans, 1g smilaxs, 1g
Stone-like omphalia, 0.5g crotons Chinese medicines are added after powder is made in 70% ethyl alcohol of 5 times of gross weights, are ground using power 1.5kW after impregnating 10min
Pulp grinder defibrination 15min, and it is heated to reflux state insulated and stirred 3h, it filters, decolorising agent is added into gained filtrate, is sufficiently stirred
After stand 30min, be filtered to remove decolorising agent again, into filtrate be added 1g sodium carboxymethylcelluloses, after stirring evenly be sent into spray
In mist drying machine, micro mist is made to get sterilization Chinese medical extract through micronizer in dry gained particle.
The preparation of decolorising agent：3g guaiacol glycerol ethers and 5g magnesium dimethacrylates are added into 50g n-butanols, and adds
Heat adds 20g aluminium-magnesium silicates to reflux state insulated and stirred 15min, continues the insulated and stirred 2h that flows back, gained mixture is through subtracting
Concentration and recovery n-butanol, condensate residue is pressed to be dried to constant weight in 120-125 DEG C of baking oven, obtained solid is through ultramicro grinding mechanism
At micro mist, the particle of 200 mesh most is made to get decolorising agent through granulator afterwards.
Embodiment 3
First natural feather is sent into rotary drum washer, and injects cleaning solution into rotary drum washer, cleaning solution is by cleaning
Agent adds water to be formulated, and cleaning solution temperature maintains 45-50 DEG C, cleans after 15min and drains cleaning solution, then to rotary drum washer
Middle injected clear water drains rinsing liquid after rinsing 10min, and then natural feather is sent into roller dryer, and in 70-75 DEG C of baking
Dry, closing temperature switchs after drying, opens lower suede after machine mouth blowing 15min.
Cleaning agent is made of the raw material of following weight percent：Ethoxylated fatty-acid methyl ester 35%, sodium cocoyl methyl
Sodium taurocholate 26%, food-grade polyglutamic acid 25%, ethoxylated lanolin 8%, sterilization Chinese medical extract 2%, cocounut oil acyl are sweet
Propylhomoserin sodium 2%, compound biological enzyme 2%.
Wherein, compound biological enzyme is made of the raw material of following weight percent：Neutral proteinase 35%, lipase 30%,
Amylase 15%, cellulase 15%, lysozyme 5%.
Sterilize the preparation of Chinese medical extract：By the 5g fruit of summer cypress, 3g frutus cnidiis, the 2g roots of Dahurain angelica, 1g castor beans, 1g smilaxs, 1g
Stone-like omphalia, 0.5g crotons Chinese medicines are added after powder is made in 70% ethyl alcohol of 5 times of gross weights, are ground using power 1.5kW after impregnating 10min
Pulp grinder defibrination 15min, and it is heated to reflux state insulated and stirred 3h, it filters, decolorising agent is added into gained filtrate, is sufficiently stirred
After stand 30min, be filtered to remove decolorising agent again, into filtrate be added 1g sodium carboxymethylcelluloses, after stirring evenly be sent into spray
In mist drying machine, micro mist is made to get sterilization Chinese medical extract through micronizer in dry gained particle.
The preparation of decolorising agent：5g guaiacol glycerol ethers and 8g magnesium dimethacrylates are added into 80g n-butanols, and adds
Heat adds 30g aluminium-magnesium silicates to reflux state insulated and stirred 15min, continues the insulated and stirred 2h that flows back, gained mixture is through subtracting
Concentration and recovery n-butanol, condensate residue is pressed to be dried to constant weight in 120-125 DEG C of baking oven, obtained solid is through ultramicro grinding mechanism
At micro mist, the particle of 200 mesh most is made to get decolorising agent through granulator afterwards.
Embodiment 4
First natural feather is sent into rotary drum washer, and injects cleaning solution into rotary drum washer, cleaning solution is by cleaning
Agent adds water to be formulated, and cleaning solution temperature maintains 45-50 DEG C, cleans after 15min and drains cleaning solution, then to rotary drum washer
Middle injected clear water drains rinsing liquid after rinsing 10min, and then natural feather is sent into roller dryer, and in 70-75 DEG C of baking
Dry, closing temperature switchs after drying, opens lower suede after machine mouth blowing 15min.
Cleaning agent is made of the raw material of following weight percent：Ethoxylated fatty-acid methyl ester 35%, sodium cocoyl methyl
Sodium taurocholate 26%, polyethylene glycol glutamic acid-cetanol carboxylate 25%, ethoxylated lanolin 8%, sterilization Chinese medicine carry
Take object 2%, sodium cocoyl glycinate 2%, compound biological enzyme 2%.
Wherein, compound biological enzyme is made of the raw material of following weight percent：Neutral proteinase 35%, lipase 30%,
Amylase 15%, cellulase 15%, lysozyme 5%.
Sterilize the preparation of Chinese medical extract：By the 5g fruit of summer cypress, 3g frutus cnidiis, the 2g roots of Dahurain angelica, 1g castor beans, 1g smilaxs, 1g
Stone-like omphalia, 0.5g crotons Chinese medicines are added after powder is made in 70% ethyl alcohol of 5 times of gross weights, are ground using power 1.5kW after impregnating 10min
Pulp grinder defibrination 15min, and it is heated to reflux state insulated and stirred 3h, it filters, decolorising agent is added into gained filtrate, is sufficiently stirred
After stand 30min, be filtered to remove decolorising agent again, into filtrate be added 1g sodium carboxymethylcelluloses, after stirring evenly be sent into spray
In mist drying machine, micro mist is made to get sterilization Chinese medical extract through micronizer in dry gained particle.Wherein, decolorising agent selects
With the active powdered carbon of 200 mesh.
The preparation of polyethylene glycol glutamic acid-cetanol carboxylate：To 5g polyethylene glycol 400s and 20g food-grades under stirring
Deionized water is added dropwise until being completely dissolved in the mixture of polyglutamic acid, and the concentrated sulfuric acid is added dropwise and adjusts solution ph to 4-5, then adds
Heat to reflux state insulated and stirred is reacted, and is waited for that 3g cetanols are added after polyethylene glycol 400 esterification, is continued reflux heat preservation
It is stirred to react, gained mixture is concentrated under reduced pressure after being fully completed and lotion is made by esterification, and lotion is through cooled to room temperature
It is sent into freeze drier afterwards, micro mist is made to get polyethylene glycol glutamic acid-whale through micronizer in dry obtained solid
Ceryl alcohol carboxylate.
Embodiment 5
First natural feather is sent into rotary drum washer, and injects cleaning solution into rotary drum washer, cleaning solution is by cleaning
Agent adds water to be formulated, and cleaning solution temperature maintains 45-50 DEG C, cleans after 15min and drains cleaning solution, then to rotary drum washer
Middle injected clear water drains rinsing liquid after rinsing 10min, and then natural feather is sent into roller dryer, and in 70-75 DEG C of baking
Dry, closing temperature switchs after drying, opens lower suede after machine mouth blowing 15min.
Cleaning agent is made of the raw material of following weight percent：Ethoxylated fatty-acid methyl ester 35%, sodium cocoyl methyl
Sodium taurocholate 26%, polyethylene glycol glutamic acid-cetanol carboxylate 25%, ethoxylated lanolin 8%, sterilization Chinese medicine carry
Take object 2%, sodium cocoyl glycinate 2%, compound biological enzyme 2%.
Wherein, compound biological enzyme is made of the raw material of following weight percent：Neutral proteinase 35%, lipase 30%,
Amylase 15%, cellulase 15%, lysozyme 5%.
Sterilize the preparation of Chinese medical extract：By the 5g fruit of summer cypress, 3g frutus cnidiis, the 2g roots of Dahurain angelica, 1g castor beans, 1g smilaxs, 1g
Stone-like omphalia, 0.5g crotons Chinese medicines are added after powder is made in 70% ethyl alcohol of 5 times of gross weights, are ground using power 1.5kW after impregnating 10min
Pulp grinder defibrination 15min, and it is heated to reflux state insulated and stirred 3h, it filters, decolorising agent is added into gained filtrate, is sufficiently stirred
After stand 30min, be filtered to remove decolorising agent again, into filtrate be added 1g sodium carboxymethylcelluloses, after stirring evenly be sent into spray
In mist drying machine, micro mist is made to get sterilization Chinese medical extract through micronizer in dry gained particle.Wherein, decolorising agent selects
With the active powdered carbon of 200 mesh.
The preparation of polyethylene glycol glutamic acid-cetanol carboxylate：To 10g polyethylene glycol 400s and 25g food under stirring
Deionized water is added dropwise until being completely dissolved in the mixture of grade polyglutamic acid, and the concentrated sulfuric acid is added dropwise and adjusts solution ph to 4-5, then
It is heated to the reaction of reflux state insulated and stirred, waits for that 5g cetanols are added after polyethylene glycol 400 esterification, continues reflux and protect
Temperature is stirred to react, and gained mixture is concentrated under reduced pressure after being fully completed and lotion is made by esterification, and lotion is through naturally cooling to room
It is sent into freeze drier after temperature, micro mist is made to get polyethylene glycol glutamic acid-through micronizer in dry obtained solid
Cetanol carboxylate.
Reference examples
First natural feather is sent into rotary drum washer, and injects cleaning solution into rotary drum washer, cleaning solution is by cleaning
Agent adds water to be formulated, and cleaning solution temperature maintains 45-50 DEG C, cleans after 15min and drains cleaning solution, then to rotary drum washer
Middle injected clear water drains rinsing liquid after rinsing 10min, and then natural feather is sent into roller dryer, and in 70-75 DEG C of baking
Dry, closing temperature switchs after drying, opens lower suede after machine mouth blowing 15min.
Cleaning agent is made of the raw material of following weight percent：Ethoxylated fatty-acid methyl ester 35%, sodium cocoyl methyl
Sodium taurocholate 26%, food-grade polyglutamic acid 25%, ethoxylated lanolin 8%, sterilization Chinese medical extract 2%, cocounut oil acyl are sweet
Propylhomoserin sodium 2%, compound biological enzyme 2%.
Wherein, compound biological enzyme is made of the raw material of following weight percent：Neutral proteinase 35%, lipase 30%,
Amylase 15%, cellulase 15%, lysozyme 5%.
Sterilize the preparation of Chinese medical extract：By the 5g fruit of summer cypress, 3g frutus cnidiis, the 2g roots of Dahurain angelica, 1g castor beans, 1g smilaxs, 1g
Stone-like omphalia, 0.5g crotons Chinese medicines are added after powder is made in 70% ethyl alcohol of 5 times of gross weights, are ground using power 1.5kW after impregnating 10min
Pulp grinder defibrination 15min, and it is heated to reflux state insulated and stirred 3h, it filters, decolorising agent is added into gained filtrate, is sufficiently stirred
After stand 30min, be filtered to remove decolorising agent again, into filtrate be added 1g sodium carboxymethylcelluloses, after stirring evenly be sent into spray
In mist drying machine, micro mist is made to get sterilization Chinese medical extract through micronizer in dry gained particle.Wherein, decolorising agent selects
With the aluminium-magnesium silicate of 200 mesh.
Embodiment 6
Embodiment 1-5, reference examples are utilized respectively to being washed with batch equivalent natural feather, wherein the mass ratio of cleaning agent and water
It is 1:30, and measure natural feather dirt removal rate and sterilizing rate and sterilize Chinese medical extract preparation decolorising agent percent of decolourization,
Loss of effective components rate, as shown in table 1.
The using effect of 1 cleaning agent of the present invention of table
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (7)
1. a kind of method for washing improving natural feather fluffy degree, it is characterised in that：First natural feather is sent into rotary drum washer, and to
Cleaning solution is injected in rotary drum washer, cleaning solution adds water to be formulated by cleaning agent, and cleaning solution temperature maintains 45-50 DEG C,
Cleaning solution, then the injected clear water into rotary drum washer are drained after cleaning 10-15min, rinsing liquid is drained after rinsing 10-15min,
Then natural feather is sent into roller dryer, and in 70-75 DEG C of drying, closing temperature switchs after drying, opens machine mouth
Lower suede after blowing 10-15min.
2. the method for washing according to claim 1 for improving natural feather fluffy degree, it is characterised in that：The cleaning agent is by as follows
The raw material of weight percent forms：
Ethoxylated fatty-acid methyl ester 20-40%, sodium cocoyl methyl sodium taurocholate 10-30%, food-grade polyglutamic acid 10-
30%, ethoxylated lanolin 5-10%, sterilization Chinese medical extract 1-2%, sodium cocoyl glycinate 1-2%, compound biological enzyme
1-2%；
The compound biological enzyme is made of the raw material of following weight percent：
Neutral proteinase 20-40%, lipase 10-30%, amylase 5-20%, cellulase 5-20%, lysozyme 1-10%.
3. the method for washing according to claim 2 for improving natural feather fluffy degree, it is characterised in that：The sterilization traditional Chinese medicine extraction
Object is extracted by the Chinese medicine fruit of summer cypress, frutus cnidii, the root of Dahurain angelica, castor bean, smilax, stone-like omphalia, crotons and is made, and preparation method is：It will be upper
It states after powder is made in Chinese medicine and is added in 70% ethyl alcohol of 5 times of gross weights, power 1.5kW paste mill grindings are utilized after impregnating 10-15min
15-30min, and it is heated to reflux state insulated and stirred 1-3h, it filters, decolorising agent is added into gained filtrate, after being sufficiently stirred
15-30min is stood, decolorising agent is filtered to remove again, sodium carboxymethylcellulose is added into filtrate, spraying is sent into after stirring evenly
In drying machine, micro mist is made to get sterilization Chinese medical extract through micronizer in dry gained particle.
4. the method for washing according to claim 3 for improving natural feather fluffy degree, it is characterised in that：The fruit of summer cypress, cnidium monnieri
Son, the root of Dahurain angelica, castor bean, smilax, stone-like omphalia, crotons, sodium carboxymethylcellulose mass ratio be 5:3:2:1:1:1:0.5:0.5-
1。
5. the method for washing according to claim 3 for improving natural feather fluffy degree, it is characterised in that：The decolorising agent, which is selected, lives
Property powdered carbon.
6. the method for washing according to claim 3 for improving natural feather fluffy degree, it is characterised in that：The decolorising agent is by silicic acid
Magnalium, guaiacol glycerol ether and magnesium dimethacrylate are made, and preparation method is：It is sweet that guaiacol is added into n-butanol
Oily ether and magnesium dimethacrylate, and it is heated to reflux state insulated and stirred 10-15min, aluminium-magnesium silicate is added, continues to flow back
Insulated and stirred 0.5-2h, gained mixture recycle n-butanol through being concentrated under reduced pressure, and condensate residue is dry in 120-125 DEG C of baking oven
To constant weight, micro mist is made through micronizer in obtained solid, and particle most is made to get decolorising agent through granulator afterwards.
7. the method for washing according to claim 6 for improving natural feather fluffy degree, it is characterised in that：The n-butanol is more created
The wooden phenol glycerin ether, magnesium dimethacrylate, aluminium-magnesium silicate mass ratio be 50-100:1-5:5-10:20-30.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110846142A (en) * | 2019-11-20 | 2020-02-28 | 安徽沃伦科技有限公司 | Efficient environment-friendly down jacket cleaning agent and cleaning method |
| CN114411269A (en) * | 2021-12-27 | 2022-04-29 | 六安市海洋羽毛有限公司 | Down feather separation production process |
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| CN103485186A (en) * | 2013-08-16 | 2014-01-01 | 陕西科技大学 | Method for improving filling power of down feather |
| CN106987908A (en) * | 2017-06-01 | 2017-07-28 | 安徽三祥羽毛股份有限公司 | A kind of method for improving eider down fluffy degree |
| CN107177424A (en) * | 2017-06-25 | 2017-09-19 | 长沙善道新材料科技有限公司 | It is a kind of to contain enzymatic detergent suitable for what low temperature was washed |
| CN107312661A (en) * | 2017-07-03 | 2017-11-03 | 深圳韩橘日化有限公司 | A kind of Antibacterial laundry detergent |
| CN107574022A (en) * | 2017-07-19 | 2018-01-12 | 苏州凯邦生物技术有限公司 | A kind of compound enzyme detergent of final finishing |
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|---|---|---|---|---|
| CN103485186A (en) * | 2013-08-16 | 2014-01-01 | 陕西科技大学 | Method for improving filling power of down feather |
| CN106987908A (en) * | 2017-06-01 | 2017-07-28 | 安徽三祥羽毛股份有限公司 | A kind of method for improving eider down fluffy degree |
| CN107177424A (en) * | 2017-06-25 | 2017-09-19 | 长沙善道新材料科技有限公司 | It is a kind of to contain enzymatic detergent suitable for what low temperature was washed |
| CN107312661A (en) * | 2017-07-03 | 2017-11-03 | 深圳韩橘日化有限公司 | A kind of Antibacterial laundry detergent |
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| CN110846142A (en) * | 2019-11-20 | 2020-02-28 | 安徽沃伦科技有限公司 | Efficient environment-friendly down jacket cleaning agent and cleaning method |
| CN114411269A (en) * | 2021-12-27 | 2022-04-29 | 六安市海洋羽毛有限公司 | Down feather separation production process |
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