CN108504132A - One plant tea contaminates the preparation method and colouring method of vegetable colour - Google Patents
One plant tea contaminates the preparation method and colouring method of vegetable colour Download PDFInfo
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- CN108504132A CN108504132A CN201810040797.6A CN201810040797A CN108504132A CN 108504132 A CN108504132 A CN 108504132A CN 201810040797 A CN201810040797 A CN 201810040797A CN 108504132 A CN108504132 A CN 108504132A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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Abstract
The present invention relates to preparation methods and colouring method that a plant tea contaminates vegetable colour, and the preparation method is that tealeaves is put into container and boiling system is added using Moganshan Mountain Huang young tea leaves leaf as primary raw material, boils to boiling and being kept for 15 20 minutes, obtains dyestuff filtrate；The colouring method, the dyestuff filtrate obtained using above-mentioned preparation method, prepare dye 1 part of object, will dye object fully impregnate, allow dye cloth fully water suction after wring out it is spare；Dye object, which is added in dyestuff filtrate, to be impregnated, dye system 5 20 minutes, in the process continuous stirring；It is put into abundant mordant dyeing in iron pulp-water mordanting bath, the equal level dyeing system of its mordant dyeing is made to be taken out after 10 25 minutes；Dyestuff filtrate is boiled to 80 100 DEG C, the dye object that iron pulp-water mordanting bath contaminated is placed in dyestuff filtrate and is impregnated 8 15 minutes, continuous stirring in the process.The present invention is dyed with the tealeaves baked, and without carcinogenic substances such as formaldehyde, be not pungent peculiar smell, safe to use, meets ecological, environmental protective standard；Processed dye object dyefastness is good, and washable and wearable has the effect of antibacterial.
Description
Technical field
The present invention relates to printing technology field, an especially plant tea contaminates the preparation method and colouring method of vegetable colour.
Background technology
Dyestuff is the substance that fiber and other materials can be made to colour, and is in direct contact the skin of people in use,
Currently used synthetic dyestuffs, raw material and intermediate often contain carcinogen, not only seriously pollute environment, also make directly to wear
Person or the producer come to harm.With the improvement of the quality of life, people increasingly pay close attention to health, most ask ecosystem and natural material
Product, and the natural dye extracted from plant is biodegradable because its being compatible with the environment property is good, nontoxic or even right
There is human body special health-care effect to have been favored by people.
Tea dye is one kind of plant dyeing technique, and by the dye object that tealeaves dyes, color and luster is simple and elegant, honest, carries tea flavour, removes
Except this, tea dying product also has the effect of antibacterial.The thin tight more millis of the shape of Moganshan Mountain Huang young tea leaves, the green micro- Huang of profit of color and luster, fragrance
Aloof from politics and material pursuits lasting, the dense alcohol of fresh taste, soup look is yellowish green limpid, and tea residue is light yellow at piece, but in currently available technology, does not record profit
Tea dyeing technique is carried out with Moganshan Mountain Huang young tea leaves.
To solve the above-mentioned problems, the present invention is proposed hereby.
Invention content
It is an advantage of the invention to provide the preparation methods that a plant tea contaminates vegetable colour, by this method can
By dyestuff filtrate made of the Huang bud finished tea of the Moganshan Mountain.
In order to realize these purposes, adopt the following technical scheme that：
One plant tea contaminate vegetable colour preparation method, the preparation method be using Moganshan Mountain Huang young tea leaves leaf as primary raw material,
Tealeaves tea is extracted by boiling and contaminates vegetable colour, is as follows, using the raw material of following parts by weight：1 part of tealeaves, water 45-
180 parts, tealeaves is put into container and boiling system is added, boiled to boiling and being kept for 15-20 minutes, be separated by filtration dye liquor and tealeaves
Slag obtains dyestuff filtrate.It is extracted by heating in 15-20 minutes in boiling, the pigment in tealeaves is extracted in water
Form pigment extract.
Further, the Moganshan Mountain Huang young tea leaves leaf using Moganshan Mountain Huang young tea leaves sample tea, the sample tea
Production process is：It picks tea-leaves, finish, rubbing, bored Huang, drying, manage bar.By such tea making process, tea making process can be offered tea and be cooked
Dye liquor color have any different.
Preferably, the water is for room temperature or less than 40 DEG C.
Further, the filtering uses screen filtration.
It is a further object of the invention to provide the colouring methods that a plant tea contaminates vegetable colour, pass through this dyeing side
Method can make dye object level dyeing, the dye object contaminated not fugitive color, and can solve to synthesize using tea dye vegetable colour dyeing
Dyestuff contains carcinogenicity substance, is damaged to human body, not environmentally friendly enough problem, meanwhile, pass through the processed dye of colouring method
Object finds to utilize dyeing made of the Huang young tea leaves of the Moganshan Mountain by examining its color fastness, chromatography and anti-microbial property
Good color fastness, chromatography be more, good antimicrobial effect.
In order to realize these purposes, adopt the following technical scheme that：
One plant tea contaminates the colouring method of vegetable colour, and the dyestuff filtrate obtained using above-mentioned preparation method is specific to dye
Method and step is as follows,
A：Prepare dye 1 part of object, will dye object fully impregnate, allow dye cloth fully water suction after wring out it is spare；
B：The dye object crossed by processing of step A is added in dyestuff filtrate and is impregnated, 5-20 minutes processed of dye, in the process constantly
Stirring, make its even dyeing and improve dye-uptake；
C：25 parts of normal-temperature waters are mixed 25 parts of boiling water to mix, 0.6 part of iron pulp-water is added, iron pulp-water mordanting bath is made, it is spare；
Iron pulp-water is as mordant, primarily to control contaminates color processed, can dye partially grey colour system；Meanwhile iron pulp-water is as matchmaker
Stain, the dye object after contaminating first time dyestuff filtrate play good tint retention；
D：Dye object in step B is wrung out, is put into abundant mordant dyeing in the iron pulp-water mordanting bath described in step C, in the process not
Disconnected stirring is taken out after making its mordant dyeing equal level dyeing 10-25 minutes, and clear water is washed 2 times, is wrung out；
E：Dyestuff filtrate in step B is boiled to 80-100 DEG C, spare, preparation is redyed again；
F：The dye object that iron pulp-water mordanting bath in step D contaminated is placed in the dyestuff filtrate described in step E and impregnates 8-15 points
Clock, in the process continuous stirring, makes its even dyeing and improves dye-uptake；
G：The processed dye objects of step F are wrung out, clear water is washed 4 times, is dried.When cleaning, first three all over water clean when color also
It is deep, the 4th time cleaning when, water is just limpider, at this time cleans up loose colour.
In one embodiment, in stepb, dye system 10 minutes.By the control of time, it is primarily due to extraction color
Needs, desired partially grey colour system can be dyed, and contaminate the not fugitive color of the dye object after the completion of system.
In one embodiment, in step D, equal level dyeing system is taken out after 15 minutes in iron pulp-water mordanting bath.
In one embodiment, in step E, filtrate is boiled to 90 DEG C.
In one embodiment, in step F, the dye that iron pulp-water mordanting bath contaminated is crossed to be placed in filtrate and impregnates 10 points
Clock, continuous stirring, makes its even dyeing in the process.
Preferably, the iron pulp-water is gone out by vinegar and iron rust infusion.The iron that vinegar and iron rust infusion boil out
There are no pollution to the environment for pulp-water, taking naturally, can increase color fastness simultaneously.
Further, the main component of the iron pulp-water is FeSO47H2O..
The beneficial technique effect of the present invention：
By adopting the above-described technical solution, the present invention has the advantages that compared with prior art：
1, tea dye vegetable colour of the present invention is prepared with natural Moganshan Mountain Huang bud organic tea, with baking
Good tealeaves is dyed, and the natural tea dye product used, without carcinogenic substances such as formaldehyde, be not pungent peculiar smell, ensures consumer
It is healthy and safe, do not add any chemical assistant, the tea perfume for itself having one light is natural non-hazardous, will not to human body
Injury is constituted, it is safe to use, comply fully with ecological, environmental protective standard；
2, good using the processed dye object dyefastness of the present invention, washable and wearable, even dyeing has the effect of antibacterial.
Specific implementation mode
The embodiment of the present invention is described below in detail.The embodiments described below is exemplary, and is only used for explaining this hair
It is bright, and be not considered as limiting the invention.Particular technique or condition are not specified in embodiment, according to text in the art
It offers described technology or condition or is carried out according to product description.Reagents or instruments used without specified manufacturer,
For can be with conventional products that are commercially available.
The present invention will be described in detail by way of examples below.
Embodiment 1
Formula：Tealeaves 100g；Water 4500g.
Preparation method：
Tealeaves is put into container and is added in normal-temperature water and is cooked, boils to boiling and being kept for 15 minutes, filtrate is obtained by filtration.
Embodiment 2
Formula：Tealeaves 100g；Water 5500g.
Preparation method：
Tealeaves is put into container and is added in normal-temperature water and is cooked, boils to boiling and being kept for 20 minutes, filtrate is obtained by filtration.
Embodiment 3
Formula：Tealeaves 100g；Water 15000g.
Preparation method：
Tealeaves is put into container and is added in 39 DEG C of water and is cooked, boils to boiling and being kept for 18 minutes, filtrate is obtained by filtration.
Embodiment 4
Formula：Tealeaves 100g；Water 18000g.
Preparation method：
Tealeaves is put into container and is added in normal-temperature water and is cooked, boils to boiling and being kept for 20 minutes, filtrate is obtained by filtration.
Embodiment 5
Material：Contaminate object 100g；
Formula：Iron pulp-water 60g, 2500g normal-temperature water, 2500g parts of boiling water.
Colouring method：
A：Will dye object fully impregnate, allow dye cloth fully water suction after wring out it is spare；
B：The dye object crossed by processing of step A is added in dyestuff filtrate and is impregnated, dye system 5 minutes, in the process constantly
Stirring, makes its even dyeing；
C：Normal-temperature water is mixed into boiling water, iron pulp-water is added, iron pulp-water mordanting bath is made, it is spare；
D：Dye object in step B is wrung out, is put into abundant mordant dyeing in the iron pulp-water mordanting bath described in step C, in the process not
Disconnected stirring makes the equal level dyeing system of its mordant dyeing take out after ten minutes, and clear water is washed 2 times, is wrung out；
E：Dyestuff filtrate in step B is boiled to 80 DEG C, spare, preparation is redyed again；
F：The dye object that iron pulp-water mordanting bath in step D contaminated is placed in the dyestuff filtrate described in step E and is impregnated 8 minutes,
Continuous stirring in the process, makes its even dyeing；
G：The processed dye objects of step F are wrung out, clear water is washed 4 times, is dried.
Embodiment 6
Material：Contaminate object 100g；
Formula：Iron pulp-water 60g, 8000g normal-temperature water, 8000g parts of boiling water.
Colouring method：
A：Will dye object fully impregnate, allow dye cloth fully water suction after wring out it is spare；
B：The dye object crossed by processing of step A is added in dyestuff filtrate and is impregnated, dye system 20 minutes, in the process constantly
Stirring, makes its even dyeing；
C：Normal-temperature water is mixed into boiling water, iron pulp-water is added, iron pulp-water mordanting bath is made, it is spare；
D：Dye object in step B is wrung out, is put into abundant mordant dyeing in the iron pulp-water mordanting bath described in step C, in the process not
Disconnected stirring makes the equal level dyeing system of its mordant dyeing be taken out after 25 minutes, and clear water is washed 2 times, is wrung out；
E：Dyestuff filtrate in step B is boiled to 100 DEG C, spare, preparation is redyed again；
F：The dye object that iron pulp-water mordanting bath in step D contaminated is placed in the dyestuff filtrate described in step E and is impregnated 15 minutes,
Continuous stirring in the process, makes its even dyeing；
G：The processed dye objects of step F are wrung out, clear water is washed 4 times, is dried.
Embodiment 7
Material：Contaminate object 100g；
Formula：Iron pulp-water 60g, 7500g normal-temperature water, 7500g parts of boiling water.
Colouring method：
A：Will dye object fully impregnate, allow dye cloth fully water suction after wring out it is spare；
B：The dye object crossed by processing of step A is added in dyestuff filtrate and is impregnated, dye system 10 minutes, in the process constantly
Stirring, makes its even dyeing；
C：Normal-temperature water is mixed into boiling water, iron pulp-water is added, iron pulp-water mordanting bath is made, it is spare；
D：Dye object in step B is wrung out, is put into abundant mordant dyeing in the iron pulp-water mordanting bath described in step C, in the process not
Disconnected stirring makes the equal level dyeing system of its mordant dyeing be taken out after 15 minutes, and clear water is washed 2 times, is wrung out；
E：Dyestuff filtrate in step B is boiled to 90 DEG C, spare, preparation is redyed again；
F：The dye object that iron pulp-water mordanting bath in step D contaminated is placed in the dyestuff filtrate described in step E and is impregnated 10 minutes,
Continuous stirring in the process, makes its even dyeing；
G：The processed dye objects of step F are wrung out, clear water is washed 4 times, is dried.
Embodiment 8
Material：Contaminate object 100g；
Formula：Iron pulp-water 60g, 7500g normal-temperature water, 7500g parts of boiling water.
Colouring method：
A：Will dye object fully impregnate, allow dye cloth fully water suction after wring out it is spare；
B：The dye object crossed by processing of step A is added in dyestuff filtrate and is impregnated, dye system 12 minutes, in the process constantly
Stirring, makes its even dyeing；
C：Normal-temperature water is mixed into boiling water, iron pulp-water is added, iron pulp-water mordanting bath is made, it is spare；
D：Dye object in step B is wrung out, is put into abundant mordant dyeing in the iron pulp-water mordanting bath described in step C, in the process not
Disconnected stirring makes the equal level dyeing system of its mordant dyeing be taken out after 15 minutes, and clear water is washed 2 times, is wrung out；
E：Dyestuff filtrate in step B is boiled to 90 DEG C, spare, preparation is redyed again；
F：The dye object that iron pulp-water mordanting bath in step D contaminated is placed in the dyestuff filtrate described in step E and is impregnated 10 minutes,
Continuous stirring in the process, makes its even dyeing；
G：The processed dye objects of step F are wrung out, clear water is washed 4 times, is dried.
The dye object that embodiment 5-8 is obtained carries out antibacterial ability, content of formaldehyde and color fastness experiment, as a result referring to table 1,
Table 2.
Table 1 contaminates antibacterial ability, the color fastness of object
Note：It contaminates object anti-microbial property to detect using respective GB standard according to the classification of dye object, for example, the antibacterial of cotton fiber
Performance is detected by GB/15979-2002 methods；The anti-microbial property of silk fabrics is detected by GB/T20944.3-2008 methods；Washable and antifriction
It wipes color fastness and presses GB/T3921-2008 and GB/T3920-2008 methods measurement respectively.
Table 2
| Embodiment | Carcinogenic substance (formaldehyde) (%) |
| 5 | Nothing |
| 6 | Nothing |
| 7 | Nothing |
| 8 | Nothing |
Note：Contaminate carcinogenic in object detect according to national standards《Fundamental Safety Technical Standard For Textiles》In《Textile
The restriction of content of formaldehyde》.
As can be seen from Table 1 and Table 2, not only there is antibacterial effect by the processed dye object of tea dye vegetable colour colouring method
Fruit, and wear-resisting ability is colour-fast washes rear color and luster variation also unobvious, more wear-resisting.
In the description of the present invention, it is to be understood that, term " first ", " second " are used for description purposes only, and cannot
It is interpreted as indicating or implies relative importance or implicitly indicate the quantity of indicated technical characteristic.Define as a result, " the
One ", the feature of " second " can explicitly or implicitly include one or more this feature.In the description of the present invention,
The meaning of " plurality " is two or more, unless otherwise specifically defined.
In the description of this specification, reference term " one embodiment ", " some embodiments ", " example ", " specifically show
The description of example " or " some examples " etc. means specific features, structure, material or spy described in conjunction with this embodiment or example
Point is included at least one embodiment or example of the invention.In the present specification, schematic expression of the above terms are not
It must be directed to identical embodiment or example.Moreover, particular features, structures, materials, or characteristics described can be in office
It can be combined in any suitable manner in one or more embodiments or example.In addition, without conflicting with each other, the skill of this field
Art personnel can tie the feature of different embodiments or examples described in this specification and different embodiments or examples
It closes and combines.
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example
Property, it is not considered as limiting the invention, those skilled in the art within the scope of the invention can be to above-mentioned
Embodiment is changed, changes, replacing and modification.
Claims (10)
1. a plant tea contaminates the preparation method of vegetable colour, which is characterized in that the preparation method is to be with Moganshan Mountain Huang young tea leaves leaf
Primary raw material extracts tealeaves tea by boiling and contaminates vegetable colour, is as follows, using the raw material of following parts by weight：Tealeaves 1
Part, tealeaves is put into container and boiling system is added, boiled to boiling and being kept for 15-20 minutes, be separated by filtration dye liquor by 45-180 parts of water
And tealeaf residue, obtain dyestuff filtrate.
2. the preparation method of tea dye vegetable colour according to claim 1, which is characterized in that the Moganshan Mountain Huang young tea leaves leaf
Using the sample tea of Moganshan Mountain Huang young tea leaves, the production process of the sample tea is：Pick tea-leaves, finish, rubbing, bored Huang, drying,
Manage bar.
3. the preparation method of tea dye vegetable colour according to claim 1, it is characterised in that：The filtering uses sieve mistake
Filter.
4. the preparation method of tea dye vegetable colour according to claim 1, which is characterized in that the water is room temperature or low
In 40 DEG C.
5. a plant tea contaminates the colouring method of vegetable colour, which is characterized in that obtained using the preparation method described in claim 1-4
Dyestuff filtrate, steps are as follows for specific colouring method,
A：Prepare 1 part of object of dye, dye object is fully impregnated, allows after dying cloth fully water suction and wring out；
B：The dye object crossed by processing of step A is added in dyestuff filtrate and is impregnated, 5-20 minutes processed of dye is constantly stirred in the process
It mixes；
C：25 parts of normal-temperature waters are mixed 25 parts of boiling water to mix, 0.6 part of iron pulp-water is added, iron pulp-water mordanting bath is made；
D：The processed dye objects of step B are wrung out, are put into abundant mordant dyeing in the iron pulp-water mordanting bath described in step C, in the process not
Disconnected stirring is taken out after making its mordant dyeing equal level dyeing 10-25 minutes, and clear water is washed 2 times, is wrung out；
E：Dyestuff filtrate in step B is boiled to 80-100 DEG C, preparation is redyed again；
F：The dye object that iron pulp-water mordanting bath in step D contaminated is placed in the dyestuff filtrate described in step E and is impregnated 8-15 minutes, mistake
It is constantly stirred in journey；
G：The processed dye objects of step F are wrung out, clear water is washed 4 times, is dried.
6. the colouring method of tea dye vegetable colour according to claim 5, which is characterized in that
In stepb, dye system 10 minutes.
7. the colouring method of tea dye vegetable colour according to claim 5, which is characterized in that
In step D, equal level dyeing system is taken out after 15 minutes in iron pulp-water mordanting bath.
8. the colouring method of tea dye vegetable colour according to claim 5, which is characterized in that
In step E, filtrate is boiled to 90 DEG C.
9. the colouring method of tea dye vegetable colour according to claim 5, it is characterised in that：
In step F, the dye that iron pulp-water mordanting bath contaminated is crossed to be placed in filtrate and is impregnated 10 minutes, continuous stirring in the process,
Make its even dyeing.
10. the colouring method of tea dye vegetable colour according to claim 5, it is characterised in that：The iron pulp-water is by eating
Gone out with vinegar and iron rust infusion.
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| CN109837773A (en) * | 2019-01-30 | 2019-06-04 | 欣龙控股（集团）股份有限公司 | A kind of dark brown spunlace non-woven material of tea perfume and preparation method thereof |
| CN111058307A (en) * | 2020-01-13 | 2020-04-24 | 徐心伶 | Chinese chive dyeing method and device |
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| CN111058307A (en) * | 2020-01-13 | 2020-04-24 | 徐心伶 | Chinese chive dyeing method and device |
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